CN111407694A

CN111407694A - Whitening and moisturizing sleeping mask and preparation method thereof

Info

Publication number: CN111407694A
Application number: CN202010184284.XA
Authority: CN
Inventors: 王国广
Original assignee: Individual
Current assignee: Individual
Priority date: 2020-03-17
Filing date: 2020-03-17
Publication date: 2020-07-14

Abstract

The invention discloses a whitening and moisturizing sleeping mask and a preparation method thereof, and belongs to the technical field of cosmetics. The product developed by the invention comprises 10-15 parts of echeveria glauca juice, 10-15 parts of castor oil, 3-5 parts of glycylglycine, 1-3 parts of lanolin, 1-3 parts of lecithin, 10-15 parts of water, 3-5 parts of graphene oxide, 2-5 parts of plant alkali, 4-8 parts of thickening agent, and inositol, caffeine and montmorillonite are also added; when in preparation, the thickening agent and water are mixed and swelled to obtain glue solution; and mixing graphene oxide, the echeveria glauca juice, glycylglycine, lanolin, lecithin, glue solution and plant alkali, performing ultrasonic dispersion, adding castor seed oil, uniformly stirring and mixing, and performing freeze thawing for 5-10 times to obtain the product. The product obtained by the invention has good whitening and moisturizing effects.

Description

Whitening and moisturizing sleeping mask and preparation method thereof

Technical Field

The invention relates to the technical field of cosmetics, in particular to a whitening and moisturizing sleeping mask and a preparation method thereof.

Background

With the improvement of living standard, more and more people are used to make up, but after the face is made up, if the face is not cleaned completely, the residual cosmetics can cause the pore blockage of the face skin, so that the secretion of oil and water of the skin is disordered, and the puzzling skin problems of acne, comedo, blackhead and the like are caused. Meanwhile, the existing environment pollution is very serious, the dust and the cosmetics are greatly damaged to the skin, and if the skin is not cleaned in time, the skin can enter hair follicles along with the breathing of pores to form cysts, and the skin is difficult to clean out after being present in the surface layer of the skin for a long time, so the cleaning link of the skin is very important. The facial mask in the prior art has the following problems: the makeup removing steps are multiple, the use is not easy, the smearing is not uniform, and the cleaning effect is poor.

Nowadays, as the quality of life of people is improved and the beauty is pursued, more and more people choose to use the facial mask for skin care. The deep cleaning mask is a carrier of beauty care products, can remove blackheads, shrink pores, has the effects of deep cleaning skin and the like, and is popular with people. Most of the deep cleaning facial masks on the market are patch facial masks. The patch type facial mask uses non-woven fabric as a substrate, and is applied on the skin by soaking essence. The main problem with this approach is that the mask does not fit perfectly to the skin due to individual differences. The application type mask solves the problem. When in use, the pasty facial mask is uniformly applied on the skin, and can be torn off after the essence is absorbed. Various brands of smearing type deep cleaning facial masks on the market are full of precious. To gain market reach, manufacturers go to great lengths to make a wide variety of products. The formula is healthy and environment-friendly, and the package is beautiful and elegant. In contrast, the visual effect of the contents themselves, which is more noticeable to the consumer, is of no particular significance. However, further studies are required for the moisturizing effect of the mask.

Disclosure of Invention

The invention aims to provide a whitening and moisturizing sleeping mask and a preparation method thereof, and aims to overcome the defect that the whitening and moisturizing effects of the mask in the prior art are poor.

In order to achieve the purpose, the invention provides the following technical scheme:

the whitening and moisturizing sleeping mask comprises the following raw materials in parts by weight: 10-15 parts of echeveria glauca juice, 10-15 parts of castor seed oil, 3-5 parts of glycylglycine, 1-3 parts of lanolin, 1-3 parts of lecithin, 10-15 parts of water, 3-5 parts of graphene oxide, 2-5 parts of plant alkali and 4-8 parts of thickening agent.

Furthermore, inositol accounting for 10-15% of the mass of the echeveria glauca juice is also included.

Furthermore, the lotus seed paste also comprises caffeine accounting for 1-3% of the mass of the lotus seed juice.

Further, the lotus seed wine also comprises montmorillonite accounting for 20-50% of the mass of the lotus seed juice.

Further, the montmorillonite is montmorillonite modified by strong acid.

Further, the plant alkaloid is solanine and berberine in a mass ratio of 1: 1-5: 1 are mixed.

Further, the thickener is any one of peach gum, xanthan gum and brown algae polysaccharide.

A preparation method of a whitening and moisturizing sleeping mask comprises the following specific preparation steps:

(1) preparing raw materials;

(2) firstly, mixing a thickening agent and water for swelling to obtain a glue solution;

(3) and mixing the graphene oxide, the echeveria glauca juice, the glycylglycine, the lanolin, the lecithin, the glue solution and the plant alkali, performing ultrasonic dispersion, adding the castor seed oil, and uniformly stirring and mixing to obtain the product.

Further, the specific preparation steps comprise:

(1) preparing raw materials;

(3) and mixing graphene oxide, the echeveria glauca juice, glycylglycine, lanolin, lecithin, glue solution and plant alkali, performing ultrasonic dispersion, adding castor seed oil, uniformly stirring and mixing, and performing freeze thawing for 5-10 times to obtain the product.

Further, the freeze-thaw cycle is: freezing the mixture for 3 to 5 hours at the temperature of between 20 ℃ below zero and 5 ℃ below zero, and naturally thawing the mixture for 6 to 8 hours at room temperature.

Has the advantages that:

(1) according to the technical scheme of the invention, by adding the castor bean oil, firstly, the castor bean oil has excellent effects of moisturizing skin, promoting tissue regeneration, relieving swelling and pain, can be beneficial to the proliferation and regeneration of facial skin cells after being used, and is beneficial to the thickening of the horny layer of the facial skin along with the continuous regeneration of the cells, so that the face skin has a good moisturizing effect due to the protective effect of the horny layer thickened on the surface of the skin even if the mask is cleaned, and the moisturizing effect of the newly-generated skin is more excellent than that of the old skin, in addition, the castor bean oil is rich in vitamins, has strong oxidation resistance and moisturizing performance, can maintain the permeability of capillary vessels, improves the blood circulation of the facial skin, promotes the regeneration and the repair of skin cells, can form an oily environment on the surface of the facial skin after being used, and reduces the stimulation of chemical substances to the skin, the stimulation of peripheral nerves can be reduced, so that good moisturizing and whitening effects are realized;

(2) according to the technical scheme, the inositol and the caffeine are added and matched to improve the outward expansion structure around the pores of the facial skin, so that the pores are refined, allergy caused by the fact that sensitive substances permeate into the skin through the pores is avoided, meanwhile, the evaporation amount of moisture in the skin can be reduced, a good moisturizing effect is achieved, and the effects of tightening the skin and improving the skin state around the pores are achieved;

(3) according to the technical scheme, the graphene oxide is added, in the preparation process, the water-based component is firstly diffused and permeated into the structure between the graphene oxide layers under the action of the emulsifier lanolin and lecithin, so that good protection is obtained, the deterioration in the storage process is avoided, the storage stability is improved, in addition, the oil castor oil is coated on the surface to form a water-in-oil emulsification structure, so that in the use process, the oil castor oil firstly contacts the skin, the water-based component slowly permeates and is absorbed by the skin under the emulsification action of the subsequent graphene oxide, and a good whitening effect is achieved.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Strong acid modified montmorillonite: montmorillonite and hydrochloric acid solution are mixed according to the mass ratio of 1: 5-1: 20, mixing and dispersing, pouring into a hydrothermal kettle, carrying out hydrothermal stirring reaction for 3-5 h at the temperature of 150-200 ℃ and the pressure of 2.0-5.0 MPa and the stirring speed of 300-500 r/min, filtering, collecting a filter cake, washing the filter cake with deionized water until the washing liquid is neutral, transferring the washed filter cake into an oven, and drying at the temperature of 105-110 ℃ to constant weight to obtain strong acid modified montmorillonite;

according to the weight parts, sequentially taking 10-15 parts of echeveria glauca juice, 10-15 parts of castor oil, 3-5 parts of glycylglycine, 1-3 parts of lanolin, 1-3 parts of lecithin, 10-15 parts of water, 3-5 parts of graphene oxide, 2-5 parts of plant alkali, 4-8 parts of thickening agent, inositol which is 10-15% of the weight of the echeveria glauca juice, caffeine which is 1-3% of the weight of the echeveria glauca juice, and strong acid modified montmorillonite which is 20-50% of the weight of the echeveria glauca juice; firstly, mixing a thickening agent and water, and standing and swelling for 8-12 hours at room temperature to obtain a glue solution; and mixing graphene oxide, echeveria glauca juice, glycylglycine, lanolin, lecithin, glue solution, vegetable alkali, inositol, caffeine and strong acid modified montmorillonite, performing ultrasonic dispersion for 4-6 hours under the condition that the ultrasonic frequency is 55-60 kHz, adding castor seed oil, stirring and mixing for 2-3 hours under the condition that the rotating speed is 1200-1800 r/min, freezing for 3-5 hours at the temperature of-20 to-5 ℃, naturally thawing for 6-8 hours at room temperature, performing freeze thawing cycle for 5-10 times, discharging and packaging to obtain the product.

The plant alkaloid is solanine and berberine in a mass ratio of 1: 1-5: 1, mixing; the thickener is any one of peach gum, xanthan gum and brown algae polysaccharide.

Example 1

Strong acid modified montmorillonite: montmorillonite and 10% hydrochloric acid solution in a mass ratio of 1: 5, mixing and dispersing, pouring into a hydrothermal kettle, carrying out hydrothermal stirring reaction for 3 hours at the temperature of 150 ℃, the pressure of 2.0MPa and the stirring speed of 300r/min, filtering, collecting a filter cake, washing the filter cake with deionized water until a washing solution is neutral, transferring the washed filter cake into a drying oven, and drying at the temperature of 105 ℃ until the weight is constant to obtain strong acid modified montmorillonite;

according to the weight parts, 10 parts of gelidium amansii juice, 10 parts of castor seed oil, 3 parts of glycylglycine, 1 part of lanolin, 1 part of lecithin, 10 parts of water, 3 parts of graphene oxide, 2 parts of plant alkali, 4 parts of thickening agent, inositol accounting for 10% of the weight of the gelidium amansii juice, caffeine accounting for 1% of the weight of the gelidium amansii juice and strong acid modified montmorillonite accounting for 20% of the weight of the gelidium amansii juice are taken in sequence; firstly, mixing a thickening agent with water, and standing and swelling for 8 hours at room temperature to obtain a glue solution; and mixing graphene oxide, echeveria glauca juice, glycylglycine, lanolin, lecithin, glue solution, vegetable alkali, inositol, caffeine and strong acid modified montmorillonite, performing ultrasonic dispersion for 4 hours under the condition that the ultrasonic frequency is 55kHz, adding castor seed oil, stirring and mixing for 2 hours under the condition that the rotating speed is 1200r/min, freezing for 3 hours at the temperature of-20 ℃, naturally thawing for 6 hours at room temperature, performing freeze thawing cycle for 5 times, discharging and packaging to obtain the product.

The plant alkaloid is solanine and berberine in a mass ratio of 1: 1, mixing; the thickening agent is peach gum.

Example 2

Strong acid modified montmorillonite: montmorillonite and a hydrochloric acid solution with the mass fraction of 12% are mixed according to the mass ratio of 1: 10, mixing and dispersing, pouring into a hydrothermal kettle, carrying out hydrothermal stirring reaction for 4 hours at the temperature of 180 ℃, the pressure of 4.0MPa and the stirring speed of 400r/min, filtering, collecting a filter cake, washing the filter cake with deionized water until a washing solution is neutral, transferring the washed filter cake into a drying oven, and drying at the temperature of 108 ℃ to constant weight to obtain strong acid modified montmorillonite;

according to the weight parts, 12 parts of gelidium amansii juice, 12 parts of castor seed oil, 4 parts of glycylglycine, 2 parts of lanolin, 2 parts of lecithin, 12 parts of water, 4 parts of graphene oxide, 4 parts of plant alkali, 5 parts of a thickening agent, inositol accounting for 12% of the weight of the gelidium amansii juice, caffeine accounting for 2% of the weight of the gelidium amansii juice, and strong acid modified montmorillonite accounting for 30% of the weight of the gelidium amansii juice are taken in sequence; firstly, mixing a thickening agent with water, and standing and swelling for 10 hours at room temperature to obtain a glue solution; and mixing graphene oxide, echeveria glauca juice, glycylglycine, lanolin, lecithin, glue solution, vegetable alkali, inositol, caffeine and strong acid modified montmorillonite, performing ultrasonic dispersion for 5 hours under the condition of ultrasonic frequency of 58kHz, adding castor seed oil, stirring and mixing for 2.5 hours under the condition of rotation speed of 1500r/min, freezing for 4 hours at the temperature of-10 ℃, naturally thawing for 7 hours at room temperature, performing freeze-thawing for 8 times in such a way, discharging, and packaging to obtain the product.

The plant alkaloid is solanine and berberine in a mass ratio of 4: 1, mixing; the thickening agent is xanthan gum.

Example 3

Strong acid modified montmorillonite: montmorillonite and 15% hydrochloric acid solution in a mass ratio of 1: 20, mixing and dispersing, pouring into a hydrothermal kettle, carrying out hydrothermal stirring reaction for 5 hours at the temperature of 200 ℃, the pressure of 5.0MPa and the stirring speed of 500r/min, filtering, collecting a filter cake, washing the filter cake with deionized water until a washing solution is neutral, transferring the washed filter cake into a drying oven, and drying at the temperature of 110 ℃ until the weight is constant to obtain strong acid modified montmorillonite;

according to the weight parts, 15 parts of gelidium amansii juice, 15 parts of castor seed oil, 5 parts of glycylglycine, 3 parts of lanolin, 3 parts of lecithin, 15 parts of water, 5 parts of graphene oxide, 5 parts of plant alkali, 8 parts of thickening agent, inositol 15% by mass of the gelidium amansii juice, caffeine 3% by mass of the gelidium amansii juice and strong acid modified montmorillonite 50% by mass of the gelidium amansii juice are taken in sequence; firstly, mixing a thickening agent with water, and standing and swelling for 12 hours at room temperature to obtain a glue solution; and mixing graphene oxide, echeveria glauca juice, glycylglycine, lanolin, lecithin, glue solution, vegetable alkali, inositol, caffeine and strong acid modified montmorillonite, performing ultrasonic dispersion for 6 hours under the condition that the ultrasonic frequency is 60kHz, adding castor seed oil, stirring and mixing for 3 hours under the condition that the rotating speed is 1800r/min, freezing for 5 hours at the temperature of-5 ℃, naturally thawing for 8 hours at room temperature, performing freeze thawing cycle for 10 times, discharging and packaging to obtain the product.

The plant alkaloid is solanine and berberine in a mass ratio of 5: 1, mixing; the thickening agent is brown algae polysaccharide.

Comparative example 1

This comparative example is compared to example 1 with the difference that no graphene oxide is added and the remaining conditions remain unchanged.

Comparative example 2

This comparative example is compared to example 1 with the difference that inositol and caffeine are not added and the remaining conditions remain unchanged.

Comparative example 3

This comparative example differs from example 1 in that: castor oil was not added and the remaining conditions were kept constant.

The examples and comparative products were tested for performance, the specific test methods and test results are as follows:

20 subjects with the age of 20-40 years are selected from each experimental group. After the face is cleaned, the facial mask is smeared on the face, washed off after 20 minutes, used for 2-3 times per week, and after ten months of continuous use, a subject is subjected to use feeling survey, and the evaluation is divided into 5 grades: more than 90% of subjects were satisfied and scored 5; 80% to 90% of subjects were satisfied and rated 4; 70-80% of subjects were satisfied and scored 3; 60-70% of the subjects are satisfied and scored as 2; less than 60% of subjects were satisfied with a score of 1.

Specific detection results are shown in table 1:

the detection results in table 1 show that the product obtained by the invention has good whitening and moisturizing effects.

It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein, and any reference thereto is therefore intended to be embraced therein.

Claims

1. The whitening and moisturizing sleeping mask is characterized by comprising the following raw materials in parts by weight: 10-15 parts of echeveria glauca juice, 10-15 parts of castor seed oil, 3-5 parts of glycylglycine, 1-3 parts of lanolin, 1-3 parts of lecithin, 10-15 parts of water, 3-5 parts of graphene oxide, 2-5 parts of plant alkali and 4-8 parts of thickening agent.

2. The whitening and moisturizing sleeping mask as claimed in claim 1, further comprising inositol accounting for 10-15% of the mass of the echeveria glauca juice.

3. The whitening and moisturizing sleeping mask as claimed in claim 1, further comprising caffeine in an amount of 1-3% by mass of the echeveria glauca juice.

4. The whitening and moisturizing sleeping mask as claimed in claim 1, further comprising montmorillonite accounting for 20-50% of the mass of the echeveria glauca juice.

5. The whitening and moisturizing sleeping mask as claimed in claim 4, wherein the montmorillonite is montmorillonite modified by strong acid.

6. The whitening and moisturizing sleeping mask as claimed in claim 1, wherein the plant alkaloid is solanine and berberine in a mass ratio of 1: 1-5: 1 are mixed.

7. The whitening and moisturizing sleeping mask as claimed in claim 1, wherein the thickener is any one of peach gum, xanthan gum and brown algae polysaccharide.

8. The preparation method of the whitening and moisturizing sleeping mask is characterized by comprising the following specific preparation steps:

(1) preparing raw materials;

9. The preparation method of the whitening and moisturizing sleeping mask as claimed in claim 8, wherein the specific preparation steps comprise:

(1) preparing raw materials;

10. The preparation method of the whitening and moisturizing sleeping mask as claimed in claim 9, wherein the freeze-thaw cycle is: freezing the mixture for 3 to 5 hours at the temperature of between 20 ℃ below zero and 5 ℃ below zero, and naturally thawing the mixture for 6 to 8 hours at room temperature.