CN111530323A - Preparation equipment for producing chemical divinylbenzene catalyst - Google Patents
Preparation equipment for producing chemical divinylbenzene catalyst Download PDFInfo
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- CN111530323A CN111530323A CN202010426106.3A CN202010426106A CN111530323A CN 111530323 A CN111530323 A CN 111530323A CN 202010426106 A CN202010426106 A CN 202010426106A CN 111530323 A CN111530323 A CN 111530323A
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- MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 title claims abstract description 36
- 239000003054 catalyst Substances 0.000 title claims abstract description 23
- 239000000126 substance Substances 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 239000007788 liquid Substances 0.000 claims abstract description 44
- 238000005070 sampling Methods 0.000 claims abstract description 31
- 230000001360 synchronised effect Effects 0.000 claims abstract description 9
- 240000007643 Phytolacca americana Species 0.000 claims description 19
- 238000007789 sealing Methods 0.000 claims description 8
- 238000007790 scraping Methods 0.000 claims description 5
- 230000003068 static effect Effects 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims description 2
- 238000003756 stirring Methods 0.000 abstract description 18
- 238000004140 cleaning Methods 0.000 abstract description 10
- 238000005192 partition Methods 0.000 description 11
- 230000000694 effects Effects 0.000 description 7
- 239000002808 molecular sieve Substances 0.000 description 6
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 6
- 239000007789 gas Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 description 2
- 239000012159 carrier gas Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000005049 silicon tetrachloride Substances 0.000 description 2
- 101150114468 TUB1 gene Proteins 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004523 catalytic cracking Methods 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
- B01F27/11—Stirrers characterised by the configuration of the stirrers
- B01F27/19—Stirrers with two or more mixing elements mounted in sequence on the same axis
- B01F27/191—Stirrers with two or more mixing elements mounted in sequence on the same axis with similar elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/62—Regenerating the filter material in the filter
- B01D29/64—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element
- B01D29/6469—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element scrapers
- B01D29/6476—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element scrapers with a rotary movement with respect to the filtering element
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/60—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
- B01F27/70—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms
- B01F27/701—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms comprising two or more shafts, e.g. in consecutive mixing chambers
- B01F27/706—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms comprising two or more shafts, e.g. in consecutive mixing chambers with all the shafts in the same receptacle
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
- B01F31/44—Mixers with shaking, oscillating, or vibrating mechanisms with stirrers performing an oscillatory, vibratory or shaking movement
- B01F31/441—Mixers with shaking, oscillating, or vibrating mechanisms with stirrers performing an oscillatory, vibratory or shaking movement performing a rectilinear reciprocating movement
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/181—Preventing generation of dust or dirt; Sieves; Filters
- B01F35/187—Preventing generation of dust or dirt; Sieves; Filters using filters in mixers, e.g. during venting
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/75—Discharge mechanisms
- B01F35/754—Discharge mechanisms characterised by the means for discharging the components from the mixer
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
- G01N1/16—Devices for withdrawing samples in the liquid or fluent state with provision for intake at several levels
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The invention provides preparation equipment for producing a chemical divinylbenzene catalyst, relates to the field of chemical catalyst preparation, and solves the problems that sampling work under different liquid level states cannot be simultaneously realized, and a sample is inconvenient to carry and move after sampling; the filter screen of the liquid discharge pipe needs to be disassembled for cleaning during cleaning, and quick cleaning on the basis of non-disassembly cannot be realized; the synchronous reverse stirring and mixing of a plurality of stirring shafts and the linkage work of two stirring structures can not be realized. The preparation equipment for producing the chemical divinylbenzene catalyst comprises a barrel body; the barrel body is filled with liquid. The sliding rod and the elastic part jointly form an elastic reset structure of the mixing plate; the length of poking rod is greater than the distance between pivot and the mixing board, and when the pivot drove the poking rod and rotate, the mixing board was up-and-down reciprocating motion state under the stirring of poking rod this moment to can realize supplementary mixing.
Description
Technical Field
The invention belongs to the technical field of chemical catalyst preparation, and particularly relates to preparation equipment for producing a chemical divinylbenzene catalyst.
Background
Styrene-divinylbenzene copolymers, most of which are produced using homogeneously soluble metallocenes as catalysts. The industrial production mainly comprises 3 processes: namely a continuous fluidized bed process, a continuous self-cleaning reaction kettle process and a continuous stirred tank reaction kettle process.
As in application No.: CN201210417927.6, an apparatus for preparing a catalytic cracking catalyst, comprising: the gas phase ultra-stable reactor can enable a molecular sieve to move from the molecular sieve inlet of the gas phase ultra-stable reactor to the molecular sieve outlet of the gas phase ultra-stable reactor under the condition of not conveying carrier gas, and enables the molecular sieve and the gas phase silicon tetrachloride to contact and react in the gas phase ultra-stable reactor. The device can be used for continuously preparing the high-silicon molecular sieve, can simplify the process flow, does not need to use carrier gas for fluidizing the molecular sieve, and can greatly reduce the consumption of the silicon tetrachloride.
The catalyst preparation apparatus similar to the above application has the following disadvantages at present:
one is that the existing device can not realize sampling work under different liquid level states at the same time when sampling, and the sample is inconvenient to carry and move after sampling; moreover, the filter screen of the liquid discharge pipe of the existing device needs to be disassembled for cleaning during cleaning, and quick cleaning on the basis of non-disassembly cannot be realized; finally, the existing device has a single stirring and mixing structure, and cannot realize synchronous reverse stirring and mixing of a plurality of stirring shafts and linkage work of two stirring structures.
Therefore, in view of the above, research and improvement are made on the existing structure and defects, and a preparation device for producing a chemical divinylbenzene catalyst is provided, so as to achieve the purpose of higher practical value.
Disclosure of Invention
In order to solve the technical problems, the invention provides preparation equipment for producing chemical divinylbenzene catalyst, which aims to solve the problems that the existing device can not realize sampling work under different liquid level states simultaneously during sampling, and the sample is inconvenient to carry and move after sampling; moreover, the filter screen of the liquid discharge pipe of the existing device needs to be disassembled for cleaning during cleaning, and quick cleaning on the basis of non-disassembly cannot be realized; finally, the existing device has a single stirring and mixing structure and cannot realize synchronous reverse stirring and mixing of a plurality of stirring shafts and linkage work of two stirring structures.
The invention is used for producing the purpose and the effect of the preparation equipment of the chemical divinylbenzene catalyst, and is achieved by the following specific technical means:
the preparation equipment for producing the chemical divinylbenzene catalyst comprises a barrel body; the barrel body is filled with liquid, the barrel body is rotatably connected with a mixing structure, and a second mixing structure is further arranged in the barrel body; two groups of three sampling structures are inserted into the barrel body, and a liquid discharge pipe structure is connected to the barrel body in a threaded manner; the drain pipe structure comprises a main pipe, a filter screen, a sleeve, a cylindrical rod and a scraper, wherein the main pipe is in threaded connection with the barrel body, and the end of the main pipe is provided with the filter screen; the sleeve is rotatably connected to the main body pipe, and a cylindrical rod is welded on the sleeve; the end of the cylindrical rod is provided with a scraper which is in contact with the filter screen, and when the sleeve is rotated, the scraper is in a scraping state, so that the filter screen can be quickly cleaned; the fluid-discharge tube structure further comprises a connecting tube, the connecting tube is rotatably connected to the tail end of the sleeve through a sealing bearing, the connecting tube is of a connecting pipeline structure connected with the fluid-discharge hose, and the connecting tube is in a relatively static state when the sleeve is rotated, so that the phenomenon of knotting caused by the fact that the fluid-discharge hose follows twisting can be avoided.
Further, the barrel body is of a rectangular barrel-shaped structure, and the top end face of the barrel body is fixedly connected with a cover plate through a bolt; the mixing structure comprises two rotating shafts and two blades, and the two rotating shafts are both connected to the barrel body in a sealing and rotating mode through sealing bearings; the blades are arranged on the two rotating shafts in a rectangular array mode, and the blades on the two rotating shafts are arranged in a staggered mode.
Furthermore, the mixing structure also comprises poke rods, belt wheels and belts, wherein two poke rods are symmetrically arranged on each rotating shaft, and one belt wheel is arranged on each rotating shaft; the two belt wheels are connected through a belt, a gear used for being connected with a driving motor is further installed on one rotating shaft on the rear side, and the two rotating shafts jointly form a reverse synchronous rotating structure.
Furthermore, the second mixing structure comprises four sliding rods, a mixing plate, a strip-shaped hole and an elastic piece, the four sliding rods are respectively welded at four corner positions of the bottom end face of the inner wall of the barrel body, and the four sliding rods are all of stepped shaft-shaped structures; the mixing plate is connected to the four sliding rods in a sliding manner, and five strip-shaped holes are formed in the top end surface of the mixing plate in a rectangular array shape; every slide bar outer wall all cup joints an elastic component in the position below the hybrid sheet, and slide bar and elastic component have constituteed the elasticity reset structure of hybrid sheet jointly.
Further, the length of toggle rod is greater than the distance between pivot and the mixing plate, and when the pivot drove the toggle rod and rotate, the mixing plate was up-and-down reciprocating motion state under the stirring of toggle rod this moment.
Furthermore, the sampling structure comprises an outer pipe, a liquid inlet hole A, an inner pipe, a hook, an elastic bolt and a liquid inlet hole B, wherein the outer pipe penetrates through the cover plate and is inserted into the barrel body, the outer pipe is of a cylindrical structure, and the outer wall of the outer pipe is provided with five liquid inlet holes A in a rectangular array shape; the inner pipe is provided with two hooks, and the inner pipe is inserted in the outer pipe through the hook lock; the outer wall of the inner pipe is provided with five liquid inlet holes B in a rectangular array shape, and the outer wall of the inner pipe is provided with five liquid inlet holes B in a rectangular array shape; the liquid inlet hole A and the liquid inlet hole B are aligned with each other.
Further, the sampling structure still includes the baffle, the inner tube inner wall is located every feed liquor hole B position department and all welds the baffle of a circular platelike structure, and divides into five sample spaces at the inner tube under the separation of baffle.
Further, the outer tube includes the draw-in groove, two draw-in grooves have been seted up to 90 contained angles on the outer tube top surface, just install an elastic bolt that is used for realizing shutting with the draw-in groove on the inner tube.
Compared with the prior art, the invention has the following beneficial effects:
the sampling structure is improved, the sampling of different liquid levels can be realized through the improvement, and the fast switch-over of sampling state and encapsulated situation still can be realized to sample back sample conveniently carries the transfer, specifically as follows: firstly, a partition plate with a circular plate-shaped structure is welded on the inner wall of the inner pipe at the position of each liquid inlet hole B, and the inner pipe is divided into five sampling spaces under the partition of the partition plate, so that sampling at different liquid levels can be performed at different times; the second, because of the outer tube top is personally submitted 90 contained angles and has been seted up two draw-in grooves, and install one on the inner tube and be used for realizing the elasticity bolt of shutting with the draw-in groove to clockwise 90 degrees rotate the inner tube and anticlockwise 90 degrees rotate the quick switch-over that the inner tube can realize sampling state and encapsulated situation, and switch into and can make things convenient for carrying and the transfer of sample behind the encapsulated situation.
The drain pipe structure is improved, the filter screen can be quickly cleaned under the condition of not being detached through improvement, and the structure is as follows: firstly, as the end of the cylindrical rod is provided with the scraper which is in contact with the filter screen, when the sleeve is rotated, the scraper is in a scraping state, so that the filter screen can be quickly cleaned; the second, still include the connecting pipe because of the fluid-discharge tube structure, the connecting pipe passes through sealed bearing and rotates to be connected at the sleeve pipe tail end, and the connecting pipe is the connecting tube structure of being connected with the flowing back hose, and the connecting pipe is in relative quiescent condition when rotating the sleeve pipe to can avoid the flowing back hose to follow the wrench movement and lead to the phenomenon of knoing.
Improved mixed structure, seen through the improvement and to realize synchronous reverse stirring and mix, and still can realize two mixed structure's linkage work, specifically as follows: firstly, the blades on the two rotating shafts are arranged in a staggered manner, so that the stirring and mixing effects can be improved when the blades are driven to rotate by the two rotating shafts; secondly, the two belt wheels are connected through a belt, a gear used for being connected with a driving motor is further installed on one rotating shaft on the rear side, and the two rotating shafts jointly form a reverse synchronous rotating structure, so that the mixing effect can be improved on the basis of saving the cost of an air source part; thirdly, the sliding rod and the elastic part form an elastic reset structure of the mixing plate; the length of poking rod is greater than the distance between pivot and the mixing board, and when the pivot drove the poking rod and rotate, the mixing board was up-and-down reciprocating motion state under the stirring of poking rod this moment to can realize supplementary mixing.
Drawings
Fig. 1 is a schematic axial view of the present invention.
Fig. 2 is a schematic axial view of the present invention in another direction of fig. 1.
Fig. 3 is a schematic view of the present invention in an axially disassembled configuration.
Fig. 4 is a schematic cross-sectional structure of the present invention.
FIG. 5 is an enlarged, axial view of a sampling structure according to the present invention.
FIG. 6 is a schematic view of a cross-sectional enlarged structure of a sampling structure of the present invention.
Fig. 7 is an enlarged schematic view of fig. 6 a according to the present invention.
Fig. 8 is an enlarged axial view of the drain structure of the present invention.
Fig. 9 is a schematic cross-sectional structure of fig. 8 of the present invention.
In the drawings, the corresponding relationship between the component names and the reference numbers is as follows:
1. a barrel body; 101. a cover plate; 2. a hybrid structure; 201. a rotating shaft; 202. a blade; 203. a poke rod; 204. a pulley; 205. a belt; 3. a second hybrid structure; 301. a slide bar; 302. a mixing plate; 303. a strip-shaped hole; 304. an elastic member; 4. a sampling structure; 401. an outer tube; 40101. a card slot; 402. a liquid inlet hole A; 403. an inner tube; 40301. hooking; 40302. an elastic bolt; 404. a liquid inlet hole B; 405. a partition plate; 5. a drain pipe structure; 501. a main body tube; 502. a filter screen; 503. a sleeve; 504. a cylindrical rod; 505. a squeegee; 506. and (4) connecting the pipes.
Detailed Description
The embodiments of the present invention will be described in further detail with reference to the drawings and examples. The following examples are intended to illustrate the invention but are not intended to limit the scope of the invention.
In the description of the present invention, "a plurality" means two or more unless otherwise specified; the terms "upper", "lower", "left", "right", "inner", "outer", "front", "rear", "head", "tail", and the like, indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, are only for convenience in describing and simplifying the description, and do not indicate or imply that the device or element referred to must have a particular orientation, be constructed in a particular orientation, and be operated, and thus, should not be construed as limiting the invention. Furthermore, the terms "first," "second," "third," and the like are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.
In the description of the present invention, it is to be noted that, unless otherwise explicitly specified or limited, the terms "connected" and "connected" are to be interpreted broadly, e.g., as being fixed or detachable or integrally connected; can be mechanically or electrically connected; may be directly connected or indirectly connected through an intermediate. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.
Example (b):
as shown in figures 1 to 9:
the invention provides a preparation device for producing a chemical divinylbenzene catalyst, which comprises a barrel body 1; the barrel body 1 is filled with liquid, the barrel body 1 is rotatably connected with a mixing structure 2, and a second mixing structure 3 is also arranged in the barrel body 1; two groups of three sampling structures 4 are inserted into the barrel body 1, and a liquid discharge pipe structure 5 is connected to the barrel body 1 in a threaded manner; referring to fig. 8 and 9, the drainage pipe structure 5 includes a main pipe 501, a filter screen 502, a sleeve 503, a cylindrical rod 504 and a scraper 505, the main pipe 501 is screwed on the tub 1, and the filter screen 502 is installed at the head end of the main pipe 501; the sleeve 503 is rotatably connected to the main body pipe 501, and a cylindrical rod 504 is welded on the sleeve 503; a scraper 505 is arranged at the head end of the cylindrical rod 504, the scraper 505 is in contact with the filter screen 502, and when the sleeve 503 is rotated, the scraper 505 is in a scraping state, so that the filter screen 502 can be quickly cleaned; referring to fig. 8 and 9, the drainage tube structure 5 further includes a connection tube 506, the connection tube 506 is rotatably connected to the rear end of the sleeve 503 through a sealed bearing, and the connection tube 506 is a connection tube structure connected to the drainage hose, and the connection tube 506 is in a relatively static state when the sleeve 503 is rotated, so as to prevent the drainage hose from twisting and knotting.
Referring to fig. 4, the barrel 1 is a rectangular barrel structure, and a cover plate 101 is fixedly connected to the top end surface of the barrel 1 through bolts; the mixing structure 2 comprises two rotating shafts 201 and two blades 202, wherein the two rotating shafts 201 are sealed and rotatably connected to the barrel body 1 through sealing bearings; the blades 202 are installed on the two rotating shafts 201 in a rectangular array shape, and the blades 202 on the two rotating shafts 201 are arranged in a staggered shape, so that the stirring and mixing effects can be improved when the two rotating shafts 201 drive the blades 202 to rotate.
Referring to fig. 4, the mixing structure 2 further includes a poke rod 203, a pulley 204 and a belt 205, two poke rods 203 are symmetrically installed on each rotating shaft 201, and one pulley 204 is installed on each rotating shaft 201; the two belt wheels 204 are connected through a belt 205, a gear used for being connected with a driving motor is further installed on one rotating shaft 201 on the rear side, and the two rotating shafts 201 jointly form a reverse synchronous rotating structure, so that the mixing effect can be improved on the basis of saving the cost of air source parts.
Referring to fig. 4, the second mixing structure 3 includes four sliding rods 301, a mixing plate 302, a strip-shaped hole 303 and an elastic member 304, the four sliding rods 301 are respectively welded at four corner positions of the bottom end surface of the inner wall of the barrel body 1, and the four sliding rods 301 are all stepped shaft-shaped structures; the mixing plate 302 is connected to the four sliding rods 301 in a sliding manner, and five strip-shaped holes 303 are formed in the top end surface of the mixing plate 302 in a rectangular array shape; an elastic piece 304 is sleeved on the outer wall of each sliding rod 301 below the mixing plate 302, and the sliding rods 301 and the elastic pieces 304 jointly form an elastic reset structure of the mixing plate 302.
Referring to fig. 4, the length of the poke rod 203 is greater than the distance between the rotating shaft 201 and the mixing plate 302, and when the rotating shaft 201 drives the poke rod 203 to rotate, the mixing plate 302 is in a vertical reciprocating motion state under the poke action of the poke rod 203, so that auxiliary mixing can be realized.
Referring to fig. 6, the sampling structure 4 includes an outer tube 401, a liquid inlet a402, an inner tube 403, a hook 40301, an elastic plug 40302, and a liquid inlet B404, the outer tube 401 passes through the cover plate 101 and is inserted into the barrel 1, the outer tube 401 is a cylindrical structure, and the outer wall of the outer tube 401 is provided with five liquid inlet a402 in a rectangular array; two hooks 40301 are arranged on the inner pipe 403, and the inner pipe 403 is locked and inserted in the outer pipe 401 through the hooks 40301; five liquid inlet holes B404 are formed in the outer wall of the inner pipe 403 in a rectangular array shape, and five liquid inlet holes B404 are formed in the outer wall of the inner pipe 403 in a rectangular array shape; the inlet holes a402 and B404 are positioned in alignment with each other.
Referring to fig. 6, the sampling structure 4 further includes a partition 405, a circular plate-shaped partition 405 is welded to the inner wall of the inner tube 403 at each liquid inlet hole B404, and the inner tube 403 is divided into five sampling spaces under the partition of the partition 405, so that samples at different liquid levels can be taken at different times.
Referring to fig. 6, the outer tube 401 includes a locking groove 40101, two locking grooves 40101 are formed at an included angle of 90 degrees at the top end surface of the outer tube 401, and an elastic bolt 40302 for locking with the locking groove 40101 is installed on the inner tube 403, so that the inner tube 403 can be rotated clockwise 90 degrees and the inner tube 403 can be rotated counterclockwise 90 degrees to realize rapid switching between a sampling state and a sealing state.
The specific use mode and function of the embodiment are as follows:
when in use, during mixing, firstly, the blades 202 on the two rotating shafts 201 are arranged in a staggered manner, so that when the two rotating shafts 201 drive the blades 202 to rotate, the stirring and mixing effects can be improved; secondly, the two belt wheels 204 are connected through the belt 205, a gear for connecting with a driving motor is further installed on one rotating shaft 201 on the rear side, and the two rotating shafts 201 jointly form a reverse synchronous rotating structure, so that the mixing effect can be improved on the basis of saving the cost of an air source part; thirdly, the sliding rod 301 and the elastic member 304 form an elastic reset structure of the mixing plate 302; the length of the poke rod 203 is larger than the distance between the rotating shaft 201 and the mixing plate 302, and when the rotating shaft 201 drives the poke rod 203 to rotate, the mixing plate 302 is in a vertical reciprocating motion state under the poke action of the poke rod 203, so that auxiliary mixing can be realized;
during sampling, firstly, a partition plate 405 with a circular plate-shaped structure is welded on the inner wall of the inner pipe 403 at the position of each liquid inlet hole B404, and the inner pipe 403 is divided into five sampling spaces under the partition of the partition plate 405, so that sampling at different liquid levels can be performed at different time; secondly, two clamping grooves 40101 are formed at an included angle of 90 degrees at the top end face of the outer tube 401, and an elastic bolt 40302 used for locking with the clamping grooves 40101 is installed on the inner tube 403, so that the inner tube 403 can be rotated clockwise 90 degrees and the inner tube 403 can be rotated anticlockwise 90 degrees to realize rapid switching between a sampling state and a sealing state.
When the drain pipe structure 5 is cleaned, firstly, as the head end of the cylindrical rod 504 is provided with the scraper 505, and the scraper 505 is in contact with the filter screen 502, when the sleeve 503 is rotated, the scraper 505 is in a scraping state, so that the filter screen 502 can be quickly cleaned; secondly, because the drain tube structure 5 further comprises a connecting tube 506, the connecting tube 506 is rotatably connected to the tail end of the sleeve 503 through a sealing bearing, and the connecting tube 506 is a connecting tube structure connected with the drain tube, when the sleeve 503 is rotated, the connecting tube 506 is in a relatively static state, so that the phenomenon of knotting caused by the fact that the drain tube follows twisting can be avoided.
The embodiments of the present invention have been presented for purposes of illustration and description, and are not intended to be exhaustive or limited to the invention in the form disclosed. Many modifications and variations will be apparent to those of ordinary skill in the art. The embodiment was chosen and described in order to best explain the principles of the invention and the practical application, and to enable others of ordinary skill in the art to understand the invention for various embodiments with various modifications as are suited to the particular use contemplated.
Claims (8)
1. A preparation equipment for producing chemical industry divinylbenzene catalyst which characterized in that: comprises a barrel body (1); the barrel body (1) is filled with liquid, the barrel body (1) is connected with a mixing structure (2) in a rotating mode, and a second mixing structure (3) is further arranged in the barrel body (1); two groups of three sampling structures (4) are inserted into the barrel body (1), and a liquid discharge pipe structure (5) is connected to the barrel body (1) in a threaded manner; the liquid discharge pipe structure (5) comprises a main pipe (501), a filter screen (502), a sleeve (503), a cylindrical rod (504) and a scraper (505), wherein the main pipe (501) is in threaded connection with the barrel body (1), and the filter screen (502) is installed at the head end of the main pipe (501); the sleeve (503) is rotatably connected to the main body pipe (501), and a cylindrical rod (504) is welded on the sleeve (503); a scraper (505) is installed at the head end of the cylindrical rod (504), the scraper (505) is in contact with the filter screen (502), and when the sleeve (503) is rotated, the scraper (505) is in a scraping state; the liquid discharge pipe structure (5) further comprises a connecting pipe (506), the connecting pipe (506) is rotatably connected to the tail end of the sleeve (503) through a sealing bearing, the connecting pipe (506) is of a connecting pipeline structure connected with a liquid discharge hose, and the connecting pipe (506) is in a relatively static state when the sleeve (503) is rotated.
2. The apparatus for preparing divinylbenzene catalyst in chemical industry according to claim 1, wherein: the barrel body (1) is of a rectangular barrel-shaped structure, and the top end face of the barrel body (1) is fixedly connected with a cover plate (101) through a bolt; the mixing structure (2) comprises two rotating shafts (201) and two blades (202), and the two rotating shafts (201) are hermetically and rotatably connected to the barrel body (1) through sealed bearings; the blades (202) are arranged on the two rotating shafts (201) in a rectangular array shape, and the blades (202) on the two rotating shafts (201) are arranged in a staggered shape.
3. The apparatus for preparing divinylbenzene catalyst in chemical industry according to claim 2, wherein: the mixing structure (2) further comprises poke rods (203), belt wheels (204) and belts (205), wherein two poke rods (203) are symmetrically arranged on each rotating shaft (201), and one belt wheel (204) is arranged on each rotating shaft (201); the two belt wheels (204) are connected through a belt (205), a gear used for being connected with a driving motor is further installed on one rotating shaft (201) on the rear side, and the two rotating shafts (201) jointly form a reverse synchronous rotating structure.
4. The apparatus for preparing divinylbenzene catalyst in chemical industry according to claim 1, wherein: the second mixing structure (3) comprises four sliding rods (301), a mixing plate (302), a strip-shaped hole (303) and an elastic piece (304), the number of the sliding rods (301) is four, the four sliding rods (301) are respectively welded at four corner positions of the bottom end face of the inner wall of the barrel body (1), and the four sliding rods (301) are all of a stepped shaft-shaped structure; the mixing plate (302) is connected to the four sliding rods (301) in a sliding mode, and five strip-shaped holes (303) are formed in the top end face of the mixing plate (302) in a rectangular array mode; the outer wall of each sliding rod (301) is positioned below the mixing plate (302) and sleeved with an elastic part (304), and the sliding rods (301) and the elastic parts (304) jointly form an elastic reset structure of the mixing plate (302).
5. The apparatus for preparing divinylbenzene catalyst in chemical industry according to claim 3, wherein: the length of the poke rod (203) is greater than the distance between the rotating shaft (201) and the mixing plate (302), and when the rotating shaft (201) drives the poke rod (203) to rotate, the mixing plate (302) is in a vertical reciprocating motion state under the poke action of the poke rod (203).
6. The apparatus for preparing divinylbenzene catalyst in chemical industry according to claim 1, wherein: the sampling structure (4) comprises an outer pipe (401), a liquid inlet hole A (402), an inner pipe (403), a hook (40301), an elastic bolt (40302) and a liquid inlet hole B (404), the outer pipe (401) penetrates through a cover plate (101) and is inserted into the barrel body (1), the outer pipe (401) is of a cylindrical structure, and five liquid inlet holes A (402) are formed in the outer wall of the outer pipe (401) in a rectangular array shape; two hooks (40301) are arranged on the inner pipe (403), and the inner pipe (403) is locked and inserted in the outer pipe (401) through the hooks (40301); five liquid inlet holes B (404) are formed in the outer wall of the inner pipe (403) in a rectangular array shape, and five liquid inlet holes B (404) are formed in the outer wall of the inner pipe (403) in a rectangular array shape; the liquid inlet hole A (402) and the liquid inlet hole B (404) are aligned with each other.
7. The apparatus for preparing divinylbenzene catalyst in chemical industry according to claim 6, wherein: sample structure (4) still include baffle (405), inner tube (403) inner wall is located every feed liquor hole B (404) position department and all welds baffle (405) of a circular platelike structure, and divides into five sample spaces inner tube (403) under the separation of baffle (405).
8. The apparatus for preparing divinylbenzene catalyst in chemical industry according to claim 6, wherein: outer tube (401) are including draw-in groove (40101), two draw-in grooves (40101) have been seted up to outer tube (401) top end face 90 contained angles, just install one on inner tube (403) and be used for realizing elastic bolt (40302) of shutting with draw-in groove (40101).
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| CN202010426106.3A CN111530323A (en) | 2020-05-19 | 2020-05-19 | Preparation equipment for producing chemical divinylbenzene catalyst |
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| CN202010426106.3A CN111530323A (en) | 2020-05-19 | 2020-05-19 | Preparation equipment for producing chemical divinylbenzene catalyst |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111821933A (en) * | 2020-07-20 | 2020-10-27 | 莱西市星脉先进材料技术中心 | Production method of chemical high polymer material |
| CN111841471A (en) * | 2020-07-20 | 2020-10-30 | 莱西市星脉先进材料技术中心 | Chemical industry macromolecular material production facility |
| CN112273204A (en) * | 2020-11-06 | 2021-01-29 | 肖占伟 | Irrigation device for crop cultivation |
| CN112619501A (en) * | 2020-11-28 | 2021-04-09 | 德清科邦晶体纤维有限公司 | Cotton pulp preparation mixing arrangement of polycrystal mullite fibreboard |
| CN113252405A (en) * | 2021-04-15 | 2021-08-13 | 河北华丰能源科技发展有限公司 | Tar sampling device |
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN204027878U (en) * | 2014-09-01 | 2014-12-17 | 梁山正大菱花生物科技有限公司 | Multilayer liquid sampler |
| CN105536594A (en) * | 2016-02-03 | 2016-05-04 | 湖南万通科技有限公司 | Material mixing device |
| CN208591736U (en) * | 2018-05-31 | 2019-03-12 | 奥格生物技术（六安）有限公司 | A kind of mixing arrangement of mixed feed production |
| CN109925954A (en) * | 2019-03-08 | 2019-06-25 | 湖南艾华集团股份有限公司 | A kind of capacitor processing powder body mixing arrangement |
| CN110215735A (en) * | 2019-06-18 | 2019-09-10 | 厦门医学院 | A kind of extraction equipment for Chinese materia medica preparation synthesis |
| US20200108361A1 (en) * | 2015-07-28 | 2020-04-09 | Surface To Surface Inc. | Mixing apparatus and system |
| CN111001205A (en) * | 2019-12-13 | 2020-04-14 | 中冶天工集团有限公司 | Sewage collection and treatment impurity self-cleaning device and using method thereof |
-
2020
- 2020-05-19 CN CN202010426106.3A patent/CN111530323A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN204027878U (en) * | 2014-09-01 | 2014-12-17 | 梁山正大菱花生物科技有限公司 | Multilayer liquid sampler |
| US20200108361A1 (en) * | 2015-07-28 | 2020-04-09 | Surface To Surface Inc. | Mixing apparatus and system |
| CN105536594A (en) * | 2016-02-03 | 2016-05-04 | 湖南万通科技有限公司 | Material mixing device |
| CN208591736U (en) * | 2018-05-31 | 2019-03-12 | 奥格生物技术（六安）有限公司 | A kind of mixing arrangement of mixed feed production |
| CN109925954A (en) * | 2019-03-08 | 2019-06-25 | 湖南艾华集团股份有限公司 | A kind of capacitor processing powder body mixing arrangement |
| CN110215735A (en) * | 2019-06-18 | 2019-09-10 | 厦门医学院 | A kind of extraction equipment for Chinese materia medica preparation synthesis |
| CN111001205A (en) * | 2019-12-13 | 2020-04-14 | 中冶天工集团有限公司 | Sewage collection and treatment impurity self-cleaning device and using method thereof |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111821933A (en) * | 2020-07-20 | 2020-10-27 | 莱西市星脉先进材料技术中心 | Production method of chemical high polymer material |
| CN111841471A (en) * | 2020-07-20 | 2020-10-30 | 莱西市星脉先进材料技术中心 | Chemical industry macromolecular material production facility |
| CN112273204A (en) * | 2020-11-06 | 2021-01-29 | 肖占伟 | Irrigation device for crop cultivation |
| CN112619501A (en) * | 2020-11-28 | 2021-04-09 | 德清科邦晶体纤维有限公司 | Cotton pulp preparation mixing arrangement of polycrystal mullite fibreboard |
| CN113252405A (en) * | 2021-04-15 | 2021-08-13 | 河北华丰能源科技发展有限公司 | Tar sampling device |
| CN113252405B (en) * | 2021-04-15 | 2022-11-11 | 河北华丰能源科技发展有限公司 | Tar sampling device |
| CN114733423A (en) * | 2022-04-19 | 2022-07-12 | 中南大学 | Preparation equipment and preparation method of surface grafting modified immobilized microbial adsorbent |
| CN114733423B (en) * | 2022-04-19 | 2023-02-21 | 中南大学 | Preparation equipment and preparation method of surface grafting modified immobilized microbial adsorbent |
| CN115532097A (en) * | 2022-12-05 | 2022-12-30 | 江苏中凯探伤设备制造有限公司 | Cleaning liquid mixing device for cleaning equipment |
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Application publication date: 20200814 |