CN111548134A - 一种新型复合陶瓷材料的制造方法 - Google Patents

一种新型复合陶瓷材料的制造方法 Download PDF

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CN111548134A
CN111548134A CN202010407593.9A CN202010407593A CN111548134A CN 111548134 A CN111548134 A CN 111548134A CN 202010407593 A CN202010407593 A CN 202010407593A CN 111548134 A CN111548134 A CN 111548134A
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鄢永高
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Abstract

本发明公开了一种新型复合陶瓷材料的制造方法,其步骤包括:(1)称取二氧化硅气凝胶粉体、陶瓷粉末和粘接剂并搅拌均匀,制成内芯混合材料;(2):将内芯混合材料填充入模具并烘烤;(3):将烘烤后的内芯从模具中取出并烧结;(4):称取耐磨金属粉末、陶瓷粉末和粘接剂并搅拌均匀,制成耐磨外层材料;(5):将耐磨外层材料浇筑到二次烘烤模具中烘烤;(6):孔洞填充;(7):将烘干后的复合陶瓷放入烧结炉进行烧结;(8):自然冷却。本发明的一种新型复合陶瓷材料的制造方法,步骤简便,耗时较短,且制造出的复合陶瓷材料,在具有优秀的耐磨性能的同时,还具有较轻的密度,减轻了施工的难度,大大提高了其实用性。

Description

一种新型复合陶瓷材料的制造方法
技术领域
本发明涉及陶瓷材料制造领域,具体是一种新型复合陶瓷材料的制造方法。
背景技术
陶瓷材料因其出色的耐热、耐压和耐火性能,在采矿、建筑等领域受到青睐;现有技术中的陶瓷材料的耐磨性能较差,而向陶瓷中加入过多的耐磨金属材料则会增加复合材料的密度,间接降低了实用性,增大了施工难度。
发明内容
为解决现有技术中存在的技术问题,本发明的目的是提供一种新型复合陶瓷材料的制造方法。
本发明采用的技术方案是:一种新型复合陶瓷材料的制造方法,包括如下步骤:
(1):称取二氧化硅气凝胶粉体、陶瓷粉末和粘接剂并搅拌均匀,制成内芯混合材料;
(2):将内芯混合材料填充入模具型腔内成型,并与模具一同放入低温烘烤炉中烘烤3小时;
(3):将烘烤后的内芯从模具中取出,并自然冷却60分钟后,放入烧结炉中烧结;烧结时间为60-120分钟;烧结温度为1200-1500℃;烧结完成后,将内芯自然冷却,即完成轻质内芯的制作;
(4):称取耐磨金属粉末、陶瓷粉末和粘接剂并搅拌均匀,制成耐磨外层材料;
(5):将烧结好的轻质内芯放入二次烘烤模具中,通过模具内部的夹持柱固定;将耐磨外层材料浇筑到二次烘烤模具中,并将模具放入烘烤炉中烘烤1小时;待烘烤完成后将复合陶瓷取出,自然冷却;
(6):将耐磨外层材料填充进复合陶瓷上的孔洞中,并将复合陶瓷放入烘干炉进行烘干3小时;
(7):将烘干后的复合陶瓷放入烧结炉进行烧结,烧结时间为2-5小时,烧结温度为1300-1550℃;
(8):待烧结完成后,将复合陶瓷从烧结炉中取出并自然冷却,即完成一种新型复合陶瓷材料的制造。
优选地,所述步骤(1)中称取的二氧化硅气凝胶粉体与陶瓷粉末的重量比为1:1-2;所述粘接剂的重量为内芯混合材料总重量的5%。
优选地,所述陶瓷粉末为氧化铝、氧化锆、碳化硅、碳化钛、碳化钨和氮化钛中的一种或多种混合而成。
优选地,所述步骤(4)中的耐磨金属粉末、陶瓷粉末和粘接剂之间的重量比为1:1-2:0.5。
优选地,所述耐磨金属粉末使用高铬铸铁粉末、高锰钢粉末、碳化铬粉末和碳化钨粉末中的一种或以上混合而成。
本发明的一种新型复合陶瓷材料的制造方法,步骤简便,耗时较短,且制造出的复合陶瓷材料,在具有优秀的耐磨性能的同时,还具有较轻的密度,减轻了施工的难度,大大提高了其实用性。
具体实施方式
下面结合实施例对本发明作进一步详细说明。
实施例
制造一批新型复合陶瓷材料,包括如下步骤:
(1):按重量份配比称取二氧化硅气凝胶粉体1份、陶瓷粉末1.5份和粘接剂0.3份并搅拌均匀,制成内芯混合材料;
(2):将内芯混合材料填充入模具型腔内成型,并与模具一同放入低温烘烤炉中烘烤3小时;
(3):将烘烤后的内芯从模具中取出,并自然冷却60分钟后,放入烧结炉中烧结;烧结时间为60-120分钟;烧结温度为1200-1500℃;烧结完成后,将内芯自然冷却,即完成轻质内芯的制作;
(4):按重量份配比称取耐磨金属粉末1份、陶瓷粉末1.5份和粘接剂0.5份并搅拌均匀,制成耐磨外层材料;
(5):将烧结好的轻质内芯放入二次烘烤模具中,通过模具内部的夹持柱固定;将耐磨外层材料浇筑到二次烘烤模具中,并将模具放入烘烤炉中烘烤1小时;待烘烤完成后将复合陶瓷取出,自然冷却;
(6):将耐磨外层材料填充进复合陶瓷上的孔洞中,并将复合陶瓷放入烘干炉进行烘干3小时;
(7):将烘干后的复合陶瓷放入烧结炉进行烧结,烧结时间为2-5小时,烧结温度为1300-1550℃;
(8):待烧结完成后,将复合陶瓷从烧结炉中取出并自然冷却,即完成一种新型复合陶瓷材料的制造。
所述陶瓷粉末为氧化铝、氧化锆、碳化硅、碳化钛、碳化钨和氮化钛混合而成;
所述耐磨金属粉末使用高铬铸铁粉末、高锰钢粉末、碳化铬粉末和碳化钨粉末混合而成。
该批次制造的复合陶瓷,具有较好的耐磨性能,且密度较同类产品下降30%-50%。

Claims (5)

1.一种新型复合陶瓷材料的制造方法,其特征在于,包括如下步骤:
(1):称取二氧化硅气凝胶粉体、陶瓷粉末和粘接剂并搅拌均匀,制成内芯混合材料;
(2):将内芯混合材料填充入模具型腔内成型,并与模具一同放入低温烘烤炉中烘烤3小时;
(3):将烘烤后的内芯从模具中取出,并自然冷却60分钟后,放入烧结炉中烧结;烧结时间为60-120分钟;烧结温度为1200-1500℃;烧结完成后,将内芯自然冷却,即完成轻质内芯的制作;
(4):称取耐磨金属粉末、陶瓷粉末和粘接剂并搅拌均匀,制成耐磨外层材料;
(5):将烧结好的轻质内芯放入二次烘烤模具中,通过模具内部的夹持柱固定;将耐磨外层材料浇筑到二次烘烤模具中,并将模具放入烘烤炉中烘烤1小时;待烘烤完成后将复合陶瓷取出,自然冷却;
(6):将耐磨外层材料填充进复合陶瓷上的孔洞中,并将复合陶瓷放入烘干炉进行烘干3小时;
(7):将烘干后的复合陶瓷放入烧结炉进行烧结,烧结时间为2-5小时,烧结温度为1300-1550℃;
(8):待烧结完成后,将复合陶瓷从烧结炉中取出并自然冷却,即完成一种新型复合陶瓷材料的制造。
2.根据权利要求1所述的一种新型复合陶瓷材料的制造方法,其特征在于,所述步骤(1)中称取的二氧化硅气凝胶粉体与陶瓷粉末的重量比为1:1-2;所述粘接剂的重量为内芯混合材料总重量的5%。
3.根据权利要求1或2所述的一种新型复合陶瓷材料的制造方法,其特征在于,所述陶瓷粉末为氧化铝、氧化锆、碳化硅、碳化钛、碳化钨和氮化钛中的一种或多种混合而成。
4.根据权利要求1所述的一种新型复合陶瓷材料的制造方法,其特征在于,所述步骤(4)中的耐磨金属粉末、陶瓷粉末和粘接剂之间的重量比为1:1-2:0.5。
5.根据权利要求1或4所述的一种新型复合陶瓷材料的制造方法,其特征在于,所述耐磨金属粉末使用高铬铸铁粉末、高锰钢粉末、碳化铬粉末和碳化钨粉末中的一种或以上混合而成。
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