CN111643600A - Traditional Chinese medicine gastric floating tablet and preparation method thereof - Google Patents
Traditional Chinese medicine gastric floating tablet and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/56—Materials from animals other than mammals
- A61K35/618—Molluscs, e.g. fresh-water molluscs, oysters, clams, squids, octopus, cuttlefish, snails or slugs
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/25—Araliaceae (Ginseng family), e.g. ivy, aralia, schefflera or tetrapanax
- A61K36/258—Panax (ginseng)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/32—Burseraceae (Frankincense family)
- A61K36/324—Boswellia, e.g. frankincense
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/32—Burseraceae (Frankincense family)
- A61K36/328—Commiphora, e.g. mecca myrrh or balm of Gilead
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/0053—Mouth and digestive tract, i.e. intraoral and peroral administration
- A61K9/0065—Forms with gastric retention, e.g. floating on gastric juice, adhering to gastric mucosa, expanding to prevent passage through the pylorus
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/20—Pills, tablets, discs, rods
- A61K9/2004—Excipients; Inactive ingredients
- A61K9/2068—Compounds of unknown constitution, e.g. material from plants or animals
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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Abstract
The invention relates to a traditional Chinese medicine gastric-floating tablet which comprises the following traditional Chinese medicine compositions in parts by weight: 15-20 parts of cuttlebone powder, 15-20 parts of calcined oyster, 10-15 parts of calcined concha arcae, 2-6 parts of bletilla striata, 23-27 parts of pseudo-ginseng powder, 3-7 parts of cattail pollen, 3-7 parts of medicated leaven, 3-7 parts of frankincense and 3-7 parts of myrrh. The invention also relates to a preparation method of the traditional Chinese medicine gastric floating tablet, which comprises the steps of decoction, filtration, powder adding and tabletting. The invention uses self adhesive as adhesive, cuttlebone powder as floating agent and medicated leaven as disintegrating agent, which is completely a traditional Chinese medicine formula and forming agent, and solves the problem of excessive use amount of auxiliary materials.
Description
Technical Field
The invention relates to the technical field of traditional Chinese medicines, in particular to a traditional Chinese medicine gastric floating tablet and a preparation method thereof.
Background
Gastric floating tablets, i.e. gastric retention tablets, are tablets which can be retained in gastric juice, prolong the release time of the drug, improve the absorption of the drug and improve the bioavailability. The prescription design of the gastric-floating tablet firstly solves the contradiction between the hardness and the density of the tablet, namely the tablet has moderate hardness and minimized density. Secondly, the type and the dosage of the auxiliary materials are screened, so that the dissolution and the release of the medicine meet the preset standard.
Notoginseng radix is dry root of Notoginseng radix of Panax of Araliaceae, also named Notoginseng radix, Ginseng radix Notoginseng radix, and rhizoma Panacis japonici. Gastrointestinal bleeding symptoms such as gastric ulcer and the like are common frequently-occurring diseases, and people can directly take the pseudo-ginseng powder to treat the gastrointestinal bleeding symptoms
And (4) treating. The yunnan white drug containing the pseudo-ginseng powder has satisfactory effect on treating internal diseases such as chronic gastritis and gastrointestinal hemorrhage. Because the degradation of the ginsenoside active ingredients in the pseudo-ginseng is faster, the pseudo-ginseng is required to be taken for a plurality of times every day to achieve a satisfactory curative effect, thereby reducing the medication compliance. If the hydrophilic gel matrix is prepared into the gastric floating tablet, in the floating process in gastric juice, the medicinal powder in the gel matrix does not contact the gastric juice and exists in a dry solid form, which is equivalent to a medicament storage pool, and the medicament is released step by step along with the continuous corrosion of the hydrophilic gel matrix, so that the aims of improving the bioavailability, reducing the dosage and reducing the administration frequency are fulfilled.
Various factors restrict the preparation of gastric floating tablets. If the content of the main drug in the tablet is high, the compression molding performance of the main drug is poor, and the screening of the adhesive is the problem to be solved firstly. The binder is not used in an amount sufficient to achieve the purpose of compression into tablets, and the binder is used in an amount sufficient to possibly mean that the amount of other auxiliary materials is not sufficient. In order to ensure the dosage of the main drug, the dosage of the gel skeleton agent is only reduced at the moment, but the floating effect of the floating tablet is influenced. If the active ingredients in the main drug are complex, for example, the traditional Chinese medicine preparation, the gastric floating tablet is preferably prepared into an erosion type so as to be beneficial to the integral synchronous release of the active ingredients of the drug. This requires screening of appropriate combinations of excipients to ensure that solubilization occurs within a specified time and that it is always in a floating state throughout the solubilization process.
Disclosure of Invention
The invention provides a traditional Chinese medicine formula and a forming agent, solves the problem of excessive use amount of auxiliary materials, and provides a traditional Chinese medicine gastric floating tablet with good drug effect and a preparation method thereof.
The technical scheme of the invention is as follows:
a traditional Chinese medicine gastric floating tablet comprises the following traditional Chinese medicine composition in parts by weight: 15-20 parts of cuttlebone powder, 15-20 parts of calcined oyster, 10-15 parts of calcined concha arcae, 2-6 parts of bletilla striata, 23-27 parts of pseudo-ginseng powder, 3-7 parts of cattail pollen, 3-7 parts of medicated leaven, 3-7 parts of frankincense and 3-7 parts of myrrh.
Preferably, 18 parts of cuttlebone powder, 18 parts of calcined oyster, 13 parts of calcined concha arcae, 5 parts of bletilla striata, 25 parts of pseudo-ginseng powder, 5 parts of cattail pollen, 5 parts of medicated leaven, 5 parts of frankincense and 5 parts of myrrh.
Preferably, the cuttlebone powder and the pseudo-ginseng powder are 200-300 meshes.
A preparation method of a traditional Chinese medicine gastric floating tablet comprises the following steps:
weighing the raw material medicines according to the parts by weight, adding distilled water into calcined oyster, calcined concha arcae, bletilla striata, cattail pollen, medicated leaven, frankincense and myrrh, boiling and decocting for 1-2 hours; the weight ratio of the calcined oyster shell, the calcined concha arcae, the bletilla striata, the cattail pollen, the medicated leaven, the frankincense and the myrrh to the distilled water is 1: 100-150;
filtering the decoction, filtering to remove residues, adding Os Sepiae powder and Notoginseng radix powder, and tabletting to obtain Chinese medicinal floating tablet.
The invention has the beneficial effects that:
the invention uses self adhesive as adhesive, cuttlebone powder as floating agent and medicated leaven as disintegrating agent, which is completely a traditional Chinese medicine formula and forming agent, and solves the problem of excessive use amount of auxiliary materials.
Detailed Description
Example 1
A traditional Chinese medicine gastric floating tablet comprises the following traditional Chinese medicine composition in parts by weight: 18 parts of cuttlebone powder, 18 parts of calcined oyster, 13 parts of calcined concha arcae, 5 parts of bletilla striata, 25 parts of pseudo-ginseng powder, 5 parts of pollen typhae, 5 parts of medicated leaven, 5 parts of frankincense and 5 parts of myrrh. The cuttlebone powder and the pseudo-ginseng powder are 300 meshes.
A preparation method of a traditional Chinese medicine gastric floating tablet comprises the following steps:
weighing the raw material medicines according to the parts by weight, adding distilled water into calcined oyster, calcined concha arcae, bletilla striata, cattail pollen, medicated leaven, frankincense and myrrh, boiling and decocting for 2 hours; the weight ratio of the calcined oyster shell, the calcined concha arcae, the bletilla striata, the cattail pollen, the medicated leaven, the frankincense and the myrrh to the distilled water is 1: 150;
filtering the decoction, filtering to remove residues, adding Os Sepiae powder and Notoginseng radix powder, and tabletting to obtain Chinese medicinal floating tablet.
Using 900 mL of artificial gastric juice as floating medium, at 37 deg.C and paddle speed of 100 r.min-1Under the conditions, the tablets were put in, the rising time was measured, and the floating and erosion of the tablets were observed. During the erosion process, the tablets are always in a floating state. The invention lasts for 20 hours of floating.
Example 2
A traditional Chinese medicine gastric floating tablet comprises the following traditional Chinese medicine composition in parts by weight: 15 parts of cuttlebone powder, 20 parts of calcined oyster, 14 parts of calcined concha arcae, 6 parts of bletilla striata, 23 parts of pseudo-ginseng powder, 7 parts of pollen typhae, 7 parts of medicated leaven, 6 parts of frankincense and 3 parts of myrrh. The cuttlebone powder and the pseudo-ginseng powder are 300 meshes.
A preparation method of a traditional Chinese medicine gastric floating tablet comprises the following steps:
weighing the raw material medicines according to the parts by weight, adding distilled water into calcined oyster, calcined concha arcae, bletilla striata, cattail pollen, medicated leaven, frankincense and myrrh, boiling and decocting for 1 hour; the weight ratio of the calcined oyster shell, the calcined concha arcae, the bletilla striata, the cattail pollen, the medicated leaven, the frankincense and the myrrh to the distilled water is 1: 100;
filtering the decoction, filtering to remove residues, adding Os Sepiae powder and Notoginseng radix powder, and tabletting to obtain Chinese medicinal floating tablet.
Using 900 mL of artificial gastric juice as floating medium, at 37 deg.C and paddle speed of 100 r.min-1Under the conditions, the tablets were put in, the rising time was measured, and the floating and erosion of the tablets were observed. During the erosion process, the tablets are always in a floating state. The invention lasts for 19.5 hours of floating.
Example 3
A traditional Chinese medicine gastric floating tablet comprises the following traditional Chinese medicine composition in parts by weight: 20 parts of cuttlebone powder, 15 parts of calcined oyster, 10 parts of calcined concha arcae, 2 parts of bletilla striata, 27 parts of pseudo-ginseng powder, 3 parts of pollen typhae, 3 parts of medicated leaven, 7 parts of frankincense and 7 parts of myrrh. The cuttlebone powder and the pseudo-ginseng powder are 250 meshes.
A preparation method of a traditional Chinese medicine gastric floating tablet comprises the following steps:
weighing the raw material medicines according to the parts by weight, adding distilled water into calcined oyster, calcined concha arcae, bletilla striata, cattail pollen, medicated leaven, frankincense and myrrh, boiling and decocting for 1.2 hours; the weight ratio of the calcined oyster shell, the calcined concha arcae, the bletilla striata, the cattail pollen, the medicated leaven, the frankincense and the myrrh to the distilled water is 1: 120;
filtering the decoction, filtering to remove residues, adding Os Sepiae powder and Notoginseng radix powder, and tabletting to obtain Chinese medicinal floating tablet.
Using 900 mL of artificial gastric juice as floating medium, at 37 deg.C and paddle speed of 100 r.min-1Under the conditions, the tablets were put in, the rising time was measured, and the floating and erosion of the tablets were observed. During the erosion process, the tablets are always in a floating state. The invention lasts for 19.6 hours of floating.
Example 4
A traditional Chinese medicine gastric floating tablet comprises the following traditional Chinese medicine composition in parts by weight: 19 parts of cuttlebone powder, 17 parts of calcined oyster, 15 parts of calcined concha arcae, 3 parts of bletilla striata, 24 parts of pseudo-ginseng powder, 4 parts of cattail pollen, 6 parts of medicated leaven, 4 parts of frankincense and 6 parts of myrrh. The cuttlebone powder and the pseudo-ginseng powder are 200 meshes.
A preparation method of a traditional Chinese medicine gastric floating tablet comprises the following steps:
weighing the raw material medicines according to the parts by weight, adding distilled water into calcined oyster, calcined concha arcae, bletilla striata, cattail pollen, medicated leaven, frankincense and myrrh, boiling and decocting for 1.2 hours; the weight ratio of the calcined oyster shell, the calcined concha arcae, the bletilla striata, the cattail pollen, the medicated leaven, the frankincense and the myrrh to the distilled water is 1: 130;
filtering the decoction, filtering to remove residues, adding Os Sepiae powder and Notoginseng radix powder, and tabletting to obtain Chinese medicinal floating tablet.
Using 900 mL of artificial gastric juice as floating medium, at 37 deg.C and paddle speed of 100 r.min-1Under the conditions, the tablets were put in, the rising time was measured, and the floating and erosion of the tablets were observed. During the erosion process, the tablets are always in a floating state. The invention lasts for 19.0 hours of floating.
Example 5
A traditional Chinese medicine gastric floating tablet comprises the following traditional Chinese medicine composition in parts by weight: 16 parts of cuttlebone powder, 17 parts of calcined oyster, 11 parts of calcined concha arcae, 4 parts of bletilla striata, 26 parts of pseudo-ginseng powder, 4 parts of pollen typhae, 4 parts of medicated leaven, 3 parts of frankincense and 4 parts of myrrh. The cuttlebone powder and the pseudo-ginseng powder are 200 meshes.
A preparation method of a traditional Chinese medicine gastric floating tablet comprises the following steps:
weighing the raw material medicines according to the parts by weight, adding distilled water into calcined oyster, calcined concha arcae, bletilla striata, cattail pollen, medicated leaven, frankincense and myrrh, boiling and decocting for 1.2 hours; the weight ratio of the calcined oyster shell, the calcined concha arcae, the bletilla striata, the cattail pollen, the medicated leaven, the frankincense and the myrrh to the distilled water is 1: 140;
filtering the decoction, filtering to remove residues, adding Os Sepiae powder and Notoginseng radix powder, and tabletting to obtain Chinese medicinal floating tablet.
Using 900 mL of artificial gastric juice as floating medium, at 37 deg.C and paddle speed of 100 r.min-1Under the conditions, the tablets were put in, the rising time was measured, and the floating and erosion of the tablets were observed. During the erosion process, the tablets are always in a floating state. The invention lasts for 19.2 hours of floating.
Claims (4)
1. The traditional Chinese medicine gastric floating tablet is characterized by comprising the following traditional Chinese medicine compositions in parts by weight: 15-20 parts of cuttlebone powder, 15-20 parts of calcined oyster, 10-15 parts of calcined concha arcae, 2-6 parts of bletilla striata, 23-27 parts of pseudo-ginseng powder, 3-7 parts of cattail pollen, 3-7 parts of medicated leaven, 3-7 parts of frankincense and 3-7 parts of myrrh.
2. The traditional Chinese medicine gastric floating tablet according to claim 1, which is characterized by comprising 18 parts of cuttlebone powder, 18 parts of calcined oyster shell, 13 parts of calcined concha arcae, 5 parts of bletilla striata, 25 parts of pseudo-ginseng powder, 5 parts of pollen typhae, 5 parts of medicated leaven, 5 parts of frankincense and 5 parts of myrrh.
3. The traditional Chinese medicine gastric floating tablet as claimed in claim 1 or 2, wherein the cuttlebone powder and the pseudo-ginseng powder are 200-300 mesh.
4. A preparation method of a traditional Chinese medicine gastric floating tablet is characterized by comprising the following steps:
weighing the raw material medicines according to the parts by weight, adding distilled water into calcined oyster, calcined concha arcae, bletilla striata, cattail pollen, medicated leaven, frankincense and myrrh, boiling and decocting for 1-2 hours; the weight ratio of the calcined oyster shell, the calcined concha arcae, the bletilla striata, the cattail pollen, the medicated leaven, the frankincense and the myrrh to the distilled water is 1: 100-150;
filtering the decoction, filtering to remove residues, adding Os Sepiae powder and Notoginseng radix powder, and tabletting to obtain Chinese medicinal floating tablet.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2020102863839 | 2020-04-13 | ||
| CN202010286383.9A CN111329957A (en) | 2020-04-13 | 2020-04-13 | Traditional Chinese medicine gastric floating tablet and preparation method thereof |
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| CN202010573216.2A Pending CN111643600A (en) | 2020-04-13 | 2020-06-22 | Traditional Chinese medicine gastric floating tablet and preparation method thereof |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1229659A (en) * | 1998-03-24 | 1999-09-29 | 王敬俭 | Chinese medicine for treating ulcer of gastrointestinal tract and its prodn. tech. |
| CN1836719A (en) * | 2005-11-08 | 2006-09-27 | 许景连 | Pharmaceutical composition for treating gastritis, gastric ulcer and duodenal ulcer |
| CN101683361A (en) * | 2008-09-24 | 2010-03-31 | 辽宁省中医药研究院 | In-stomach floating type sustained-release pellet prepared from traditional Chinese medicine compound preparations |
| CN102139016A (en) * | 2011-04-07 | 2011-08-03 | 刘宝虎 | Medlar floating tablet for treating chronic gastritis and preparation method thereof |
| CN105521492A (en) * | 2015-12-14 | 2016-04-27 | 成都中医药大学 | Porous bletilla gum, preparation method therefor and application thereof |
-
2020
- 2020-04-13 CN CN202010286383.9A patent/CN111329957A/en active Pending
- 2020-06-22 CN CN202010573216.2A patent/CN111643600A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1229659A (en) * | 1998-03-24 | 1999-09-29 | 王敬俭 | Chinese medicine for treating ulcer of gastrointestinal tract and its prodn. tech. |
| CN1836719A (en) * | 2005-11-08 | 2006-09-27 | 许景连 | Pharmaceutical composition for treating gastritis, gastric ulcer and duodenal ulcer |
| CN101683361A (en) * | 2008-09-24 | 2010-03-31 | 辽宁省中医药研究院 | In-stomach floating type sustained-release pellet prepared from traditional Chinese medicine compound preparations |
| CN102139016A (en) * | 2011-04-07 | 2011-08-03 | 刘宝虎 | Medlar floating tablet for treating chronic gastritis and preparation method thereof |
| CN105521492A (en) * | 2015-12-14 | 2016-04-27 | 成都中医药大学 | Porous bletilla gum, preparation method therefor and application thereof |
Non-Patent Citations (1)
| Title |
|---|
| 沈阳药学院主编: "《药剂学》", 31 May 1980, 人民卫生出版社 * |
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