CN111617133A - Process for preparing medicated liquor containing cyclocarya paliurus - Google Patents

Process for preparing medicated liquor containing cyclocarya paliurus Download PDF

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Publication number
CN111617133A
CN111617133A CN202010577430.5A CN202010577430A CN111617133A CN 111617133 A CN111617133 A CN 111617133A CN 202010577430 A CN202010577430 A CN 202010577430A CN 111617133 A CN111617133 A CN 111617133A
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CN
China
Prior art keywords
cyclocarya paliurus
medicinal liquor
leaves
raw material
cyclocarya
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202010577430.5A
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Chinese (zh)
Inventor
戴建华
李锋涛
黄美子
徐朋朋
曹田
王倩
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangsu Shenqi Chinese Medicine Technology Co ltd
Jiangsu Agri Animal Husbandry Vocational College
Original Assignee
Jiangsu Shenqi Chinese Medicine Technology Co ltd
Jiangsu Agri Animal Husbandry Vocational College
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Filing date
Publication date
Application filed by Jiangsu Shenqi Chinese Medicine Technology Co ltd, Jiangsu Agri Animal Husbandry Vocational College filed Critical Jiangsu Shenqi Chinese Medicine Technology Co ltd
Priority to CN202010577430.5A priority Critical patent/CN111617133A/en
Publication of CN111617133A publication Critical patent/CN111617133A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/52Juglandaceae (Walnut family)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/06Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
    • A61K47/08Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite containing oxygen, e.g. ethers, acetals, ketones, quinones, aldehydes, peroxides
    • A61K47/14Esters of carboxylic acids, e.g. fatty acid monoglycerides, medium-chain triglycerides, parabens or PEG fatty acid esters
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/0087Galenical forms not covered by A61K9/02 - A61K9/7023
    • A61K9/0095Drinks; Beverages; Syrups; Compositions for reconstitution thereof, e.g. powders or tablets to be dispersed in a glass of water; Veterinary drenches
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P1/00Drugs for disorders of the alimentary tract or the digestive system
    • A61P1/14Prodigestives, e.g. acids, enzymes, appetite stimulants, antidyspeptics, tonics, antiflatulents
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P9/00Drugs for disorders of the cardiovascular system
    • A61P9/10Drugs for disorders of the cardiovascular system for treating ischaemic or atherosclerotic diseases, e.g. antianginal drugs, coronary vasodilators, drugs for myocardial infarction, retinopathy, cerebrovascula insufficiency, renal arteriosclerosis
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P9/00Drugs for disorders of the cardiovascular system
    • A61P9/12Antihypertensives
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/04Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
    • C12G3/05Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with health-improving ingredients, e.g. flavonoids, flavones, polyphenols or polysaccharides
    • C12G3/055Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with health-improving ingredients, e.g. flavonoids, flavones, polyphenols or polysaccharides extracted from plants
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/04Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
    • C12G3/06Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with flavouring ingredients

Abstract

The invention provides a manufacturing process of medicinal liquor containing cyclocarya paliurus, and relates to the technical field of health-care medicinal liquor. The preparation process of the medicinal liquor based on the cyclocarya paliurus comprises cyclocarya paliurus raw materials, raw material liquor, aromatic ester and production process steps. According to the invention, through the sorting process, the cyclocarya paliurus leaves with good quality are screened out and placed in the medicinal liquor bottle, the medicinal efficacy can still be dispersed when the medicinal liquor is stored, the quality of the medicinal liquor is prolonged, the attractiveness of the medicinal liquor is improved, the commercial competitiveness of the medicinal liquor is enhanced, and the low-quality cyclocarya paliurus leaves are subjected to crushing treatment, so that the soaking and extraction efficiency can be greatly improved, the production time is shortened, the production cost is reduced, the large-scale production can be realized, the annual production is not limited by climate, the utilization rate of raw materials is high, the production rate of the medicinal liquor is improved, and the commercial value is further improved.

Description

Process for preparing medicated liquor containing cyclocarya paliurus
Technical Field
The invention relates to the technical field of health-care medicinal liquor, in particular to a process for manufacturing medicinal liquor containing cyclocarya paliurus.
Background
Cyclocarya paliurus (Batal.) Lljinsk is prepared from bark, root or leaf of cyclocarya paliurus (Batal.) Lljinsk of Juglandaceae. Cyclocarya paliurus is mainly distributed in southern Shaanxi, Jiangsu, Anhui, Zhejiang, Jiangxi, Fujian, Taiwan, Hubei, Hunan, Guangdong, Guangxi, Sichuan, Guizhou, Yunnan and other places. Has effects of dispelling pathogenic wind, relieving inflammation and pain, killing parasite, and relieving itching, and has more broken lobules, which are in the shape of wide needles, 5-14cm long, 2-6cm wide, tapered tip, oblique base, sawtooth at edge, gray green upper surface, yellow green or brown lower surface, and shield-like gland and leathery texture. Fragrant smell and light taste. The tea is good for patients with more leaves, green color and fragrant smell, and has the effects of dilating blood vessels, improving blood circulation of heart, lowering blood pressure and promoting gastrointestinal motility.
The alcohol is a good semi-polar organic solvent, various active ingredients of the traditional Chinese medicines are easily dissolved in the alcohol, the efficacy of the medicines is fully exerted by the aid of the alcohol potency and the alcohol-assisted potency, the curative effect is improved, but a commercial medicinal liquor manufacturing process related to the cyclocarya paliurus is not found in the market, the existing cyclocarya paliurus medicinal liquor is basically self-used for individual production, the time consumption is long, the process is old, and the production rate is low.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a process for manufacturing medicinal liquor containing cyclocarya paliurus, which solves the problems of long production time, old process and low production rate of the existing cyclocarya paliurus medicinal liquor.
(II) technical scheme
In order to achieve the purpose, the invention is realized by the following technical scheme: a process for preparing medicated wine containing cyclocarya paliurus comprises cyclocarya paliurus raw materials, raw material wine and aromatic ester, and is characterized in that: the process comprises the following steps:
s1, rinsing the cyclocarya paliurus raw material in a cleaning pool, fishing out the cyclocarya paliurus raw material after cleaning, and sterilizing by ultraviolet rays in the drying process;
s2, sorting the dried cyclocarya paliurus raw material into high-grade cyclocarya paliurus leaves and low-grade cyclocarya paliurus leaves according to the integrity, size and shape through a sorting production line;
s3, feeding the sorted high-grade cyclocarya paliurus leaves into another production line for further selection, and filling the leaves into a medicinal liquor bottle to be filled according to the specification of one part of three cyclocarya paliurus leaves;
s4, uniformly crushing the sorted low-grade cyclocarya paliurus leaves and the high-grade cyclocarya paliurus leaves left after further screening by a crusher;
s5, adding the crushed cyclocarya paliurus leaf powder into an extraction tank of raw material wine, mixing and stirring by using stirring equipment, and adding aromatic ester in a certain proportion in the stirring process;
s6, after stirring, sealing the extraction tank, and standing and sealing for four to six days at thirty to forty ℃;
s7, taking out the stock solution of the medicinal liquor after soaking and extraction, purifying and filtering the stock solution by a filter, and removing extraction residues;
s8, filling the purified and filtered medicinal liquor stock solution into a medicinal liquor bottle filled with three cyclocarya paliurus leaves through an automatic filling assembly line, and sealing;
and S9, finally, uniformly packaging and sealing the filled medicinal liquor and transferring the medicinal liquor into a warehouse through internal logistics.
Preferably, the cyclocarya paliurus raw material is a semi-finished product raw material obtained by performing preliminary de-enzyming, rinsing and drying on cyclocarya paliurus leaves picked in the current year.
Preferably, the raw material wine is distilled wine with the alcoholic strength of 30% -45% brewed by corn.
Preferably, the aromatic ester is formed by mixing 80% -90% of ethyl acetate and 10% -20% of isoamyl acetate.
Preferably, the weight percentages of the cyclocarya paliurus leaf powder, the raw material wine and the aromatic ester are respectively 3% -5%, 95% -97% and 0.05% -0.09%.
Preferably, the specification proportion of the cyclocarya paliurus leaves to the medicinal liquor is that three cyclocarya paliurus leaves are added into two hundred milliliters of medicinal liquor.
(III) advantageous effects
The invention provides a process for preparing medicinal liquor containing cyclocarya paliurus. The method has the following beneficial effects:
1. according to the invention, through the sorting process, the cyclocarya paliurus leaves with good quality are screened out and placed in the medicinal liquor bottle, so that the medicinal efficacy can still be dispersed when the medicinal liquor is stored, the quality of the medicinal liquor is prolonged, the attractiveness of the medicinal liquor is improved, and the commercial competitiveness of the medicinal liquor is enhanced.
2. According to the invention, the low-grade cyclocarya paliurus leaves are subjected to crushing treatment, so that the soaking and extracting efficiency can be greatly improved, the production time is shortened, the production cost is reduced, and the commercial value is improved.
3. The invention can be produced in large scale, can be produced all year round without being limited by climate, has high utilization rate of raw materials, improves the productivity of the medicinal liquor and further improves the commercial value.
Drawings
FIG. 1 is a process flow diagram of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows:
as shown in the figure, the embodiment of the invention provides a process for preparing medicinal liquor containing cyclocarya paliurus, which comprises cyclocarya paliurus raw materials, raw material wine and aromatic ester, and comprises the following steps in a growing season of cyclocarya paliurus leaves:
s1, rinsing the cyclocarya paliurus raw material in a cleaning pool, fishing out the cyclocarya paliurus raw material after cleaning, and sterilizing by ultraviolet rays in the drying process;
s2, sorting the dried cyclocarya paliurus raw material into high-grade cyclocarya paliurus leaves and low-grade cyclocarya paliurus leaves according to the integrity, size and shape through a sorting production line;
s3, the sorted high-grade cyclocarya paliurus leaves enter another assembly line for further selection, and the sorted high-grade cyclocarya paliurus leaves are divided into three cyclocarya paliurus leaves, and the three cyclocarya paliurus leaves are filled into a medicinal liquor bottle to be filled, so that the medicinal liquor still can disperse the medicinal efficacy when being stored, the quality of the medicinal liquor is prolonged, the attractiveness of the medicinal liquor is improved, and the commercial competitiveness of the medicinal liquor is enhanced;
s4, uniformly crushing the sorted low-grade cyclocarya paliurus leaves and the high-grade cyclocarya paliurus leaves left after further screening by using a crusher, so that the efficiency of soaking and extracting can be greatly improved, the production time is shortened, the production cost is reduced, and the commercial value is improved;
s5, adding the crushed cyclocarya paliurus leaf powder into an extraction tank of raw material wine, mixing and stirring by using stirring equipment, and adding a certain proportion of aromatic ester in the stirring process to improve the taste and flavor of the medicinal liquor and enhance the market competitiveness of the medicinal liquor;
s6, after stirring, sealing the extraction tank, standing and sealing for six days at thirty ℃ for extracting the effective components of cyclocarya paliurus;
s7, taking out the stock solution of the medicinal liquor after soaking and extraction, purifying and filtering the stock solution by a filter, and removing extraction residues;
s8, filling the purified and filtered medicinal liquor stock solution into a medicinal liquor bottle filled with three cyclocarya paliurus leaves through an automatic filling assembly line, and sealing;
and S9, finally, uniformly packaging and sealing the filled medicinal liquor and transferring the medicinal liquor into a warehouse through internal logistics.
The cyclocarya paliurus raw material is a semi-finished product raw material obtained by preliminarily deactivating enzymes, rinsing and drying cyclocarya paliurus leaves picked in the current year, has certain storage capacity and reduces interference of seasonal climate, the raw material wine is distilled wine with the alcoholic strength of 30-45% brewed from corn, the raw material cost is low, the taste is good, aromatic ester is formed by mixing 80-90% of ethyl acetate and 10-20% of isoamyl acetate, so that the wine has certain fruit fragrance, the weight percentages of cyclocarya paliurus leaf powder, the raw material wine and the aromatic ester are 3-5%, 95-97% and 0.05-0.09%, and the specification ratio of the cyclocarya paliurus leaves to the medicinal wine is that three cyclocarya paliurus leaves are added into two hundred milliliters of medicinal wine.
Example two:
the difference between the present embodiment and the first embodiment is: in the season of the high yield of the cyclocarya paliurus leaves, the extraction tank can be sealed, and is placed at the temperature of forty ℃ for standing and sealing for four days, then purification and filtration can be carried out through the filter, extraction residues are removed for subsequent filling, the production time is reduced, the production cost of the medicinal liquor is further reduced, and the commercial value is improved.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (6)

1. A process for preparing medicated wine containing cyclocarya paliurus comprises cyclocarya paliurus raw materials, raw material wine and aromatic ester, and is characterized in that: the process comprises the following steps:
s1, rinsing the cyclocarya paliurus raw material in a cleaning pool, fishing out the cyclocarya paliurus raw material after cleaning, and sterilizing by ultraviolet rays in the drying process;
s2, sorting the dried cyclocarya paliurus raw material into high-grade cyclocarya paliurus leaves and low-grade cyclocarya paliurus leaves according to the integrity, size and shape through a sorting production line;
s3, feeding the sorted high-grade cyclocarya paliurus leaves into another production line for further selection, and filling the leaves into a medicinal liquor bottle to be filled according to the specification of one part of three cyclocarya paliurus leaves;
s4, uniformly crushing the sorted low-grade cyclocarya paliurus leaves and the high-grade cyclocarya paliurus leaves left after further screening by a crusher;
s5, adding the crushed cyclocarya paliurus leaf powder into an extraction tank of raw material wine, mixing and stirring by using stirring equipment, and adding aromatic ester in a certain proportion in the stirring process;
s6, after stirring, sealing the extraction tank, and standing and sealing for four to six days at thirty to forty ℃;
s7, taking out the stock solution of the medicinal liquor after soaking and extraction, purifying and filtering the stock solution by a filter, and removing extraction residues;
s8, filling the purified and filtered medicinal liquor stock solution into a medicinal liquor bottle filled with three cyclocarya paliurus leaves through an automatic filling assembly line, and sealing;
and S9, finally, uniformly packaging and sealing the filled medicinal liquor and transferring the medicinal liquor into a warehouse through internal logistics.
2. The manufacturing process of the medicinal liquor containing cyclocarya paliurus according to claim 1, which is characterized in that: the cyclocarya paliurus raw material is a semi-finished product raw material obtained by carrying out primary de-enzyming, rinsing and drying on cyclocarya paliurus leaves picked in the current year.
3. The manufacturing process of the medicinal liquor containing cyclocarya paliurus according to claim 1, which is characterized in that: the raw material wine is distilled wine with the alcoholic strength of 30-45 percent brewed by corn.
4. The manufacturing process of the medicinal liquor containing cyclocarya paliurus according to claim 1, which is characterized in that: the aromatic ester is formed by mixing 80% -90% of ethyl acetate and 10% -20% of isoamyl acetate.
5. The manufacturing process of the medicinal liquor containing cyclocarya paliurus according to claim 1, which is characterized in that: the weight percentages of the cyclocarya paliurus leaf powder, the raw material wine and the aromatic ester are respectively 3% -5%, 95% -97% and 0.05% -0.09%.
6. The manufacturing process of the medicinal liquor containing cyclocarya paliurus according to claim 1, which is characterized in that: the specification ratio of the cyclocarya paliurus leaves to the medicinal liquor is that three cyclocarya paliurus leaves are added into two hundred milliliters of medicinal liquor.
CN202010577430.5A 2020-06-23 2020-06-23 Process for preparing medicated liquor containing cyclocarya paliurus Pending CN111617133A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106381257A (en) * 2016-08-31 2017-02-08 贵州百佳尚品农业综合开发有限公司 Cyclocarya paliurus wine formula and preparation method thereof
CN107586641A (en) * 2017-09-12 2018-01-16 茂名阿奎叔食品有限公司 A kind of Qingqian Willow leaf tea wine
CN107603806A (en) * 2017-09-28 2018-01-19 浙江农林大学 The production method of low red rice yellow wine rich in Qingqian Willow leaf active ingredient

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106381257A (en) * 2016-08-31 2017-02-08 贵州百佳尚品农业综合开发有限公司 Cyclocarya paliurus wine formula and preparation method thereof
CN107586641A (en) * 2017-09-12 2018-01-16 茂名阿奎叔食品有限公司 A kind of Qingqian Willow leaf tea wine
CN107603806A (en) * 2017-09-28 2018-01-19 浙江农林大学 The production method of low red rice yellow wine rich in Qingqian Willow leaf active ingredient

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
北京市糖业烟酒公司编: "《中国酒》", 30 November 1980, 中国时政经济出版社 *

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Application publication date: 20200904