CN111407786A - Squeezing method of three-delicacy raw material of medicated leaven - Google Patents
Squeezing method of three-delicacy raw material of medicated leaven Download PDFInfo
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- CN111407786A CN111407786A CN201911201253.4A CN201911201253A CN111407786A CN 111407786 A CN111407786 A CN 111407786A CN 201911201253 A CN201911201253 A CN 201911201253A CN 111407786 A CN111407786 A CN 111407786A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/282—Artemisia, e.g. wormwood or sagebrush
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/70—Polygonaceae (Buckwheat family), e.g. spineflower or dock
- A61K36/704—Polygonum, e.g. knotweed
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/19—Preparation or pretreatment of starting material involving fermentation using yeast, bacteria or both; enzymatic treatment
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
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Abstract
The invention relates to the technical field of medicine preparation, and provides a squeezing method of a three-delicacy raw material of medicated leaven, aiming at solving the problems of low extraction rate and volatile effective components of the traditional squeezing method of the three-delicacy raw material of the medicated leaven, which comprises the following steps: (1) cleaning the raw materials, mashing, and ultrasonically soaking in a wall-breaking dissociation liquid; the three fresh raw materials comprise fresh sweet wormwood, fresh red-knees herb and fresh xanthium sibiricum in equal mass ratio; (2) cleaning, draining, adding water, and squeezing in a squeezing device to obtain juice. Before squeezing the fresh sweet wormwood, the fresh red-knees herb and the fresh xanthium sibiricum, wall breaking treatment of plant cell walls is carried out in a wall breaking dissociation liquid, and in a squeezing process, effective components in the three fresh raw materials can be better extracted; the squeezing device is additionally provided with a temperature control layer containing a phase-change composite material, so that the volatilization of effective components in fresh sweet wormwood herb, fresh polygonum hydropiper and fresh xanthium sibiricum caused by system overheating in the squeezing process is avoided.
Description
Technical Field
The invention relates to the technical field of medicine preparation, in particular to a squeezing method of a three-delicacy raw material of medicated leaven.
Background
Medicated leaven (Medicated L easen Massa), also called Medicated leaven and Medicated leaven, is one of the commonly used digestion-helping medicines, is prepared by mixing the natural juice of three fresh raw materials (fresh sweet wormwood, fresh cocklebur grass and fresh red-knees herb) with bitter almond powder, red bean powder, wheat bran and flour in proportion and fermenting under proper conditions, is the most widely applied one in the traditional leaven agent, and has the effects of helping digestion, strengthening stomach, regulating middle warmer and stopping diarrhea.
In the prior art, after fresh sweet wormwood, fresh xanthium sibiricum and fresh polygonum hydropiper which are three fresh raw materials of medicated leaven are smashed and soaked in water, juice is directly squeezed by a squeezer, but the fresh xanthium sibiricum is more wrinkled, the stem is bent, the skin is light green to light yellow, and the fresh xanthium sibiricum is covered by grey brown hair. The quality is crisp, easily rolls over, and the section unevenness directly squeezes can not draw out active ingredient completely, only adopts machinery to squeeze simultaneously and still can lead to the process of squeezing the juice to produce a large amount of heats, causes volatilizing of active ingredient, and mechanical broken wall method can the broken wall, but is not abundant enough, also can produce high temperature when mechanical broken wall simultaneously, can influence the active resource utilization ratio of inside and outside active material of cell low.
Disclosure of Invention
The invention provides a squeezing method of a three-delicacy raw material of medicated leaven, which has high extraction rate and good stability and aims to overcome the problems of low extraction rate and volatile effective components of the traditional squeezing method of the three-delicacy raw material of the medicated leaven.
In order to achieve the purpose, the invention adopts the following technical scheme:
a squeezing method of a three-delicacy raw material of medicated leaven comprises the following steps:
(1) cleaning the raw materials, mashing, and ultrasonically soaking in a wall-breaking dissociation liquid; the three fresh raw materials comprise fresh sweet wormwood, fresh red-knees herb and fresh xanthium sibiricum in equal mass ratio;
(2) and (2) cleaning the raw materials of the three delicacies treated in the step (1), draining, adding water, putting into a squeezing device, and squeezing to obtain juice.
Before squeezing the fresh sweet wormwood, the fresh red-knees herb and the fresh xanthium sibiricum, the invention carries out wall breaking treatment on plant cell walls in the wall breaking dissociation liquid, and in the squeezing process, effective components in the three fresh raw materials can be better extracted.
Preferably, the wall-breaking dissociation liquid consists of the following components in percentage by mass: 10-20% of pectinase, 0.2-1.5% of cellulase, 0.02-0.05% of cysteine and cyclodextrin modified g-C3N40.03-0.05% of quantum dots and the balance of water.
The main components of the plant cell wall are cellulose and pectin, the invention carries out enzymolysis on the cell wall of the three-delicacy raw material by using pectinase and cellulase in the wall breaking dissociation liquid, the cellulase is a multi-component enzyme system, and the substrate structure is extremely complex. Adsorption by cellulase replaces the ES complex process formed by the enzyme and substrate due to the water insolubility of the substrate. Cellulase enzymes adsorb specifically on the substrate cellulose and then break down the cellulose into glucose under the synergistic effect of several components. The cell walls of the three fresh raw materials contain natural cellulase inhibitors, which can reduce the enzymolysis efficiency, and the invention adds cyclodextrin to modify g-C in the system3N4Quantum dots, cyclodextrins and g-C3N4-NH at the periphery of quantum dots2Cyclodextrin modified g-C forming a network structure after condensation3N4The quantum dots have excellent biocompatibility, can be tightly combined with cell walls, and the g-C is modified by cysteine and cyclodextrin3N4The quantum dots synergistically inhibit the release of a natural cellulase inhibitor in the cell wall of the raw materials of the three delicacies, and the enzymolysis efficiency of cellulase and pectin is improved.
Preferably, the cyclodextrin modifies g-C3N4The preparation method of the quantum dot comprises the following steps: dispersing cyclodextrin in g-C3N4Quantum dotsUniformly mixing the solution at the temperature of 80-120 ℃ to obtain the cyclodextrin modified g-C3N4And (4) quantum dots.
Preferably, the cyclodextrin is reacted with g-C3N4The mass ratio of the quantum dots is (4-6): 1.
preferably, the pH value of the wall-breaking dissociation liquid is controlled to be 4.5-6.5, and the cellulase and pectinase have the highest activity under the environment.
Preferably, the ultrasonic soaking temperature is 10-15 ℃, the ultrasonic power is 40-60 KHZ, and the time is 30-60 min.
Preferably, in the step (2), the squeezing device comprises a driving mechanism, a squeezing mechanism, a juice outlet mechanism and a temperature control mechanism. The juice outlet mechanism is provided with a punching area.
Preferably, a temperature control layer is arranged in the temperature control mechanism, and the phase-change composite material is filled in the temperature control layer. The phase change composite material is a substance which changes the state of the substance under the condition of constant temperature and can provide latent heat. The process of converting the physical property is called a phase change process, and at the moment, the phase change material absorbs or releases a large amount of latent heat, so that the volatilization of effective components in the fresh sweet wormwood, the fresh red-knees herb and the fresh xanthium sibiricum caused by system overheating in the squeezing process is avoided.
Preferably, the phase-change composite material is paraffin, and the latent heat value of the paraffin is 190 Kj/kg.
Therefore, the invention has the following beneficial effects: before squeezing the fresh sweet wormwood, the fresh red-knees herb and the fresh xanthium sibiricum, wall breaking treatment of plant cell walls is carried out in a wall breaking dissociation liquid, and in a squeezing process, effective components in the three fresh raw materials can be better extracted; the squeezing device is additionally provided with a temperature control layer containing a phase-change composite material, so that the volatilization of effective components in fresh sweet wormwood herb, fresh polygonum hydropiper and fresh xanthium sibiricum caused by system overheating in the squeezing process is avoided.
Drawings
Fig. 1 is a schematic view of a press apparatus.
In the figure: the oil cylinder 1, the oil pipe 2, the hydraulic station 3, the punching area 4 and the temperature control layer 5.
Detailed Description
The technical solution of the present invention is further specifically described below by using specific embodiments and with reference to the accompanying drawings.
In the present invention, all the equipment and materials are commercially available or commonly used in the art, and the methods in the following examples are conventional in the art unless otherwise specified.
As shown in fig. 1, the squeezing device according to the following embodiments of the present invention includes a driving mechanism, a squeezing mechanism, a juice discharging mechanism and a temperature control mechanism (not fully shown in the figure), the driving mechanism is an oil cylinder 1, the oil cylinder 1 is communicated with a hydraulic station 3 through an oil pipe 2, the juice discharging mechanism is provided with a punching area 4, and the temperature control mechanism is provided with a temperature control layer 5.
Example 1
(1) Cleaning fresh herba Artemisiae Annuae, fresh herba Polygoni Hydropiperis, and fresh herba Xanthii each 100kg, mashing, and ultrasonically soaking in wall-breaking dissociation liquid; the three-delicacy raw materials consist of fresh sweet wormwood, fresh red-knees herb and fresh siberian cocklebur grass in equal mass ratio; the wall breaking dissociation liquid consists of the following components in percentage by mass: 10% of pectinase, 1.5% of cellulase, 0.02% of cysteine and cyclodextrin modified g-C3N40.03 percent of quantum dots and the balance of water; controlling pH value of the dissociation liquid at 4.5, ultrasonic soaking temperature at 10 deg.C, ultrasonic power at 60KHZ, and time at 30 min;
cyclodextrin modified g-C3N4The preparation method of the quantum dot comprises the following steps: dispersing cyclodextrin in g-C3N4Mixing the quantum dot solution uniformly at 80 ℃ to obtain cyclodextrin modified g-C3N4Quantum dots; cyclodextrin with g-C3N4The mass ratio of the quantum dots is 4: 1;
(2) cleaning and draining the raw materials of the three delicacies treated in the step (1), adding 55kg of water, putting into the squeezing device, and filling paraffin into the temperature control layer; squeezing to obtain juice, wherein the juice can be stored for 24 hr or less.
Example 2
(1) Collecting fresh herba Artemisiae Annuae, fresh herba Polygoni Hydropiperis, and fresh herba Xanthii each 100kg, cleaning, and mashingUltrasonic soaking in wall breaking dissociation liquid; the three-delicacy raw materials consist of fresh sweet wormwood, fresh red-knees herb and fresh siberian cocklebur grass in equal mass ratio; the wall breaking dissociation liquid consists of the following components in percentage by mass: 20% of pectinase, 0.2% of cellulase, 0.05% of cysteine and cyclodextrin modified g-C3N40.03 percent of quantum dots and the balance of water; controlling pH value of the dissociation liquid at 6.5, ultrasonic soaking temperature at 10 deg.C, ultrasonic power at 40KHZ, and time at 60 min;
cyclodextrin modified g-C3N4The preparation method of the quantum dot comprises the following steps: dispersing cyclodextrin in g-C3N4Mixing the quantum dot solution uniformly at 120 ℃ to obtain cyclodextrin modified g-C3N4Quantum dots; cyclodextrin with g-C3N4The mass ratio of the quantum dots is 6: 1;
(2) cleaning and draining the raw materials of the three delicacies treated in the step (1), adding 55kg of water, putting into the squeezing device, and filling paraffin into the temperature control layer; squeezing to obtain juice, wherein the juice can be stored for 24 hr or less.
Example 3
(1) Cleaning fresh herba Artemisiae Annuae, fresh herba Polygoni Hydropiperis, and fresh herba Xanthii each 100kg, mashing, and ultrasonically soaking in wall-breaking dissociation liquid; the three-delicacy raw materials consist of fresh sweet wormwood, fresh red-knees herb and fresh siberian cocklebur grass in equal mass ratio; the wall breaking dissociation liquid consists of the following components in percentage by mass: 15% of pectinase, 1.0% of cellulase, 0.03% of cysteine and cyclodextrin modified g-C3N40.04% of quantum dots and the balance of water; controlling pH value of the dissociation liquid at 5, ultrasonic soaking temperature at 12 deg.C, ultrasonic power at 50KHZ, and time at 50 min;
cyclodextrin modified g-C3N4The preparation method of the quantum dot comprises the following steps: dispersing cyclodextrin in g-C3N4The quantum dots are evenly mixed in the solution at the temperature of 100 ℃ to obtain the cyclodextrin modified g-C3N4Quantum dots; cyclodextrin with g-C3N4The mass ratio of the quantum dots is 5: 1;
(2) cleaning and draining the raw materials of the three delicacies treated in the step (1), adding 55kg of water, putting into the squeezing device, and filling paraffin into the temperature control layer; squeezing to obtain juice, wherein the juice can be stored for 24 hr or less.
Comparative example 1 (cyclodextrin-free modified g-C in the dissociation liquid after wall breaking3N4Quantum dot)
The difference between the comparative example 1 and the example 1 is that the wall-breaking dissociation liquid consists of the following components in percentage by mass: 10% of pectinase, 1.5% of cellulase, 0.02% of cysteine and the balance of water; the rest of the process is completely the same.
Comparative example 2 (cysteine was not added to the cell wall breaking dissociation solution)
The difference between the comparative example 2 and the example 1 is that the wall-breaking dissociation liquid consists of the following components in percentage by mass: 10% of pectinase, 1.5% of cellulase and cyclodextrin modified g-C3N40.03 percent of quantum dots and the balance of water; the rest of the process is completely the same.
Comparative example 3 (pressing device not containing temperature control layer)
Comparative example 2 differs from example 1 in that the press device does not contain a temperature control layer and the rest of the process is exactly the same.
Comparative example 4 (No dissociation process, squeezing device not containing temperature control layer)
The preparation method comprises the steps of smashing (cutting) fresh sweet wormwood, fresh polygonum hydropiper and fresh xanthium sibiricum, adding water (soaking for more than 3 hours and less than 12 hours), squeezing to obtain juice (100 kg of each of the fresh sweet wormwood, the fresh polygonum hydropiper and the fresh xanthium sibiricum and 55kg of each of the fresh xanthium sibiricum), weighing the juice, and storing the juice for less than 24 hours.
The performance indexes of the juices of examples 1-3 and comparative examples 1-2 were measured, and the results are shown in Table 1:
TABLE 1 test results
| Numbering | Juice yield (%) | Loss ratio of active ingredient (%) |
| Example 1 | 80 | 15 |
| Example 2 | 79 | 18 |
| Example 3 | 85 | 20 |
| Comparative example 1 | 55 | 17 |
| Comparative example 2 | 60 | 16 |
| Comparative example 3 | 80 | 45 |
| Comparative example 4 | 40 | 55 |
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in any way, and other variations and modifications may be made without departing from the spirit of the invention as set forth in the claims.
Claims (8)
1. A squeezing method of a three-delicacy raw material of medicated leaven is characterized by comprising the following steps:
(1) cleaning the raw materials, mashing, and ultrasonically soaking in a wall-breaking dissociation liquid; the three fresh raw materials comprise fresh sweet wormwood, fresh red-knees herb and fresh xanthium sibiricum in equal mass ratio;
(2) and (2) cleaning the raw materials of the three delicacies treated in the step (1), draining, adding water, putting into a squeezing device, and squeezing to obtain juice.
2. The squeezing method of the three delicacies of medicated leaven raw material as claimed in claim 1, wherein the wall breaking dissociation liquid comprises the following components in percentage by mass: 10-20% of pectinase, 0.2-1.5% of cellulase, 0.02-0.05% of cysteine and cyclodextrin modified g-C3N40.03-0.05% of quantum dots and the balance of water.
3. The method for squeezing three delicacies of medicated leaven raw material as claimed in claim 2, wherein the cyclodextrin modified g-C3N4The preparation method of the quantum dot comprises the following steps: dispersing cyclodextrin in g-C3N4Uniformly mixing the quantum dot solution at the temperature of 80-120 ℃ to obtain cyclodextrin modified g-C3N4And (4) quantum dots.
4. The method as claimed in claim 3, wherein the cyclodextrin is mixed with g-C3N4The mass ratio of the quantum dots is (4-6): 1.
5. the squeezing method of the three delicacies of medicated leaven raw material as claimed in claim 1, wherein the pH value of the wall-breaking dissociation liquid is controlled to be 4.5-6.5.
6. The squeezing method of the fresh Massa Medicata Fermentata raw material as claimed in claim 1, wherein in step (1), the temperature of ultrasonic soaking is 10-15 deg.C, the ultrasonic power is 40-60 KHZ, and the time is 30-60 min.
7. The method for squeezing three fresh ingredients of medicated leaven according to any one of claims 1 to 6, wherein in the step (2), the squeezing device comprises a driving mechanism, a squeezing mechanism, a juice outlet mechanism and a temperature control mechanism.
8. The method for squeezing a three-delicacy raw material of medicated leaven according to claim 7, wherein a temperature control layer is arranged in the temperature control mechanism, and the temperature control layer is filled with a phase change composite material.
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN204757440U (en) * | 2015-05-20 | 2015-11-11 | 佛山市顺德区美的电热电器制造有限公司 | Refrigerating plant and electric refrigerator |
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN204757440U (en) * | 2015-05-20 | 2015-11-11 | 佛山市顺德区美的电热电器制造有限公司 | Refrigerating plant and electric refrigerator |
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| 刘锴栋等: "果胶酶对番石榴出汁率的影响", 《食品工业》 * |
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Application publication date: 20200714 |