CN111481488B - Formula and preparation method of plant shampoo capable of preventing white hair and blackening and strengthening hair - Google Patents
Formula and preparation method of plant shampoo capable of preventing white hair and blackening and strengthening hair Download PDFInfo
- Publication number
- CN111481488B CN111481488B CN202010328428.4A CN202010328428A CN111481488B CN 111481488 B CN111481488 B CN 111481488B CN 202010328428 A CN202010328428 A CN 202010328428A CN 111481488 B CN111481488 B CN 111481488B
- Authority
- CN
- China
- Prior art keywords
- parts
- phase
- plant
- hair
- stirring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
- A61K8/9761—Cupressaceae [Cypress family], e.g. juniper or cypress
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Botany (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a formula of a plant shampoo capable of preventing white hair and blackening and strengthening hair and a preparation method thereof, belonging to the technical field of daily cosmetic production. The plant shampoo comprises plant composition ingredients, wherein the plant composition comprises the following components in parts by weight: 8-20 parts of eclipta, 8-20 parts of cacumen biotae, 8-20 parts of black bean coat, 5-15 parts of mulberry leaf, 5-15 parts of glossy privet fruit, 5-15 parts of radix sophorae flavescentis, 5-15 parts of fructus cnidii, 4-20 parts of angelica sinensis, 4-12 parts of radix rehmanniae preparata, 4-12 parts of cortex moutan, 3-8 parts of lavender, 3-8 parts of liquorice, 3-8 parts of salvia miltiorrhiza, 2-6 parts of rhizoma zingiberis and 2-6 parts of broadleaf holly leaf. The plant shampoo disclosed by the invention is safe and reliable in formula effect, mild in performance, rich in foam, free of adverse reaction, simple in preparation method and good in application prospect, and has the effects of preventing white hair, blackening hair and strengthening hair.
Description
Technical Field
The invention belongs to the technical field of daily cosmetic production, and particularly relates to a formula of a plant shampoo capable of preventing white hair and blackening and strengthening hair and a preparation method thereof.
Background
White hair is divided into premature white hair and senile white hair, the premature white hair is premature gray hair, and is called 'young white hair' in folk, which occurs in young and even children, belongs to pathology and is mostly autosomal dominant inheritance. Senile canities are common, generally, after the age of 35, the enzyme tyrosine is gradually lost, melanin produced by melanocytes in hair papillae is reduced, so that pigment in hair shafts is disappeared, canities begin to appear, after the age of 60, the canities are increased, the number of melanocytes in gray hair is normal, cells can contain vacuoles, and melanosomes with normal appearance are provided, but melanin is rarely contained. The number of melanocytes is rare or lacking in white hair, melanin granules are also significantly reduced, and melanocytes and melanin granules are also rare in the papilla of the hair bulb. Senile gray hair usually starts from two temples and develops to the top of the head in a chronic way, beard, vibrissa and the like also turn grey after years, but chest hair, yin hair and axillary hair do not turn white even to the elderly. The senile poliosis belongs to a normal physiological phenomenon, but in recent years, the age of the poliosis population is advanced, the degree of the poliosis is increased, the speed of the poliosis population is increased, and the senile physiological symptoms obviously tend to be abnormal.
At present, the method for solving the white hair problem mainly comprises the traditional Chinese medicine oral administration, the traditional Chinese medicine external administration, diet therapy and the like, but the traditional Chinese medicine or the traditional Chinese medicine mostly has some side effects, and the diet therapy effect is safe but the effect is not obvious. Therefore, the shampoo product with the effects of preventing white hair, blackening hair and the like is developed, and meanwhile, the shampoo product is safe to use, has no adverse reaction and is very important for white hair patients.
In view of the above, the invention provides the formula of the plant shampoo capable of preventing white hair and blackening and strengthening hair and the preparation method thereof, and the preparation process is simplified and high in safety.
Disclosure of Invention
In order to solve the technical problems, the invention provides a formula of a plant shampoo capable of preventing white hair and blackening and strengthening hair and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
the formula of the plant shampoo capable of preventing white hair and blackening and strengthening hair comprises plant composition components, wherein the plant composition comprises the following components in parts by weight:
8-20 parts of eclipta, 8-20 parts of cacumen biotae, 8-20 parts of black bean coat, 5-15 parts of mulberry leaf, 5-15 parts of glossy privet fruit, 5-15 parts of radix sophorae flavescentis, 5-15 parts of fructus cnidii, 4-20 parts of angelica sinensis, 4-12 parts of radix rehmanniae preparata, 4-12 parts of cortex moutan, 3-8 parts of lavender, 3-8 parts of liquorice, 3-8 parts of salvia miltiorrhiza, 2-6 parts of rhizoma zingiberis and 2-6 parts of broadleaf holly leaf.
The plant composition also comprises 1-4 parts of sunflower discs.
Preferably, the weight ratio of the sunflower discs, the lavender and the broadleaf holly leaves is 5-6:3.5-4.5:2-3, and more preferably 5.5:4: 2.5.
Wherein the content of the first and second substances,
the weight percentage of the plant composition in the plant shampoo formula is 60-80%, preferably 65%.
The plant shampoo formula also comprises the phase A, wherein the phase A comprises allantoin, laureth ammonium sulfate and cocamidopropyl betaine.
The above plant shampoo formula further comprises phase B, wherein phase B comprises hydroxypropyl methylcellulose, citric acid, guar hydroxypropyl trimonium chloride, cetyl alcohol, cocoamide, ethylene glycol distearate, polyquaternium-10, lauryl glucoside and decyl glucoside.
The above plant shampoo formula further comprises the phase C, wherein the phase C comprises aminoterminal polydimethylsiloxane/C12-14 secondary alkanol polyether-9/tridecanol polyether-6/glycerol, hydroxypropyl trimethyl ammonium chloride hydrolyzed wheat protein, menthol, hydantoin and water/methylchloroisothiazolinone/methylisothiazolinone/magnesium chloride/magnesium nitrate.
The plant shampoo formula comprises the following components in percentage by weight:
60-80% of plant composition;
phase A: allantoin 0.08-0.12%, laureth sulfate ammonium 3.0-4.0%, laureth sulfate ammonium 1.5-1.9%, and cocamidopropyl betaine 1.5-2.0%;
phase B: hydroxypropyl methylcellulose 0.35-0.45%, citric acid 0.01-0.03%, guar hydroxypropyl trimethyl ammonium chloride 0.21-0.25%, cetyl alcohol 0.19-0.23%, cocoamide 0.9-1.2%, ethylene glycol distearate 0.85-1.15%, polyquaternium-100.06-0.10%, lauryl glucoside 4.0-7.0% and decyl glucoside 1.5-2.5%;
and C phase: aminoterminal polydimethylsiloxane/C12-14 secondary alkanol polyether-9/tridecyl alcohol polyether-6/glycerol 0.10-0.14%, hydroxypropyl trimethyl ammonium chloride hydrolyzed wheat protein 0.15-0.17%, menthol 0.05-0.07%, hydantoin 0.25-0.35%, and water/methylchloroisothiazolinone/methylisothiazolinone/magnesium chloride/magnesium nitrate 0.035-0.037%;
and the balance water.
Preferably, the plant shampoo formula comprises the following components in percentage by weight:
65% of plant composition;
phase A: allantoin 0.1%, laureth sulfate ammonium 3.5%, laureth sulfate ammonium 1.7% and cocamidopropyl betaine 1.8%;
phase B: hydroxypropyl methylcellulose 0.4%, citric acid 0.02%, guar hydroxypropyl trimonium chloride 0.23%, whale 5 cetyl alcohol 0.21%, cocamide MEA 1.1%, ethylene glycol distearate 1%, polyquaternium-100.08%, lauryl glucoside 5% and decyl glucoside 2.0%;
and C phase: aminoterminal polydimethylsiloxane/C12-14 secondary alkanol polyether-9/tridecyl alcohol polyether-6/glycerol 0.12%, hydroxypropyl trimethyl ammonium chloride hydrolyzed wheat protein 0.16%, menthol 0.06%, DMDM hydantoin 0.3% and water/methylchloroisothiazolinone/methylisothiazolinone/magnesium chloride/magnesium nitrate 0.036%;
and the balance water.
In addition, the invention also provides a method for preparing the plant shampoo formula, which comprises the following steps:
s1, an extraction method of the plant composition: pulverizing Ecliptae herba, folium Platycladi, semen Sojae Atricolor coat, folium Mori, fructus Ligustri Lucidi, radix Sophorae Flavescentis 5-15 parts, fructus Cnidii, radix Angelicae sinensis, radix rehmanniae Preparata, cortex moutan, Lavender, Glycyrrhrizae radix, Saviae Miltiorrhizae radix, Zingiberis rhizoma, Folum Ilicis and sunflower disc, decocting in water to obtain plant composition extractive solution;
s2, adding allantoin, ammonium laureth sulfate and cocamidopropyl betaine in formula ratio into the extract obtained in the step S1, and stirring and homogenizing to obtain a phase A mixed solution;
s3, adding hydroxypropyl methyl cellulose, citric acid, guar gum hydroxypropyl trimethyl ammonium chloride, cetyl alcohol, cocamide, ethylene glycol distearate, polyquaternium-10, lauryl glucoside and decyl glucoside in formula amounts to the A phase mixed solution obtained in the step S2 in sequence, stirring and preserving heat to obtain an AB phase mixed solution;
s4, cooling the AB phase mixed solution obtained in the step S3, sequentially adding amino-terminated polydimethylsiloxane/C12-14 sec-alkanol polyether-9/tridecanol polyether-6/glycerol, hydroxypropyl trimethyl ammonium chloride hydrolyzed wheat protein, menthol, hydantoin and water/methylchloroisothiazolinone/methylisothiazolinone/magnesium chloride/magnesium nitrate in a formula amount, and stirring to obtain ABC phase mixed solution;
s5, cooling the ABC phase mixed liquid obtained in the step S4, and filtering to obtain the plant shampoo formula.
Wherein the content of the first and second substances,
the pulverization in the step S1 is to pulverize to a particle size of 10-20 μm; the water-adding decoction comprises the following steps: adding water into the plant composition according to the mass ratio of 1:2-3, and decocting at 90-100 deg.C for 3.5-4.5 h.
In step S2, the stirring and homogenizing step includes: heating to 80-85 deg.C at rotation speed of 33-37r/min, stirring and homogenizing for 4-6 min; in the step S3, the stirring and heat preservation are as follows: keeping the temperature of 80-85 ℃ for 30min at the rotating speed of 33-37 r/min; in step S4, the cooling is: cooling to 43-47 ℃, wherein the stirring is as follows: stirring at 28-32r/min for 20-25 min; in step S5, the filtering is to pass through a 70-90 mesh sieve.
The invention has the beneficial effects that:
(1) the hair-blackening cream is prepared by compounding plant components such as eclipta, cacumen biotae, black soybean coat, mulberry leaf, glossy privet fruit, 5-15 parts of radix sophorae flavescentis, fructus cnidii, angelica sinensis, radix rehmanniae, prepared rhizome of rehmannia, cortex moutan, lavender, liquorice, salvia miltiorrhiza, dried ginger and broadleaf holly leaf, and adding a sunflower disc, so that a synergistic effect is achieved, and the hair-blackening curative effect is greatly improved.
(2) The plant shampoo disclosed by the invention takes natural plants as main components, is safe and reliable, mild in performance and rich in foam, has the effects of preventing white hair, blacking hair and strengthening hair, and does not have adverse reactions.
(3) The preparation method is simple, does not need complex production equipment, has moderate cost and is suitable for large-scale production.
Detailed Description
The embodiments of the present invention are described below with reference to specific embodiments, and other advantages and effects of the present invention will be easily understood by those skilled in the art from the disclosure of the present specification. The invention is capable of other and different embodiments and of being practiced or of being carried out in various ways, and its several details are capable of modification in various respects, all without departing from the spirit and scope of the present invention.
Before the present embodiments are further described, it is to be understood that the scope of the invention is not limited to the particular embodiments described below; it is also to be understood that the terminology used in the examples is for the purpose of describing particular embodiments only, and is not intended to limit the scope of the present invention.
When numerical ranges are given in the examples, it is understood that both endpoints of each of the numerical ranges and any value therebetween can be selected unless the invention otherwise indicated. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs.
The sources of the raw materials used in the present invention are not limited, and the raw materials used in the present invention are all those commonly available in the art unless otherwise specified. Of these, aminoterminated polydimethylsiloxane/C12-14 secondary alkanol polyether-9/tridecyl polyether-6/glycerol, available from Michigan advanced materials (Nantong) Inc., under the trade designation Silsoft AM 1020N; water/methylchloroisothiazolinone/methylisothiazolinone/magnesium chloride/magnesium nitrate, available from toler specialty chemicals (zhenjiang) ltd under the trade name Microcare CM. Both suppliers of raw materials are Guangzhou Liuhao trade development Limited.
Examples 1 to 7
The formula of the plant shampoo capable of preventing white hair and blackening and strengthening hair comprises the following components in percentage by weight:
65% of plant composition;
phase A: allantoin 0.1%, laureth sulfate ammonium 3.5%, laureth sulfate ammonium 1.7% and cocamidopropyl betaine 1.8%;
phase B: hydroxypropyl methylcellulose 0.4%, citric acid 0.02%, guar hydroxypropyl trimonium chloride 0.23%, whale 5 cetyl alcohol 0.21%, cocamide MEA 1.1%, ethylene glycol distearate 1%, polyquaternium-100.08%, lauryl glucoside 5% and decyl glucoside 2.0%;
and C phase: aminoterminal polydimethylsiloxane/C12-14 secondary alkanol polyether-9/tridecyl alcohol polyether-6/glycerol 0.12%, hydroxypropyl trimethyl ammonium chloride hydrolyzed wheat protein 0.16%, menthol 0.06%, DMDM hydantoin 0.3% and water/methylchloroisothiazolinone/methylisothiazolinone/magnesium chloride/magnesium nitrate 0.036%;
and the balance water.
The components and amounts of the plant compositions of examples 1-7 are shown in Table 1.
TABLE 1 Components and amounts of the botanical compositions of examples 1-7
| Parts by weight | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 | Example 7 |
| Herba Ecliptae | 8 | 12 | 16 | 20 | 14 | 14 | 14 |
| Cacumen Platycladi | 16 | 8 | 20 | 12 | 14 | 14 | 14 |
| Black bean clothes | 8 | 20 | 12 | 16 | 14 | 14 | 14 |
| Mulberry leaf | 11 | 8 | 15 | 5 | 10 | 10 | 10 |
| Glossy privet fruit | 5 | 15 | 8 | 11 | 10 | 10 | 10 |
| Sophora flavescens ait | 15 | 5 | 14 | 6 | 10 | 10 | 10 |
| Fructus cnidii | 5 | 10 | 7 | 15 | 10 | 10 | 10 |
| Radix Angelicae sinensis | 20 | 4 | 12 | 8 | 12 | 12 | 12 |
| Dried rehmannia root | 6 | 12 | 8 | 4 | 8 | 8 | 8 |
| Prepared rhizome of rehmannia | 4 | 12 | 6 | 10 | 8 | 8 | 8 |
| Root-bark of tree peony | 4 | 12 | 8 | 10 | 8 | 8 | 8 |
| Lavender | 3 | 8 | 3.5 | 7.5 | 5.5 | 5 | 6 |
| Licorice root, radix Glycyrrhizae | 7 | 3 | 8 | 4 | 5.5 | 5.5 | 5.5 |
| Root of red-rooted salvia | 6 | 8 | 3 | 5 | 5.5 | 5.5 | 5.5 |
| Dried ginger | 4 | 2 | 6 | 3 | 4 | 4 | 4 |
| Broadleaf holly leaf tea | 2 | 6 | 2.5 | 5.5 | 4 | 3.5 | 4.5 |
| Sunflower disk | - | - | 4.5 | 1 | 2.5 | 3 | 2 |
The preparation method of the plant shampoo comprises the following steps:
s1, an extraction method of the plant composition: grinding herba Ecliptae, folium Platycladi, semen Sojae Atricolor coat, folium Mori, fructus Ligustri Lucidi, radix Sophorae Flavescentis, fructus Cnidii, radix Angelicae sinensis, radix rehmanniae Preparata, cortex moutan, Lavender, Glycyrrhrizae radix, Saviae Miltiorrhizae radix, Zingiberis rhizoma, Folum Ilicis and sunflower disc into particle size of 15 μm, adding water at a mass ratio of 1:2, and decocting at 100 deg.C for 4 hr to obtain plant composition extractive solution;
s2, adding allantoin, ammonium laureth sulfate and cocamidopropyl betaine according to the formula ratio into the extract obtained in the step S1 in sequence, heating to 80-85 ℃ at the rotation speed of 35r/min, and stirring and homogenizing for 5min to obtain a phase A mixed solution;
s3, adding hydroxypropyl methyl cellulose, citric acid, guar gum hydroxypropyl trimethyl ammonium chloride, cetyl alcohol, cocamide, ethylene glycol distearate, polyquaternium-10, lauryl glucoside and decyl glucoside in formula amounts sequentially into the A phase mixed solution obtained in the step S2, and preserving heat for 30min at the rotating speed of 35r/min and the temperature of 80-85 ℃ to obtain an AB phase mixed solution;
s4, cooling the AB phase mixed solution obtained in the step S3 to 45 ℃, sequentially adding amino-terminated polydimethylsiloxane/C12-14 sec-alkanol polyether-9/tridecanol polyether-6/glycerol, hydroxypropyl trimethyl ammonium chloride hydrolyzed wheat protein, menthol, hydantoin and water/methylchloroisothiazolinone/methylisothiazolinone/magnesium chloride/magnesium nitrate according to the formula amount, and stirring for 20min at 30r/min to obtain ABC phase mixed solution;
s5, cooling the ABC phase mixed liquid obtained in the step S4 to 38 ℃, and sieving the ABC phase mixed liquid with a 80-mesh sieve to obtain the plant shampoo.
Example 8
The difference between the present embodiment and embodiment 5 is that the plant shampoo formula comprises the following components in percentage by weight:
60% of plant composition;
phase A: allantoin 0.12%, laureth sulfate ammonium 4%, laureth sulfate ammonium 1.9% and cocamidopropyl betaine 2%;
phase B: hydroxypropyl methylcellulose 0.45%, citric acid 0.03%, guar hydroxypropyl trimethyl chloride 0.25%, cetyl alcohol 0.23%, cocamide MEA 1.2%, ethylene glycol distearate 1.15%, polyquaternium-100.1%, lauryl glucoside 7% and decyl glucoside 2.5%;
and C phase: aminoterminal polydimethylsiloxane/C12-14 secondary alkanol polyether-9/tridecyl alcohol polyether-6/glycerol 0.14%, hydroxypropyl trimethyl ammonium chloride hydrolyzed wheat protein 0.17%, menthol 0.07%, DMDM hydantoin 0.35% and water/methylchloroisothiazolinone/methylisothiazolinone/magnesium chloride/magnesium nitrate 0.037%;
and the balance water.
Example 9
The difference between the present embodiment and embodiment 5 is that the plant shampoo formula comprises the following components in percentage by weight:
80% of plant composition;
phase A: allantoin 0.08%, laureth sulfate ammonium 3%, laureth sulfate ammonium 1.5% and cocamidopropyl betaine 1.5%;
phase B: hydroxypropyl methylcellulose 0.35%, citric acid 0.01%, guar hydroxypropyl trimethyl chloride 0.21%, cetyl alcohol 0.19%, cocamide MEA 0.9%, ethylene glycol distearate 0.85%, polyquaternium-100.06%, lauryl glucoside 4% and decyl glucoside 1.5%;
and C phase: amino-terminated polydimethylsiloxane/C12-14 secondary alkanol polyether-9/tridecanol polyether-6/glycerol 0.10%, hydroxypropyl trimethyl ammonium chloride hydrolyzed wheat protein 0.15%, menthol 0.05%, DMDM hydantoin 0.25% and water/methylchloroisothiazolinone/methylisothiazolinone/magnesium chloride/magnesium nitrate 0.035%;
and the balance water.
Comparative example 1
This comparative example differs from example 5 in that: the plant composition does not contain lavender.
Comparative example 2
This comparative example differs from example 5 in that: the plant composition does not contain Folum Ilicis.
Comparative example 3
This comparative example differs from example 5 in that: the content of the sunflower discs in the plant composition is 6 parts.
Comparative example 4
This comparative example differs from example 5 in that: the weight parts of the lavender, the broadleaf holly leaf and the sunflower disc in the plant composition are 8, 2 and 4.5 parts respectively.
Test example
840 volunteers with early graying symptoms are selected, aged 18-35 years and randomly divided into 14 groups, 60 persons in each group are respectively used for washing hair once a day by using prepared examples, comparative examples and shampoo sold in the market, the duration of each time is the same, and the using effect of the volunteers is observed and counted after the continuous use for 6 months, and the results are shown in table 2.
The curative effect standard is as follows: the effect is shown: turning the newly born hair root part into black; the method has the following advantages: the newly born hair roots are obviously blackened; and (4) invalidation: white hair is substantially unchanged. Effective rate (effective + significant) x 100/total number of people.
Table 2.
| Group of | Show effect/human | Effective/human | Invalid/human | Effective rate% | The rate of adverse reactions% |
| EXAMPLE 1 group | 42 | 12 | 6 | 90 | 0 |
| EXAMPLE 2 group | 41 | 13 | 6 | 90 | 0 |
| EXAMPLE 3 group | 45 | 11 | 4 | 93.3 | 0 |
| EXAMPLE 4 group | 44 | 11 | 5 | 91.7 | 0 |
| EXAMPLE 5 group | 56 | 4 | 0 | 100 | 0 |
| EXAMPLE 6 group | 48 | 9 | 3 | 95 | 0 |
| EXAMPLE 7 group | 49 | 9 | 2 | 96.7 | 0 |
| EXAMPLE 8 group | 51 | 9 | 0 | 100 | 0 |
| EXAMPLE 9 group | 50 | 10 | 0 | 100 | 0 |
| Comparative example 1 group | 28 | 15 | 17 | 71.7 | 0 |
| Comparative example 2 group | 25 | 17 | 18 | 70.0 | 0 |
| Comparative example 3 group | 35 | 14 | 11 | 81.7 | 0 |
| Comparative example 4 group | 36 | 13 | 11 | 81.7 | 0 |
| Commercial hair-growing shampoo | 30 | 16 | 14 | 76.7 | 3.3 |
840 volunteers with gray hair symptoms are selected, aged 35-65 years and randomly divided into 14 groups, 60 persons in each group are respectively washed once a day by using the prepared examples, comparative examples and shampoo sold in the market, the duration of each time is the same, and the using effect of the volunteers is observed and counted after the continuous use for 8 months, and the results are shown in table 3.
The curative effect standard is as follows: the effect is shown: turning the newly born hair root part into black; the method has the following advantages: the newly born hair roots are obviously blackened; and (4) invalidation: white hair is substantially unchanged.
Table 3.
As can be seen from the table 2, the plant shampoo formula can effectively prevent and treat premature white hair of people, and has a good curative effect on premature white hair patients, wherein the efficiency reaches 100% when the weight ratio of the sunflower disc, the lavender and the broadleaf holly leaf is 5-6:3.5-4.5:2-3 after the sunflower disc is added, and the effective number is obviously increased when the weight ratio is 5.5:4: 2.5.
As can be seen from the table 3, the invention has good hair-blacking and hair-strengthening curative effects and can restore the vitality of new hair roots of aging people, wherein the effective rate of the sunflower disc, the lavender and the broadleaf holly leaf can reach more than 90% when the weight ratio of the sunflower disc to the lavender to the broadleaf holly leaf is 5-6:3.5-4.5:2-3, and the number of effective people is obviously increased when the weight ratio of the sunflower disc to the lavender to the broadleaf holly leaf is 5.5:4: 2.5.
In conclusion, the plant shampoo is prepared by compounding plant components such as eclipta, cacumen biotae, black bean coat, mulberry leaf, glossy privet fruit, radix sophorae flavescentis, fructus cnidii, angelica sinensis, radix rehmanniae, prepared rhizome of rehmannia, cortex moutan, lavender, liquorice, salvia miltiorrhiza, dried ginger and broadleaf holly leaf and adding sunflower disc components, can achieve excellent white hair resistance and hair blacking and hair care effects, is safe and reliable, is mild in performance, rich in foam and free of adverse reaction, and the natural plants are used as main components in the formula of the prepared plant shampoo. Meanwhile, the preparation method is simple, does not need complex production equipment, has moderate cost and is suitable for large-scale production.
Claims (8)
1. A plant shampoo for preventing white hair and blackening and strengthening hair is characterized by comprising a plant composition;
the plant composition comprises the following components in parts by weight:
8-20 parts of yerbadetajo herb, 8-20 parts of cacumen biotae, 8-20 parts of black bean coat, 5-15 parts of mulberry leaf, 5-15 parts of glossy privet fruit, 5-15 parts of radix sophorae flavescentis, 5-15 parts of fructus cnidii, 4-20 parts of angelica sinensis, 4-12 parts of radix rehmanniae, 4-12 parts of prepared rhizome of rehmannia, 4-12 parts of cortex moutan, 3-8 parts of lavender, 3-8 parts of liquorice, 3-8 parts of salvia miltiorrhiza, 2-6 parts of dried ginger, 2-6 parts of ilex latifolia thumb and 1-4 parts of sunflower disc,
the weight ratio of the lavender to the broadleaf holly leaf to the sunflower disc is 5-6:3.5-4.5: 2-3.
2. The plant shampoo according to claim 1, further comprising phase A, wherein phase A comprises allantoin, ammonium laureth sulfate, and cocamidopropyl betaine.
3. The plant shampoo according to claim 1, further comprising a phase B, wherein the phase B comprises hydroxypropyl methylcellulose, citric acid, guar hydroxypropyltrimonium chloride, cetyl alcohol, cocamide, ethylene glycol distearate, polyquaternium-10, lauryl glucoside, and decyl glucoside.
4. The vegetable shampoo as defined in claim 1 further comprising phase C comprising amodimethicone/C12-14 secondary alkanol polyether-9/tridecanol polyether-6/glycerin, hydroxypropyltrimonium chloride hydrolyzed wheat protein, menthol, hydantoin, and water/methylchloroisothiazolinone/methylisothiazolinone/magnesium chloride/magnesium nitrate.
5. The plant shampoo as claimed in any one of claims 1 to 4, wherein the plant shampoo comprises the following components in percentage by weight:
60-80% of plant composition;
phase A: allantoin 0.08-0.12%, laureth sulfate ammonium 3.0-4.0%, laureth sulfate ammonium 1.5-1.9%, and cocamidopropyl betaine 1.5-2.0%;
phase B: hydroxypropyl methylcellulose 0.35-0.45%, citric acid 0.01-0.03%, guar hydroxypropyl trimethyl ammonium chloride 0.21-0.25%, cetyl alcohol 0.19-0.23%, cocoamide 0.9-1.2%, ethylene glycol distearate 0.85-1.15%, polyquaternium-100.06-0.10%, lauryl glucoside 4.0-7.0% and decyl glucoside 1.5-2.5%;
and C phase: aminoterminal polydimethylsiloxane/C12-14 secondary alkanol polyether-9/tridecyl alcohol polyether-6/glycerol 0.10-0.14%, hydroxypropyl trimethyl ammonium chloride hydrolyzed wheat protein 0.15-0.17%, menthol 0.05-0.07%, hydantoin 0.25-0.35%, and water/methylchloroisothiazolinone/methylisothiazolinone/magnesium chloride/magnesium nitrate 0.035-0.037%;
and the balance water.
6. Method for preparing a plant shampoo according to claim 5, characterized in that it comprises the following steps:
s1, extraction of the plant composition: pulverizing Ecliptae herba, folium Platycladi, semen Sojae Atricolor coat, folium Mori, fructus Ligustri Lucidi, radix Sophorae Flavescentis 5-15 parts, fructus Cnidii, radix Angelicae sinensis, radix rehmanniae Preparata, cortex moutan, Lavender, Glycyrrhrizae radix, Saviae Miltiorrhizae radix, Zingiberis rhizoma, Folum Ilicis and sunflower disc, decocting in water to obtain plant composition extractive solution;
s2, adding allantoin, ammonium laureth sulfate and cocamidopropyl betaine in formula ratio into the extract obtained in the step S1, and stirring and homogenizing to obtain a phase A mixed solution;
s3, adding hydroxypropyl methyl cellulose, citric acid, guar gum hydroxypropyl trimethyl ammonium chloride, cetyl alcohol, cocamide, ethylene glycol distearate, polyquaternium-10, lauryl glucoside and decyl glucoside in formula amounts to the A phase mixed solution obtained in the step S2 in sequence, stirring and preserving heat to obtain an AB phase mixed solution;
s4, cooling the AB phase mixed solution obtained in the step S3, sequentially adding amino-terminated polydimethylsiloxane/C12-14 sec-alkanol polyether-9/tridecanol polyether-6/glycerol, hydroxypropyl trimethyl ammonium chloride hydrolyzed wheat protein, menthol, hydantoin and water/methylchloroisothiazolinone/methylisothiazolinone/magnesium chloride/magnesium nitrate in a formula amount, and stirring to obtain ABC phase mixed solution;
s5, cooling the ABC phase mixed liquid obtained in the step S4, and filtering to obtain the plant shampoo.
7. The production method according to claim 6, wherein in step S1, the pulverization is carried out to a particle size of 10 to 20 μm; the water-adding decoction comprises the following steps: adding water into the plant composition according to the mass ratio of 1:2-3, and decocting at 90-100 deg.C for 3.5-4.5 h.
8. The method of claim 7, wherein the stirring and homogenizing in step S2 is: heating to 80-85 deg.C at rotation speed of 33-37r/min, stirring and homogenizing for 4-6 min; in the step S3, the stirring and heat preservation are as follows: keeping the temperature of 80-85 ℃ for 30min at the rotating speed of 33-37 r/min; in step S4, the cooling is: cooling to 43-47 ℃, wherein the stirring is as follows: stirring at 28-32r/min for 20-25 min; in step S5, the filtering is to pass through a 70-90 mesh sieve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010328428.4A CN111481488B (en) | 2020-04-23 | 2020-04-23 | Formula and preparation method of plant shampoo capable of preventing white hair and blackening and strengthening hair |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010328428.4A CN111481488B (en) | 2020-04-23 | 2020-04-23 | Formula and preparation method of plant shampoo capable of preventing white hair and blackening and strengthening hair |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN111481488A CN111481488A (en) | 2020-08-04 |
| CN111481488B true CN111481488B (en) | 2020-12-22 |
Family
ID=71790422
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202010328428.4A Active CN111481488B (en) | 2020-04-23 | 2020-04-23 | Formula and preparation method of plant shampoo capable of preventing white hair and blackening and strengthening hair |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN111481488B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112842972A (en) * | 2021-04-02 | 2021-05-28 | 广州莎莎化妆品制造有限公司 | Hair blackening liquid and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU2016222314A1 (en) * | 2016-08-29 | 2018-03-15 | Holland, Skye MS | Hair and scalp compositions |
| US10278915B1 (en) * | 2015-04-10 | 2019-05-07 | Uno Beauty, Inc. | Anti-aging hair treatment composition and method |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102871904A (en) * | 2012-09-21 | 2013-01-16 | 周智凯 | Shampoo with hair blacking effect and preparation method thereof |
| CN107625719A (en) * | 2017-09-26 | 2018-01-26 | 贵州健瑞安药业有限公司 | A kind of improvement white hair, Anti-hair loss, anti-dandruff whole plant washing preparations |
| CN107982182A (en) * | 2018-01-29 | 2018-05-04 | 江西全然生态科技有限公司 | A kind of nutrition can delay plant formula shampoo of white hair and preparation method thereof |
| CN110123663A (en) * | 2019-05-16 | 2019-08-16 | 菏泽龙池生物科技有限公司 | A kind of shampoo and preparation method thereof cleaning scalp grease |
| CN110433129A (en) * | 2019-09-11 | 2019-11-12 | 成都卓蓝雅商务信息咨询有限公司 | Maintaining shampoo and preparation method thereof with anti-alopecia function |
-
2020
- 2020-04-23 CN CN202010328428.4A patent/CN111481488B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10278915B1 (en) * | 2015-04-10 | 2019-05-07 | Uno Beauty, Inc. | Anti-aging hair treatment composition and method |
| AU2016222314A1 (en) * | 2016-08-29 | 2018-03-15 | Holland, Skye MS | Hair and scalp compositions |
Also Published As
| Publication number | Publication date |
|---|---|
| CN111481488A (en) | 2020-08-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105997836A (en) | Ferment liquid shampoo and preparation method thereof | |
| CN108785198B (en) | Hair-strengthening composition, shampoo and preparation method thereof | |
| KR102533052B1 (en) | Korean traditional herbs shampoo composition | |
| CN109568556B (en) | Traditional Chinese medicine composition and shampoo for treating alopecia | |
| CN101559034B (en) | Shampoo powder for promoting hair to regrow and preventing trichomadesis | |
| CN110604706A (en) | Hair loss preventing and caring plant composition, preparation method and application | |
| CN102018771A (en) | Hair anti-dropping medical pilatory | |
| CN110327271A (en) | A kind of anti-dandruff and itching-relieving plant composition, preparation method and application | |
| KR20100112720A (en) | Shampoo composition containing oriental medicine and manufacturing method thereof | |
| CN110075049B (en) | Traditional Chinese medicine extract and preparation method and application thereof | |
| CN111481488B (en) | Formula and preparation method of plant shampoo capable of preventing white hair and blackening and strengthening hair | |
| CN111388395B (en) | Formula of plant shampoo capable of effectively relieving itching and removing dandruff and preparation method thereof | |
| KR101867361B1 (en) | Composition for improving condition of hair and head skin, and manufacturing method thereof | |
| KR20080080792A (en) | Growing hair-functional soap for medical herb extracts and its manufacturing method | |
| CN105168074A (en) | Antidandruff and antipruritic traditional Chinese medicine composition and application and preparation method thereof | |
| CN115006336B (en) | Plant shampoo capable of preventing hair loss, strengthening hair, removing dandruff and relieving itching and preparation method thereof | |
| CN104257816B (en) | A kind of composition for treating berloque dermatitis and preparation method thereof | |
| CN110123725A (en) | A kind of facial mask of anti-inflammatory calmness anti-acne | |
| CN108653707A (en) | Dark hair Chinese medicine composition | |
| CN114504616A (en) | Hair treatment formula | |
| JPH0217118A (en) | Japanese and chinese drug for hair growth | |
| CN106880800A (en) | With Chinese medicine composition for educating hair effect and its preparation method and application | |
| CN110547988A (en) | hair-blacking, hair-protecting and color-protecting plant composition, preparation method and application | |
| CN109010182B (en) | Anti-hair loss composition and application thereof in preparation of hair washing and caring products | |
| CN111419750B (en) | Plant shampoo formula capable of effectively promoting hair growth and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |