CN111453998B - High-efficiency glass casing metal texture surface treatment equipment and method - Google Patents

High-efficiency glass casing metal texture surface treatment equipment and method Download PDF

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CN111453998B
CN111453998B CN202010451864.0A CN202010451864A CN111453998B CN 111453998 B CN111453998 B CN 111453998B CN 202010451864 A CN202010451864 A CN 202010451864A CN 111453998 B CN111453998 B CN 111453998B
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temperature
liquid
etching
etching liquid
frame body
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CN111453998A (en
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张源兴
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Fujian Heda Glass Technology Co ltd
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Fujian Heda Glass Technology Co ltd
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C15/00Surface treatment of glass, not in the form of fibres or filaments, by etching
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50Manufacturing or production processes characterised by the final manufactured product

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  • Life Sciences & Earth Sciences (AREA)
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  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Surface Treatment Of Glass (AREA)
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Abstract

The invention relates to a high-efficiency glass casing metal texture surface treatment device and a method, which are used for carrying out surface treatment on a glass casing to realize a metal texture surface effect, the cold chamber is arranged at the lower side of the top cover, the distance between the bottom of the cold chamber and the top cover is larger than the distance between the bottom of the frame body and the top cover, ultralow temperature media are arranged in the cold chamber, when the surface of the glass shell is treated, the ejector rod drives the material frame to firstly descend to a first height, at the moment, the frame body is not immersed below the liquid level of the etching liquid, the cold cavity is partially immersed below the liquid level of the etching liquid in the inner container, the cold cavity cools the etching liquid, the temperature of the etching liquid is reduced to a second temperature, then the ejector rod drives the material frame to descend to a second height, the frame body is immersed below the liquid level of the etching liquid, and the etching liquid enters the frame body through the interval between the upright columns to perform low-temperature surface treatment on the glass shell.

Description

High-efficiency glass casing metal texture surface treatment equipment and method
Technical Field
The invention relates to the field of display, in particular to high-efficiency glass shell metal texture surface treatment equipment and method.
Background
With the popularization and use of smart phones, users pay more and more attention to the appearance of smart phones. The appearance decoration effect of the smart phone shell and the super-hard material shell such as metal, glass and ceramic are highly concerned by the whole industry. Among the materials, the glass has the characteristics of lightness, thinness, transparency, cleanness and the like, does not have the electromagnetic shielding problem of a metal casing, is compatible with a new communication technology and a wireless charging technology, and also has the advantage of easy processing and forming, so that the glass casing has obvious competitiveness. However, how to realize a surface texture with good texture while maintaining the performance advantages of the glass housing becomes a big problem. Compared with printing, coating and other processes, the surface texture effect with good texture and high reliability can be obtained by adopting chemical etching for surface treatment.
The key point of realizing the metal texture surface of the glass shell by chemical etching is to accurately control the temperature of etching liquid so as to realize pit etching on the surface of the glass shell. However, the temperature of the glass cabinet is ambient temperature before entering the etching liquid, which is different from the temperature of the etching liquid, and the glass cabinet reaches thermal equilibrium with the etching liquid through heat exchange after entering the etching liquid, which causes the temperature of the etching liquid to change. On the other hand, because the chemical etching of the glass machine shell needs to adopt strong acids such as hydrogen fluoride and the like as etching liquid, a container for containing the etching liquid and parts entering the etching liquid groove need to adopt a teflon lining capable of resisting strong acid corrosion, and the teflon is a resin material with low thermal conductivity, so that the temperature of the etching liquid is difficult to regulate and control in time. Therefore, how to effectively control the temperature of the etching liquid becomes a technical problem which needs to be solved urgently.
Chinese patent CN105152542A, etc. adopts the formula of etching solution for adjusting chemical etching to improve the surface treatment effect of the glass housing. The method has the disadvantages that the glass shell is placed into an empty etching tank, the etching solution is injected into the etching tank, and the etching solution is emptied after the etching is finished, so that the production efficiency is limited; the etching process does not realize accurate temperature control, pit etching can not be realized on the surface of the glass shell, and the metal texture surface texture effect can not be obtained.
Disclosure of Invention
In view of the above, it is desirable to provide a high-efficiency surface treatment apparatus and method for glass housing with metal texture. In order to solve the technical problems, the technical scheme of the invention is as follows: a high-efficiency glass casing metal texture surface treatment device is used for carrying out surface treatment on a glass casing to realize metal texture surface effect, and is provided with an etching groove, a material frame and a fixing frame, wherein the etching groove is provided with a low-temperature bath groove and a liner, etching liquid is arranged in the liner, a hydraulic cylinder is arranged on the fixing frame, an ejector rod is arranged on the hydraulic cylinder, the material frame is arranged at the lower end part of the ejector rod, the material frame is provided with a top cover, a connecting rod, a frame body, a cold trap body and an infrared temperature measurement sensor, the top part of the top cover is connected with the ejector rod, the connecting rod is arranged on the lower surface of the top cover, the frame body is arranged at the lower end part of the connecting rod, the frame body is provided with stand columns and a bottom mesh plate, intervals are arranged between the stand columns, the glass casing is arranged in the frame body, and the cold trap body and the infrared temperature measurement sensor are both arranged on the top cover, the cold trap body is sequentially provided with a cold cavity, an injection pipe body and an explosion-proof plug from bottom to top, the cold cavity is arranged on the lower side of the top cover, the distance between the bottom of the cold cavity and the top cover is larger than the distance between the bottom of the frame body and the top cover, an ultralow temperature medium is arranged in the cold cavity, the infrared temperature sensor is provided with a temperature probe, the temperature probe is arranged on the lower side of the top cover and faces towards the inner container, the width of the top cover is larger than the width of the inner container of the etching tank, when the surface treatment is carried out on the glass shell, the ejector rod drives the material frame to firstly descend to a first height, at the moment, the frame body is not immersed under the liquid level of etching liquid, the cold cavity is partially immersed under the liquid level of the inner container, the cold cavity cools the etching liquid, the temperature of the etching liquid is reduced to a second temperature, and then the ejector rod drives the material frame to descend to a second height, and immersing the frame body below the liquid level of the etching liquid, wherein the etching liquid enters the frame body through the intervals between the upright posts to perform low-temperature surface treatment on the glass shell.
The etching bath is further provided with a stirring device and a circulating cooling device, the inner container is arranged in the low-temperature bath, cooling liquid is arranged between the low-temperature bath and the inner container, the stirring device is provided with a driving unit, a rotating shaft and stirring blades, the rotating shaft is connected with the driving unit and the blades, the driving unit is arranged outside the low-temperature bath, the stirring blades are arranged inside the inner container and located at the bottom of the inner container, the rotating shaft penetrates through the low-temperature bath and extends into the inner container, the circulating cooling device is provided with a liquid inlet pipe and a liquid outlet pipe, the liquid inlet pipe and the liquid outlet pipe are respectively communicated with the cooling liquid in the low-temperature bath, the circulating cooling device controls the temperature of the cooling liquid at a first temperature, and the first temperature is higher than a second temperature.
The cooling liquid in the low-temperature bath is absolute ethyl alcohol, the ultralow-temperature medium is a mixture of propylamine and liquid nitrogen, or a mixture of acetone and dry ice, or a mixture of ethyl acetate and dry ice, or a mixture of chloroform and dry ice, or a mixture of ethyl alcohol and dry ice, or a mixture of chloroethane and dry ice, or a mixture of isopropyl ether and dry ice, or a mixture of n-octane and dry ice, or a mixture of diethylene glycol diethyl ether and dry ice, or a mixture of m-xylene and dry ice, or a mixture of pyridine and dry ice, or a mixture of m-toluidine and dry ice, or a mixture of o-xylene and dry ice.
The infrared temperature measuring sensors are arranged on the front side and the rear side of the frame body, the cold trap body is arranged on the left side and the right side of the frame body, transverse barrier strips are further arranged on the side faces of the stand columns of the frame body, at least one side door capable of being opened is arranged on the frame body, the glass casing is taken and placed from the side door, positioning stop blocks are arranged on the stand columns and the bottom mesh plate, and the positioning stop blocks limit the glass casing.
The anti-explosion device comprises a frame body, a top cover, a plurality of cold trap bodies and an explosion-proof plug, wherein the number of the cold trap bodies is even, the distance between every two adjacent cold trap bodies is larger than the width of the frame body, the cold trap bodies are further provided with installation structures, the installation structures are arranged on the side walls of the injection pipe body, the explosion-proof plug is arranged at the top of the injection pipe body, a through hole is formed in the position, corresponding to the cold trap bodies, of the top cover, and the top of the injection pipe body penetrates out of the through hole, so that the explosion-proof plug is exposed out of the upper surface of the top cover.
A high-efficiency surface treatment method for a glass shell with metal texture specifically comprises the following steps:
s101: the circulating cooling device controls the temperature of the cooling liquid at a first temperature;
s102: the hydraulic cylinder pushes out the ejector rod downwards, the ejector rod drives the material frame to descend to a first height, the frame body is not immersed below the liquid level of the etching liquid in the inner container, the cold cavity is partially immersed below the liquid level of the etching liquid, the etching liquid is cooled by the cold cavity through heat exchange, the stirring blades continuously rotate, and the temperature of the etching liquid is reduced to a second temperature;
s103: the hydraulic cylinder continues to push out the ejector rod downwards, the ejector rod drives the material frame to descend to a second height, the frame body is immersed below the liquid level of the etching liquid, the stirring blades continuously rotate, and the etching liquid enters the frame body through the intervals between the stand columns to perform low-temperature surface treatment on the glass casing;
s104: the infrared temperature measurement sensor monitors the temperature of the etching liquid, and timing is started when the temperature of the etching liquid reaches a first temperature;
s105: when the timing reaches the designated time length, the hydraulic cylinder upwards withdraws the ejector rod to lift the material frame, and the frame body and the cold cavity are completely separated from the etching liquid.
S106: the top travelling crane moves forward, and the material frame leaves the upper part of the etching tank.
Further preferably, the circulating cooling device controls the temperature of the cooling liquid at a first temperature, and further comprises,
the etching bath is also provided with a stirring device and a circulating cooling device, the inner container is arranged in the low-temperature bath, cooling liquid is arranged between the low-temperature bath and the inner container, the circulating cooling device is provided with a liquid inlet pipe and a liquid outlet pipe, the liquid inlet pipe and the liquid outlet pipe are respectively communicated with the cooling liquid in the low-temperature bath, the circulating cooling device controls the temperature of the cooling liquid at a first temperature which is minus 15 ℃,
the inner wall of the inner container is made of a teflon material, and a temperature difference exists between etching liquid in the inner container and cooling liquid in the low-temperature bath tank.
Further preferably, the hydraulic cylinder pushes out the ejector rod downwards, the ejector rod drives the material frame to descend to a first height, at the moment, the frame body is not immersed below the liquid level of the etching liquid in the inner container, the cold cavity is partially immersed below the liquid level of the etching liquid, the cold cavity cools the etching liquid through heat exchange, the stirring blades continuously rotate, the temperature of the etching liquid is reduced to a second temperature, and the device further comprises,
the high-efficiency glass machine shell metal texture surface treatment equipment is characterized in that a control module is further arranged, an output port of the infrared temperature measurement sensor is connected with an input port of the control module, the control module is further provided with a storage unit, a calculation unit and a timing unit, designated time, a first temperature and a second temperature are stored in the storage unit, the first output port of the control module is connected with the input port of the hydraulic cylinder, the second output port of the control module is connected with an input port of a driving unit of the stirring device, the first temperature is 15 ℃ below zero, the second temperature is 25 ℃ below zero,
the stirring device is provided with a driving unit, a rotating shaft and stirring blades, the rotating shaft is connected with the driving unit and the blades, the driving unit is arranged outside the low-temperature bath tank, the stirring blades are arranged inside the inner container and positioned at the bottom of the inner container, the rotating shaft penetrates through the low-temperature bath tank and extends into the inner container,
the second output port of the control module outputs a start signal to the input port of the stirring device driving unit, the stirring blade starts to rotate,
meanwhile, a first output port of the control module outputs a first descending instruction to the hydraulic cylinder, the hydraulic cylinder pushes the ejector rod downwards, the ejector rod drives the material frame to descend to a first height,
the infrared temperature measurement sensor measures the temperature of the etching liquid and sends the measured temperature value to the control module through an input port of the control module, the control module calculation unit compares the received temperature value with the second temperature value stored in the storage unit, when the measured temperature value is equal to the stored second temperature value, the control module outputs a second descending instruction to the hydraulic cylinder through the first output port, the hydraulic cylinder continues to push the ejector rod downwards, and the ejector rod drives the material frame to descend to a second height.
Preferably, after the control module outputs a second descending instruction to the hydraulic cylinder through the first output port, the infrared temperature measurement sensor measures the temperature of the etching liquid in real time and sends the measured temperature value to the control module through the input port of the control module, the control module calculation unit compares the temperature value with the stored first temperature value, when the temperature value measured by the infrared temperature measurement sensor is equal to the first temperature value, the timing unit starts timing, and when the timing reaches a specified time length stored in the storage unit, the first output port of the control module outputs an ascending instruction to the hydraulic cylinder,
meanwhile, the second output port of the control module outputs a stop signal to the input port of the stirring device driving unit, and the stirring blade stops rotating.
Further preferably, the top travelling crane is moved forward, the material frame leaves above the etching tank, and the method also comprises,
still be provided with the driving track, be provided with the top driving on the driving track, the mount is installed on the top driving and is located the top driving under, the etching groove set up in under the driving track.
Compared with the prior art, the invention has the following beneficial effects: the etching liquid in the inner container is kept in a temperature state close to that required by etching at any time by adopting the low-temperature bath, the etching liquid is temporarily cooled by adopting the cold trap body, the etching liquid is supercooled before the glass shell enters the etching liquid, and after the glass shell is immersed in the etching liquid, heat exchange is carried out between the glass shell and the etching liquid, so that when the glass shell and the etching liquid reach thermal balance, the temperature of the glass shell and the etching liquid just reaches the temperature requirement of pit etching, and the metal texture surface treatment effect is realized.
In order to make the aforementioned and other objects, features and advantages of the invention comprehensible, preferred embodiments accompanied with figures are described in detail below.
Drawings
Fig. 1 is a schematic view of a material frame of a high-efficiency glass housing metallic surface treatment device descending to a first height according to an embodiment of the present invention.
Fig. 2 is a schematic view illustrating a material frame of the high-efficiency glass housing metallic surface treatment apparatus descending to a second height according to the first embodiment of the present invention.
Fig. 3 is a schematic view of a material frame according to a first embodiment of the invention.
Fig. 4 is a schematic diagram of a cold trap body according to a first embodiment of the present invention.
Detailed Description
To further illustrate the technical means and effects of the present invention adopted to achieve the predetermined objects, the following detailed description of the embodiments, structures, features and effects according to the present invention will be made with reference to the accompanying drawings and preferred embodiments.
Example one
Referring to fig. 1 to 4, a high-efficiency glass casing metal texture surface treatment device is used for performing surface treatment on a glass casing 1 to achieve a metal texture surface effect, and is provided with an etching bath 8, a material frame and a fixed frame 2, wherein the etching bath 8 is provided with a low-temperature bath 81 and an inner container 82, etching liquid 83 is arranged in the inner container 82, a hydraulic cylinder 21 is arranged on the fixed frame 2, the hydraulic cylinder 21 is provided with an ejector rod 22, the material frame is arranged at the lower end part of the ejector rod 22, the material frame is provided with a top cover 3, a connecting rod 4, a frame body 5, a cold trap body 6 and an infrared temperature measurement sensor 7, the top part of the top cover 3 is connected with the ejector rod 22, the connecting rod 4 is arranged on the lower surface of the top cover 3, the frame body 5 is arranged at the lower end part of the connecting rod 4, the frame body 5 is provided with upright columns 51 and a bottom mesh plate 52, and intervals are arranged between the upright columns 51, the glass casing 1 is arranged in the frame body 5, the cold trap body 6 and the infrared temperature measuring sensor 7 are both arranged on the top cover 3, the cold trap body 6 is sequentially provided with a cold chamber 61, an injection pipe body 62 and an explosion-proof plug 63 from bottom to top, the cold chamber 61 is arranged at the lower side of the top cover 3, the distance between the bottom of the cold chamber 61 and the top cover 3 is greater than the distance between the bottom of the frame body 5 and the top cover 3, an ultralow temperature medium 65 is arranged in the cold chamber 61, the infrared temperature measuring sensor 7 is provided with a temperature measuring probe which is arranged at the lower side of the top cover 3 and faces the inner container 82, the width of the top cover 3 is greater than the width of the inner container 82 of the etching groove 8, when the surface treatment is carried out on the glass casing 1, the ejector rod 22 drives the material frame to firstly descend to a first height, at the moment, the frame body 5 is not immersed under the liquid level of the etching liquid 83, the cold chamber 61 is partially immersed under the liquid level 83 inside the inner container 82, the cold chamber 61 cools the etching liquid 83, the temperature of the etching liquid 83 is reduced to a second temperature, then the ejector rod 22 drives the material frame to be lowered to a second height, the frame body 5 is immersed below the liquid level of the etching liquid 83, and the etching liquid 83 enters the frame body 5 through the interval between the upright posts 51 to perform low-temperature surface treatment on the glass casing 1.
The etching liquid 83 is a mixture of hydrogen fluoride, ammonium fluoride, sulfuric acid, and nitric acid.
The etching bath 8 is further provided with a stirring device and a circulating cooling device 10, the inner container 82 is arranged in the low-temperature bath 81, cooling liquid 84 is arranged between the low-temperature bath 81 and the inner container 82, the stirring device is provided with a driving unit 91, a rotating shaft 92 and stirring blades 93, the rotating shaft 92 is connected with the driving unit 91 and the blades, the driving unit 91 is arranged outside the low-temperature bath 81, the stirring blades 93 are arranged inside the inner container 82 and located at the bottom position of the inner container 82, the rotating shaft 92 penetrates through the low-temperature bath 81 and extends into the inner container 82, the circulating cooling device 10 is provided with a liquid inlet pipe and a liquid outlet pipe, the liquid inlet pipe and the liquid outlet pipe are respectively communicated with the cooling liquid 84 in the low-temperature bath 81, the circulating cooling device 10 controls the temperature of the cooling liquid 84 at a first temperature, and the first temperature is higher than a second temperature. Sealing rings made of Teflon materials are arranged between the rotating shaft 92 and the walls of the low-temperature bath tank 81 and the inner container 82.
The cooling liquid 84 in the low-temperature bath 81 is absolute ethyl alcohol, the ultralow-temperature medium 65 is a mixture of propylamine and liquid nitrogen, or a mixture of acetone and dry ice, or a mixture of ethyl acetate and dry ice, or a mixture of chloroform and dry ice, or a mixture of ethyl alcohol and dry ice, or a mixture of chloroethane and dry ice, or a mixture of isopropyl ether and dry ice, or a mixture of n-octane and dry ice, or a mixture of diethylene glycol diethyl ether and dry ice, or a mixture of m-xylene and dry ice, or a mixture of pyridine and dry ice, or a mixture of m-toluidine and dry ice, or a mixture of o-xylene and dry ice.
The infrared temperature measuring sensors 7 are arranged on the front side and the rear side of the frame body 5, the cold trap body 6 is arranged on the left side and the right side of the frame body 5, transverse barrier strips 53 are further arranged on the side faces of the upright posts 51 of the frame body 5, at least one side door capable of being opened is arranged on the frame body 5, the glass casing 1 is taken and placed from the side door, positioning stop blocks 54 are arranged on the upright posts 51 and the bottom mesh plate 52, and the positioning stop blocks 54 limit the glass casing 1.
The cold trap body 6 is provided with 4, the interval between two adjacent cold trap bodies 6 is greater than the width of framework 5, still be provided with mounting structure 64 on the cold trap body 6, mounting structure 64 set up in on the lateral wall of injection pipe body 62, explosion-proof stopper 63 set up in the top of injection pipe body 62, be provided with the via hole corresponding to the position of cold trap body 6 on the top cap 3, the top of injection pipe body 62 is followed the via hole is worn out, makes explosion-proof stopper 63 follow the upper surface of top cap 3 exposes.
The injection pipe body 62 is a hollow pipe body, and the ultralow temperature medium 65 is poured into the cold chamber 61 from the injection pipe body 62.
A high-efficiency surface treatment method for a glass shell with metal texture specifically comprises the following steps:
s101: the hydronic apparatus 10 controls the temperature of the cooling liquid 84 at a first temperature, the first temperature being-15 ℃;
s102: the hydraulic cylinder 21 pushes out the ejector rod 22 downwards, the ejector rod 22 drives the material frame to descend to a first height, at the moment, the frame body 5 is not immersed below the liquid level of the etching liquid 83 in the inner container 82, the cold cavity 61 is partially immersed below the liquid level of the etching liquid 83, the cold cavity 61 cools the etching liquid 83 through heat exchange, the stirring blades 93 rotate continuously, the temperature of the etching liquid 83 is reduced to a second temperature, and the second temperature is 25 ℃ below zero;
s103: the hydraulic cylinder 21 continues to push out the ejector rod 22 downwards, the ejector rod 22 drives the material frame to descend to a second height, the frame body 5 is immersed below the liquid level of the etching liquid 83, the stirring blades 93 rotate continuously, and the etching liquid 83 enters the frame body 5 through the interval between the upright columns 51 to perform low-temperature surface treatment on the glass casing 1;
s104: after the frame body 5 is immersed below the liquid level of the etching liquid 83, the frame body 5 absorbs heat from the etching liquid 83 to enable the etching liquid 83 and the etching liquid 83 to reach thermal equilibrium, the temperature of the etching liquid 83 is increased in the process, the infrared temperature measurement sensor 7 monitors the temperature of the etching liquid 83, and timing is started when the temperature of the etching liquid 83 reaches a first temperature;
s105: when the timing reaches a designated time, the hydraulic cylinder 21 retracts the ejector rod 22 upward to lift the material frame, and the frame body 5 and the cold chamber 61 are all separated from the etching liquid 83.
S106: the top travelling crane moves forward, and the material frame leaves the upper part of the etching tank 8.
The hydronic apparatus 10 controls the temperature of the cooling liquid 84 to a first temperature, further comprising,
the etching bath 8 is also provided with a stirring device and a circulating cooling device 10, the inner container 82 is arranged in the low-temperature bath tank 81, cooling liquid 84 is arranged between the low-temperature bath tank 81 and the inner container 82, the circulating cooling device 10 is provided with a liquid inlet pipe and a liquid outlet pipe, the liquid inlet pipe and the liquid outlet pipe are respectively communicated with the cooling liquid 84 in the low-temperature bath tank 81, the circulating cooling device 10 controls the temperature of the cooling liquid 84 at a first temperature,
the inner wall of the inner container 82 is made of teflon, and a temperature difference exists between the etching liquid 83 in the inner container 82 and the cooling liquid 84 in the low-temperature bath 81. The frame body 5, the rotating shaft 92 and the stirring blades 93 are also made of teflon materials. The outer surface of the cold trap body 6 is also coated with a teflon material.
The hydraulic cylinder 21 pushes out the ejector rod 22 downwards, the ejector rod 22 drives the material frame to descend to a first height, at the moment, the frame body 5 is not immersed below the liquid level of the etching liquid 83 in the inner container 82, the cold cavity 61 is partially immersed below the liquid level of the etching liquid 83, the cold cavity 61 cools the etching liquid 83 through heat exchange, the stirring blade 93 continuously rotates, the temperature of the etching liquid 83 is reduced to a second temperature, and the method further comprises,
the high-efficiency glass machine shell metal texture surface treatment equipment is characterized in that a control module is further arranged, an output port of the infrared temperature measurement sensor 7 is connected with an input port of the control module, the control module is further provided with a storage unit, a calculation unit and a timing unit, designated time, a first temperature and a second temperature are stored in the storage unit, the first output port of the control module is connected with the input port of the hydraulic cylinder 21, the second output port of the control module is connected with the input port of the stirring device driving unit 91, and the first temperature is 15 ℃ below zero
The hydraulic cylinder 21 is further provided with a liquid path system, the liquid path system comprises a liquid path motor and a servo valve, the servo valve is arranged on a liquid path for pushing the ejector rod 22, an input port of the hydraulic cylinder 21 is arranged on the electromagnetic valve, a first output port of the control module outputs a voltage signal to the servo valve, and a control command output by the control module to the servo valve is a voltage signal and is controlled by 0-10V; the flow and the direction of a liquid path where the servo valve is located are controlled by the size of a voltage signal output to the servo valve by the control module; wherein the low voltage interval value is 0.5-4.5V corresponding to the pushing-out rod 22, and the high voltage interval value is 5.5-9.5V corresponding to the retracting-out rod 22.
The stirring device is provided with a driving unit 91, a rotating shaft 92 and stirring blades 93, the rotating shaft 92 is connected with the driving unit 91 and the blades, the driving unit 91 is arranged outside the low-temperature bath tank 81, the stirring blades 93 are arranged inside the inner container 82 and positioned at the bottom of the inner container 82, the rotating shaft 92 penetrates through the low-temperature bath tank 81 and extends into the inner container 82,
the second output port of the control module outputs a start signal to the input port of the stirring device driving unit 91, the stirring blade 93 starts to rotate,
meanwhile, a first output port of the control module outputs a first descending instruction to the hydraulic cylinder 21, the hydraulic cylinder 21 pushes the ejector rod 22 downwards, the ejector rod 22 drives the material frame to descend to a first height,
the infrared temperature measurement sensor 7 measures the temperature of the etching liquid 83, the measured temperature value is sent to the control module through an input port of the control module, the control module calculation unit compares the received temperature value with the second temperature value stored in the storage unit, when the measured temperature value is equal to the stored second temperature value, the control module outputs a second descending instruction to the hydraulic cylinder 21 through the first output port, the hydraulic cylinder 21 continues to push the ejector rod 22 downwards, and the ejector rod 22 drives the material frame to descend to a second height.
After the control module outputs a second descending instruction to the hydraulic cylinder 21 through the first output port, the infrared temperature measurement sensor 7 measures the temperature of the etching liquid 83 in real time and sends the measured temperature value to the control module through the input port of the control module, the control module computing unit compares the temperature value with the stored first temperature value, when the temperature value measured by the infrared temperature measurement sensor 7 is equal to the first temperature value, the timing unit starts timing, and when the timing reaches the specified time length stored in the storage unit, the first output port of the control module outputs an ascending instruction to the hydraulic cylinder 21,
meanwhile, the second output port of the control module outputs a stop signal to the input port of the stirring device driving unit 91, and the rotation of the stirring blade 93 is stopped.
The top travelling crane moves forwards, the material frame leaves above the etching tank 8, and the device also comprises,
still be provided with the driving track, be provided with the top driving on the driving track, mount 2 is installed on the top driving and is located the top driving under, etch the groove 8 set up in under the driving track.
Example two
A high-efficiency surface treatment method for glass cabinet with metal texture, which further comprises the following steps between S104 and S105:
s107: after the timing is started, the ejector rod 22 drives the material frame to vertically shake with a small amplitude, and the frame body 5 is always immersed under the liquid level of the etching liquid 83 in the shaking process.
The rest is the same as the first embodiment.
Although the present invention has been described with reference to the preferred embodiments, it should be understood that various changes, substitutions and alterations can be made herein without departing from the spirit and scope of the invention as defined by the appended claims.

Claims (9)

1. A high-efficiency glass casing metal texture surface treatment device is used for carrying out surface treatment on a glass casing and realizing metal texture surface effect, and is characterized in that an etching groove, a material frame and a fixing frame are arranged, the etching groove is provided with a low-temperature bath and a liner, etching liquid is arranged in the liner, a hydraulic cylinder is arranged on the fixing frame, the hydraulic cylinder is provided with an ejector rod, the material frame is arranged at the lower end part of the ejector rod, the material frame is provided with a top cover, a connecting rod, a frame body, a cold trap body and an infrared temperature measurement sensor, the top part of the top cover is connected with the ejector rod, the connecting rod is arranged at the lower surface of the top cover, the frame body is arranged at the lower end part of the connecting rod, the frame body is provided with stand columns and a bottom mesh plate, intervals are arranged among the stand columns, the glass casing is arranged in the frame body, and the cold trap body and the infrared temperature measurement sensor are both arranged on the top cover, the cold trap body is sequentially provided with a cold cavity, an injection pipe body and an explosion-proof plug from bottom to top, the cold cavity is arranged on the lower side of the top cover, the distance between the bottom of the cold cavity and the top cover is larger than the distance between the bottom of the frame body and the top cover, an ultralow temperature medium is arranged in the cold cavity, the infrared temperature sensor is provided with a temperature probe, the temperature probe is arranged on the lower side of the top cover and faces towards the inner container, the width of the top cover is larger than the width of the inner container of the etching tank, when the surface treatment is carried out on the glass shell, the ejector rod drives the material frame to firstly descend to a first height, at the moment, the frame body is not immersed under the liquid level of etching liquid, the cold cavity is partially immersed under the liquid level of the inner container, the cold cavity cools the etching liquid, the temperature of the etching liquid is reduced to a second temperature, and then the ejector rod drives the material frame to descend to a second height, immersing the frame body below the liquid level of the etching liquid, and allowing the etching liquid to enter the frame body through the intervals between the upright columns to perform low-temperature surface treatment on the glass shell; the etching bath is further provided with a stirring device and a circulating cooling device, the inner container is arranged in the low-temperature bath, cooling liquid is arranged between the low-temperature bath and the inner container, the stirring device is provided with a driving unit, a rotating shaft and stirring blades, the rotating shaft is connected with the driving unit and the blades, the driving unit is arranged outside the low-temperature bath, the stirring blades are arranged inside the inner container and at the bottom of the inner container, the rotating shaft penetrates through the low-temperature bath and extends into the inner container, the circulating cooling device is provided with a liquid inlet pipe and a liquid outlet pipe, the liquid inlet pipe and the liquid outlet pipe are respectively communicated with the cooling liquid in the low-temperature bath, the circulating cooling device controls the temperature of the cooling liquid at a first temperature, and the first temperature is higher than a second temperature.
2. The apparatus as claimed in claim 1, wherein the cooling liquid in the low temperature bath is absolute ethanol, and the ultra-low temperature medium is a mixture of propylamine and liquid nitrogen, or a mixture of acetone and dry ice, or a mixture of ethyl acetate and dry ice, or a mixture of chloroform and dry ice, or a mixture of ethanol and dry ice, or a mixture of chloroethane and dry ice, or a mixture of isopropyl ether and dry ice, or a mixture of n-octane and dry ice, or a mixture of diethylene glycol diethyl ether and dry ice, or a mixture of m-xylene and dry ice, or a mixture of pyridine and dry ice, or a mixture of m-toluidine and dry ice, or a mixture of o-xylene and dry ice.
3. The metal texture surface treatment equipment for the high-efficiency glass casing as claimed in claim 1, wherein the infrared temperature measuring sensors are arranged on the front side and the rear side of the frame body, the cold trap bodies are arranged on the left side and the right side of the frame body, a transverse barrier strip is further arranged on the side surface of the upright column of the frame body, the frame body is provided with at least one side door capable of being opened, the glass casing is taken and placed from the side door, positioning stop blocks are arranged on the upright column and the bottom mesh plate, and the positioning stop blocks limit the glass casing.
4. The metal-textured surface treatment device for the high-efficiency glass casing according to claim 1, wherein an even number of cold trap bodies are arranged, the distance between every two adjacent cold trap bodies is larger than the width of the frame body, the cold trap bodies are further provided with mounting structures, the mounting structures are arranged on the side walls of the injection pipe body, the anti-explosion plug is arranged at the top of the injection pipe body, a through hole is arranged on the top cover corresponding to the position of the cold trap body, and the top of the injection pipe body penetrates out of the through hole, so that the anti-explosion plug is exposed out of the upper surface of the top cover.
5. A high-efficiency surface treatment method with metal texture for a glass shell is applied to the equipment of any one of claims 1 to 4, and the treatment method specifically comprises the following steps:
s101: the circulating cooling device controls the temperature of the cooling liquid at a first temperature;
s102: the hydraulic cylinder pushes out the ejector rod downwards, the ejector rod drives the material frame to descend to a first height, the frame body is not immersed below the liquid level of the etching liquid in the inner container, the cold cavity is partially immersed below the liquid level of the etching liquid, the etching liquid is cooled by the cold cavity through heat exchange, the stirring blades continuously rotate, and the temperature of the etching liquid is reduced to a second temperature;
s103: the hydraulic cylinder continues to push out the ejector rod downwards, the ejector rod drives the material frame to descend to a second height, the frame body is immersed below the liquid level of the etching liquid, the stirring blades continuously rotate, and the etching liquid enters the frame body through the intervals between the stand columns to perform low-temperature surface treatment on the glass casing;
s104: the infrared temperature measurement sensor monitors the temperature of the etching liquid, and starts to time when the temperature of the etching liquid reaches a first temperature;
s105: when the timing reaches a specified length, the hydraulic cylinder retracts the ejector rod upwards to lift the material frame, and the frame body and the cold cavity are all separated from the etching liquid;
s106: the top travelling crane moves forwards, and the material frame leaves the upper part of the etching tank.
6. The method as claimed in claim 5, wherein the etching bath further comprises a stirring device and a circulating cooling device, the inner container is disposed in the low temperature bath, a cooling liquid is disposed between the low temperature bath and the inner container, the circulating cooling device comprises a liquid inlet pipe and a liquid outlet pipe, the liquid inlet pipe and the liquid outlet pipe are respectively communicated with the cooling liquid in the low temperature bath, the inner wall of the inner container is made of Teflon, and a temperature difference exists between the etching liquid in the inner container and the cooling liquid in the low temperature bath.
7. The method as claimed in claim 5, wherein the hydraulic cylinder pushes out an ejector rod downwards, the ejector rod drives the material frame to descend to a first height, the frame body is not immersed under the etching liquid level in the inner container at the moment, the cold chamber is partially immersed under the etching liquid level, the cold chamber cools the etching liquid through heat exchange, the stirring blades continuously rotate, the temperature of the etching liquid is reduced to a second temperature, the apparatus further comprises a control module, an output port of the infrared temperature sensor is connected with an input port of the control module, the control module is further provided with a storage unit, a calculation unit and a timing unit, the storage unit stores the specified duration, the first temperature and the second temperature, and the first output port of the control module is connected with the input port of the hydraulic cylinder, the second output port of the control module is connected with the input port of the driving unit of the stirring device, the stirring device is provided with a driving unit, a rotating shaft and stirring blades, the rotating shaft is connected with the driving unit and the blades, the driving unit is arranged outside the low-temperature bath tank, the stirring blades are arranged inside the inner container and positioned at the bottom of the inner container, the rotating shaft penetrates through the low-temperature bath tank and extends into the inner container, the second output port of the control module outputs a starting signal to the input port of the driving unit of the stirring device, and the stirring blades start to rotate,
meanwhile, a first output port of the control module outputs a first descending instruction to the hydraulic cylinder, the hydraulic cylinder pushes the ejector rod downwards, the ejector rod drives the material frame to descend to a first height,
the infrared temperature measurement sensor measures the temperature of the etching liquid and sends the measured temperature value to the control module through an input port of the control module, the control module calculation unit compares the received temperature value with the second temperature value stored in the storage unit, when the measured temperature value is equal to the stored second temperature value, the control module outputs a second descending instruction to the hydraulic cylinder through the first output port, the hydraulic cylinder continues to push the ejector rod downwards, and the ejector rod drives the material frame to descend to a second height.
8. The method as claimed in claim 7, wherein the infrared temperature sensor measures the temperature of the etching liquid in real time and sends the measured temperature value to the control module through an input port of the control module after the control module outputs a second down command to the hydraulic cylinder through a first output port, the control module computing unit compares the temperature value with the stored first temperature value, when the temperature value measured by the infrared temperature sensor is equal to the first temperature value, the timing unit starts timing until the timing reaches a specified duration stored in the storage unit, the first output port of the control module outputs an up command to the hydraulic cylinder, and simultaneously, the second output port of the control module outputs a stop signal to an input port of the stirring device driving unit, the agitating blade stops rotating.
9. The method as claimed in claim 5, wherein the top carriage moves forward and the frame leaves the etching chamber, further comprising,
still be provided with the driving track, be provided with the top driving on the driving track, the mount is installed on the top driving and is located the top driving under, the etching groove set up in under the driving track.
CN202010451864.0A 2020-05-25 2020-05-25 High-efficiency glass casing metal texture surface treatment equipment and method Active CN111453998B (en)

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JPH06120203A (en) * 1992-10-06 1994-04-28 Hitachi Ltd Temperature control method for liquid and temperature controller for liquid
JP2000234186A (en) * 1999-02-10 2000-08-29 Sharp Corp Etching device
CN1713359A (en) * 2004-06-22 2005-12-28 茂德科技股份有限公司 Etching system and treatment of etching agent
CN101329992A (en) * 2007-06-20 2008-12-24 辛耘企业股份有限公司 Fluid temperature control system and temperature regulating equipment
CN202576240U (en) * 2012-04-05 2012-12-05 江西沃格光电科技有限公司 Glass substrate reduction etching groove
CN102863153A (en) * 2011-07-08 2013-01-09 株式会社M-M技术 Glass thinning system
WO2016113970A1 (en) * 2015-01-14 2016-07-21 セントラル硝子株式会社 Antiglare glass sheet article for display device and method of manufacturing same
CN111180352A (en) * 2018-11-12 2020-05-19 长鑫存储技术有限公司 Constant-temperature wet etching equipment and method

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TWI235425B (en) * 2004-05-26 2005-07-01 Promos Technologies Inc Etching system and method for treating the etching solution thereof

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06120203A (en) * 1992-10-06 1994-04-28 Hitachi Ltd Temperature control method for liquid and temperature controller for liquid
JP2000234186A (en) * 1999-02-10 2000-08-29 Sharp Corp Etching device
CN1713359A (en) * 2004-06-22 2005-12-28 茂德科技股份有限公司 Etching system and treatment of etching agent
CN101329992A (en) * 2007-06-20 2008-12-24 辛耘企业股份有限公司 Fluid temperature control system and temperature regulating equipment
CN102863153A (en) * 2011-07-08 2013-01-09 株式会社M-M技术 Glass thinning system
CN202576240U (en) * 2012-04-05 2012-12-05 江西沃格光电科技有限公司 Glass substrate reduction etching groove
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CN111180352A (en) * 2018-11-12 2020-05-19 长鑫存储技术有限公司 Constant-temperature wet etching equipment and method

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