CN111378526A - Preparation method of linseed essence - Google Patents
Preparation method of linseed essence Download PDFInfo
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- CN111378526A CN111378526A CN201811626886.5A CN201811626886A CN111378526A CN 111378526 A CN111378526 A CN 111378526A CN 201811626886 A CN201811626886 A CN 201811626886A CN 111378526 A CN111378526 A CN 111378526A
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- Prior art keywords
- linseed
- essence
- extract
- flask
- preparation
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention belongs to the technical field of flavors and fragrances, and particularly relates to a preparation method of linseed essence. A preparation method of linseed essence comprises the following steps: step 1: extracting semen Lini powder to obtain extract; step 2: adding the extract into a vacuum flask, and heating the vacuum flask under 180 ℃ silicone oil to obtain the linseed essence. The invention provides a preparation method of linseed essence, which solves the technical problems that linseed is not used as a product applied to tobacco products and is used as a food additive with special flavor in the prior art.
Description
Technical Field
The invention belongs to the technical field of flavors and fragrances, and particularly relates to a preparation method of linseed essence.
Background
As an agricultural product, flax seeds are commonly used as a food additive for the production of flax oil products, roughage, or more specifically. Existing processed flaxseed products include flaxseed oil, flaxseed crisps, flaxseed-based beverages, flaxseed wine, and flaxseed hair care essential oils.
The existing flaxseed products lack the application of flaxseed in tobacco products and are used as food additives with special flavor. .
Disclosure of Invention
In view of the above, the invention provides a preparation method of linseed essence, which solves the technical problems that linseed is not used as a product applied to tobacco products and is used as a food additive with a special flavor in the prior art.
The invention provides a preparation method of linseed essence, which comprises the following steps:
step 1: extracting semen Lini powder to obtain extract;
step 2: adding the extract into a vacuum flask, and heating the vacuum flask under 180 ℃ silicone oil to obtain the linseed essence.
Preferably, the volume ratio of the mass of the linseed powder to the volume of the alcohol is 1: 1-20.
Preferably, the vacuum flask is in particular a flask filled with carbon dioxide and/or nitrogen.
Preferably, the method further comprises adding propylene glycol or glycerol to the vacuum flask after adding the extract to the vacuum flask and before heating the vacuum flask.
Preferably, the mass ratio of the volume of the propylene glycol or glycerol to the flaxseed extract is 0.01-20: 1.
Preferably, the step 1 specifically comprises mixing the flaxseed meal and alcohol for extraction to obtain the extract.
Preferably, the concentration of the alcohol is 0.01% to 95%.
Compared with other flax seed product processing technologies, the flax seed essence provided by the invention utilizes chemical components contained in flax seed in a local province to carry out Maillard reaction and recombine some chemical components in the flax seed, and decomposes some chemical components into substances with smaller molecular weight, thereby greatly increasing the richness of the chemical components of the flax seed essence and simultaneously changing the fragrance characteristics of the flax seed. The preparation method provided by the invention adds the linseed essence into the tobacco product, and the linseed essence has a remarkable aroma-enhancing effect on the tobacco product compared with the linseed extract which is not treated by the process by heating the tobacco product or burning the tobacco product.
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The embodiment of the invention provides a preparation method of linseed essence, and solves the technical problems that a product applying linseed in a tobacco product and a food additive with a special flavor are lacked in the prior art.
Example 1
Mixing 1 kg of semen Lini powder and 5L of 50% ethanol, adding into ultrasonic extractor, maintaining the extraction temperature at 50 deg.C, extracting for 1 hr, filtering, collecting filtrate, and distilling off most solvent to make the extract still have fluidity. The concentrated extract was transferred to a 5L flask, and the flask was equipped with a stirring and reflux condenser, and the air in the flask was replaced with nitrogen. Placing the flask into a silicone oil heated to 180 deg.C in advance, keeping stirring the linseed extract, taking out the flask from the silicone oil after 20min, and cooling to normal temperature to obtain the linseed essence.
Example 2
Mixing 1 kg of semen Lini powder and 5L of 50% ethanol, adding into ultrasonic extractor, maintaining the extraction temperature at 50 deg.C, extracting for 1 hr, filtering, collecting filtrate, and distilling off most solvent to make the extract still have fluidity. The concentrated extract was transferred to a 5L flask, and the flask was equipped with a stirring and condensing reflux apparatus, and the air in the flask was replaced with carbon dioxide. Placing the flask into a silicone oil heated to 180 deg.C in advance, keeping stirring the linseed extract, taking out the flask from the silicone oil after 20min, and cooling to normal temperature to obtain the linseed essence.
Example 3
Mixing 1 kg of semen Lini powder with 5L of 50% ethanol, extracting at 50 deg.C for 1 hr in ultrasonic extractor, filtering, and distilling off most solvent to make the extract still have fluidity. The concentrated extract was transferred to a 5L flask, and 100mL of glycerin was added, and the flask was equipped with a stirring and condensing reflux apparatus, and the air in the flask was replaced with nitrogen. Placing the flask into a silicone oil heated to 180 deg.C in advance, keeping stirring the linseed extract, taking out the flask from the silicone oil after 20min, and cooling to normal temperature to obtain the linseed essence.
Example 4
Mixing 1 kg of semen Lini powder with 5L of 50% ethanol, extracting at 50 deg.C for 1 hr in ultrasonic extractor, filtering, and distilling off most solvent to make the extract still have fluidity. The concentrated extract was transferred to a 5L flask, 100mL of propylene glycol was added, stirring and reflux condenser were attached to the flask, and the air in the flask was replaced with nitrogen. Placing the flask into a silicone oil heated to 180 deg.C in advance, keeping stirring the linseed extract, taking out the flask from the silicone oil after 20min, and cooling to normal temperature to obtain the linseed essence.
When the linseed essence prepared by the embodiment of the invention is added into a tobacco product, the tobacco product can be heated or combusted, so that the linseed essence can have an obvious aroma-enhancing effect on the tobacco product.
The above description is only a preferred embodiment of the present invention, and it should be noted that various modifications to these embodiments can be implemented by those skilled in the art without departing from the technical principle of the present invention, and these modifications should be construed as the scope of the present invention.
Claims (7)
1. The preparation method of the linseed essence is characterized by comprising the following steps of:
step 1: extracting semen Lini powder to obtain extract;
step 2: adding the extract into a vacuum flask, and heating the vacuum flask under 180 ℃ silicone oil to obtain the linseed essence.
2. The preparation method of linseed essence according to claim 1, wherein the volume ratio of the mass of the linseed powder to the volume of the alcohol is 1: 1-20.
3. The method for preparing linseed essence according to claim 1, wherein the vacuum flask is a flask filled with carbon dioxide and/or nitrogen.
4. The method of claim 1, wherein the step of adding propylene glycol or glycerin to the vacuum flask is further included after the step of adding the extract to the vacuum flask and before the step of heating the vacuum flask.
5. The method of claim 4, wherein the volume of the propylene glycol or glycerol to the weight ratio of the linseed extract is 0.01-20: 1.
6. The method for preparing linseed essence according to claim 1, wherein the step 1 specifically comprises mixing the linseed powder and alcohol to extract an extract.
7. The method for preparing linseed essence according to claim 6, wherein the concentration of the alcohol is 0.01% -95%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811626886.5A CN111378526A (en) | 2018-12-28 | 2018-12-28 | Preparation method of linseed essence |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811626886.5A CN111378526A (en) | 2018-12-28 | 2018-12-28 | Preparation method of linseed essence |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN111378526A true CN111378526A (en) | 2020-07-07 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811626886.5A Pending CN111378526A (en) | 2018-12-28 | 2018-12-28 | Preparation method of linseed essence |
Country Status (1)
| Country | Link |
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| CN (1) | CN111378526A (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB191101637A (en) * | 1911-01-21 | 1911-08-03 | Lodovico Lucietto | Ceramic Tiles for Decorations Imitating Mosaics. |
| US7001880B1 (en) * | 2000-05-31 | 2006-02-21 | Shiseido Co., Ltd. | Method of collection of fragrance ingredient, perfume composition containing this fragrance ingredient and cosmetics containing this fragrance ingredient |
| WO2010137783A1 (en) * | 2009-05-28 | 2010-12-02 | Shin Bong Seok | Food additive composition containing water-soluble flaxseed oil in which foul odor and cyanide (-cn) toxicity are eliminated for manufacturing foods containing omega-3 fatty acid |
| CN103451019A (en) * | 2013-09-04 | 2013-12-18 | 湖北中烟工业有限责任公司 | Microcapsule essence perfume for cigarettes as well as preparation method of microcapsule essence perfume |
| CN104757704A (en) * | 2014-12-31 | 2015-07-08 | 贵州中烟工业有限责任公司 | Preparation method for tobacco extract and composition with the tobacco extract |
| CN105296140A (en) * | 2015-11-25 | 2016-02-03 | 石河子大学 | Method based on Maillard reaction for preparing strong aromatic flaxseed oil |
| CN108338299A (en) * | 2018-02-08 | 2018-07-31 | 佛山市三水区嘉华化学研究院（普通合伙） | A kind of teenager's flaxseed nutrition sports drink and preparation method thereof |
-
2018
- 2018-12-28 CN CN201811626886.5A patent/CN111378526A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB191101637A (en) * | 1911-01-21 | 1911-08-03 | Lodovico Lucietto | Ceramic Tiles for Decorations Imitating Mosaics. |
| US7001880B1 (en) * | 2000-05-31 | 2006-02-21 | Shiseido Co., Ltd. | Method of collection of fragrance ingredient, perfume composition containing this fragrance ingredient and cosmetics containing this fragrance ingredient |
| WO2010137783A1 (en) * | 2009-05-28 | 2010-12-02 | Shin Bong Seok | Food additive composition containing water-soluble flaxseed oil in which foul odor and cyanide (-cn) toxicity are eliminated for manufacturing foods containing omega-3 fatty acid |
| CN103451019A (en) * | 2013-09-04 | 2013-12-18 | 湖北中烟工业有限责任公司 | Microcapsule essence perfume for cigarettes as well as preparation method of microcapsule essence perfume |
| CN104757704A (en) * | 2014-12-31 | 2015-07-08 | 贵州中烟工业有限责任公司 | Preparation method for tobacco extract and composition with the tobacco extract |
| CN105296140A (en) * | 2015-11-25 | 2016-02-03 | 石河子大学 | Method based on Maillard reaction for preparing strong aromatic flaxseed oil |
| CN108338299A (en) * | 2018-02-08 | 2018-07-31 | 佛山市三水区嘉华化学研究院（普通合伙） | A kind of teenager's flaxseed nutrition sports drink and preparation method thereof |
Non-Patent Citations (5)
| Title |
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| 建华: "萃取芬芳――香料的提取与分离", 《生命世界》 * |
| 赵新海，等: "固体酸催化剂在香料合成中的应用", 《安徽农业科学》 * |
| 邹演，等: "亚麻籽粕制备多肽饮料的研究", 《食品工业》 * |
| 陈海华，等: "亚麻籽胶的研究进展与应用", 《食品与发酵工业》 * |
| 魏长庆，等: "亚麻籽油中maillard源挥发性香气形成机理的初步研究", 《中国油脂》 * |
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Application publication date: 20200707 |