CN111543548A - Compound granular origanum oil premix and preparation method thereof - Google Patents
Compound granular origanum oil premix and preparation method thereof Download PDFInfo
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- CN111543548A CN111543548A CN202010481907.XA CN202010481907A CN111543548A CN 111543548 A CN111543548 A CN 111543548A CN 202010481907 A CN202010481907 A CN 202010481907A CN 111543548 A CN111543548 A CN 111543548A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
- A23K10/37—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/105—Aliphatic or alicyclic compounds
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/158—Fatty acids; Fats; Products containing oils or fats
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
- A23K20/28—Silicates, e.g. perlites, zeolites or bentonites
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K40/00—Shaping or working-up of animal feeding-stuffs
- A23K40/10—Shaping or working-up of animal feeding-stuffs by agglomeration; by granulation, e.g. making powders
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
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Abstract
The invention discloses a compound granular oregano oil premix and a preparation method thereof, belonging to the technical field of animal feed additive processing and comprising the following raw materials in parts by weight: 3-7 parts of oregano oil, 0.5-2 parts of a flavoring agent I, 1-4 parts of a flavoring agent II, 3-7 parts of an inorganic auxiliary agent, 1-4 parts of an emulsifying agent and 3-5 parts of purified water, wherein the inorganic auxiliary agent is one or more of diatomite, silicon dioxide and montmorillonite. According to the compound granular oregano oil, the uniform and controllable adsorption of the oregano oil and the flavoring agent I is regulated and controlled by the emulsifier, so that the uniform and stable drug effect of the compound granular oregano oil is ensured; the flavoring agent I (garlic oil, geranium oil and cypress oil) and the flavoring agent II (pomegranate rind, dandelion and phellodendron bark) not only have the taste of the compound granular oregano oil premix which is adjusted from inside to outside and promote the feeding and digestion of the livestock, but also can improve the drug effect by the synergistic effect of the oregano oil, thereby reducing the dosage of the invention.
Description
Technical Field
The invention belongs to the technical field of animal feed additive processing, and particularly relates to a compound granular origanum oil premix and a preparation method thereof.
Background
Oregano oil is volatile oil extracted from origanum vulgare (ORIGZNUM vulgare) of origanum of Labiatae, and mainly comprises carvacrol and thymol, wherein the ratio of carvacrol to thymol is the main index for determining the bactericidal effect of origanum vulgare oil. Has strong antibacterial and bacteriostatic effects of clearing heat, eliminating dampness, dispelling summerheat, relieving exterior syndrome, and regulating qi-flowing. Is one of the feed drug additives approved by the Ministry of agriculture in China, and is a pure natural traditional Chinese medicine additive with higher active ingredient ratio, which is safe, efficient, green and free of incompatibility.
The oregano oil has the effects of sterilization, bacteriostasis and antioxidation, has better effects on preventing and treating bacterial diseases of digestive tracts of livestock and poultry, such as escherichia coli, salmonella and staphylococcus aureus, and is not easy to generate drug resistance. The oregano oil has good antibacterial effect and also has the effect of promoting the growth of livestock and poultry, so the oregano oil is widely applied. Most of common preparations supplied in the market are solution agents and premix agents, and are mainly used for preventing and treating diarrhea caused by pigs, chickens, escherichia coli and salmonella. Also used for promoting the growth of livestock and poultry and improving the feed conversion rate, namely, the chemical drug volume of the pharmacopoeia of the people's republic of China and the use guideline of veterinary drugs, the second 00 five-year edition, the Chinese agriculture publishing house, pages 92 to 93).
However, the origanum oil solution is difficult to be uniformly mixed with feed due to small dosage, so that the dosage is difficult to control, the origanum oil solution is directly taken orally, and the origanum oil solution is often refused by sick livestock due to thick smell, thereby causing great inconvenience for use. The origanum oil premix improves the use convenience and can be uniformly mixed into feed for application. Publication No. CN102511666A discloses an origanum oil premix for livestock and poultry and a preparation method thereof, wherein the origanum oil premix comprises 2.5-10% of origanum oil, 2.5-10% of silicon dioxide powder and 80-95% of montmorillonite powder. The new premix product composed of the origanum oil and the montmorillonite powder has small particle size of the finished product, good fluidity and easy and uniform material mixing. Due to the existence of the surface energy of the montmorillonite powder and the oregano oil, the amount of the oregano oil adsorbed by the montmorillonite powder is small; in addition, although the oil premix has small particle size, good fluidity and easy and uniform mixing, the existence of the pungent smell of the oregano oil can still cause the refusal of the livestock and poultry.
Disclosure of Invention
The invention aims to: aiming at the problems of the existing oregano oil adsorption effect and poor taste, the invention provides the compound granular oregano oil premix and the preparation method thereof, which are convenient for regulating and controlling the oregano oil adsorption quantity and have good taste.
The technical scheme adopted by the invention is as follows:
a compound granular origanum oil premix is composed of the following raw materials in parts by weight: 3-7 parts of oregano oil, 0.5-2 parts of a flavoring agent I, 1-4 parts of a flavoring agent II, 3-7 parts of an inorganic auxiliary agent, 1-4 parts of an emulsifying agent and 3-5 parts of purified water, wherein the inorganic auxiliary agent is one or more of diatomite, silicon dioxide and montmorillonite.
According to the compound granular oregano oil, the uniform and controllable adsorption of the oregano oil and the flavoring agent I is regulated and controlled by the emulsifier, so that the uniform and stable drug effect of the compound granular oregano oil is ensured; the flavoring agent I (garlic oil, geranium oil and cypress oil) and the flavoring agent II (pomegranate rind, dandelion and phellodendron bark) not only have the taste of the compound granular oregano oil premix which is adjusted from inside to outside and promote the feeding and digestion of the livestock, but also can improve the drug effect by the synergistic effect of the oregano oil, thereby reducing the dosage of the invention.
Preferably, the flavoring agent I is one or more of garlic oil, geranium oil and cypress oil.
Preferably, the flavoring agent II is one or more of pomegranate rind, dandelion and phellodendron.
Preferably, the emulsifier is one or more of poloxamer, tween 80 and polyglycerol fatty acid ester.
Preferably, the feed consists of the following raw materials in parts by weight: 5 parts of oregano oil, 1 part of flavoring agent I, 2 parts of flavoring agent II, 6 parts of inorganic auxiliary agent, 2 parts of emulsifier and 3-5 parts of purified water, wherein the flavoring agent I is garlic oil, the flavoring agent II is pomegranate rind, the inorganic auxiliary agent is diatomite, and the emulsifier is poloxamer.
Preferably, the feed consists of the following raw materials in parts by weight: 5 parts of oregano oil, 1 part of flavoring agent I, 2 parts of flavoring agent II, 5 parts of inorganic auxiliary agent, 3 parts of emulsifier and 3-5 parts of purified water, wherein the flavoring agent I is geranium oil, the flavoring agent II is dandelion, the inorganic auxiliary agent is silicon dioxide, and the emulsifier is tween 80.
Preferably, the feed consists of the following raw materials in parts by weight: 5 parts of oregano oil, 1 part of flavoring agent I, 3 parts of flavoring agent II, 4 parts of inorganic auxiliary agent, 2 parts of emulsifying agent and 3-5 parts of purified water, wherein the flavoring agent I is cypress oil, the flavoring agent II is phellodendron, the inorganic auxiliary agent is montmorillonite, and the emulsifying agent is polyglycerol fatty acid ester.
A preparation method of a compound granular origanum oil premix comprises the following steps:
s1, adding 1 part of oregano oil and flavoring agent I into purified water in certain parts by weight, and then adding an emulsifier for emulsification to form suspension beads with the particle size within the range of 1-2 mu m;
s2, uniformly adsorbing the emulsified mixture onto an inorganic auxiliary agent to obtain a powdery substance;
s3, mixing a flavoring agent II with a particle size of 50-70 meshes with the powdery substance;
s4, the mixture obtained in the step S3 is pressed, crushed, discharged and sieved to obtain the 100-120-mesh compound origanum oil premix.
Compared with the prior art, the invention has the beneficial effects that:
(1) according to the novel oregano oil premix prepared by the method, a great amount of screening and optimization are carried out on the flavoring agent I, the flavoring agent II, the preparation process and the like, so that the special pungent smell of oregano oil can be covered from inside to outside, the volatilization of the oregano oil can be well prevented, and the product stability is good; the preparation method is simple and easy to implement, has low cost and is suitable for industrial large-scale production;
(2) according to the compound granular oregano oil premix, the flavor of the compound granular oregano oil premix can be adjusted from inside to outside through the flavoring agent I (garlic oil, geranium oil and cypress oil) and the flavoring agent II (pomegranate rind, dandelion and golden cypress), the feeding and digestion of livestock are promoted, and the drug effect can be improved under the synergistic effect of the compound granular oregano oil premix and the oregano oil, so that the dosage of the compound granular oregano oil premix is reduced, and the effect is good;
(3) compared with the prior art, the finished product has small particle size (100-120 meshes), fine powder, good fluidity, easy and uniform mixing, and good absorption, utilization and feeding effects.
Detailed Description
The present invention will be described in further detail in order to make the objects, technical solutions and advantages of the present invention more apparent. It should be understood that the detailed description and specific examples, while indicating the preferred embodiment of the invention, are intended for purposes of illustration only and are not intended to limit the scope of the invention.
Example 1
A compound granular origanum oil premix is composed of the following raw materials in parts by weight: 5 parts of oregano oil, 1 part of flavoring agent I, 2 parts of flavoring agent II, 6 parts of inorganic auxiliary agent, 2 parts of emulsifier and 3-5 parts of purified water, wherein the flavoring agent I is garlic oil, the flavoring agent II is pomegranate rind, the inorganic auxiliary agent is diatomite, and the emulsifier is poloxamer.
A preparation method of a compound granular origanum oil premix comprises the following steps:
s1, adding 1 part of oregano oil and flavoring agent I into purified water in certain parts by weight, adding an emulsifier for emulsification to form suspension beads with the particle size within the range of 1-2 mu m, and characterizing by using a particle sizer, which is the same as the description below;
s2, uniformly adsorbing the emulsified mixture onto an inorganic auxiliary agent to obtain a powdery substance;
s3, mixing a flavoring agent II with a particle size of 50-70 meshes with the powdery substance;
s4, the mixture obtained in the step S3 is pressed, crushed, discharged and sieved to obtain the 100-120-mesh compound origanum oil premix.
Example 2
A compound granular origanum oil premix is composed of the following raw materials in parts by weight: 5 parts of oregano oil, 1 part of flavoring agent I, 2 parts of flavoring agent II, 5 parts of inorganic auxiliary agent, 3 parts of emulsifier and 3-5 parts of purified water, wherein the flavoring agent I is geranium oil, the flavoring agent II is dandelion, the inorganic auxiliary agent is silicon dioxide, and the emulsifier is tween 80.
A preparation method of a compound granular origanum oil premix comprises the following steps:
s1, adding 1 part of oregano oil and flavoring agent I into purified water in certain parts by weight, and then adding an emulsifier for emulsification to form suspension beads with the particle size within the range of 1-2 mu m;
s2, uniformly adsorbing the emulsified mixture onto an inorganic auxiliary agent to obtain a powdery substance;
s3, mixing a flavoring agent II with a particle size of 50-70 meshes with the powdery substance;
s4, the mixture obtained in the step S3 is pressed, crushed, discharged and sieved to obtain the 100-120-mesh compound origanum oil premix.
Example 3
A compound granular origanum oil premix is composed of the following raw materials in parts by weight: 5 parts of oregano oil, 1 part of flavoring agent I, 3 parts of flavoring agent II, 4 parts of inorganic auxiliary agent, 2 parts of emulsifying agent and 3-5 parts of purified water, wherein the flavoring agent I is cypress oil, the flavoring agent II is phellodendron, the inorganic auxiliary agent is montmorillonite, and the emulsifying agent is polyglycerol fatty acid ester.
A preparation method of a compound granular origanum oil premix comprises the following steps:
s1, adding 1 part of oregano oil and flavoring agent I into purified water in certain parts by weight, and then adding an emulsifier for emulsification to form suspension beads with the particle size within the range of 1-2 mu m;
s2, uniformly adsorbing the emulsified mixture onto an inorganic auxiliary agent to obtain a powdery substance;
s3, mixing a flavoring agent II with a particle size of 50-70 meshes with the powdery substance;
s4, the mixture obtained in the step S3 is pressed, crushed, discharged and sieved to obtain the 100-120-mesh compound origanum oil premix.
Comparative example 1
Compared with the example 1, the emulsifying agent is not added for emulsification, and the rest of the example 1 is the same.
Comparative example 2
In comparison with example 1, the same procedure as in example 1 was repeated except that neither seasoning I nor seasoning II was added.
Comparative example 3
In comparison with example 1, the same procedure as in example 1 was followed without adding flavoring agent I.
Experimental part
1. Taking the oregano oil premix prepared in the examples 1-3 and the comparative examples 1-2, carrying out sensory test for 2 times, wherein the size of the pungent smell is marked by plus, and the larger the plus, the larger the pungent smell is; sensory test I directly performs pungent odor test, and sensory test II takes 1g of the prepared oregano oil premix and puts the oregano oil premix into 5mL of purified water for performing pungent odor test; and simultaneously carrying out the detection of the stability of the content of the oregano oil (the sample is heated for 2 hours at the temperature of 60 +/-1 ℃, and the content of the oregano oil in the heated premix is measured by using a gas chromatography, wherein the content is expressed by marked percentage, and the marked percentage before heating is all set as 100%). The results of the measurements are shown in the following table:
table 1 odor and stability test results of the present invention
As can be seen from the table, the flavoring agent I (garlic oil, geranium oil and cypress oil) and the flavoring agent II (pomegranate rind, dandelion and phellodendron bark) have the taste of the compound granular oregano oil premix adjusted from inside to outside, and the product stability is good.
2. Clinical experiments
Test animals: the test chicken 600 is provided by a certain feed breeding company and is healthy.
The experimental feed: the complete granulated feed for chicken is provided by a certain feed breeding company
Selecting 600 test chickens of 1-2 months old with the weight of 300-; the test groups were randomly divided into 6 groups, 3 test groups and 3 control groups, and the number of the test groups was 100. Every 100 jin of feed of each test group is mixed with 1.5 jin of corresponding 2 jin of the product of the invention in the embodiment 1-3, and the product is fed normally; and (3) mixing 2 jin of corresponding products in the control groups 1-3 with 2 jin of feed in each 100 jin of feed in the control groups, feeding normally, and counting the weight gain rate after one month.
Table 2 results of measuring amounts of the present invention
| Experimental group 1 | Experimental group 2 | Experimental group 3 | Control group 1 | Control group 2 | Control group 3 | |
| The weight gain rate% | 45 | 43 | 46 | 34 | 25 | 29 |
In conclusion, the uniform and controllable adsorption of the compound granular oregano oil and the flavoring agent I is regulated and controlled by the emulsifier, so that the uniform and stable drug effect of the compound granular oregano oil is ensured; the flavoring agent I (garlic oil, geranium oil and cypress oil) and the flavoring agent II (pomegranate rind, dandelion and phellodendron bark) not only have the taste of the compound granular oregano oil premix which is adjusted from inside to outside and promote the feeding and digestion of the livestock, but also can improve the drug effect under the synergistic action of the oregano oil, have small dosage and good effect and improve the conversion rate of the feed.
The above-mentioned embodiments only express the specific embodiments of the present application, and the description thereof is more specific and detailed, but not construed as limiting the scope of the present application. It should be noted that, for those skilled in the art, without departing from the technical idea of the present application, several changes and modifications can be made, which are all within the protection scope of the present application.
Claims (8)
1. The compound granular origanum oil premix is characterized by comprising the following raw materials in parts by weight: 3-7 parts of oregano oil, 0.5-2 parts of a flavoring agent I, 1-4 parts of a flavoring agent II, 3-7 parts of an inorganic auxiliary agent, 1-4 parts of an emulsifying agent and 3-5 parts of purified water, wherein the inorganic auxiliary agent is one or more of diatomite, silicon dioxide and montmorillonite.
2. The compound granular oregano oil premix as claimed in claim 1, wherein the flavoring agent I is one or more of garlic oil, geranium oil and cypress oil.
3. The compound granular oregano oil premix as claimed in claim 1, wherein the flavoring agent II is one or more of pomegranate rind, dandelion and phellodendron bark.
4. The compound granular oregano oil premix as claimed in claim 1, wherein the emulsifier is one or more of poloxamer, tween 80, and polyglycerol fatty acid ester.
5. The compound granular oregano oil premix as claimed in claim 1, which is prepared from the following raw materials in parts by weight: 5 parts of oregano oil, 1 part of flavoring agent I, 2 parts of flavoring agent II, 6 parts of inorganic auxiliary agent, 2 parts of emulsifier and 3-5 parts of purified water, wherein the flavoring agent I is garlic oil, the flavoring agent II is pomegranate rind, the inorganic auxiliary agent is diatomite, and the emulsifier is poloxamer.
6. The compound granular oregano oil premix as claimed in claim 1, which is prepared from the following raw materials in parts by weight: 5 parts of oregano oil, 1 part of flavoring agent I, 2 parts of flavoring agent II, 5 parts of inorganic auxiliary agent, 3 parts of emulsifier and 3-5 parts of purified water, wherein the flavoring agent I is geranium oil, the flavoring agent II is dandelion, the inorganic auxiliary agent is silicon dioxide, and the emulsifier is tween 80.
7. The compound granular oregano oil premix as claimed in claim 1, which is prepared from the following raw materials in parts by weight: 5 parts of oregano oil, 1 part of flavoring agent I, 3 parts of flavoring agent II, 4 parts of inorganic auxiliary agent, 2 parts of emulsifying agent and 3-5 parts of purified water, wherein the flavoring agent I is cypress oil, the flavoring agent II is phellodendron, the inorganic auxiliary agent is montmorillonite, and the emulsifying agent is polyglycerol fatty acid ester.
8. The preparation method of the compound granular oregano oil premix based on any one of claims 1-7, characterized by comprising the following steps:
s1, adding 1 part of oregano oil and flavoring agent I into purified water in certain parts by weight, and then adding an emulsifier for emulsification to form suspension beads with the particle size within the range of 1-2 mu m;
s2, uniformly adsorbing the emulsified mixture onto an inorganic auxiliary agent to obtain a powdery substance;
s3, mixing a flavoring agent II with a particle size of 50-70 meshes with the powdery substance;
s4, the mixture obtained in the step S3 is pressed, crushed, discharged and sieved to obtain the 100-120-mesh compound origanum oil premix.
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| CN114376080A (en) * | 2020-10-20 | 2022-04-22 | 河北科星药业有限公司 | Cow feed additive containing amino acid, preparation method and application |
| WO2024084216A1 (en) * | 2022-10-20 | 2024-04-25 | Ecospray Ltd | An improved biopesticide |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114376080A (en) * | 2020-10-20 | 2022-04-22 | 河北科星药业有限公司 | Cow feed additive containing amino acid, preparation method and application |
| WO2024084216A1 (en) * | 2022-10-20 | 2024-04-25 | Ecospray Ltd | An improved biopesticide |
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| CN111543548B (en) | 2023-07-28 |
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