CN111280310A - Rice bran oil fat powder and preparation method and application thereof - Google Patents
Rice bran oil fat powder and preparation method and application thereof Download PDFInfo
- Publication number
- CN111280310A CN111280310A CN202010176500.6A CN202010176500A CN111280310A CN 111280310 A CN111280310 A CN 111280310A CN 202010176500 A CN202010176500 A CN 202010176500A CN 111280310 A CN111280310 A CN 111280310A
- Authority
- CN
- China
- Prior art keywords
- rice bran
- oil
- bran oil
- fat powder
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000019774 Rice Bran oil Nutrition 0.000 title claims abstract description 97
- 239000008165 rice bran oil Substances 0.000 title claims abstract description 97
- 239000000843 powder Substances 0.000 title claims abstract description 52
- 238000002360 preparation method Methods 0.000 title abstract description 30
- 239000003921 oil Substances 0.000 claims abstract description 41
- 235000019198 oils Nutrition 0.000 claims abstract description 41
- 150000002148 esters Chemical class 0.000 claims abstract description 31
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 claims abstract description 24
- 241001465754 Metazoa Species 0.000 claims abstract description 21
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 17
- 150000003904 phospholipids Chemical class 0.000 claims abstract description 15
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 14
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 14
- 241000628997 Flos Species 0.000 claims abstract description 12
- 235000010265 sodium sulphite Nutrition 0.000 claims abstract description 12
- 238000002156 mixing Methods 0.000 claims description 34
- 238000011282 treatment Methods 0.000 claims description 26
- 238000000034 method Methods 0.000 claims description 19
- 235000007164 Oryza sativa Nutrition 0.000 claims description 13
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 13
- 238000004945 emulsification Methods 0.000 claims description 13
- 229930195729 fatty acid Natural products 0.000 claims description 13
- 239000000194 fatty acid Substances 0.000 claims description 13
- 235000009566 rice Nutrition 0.000 claims description 13
- 239000007790 solid phase Substances 0.000 claims description 12
- 235000012054 meals Nutrition 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 239000007921 spray Substances 0.000 claims description 9
- 239000000839 emulsion Substances 0.000 claims description 8
- 238000000265 homogenisation Methods 0.000 claims description 8
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims description 8
- GHVNFZFCNZKVNT-UHFFFAOYSA-N decanoic acid Chemical compound CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 7
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 6
- 230000001877 deodorizing effect Effects 0.000 claims description 6
- 239000012071 phase Substances 0.000 claims description 6
- BGNXCDMCOKJUMV-UHFFFAOYSA-N Tert-Butylhydroquinone Chemical compound CC(C)(C)C1=CC(O)=CC=C1O BGNXCDMCOKJUMV-UHFFFAOYSA-N 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 239000004250 tert-Butylhydroquinone Substances 0.000 claims description 5
- 235000019281 tert-butylhydroquinone Nutrition 0.000 claims description 5
- BVCOHOSEBKQIQD-UHFFFAOYSA-N 2-tert-butyl-6-methoxyphenol Chemical compound COC1=CC=CC(C(C)(C)C)=C1O BVCOHOSEBKQIQD-UHFFFAOYSA-N 0.000 claims description 4
- 229920001661 Chitosan Polymers 0.000 claims description 4
- 244000269722 Thea sinensis Species 0.000 claims description 4
- 238000004332 deodorization Methods 0.000 claims description 4
- 238000001179 sorption measurement Methods 0.000 claims description 4
- -1 sucrose fatty acid ester Chemical class 0.000 claims description 4
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 4
- 239000008158 vegetable oil Substances 0.000 claims description 4
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims description 3
- AZJQQNWSSLCLJN-UHFFFAOYSA-N 2-ethoxyquinoline Chemical compound C1=CC=CC2=NC(OCC)=CC=C21 AZJQQNWSSLCLJN-UHFFFAOYSA-N 0.000 claims description 3
- 244000060011 Cocos nucifera Species 0.000 claims description 3
- 235000013162 Cocos nucifera Nutrition 0.000 claims description 3
- 235000019482 Palm oil Nutrition 0.000 claims description 3
- 235000019779 Rapeseed Meal Nutrition 0.000 claims description 3
- 235000019484 Rapeseed oil Nutrition 0.000 claims description 3
- 229930006000 Sucrose Natural products 0.000 claims description 3
- 240000008042 Zea mays Species 0.000 claims description 3
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 claims description 3
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims description 3
- 239000004927 clay Substances 0.000 claims description 3
- 235000005822 corn Nutrition 0.000 claims description 3
- 235000012343 cottonseed oil Nutrition 0.000 claims description 3
- 238000004042 decolorization Methods 0.000 claims description 3
- 239000000787 lecithin Substances 0.000 claims description 3
- 229940067606 lecithin Drugs 0.000 claims description 3
- 235000010445 lecithin Nutrition 0.000 claims description 3
- 238000006386 neutralization reaction Methods 0.000 claims description 3
- 229960002446 octanoic acid Drugs 0.000 claims description 3
- 239000002540 palm oil Substances 0.000 claims description 3
- 239000000473 propyl gallate Substances 0.000 claims description 3
- 235000010388 propyl gallate Nutrition 0.000 claims description 3
- 229940075579 propyl gallate Drugs 0.000 claims description 3
- 239000004456 rapeseed meal Substances 0.000 claims description 3
- 229940080352 sodium stearoyl lactylate Drugs 0.000 claims description 3
- ODFAPIRLUPAQCQ-UHFFFAOYSA-M sodium stearoyl lactylate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC(=O)OC(C)C(=O)OC(C)C([O-])=O ODFAPIRLUPAQCQ-UHFFFAOYSA-M 0.000 claims description 3
- 235000012424 soybean oil Nutrition 0.000 claims description 3
- 239000003549 soybean oil Substances 0.000 claims description 3
- 238000005507 spraying Methods 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 239000005720 sucrose Substances 0.000 claims description 3
- KNENSDLFTGIERH-UHFFFAOYSA-N 2,2,4,4-tetramethyl-3-phenylpentan-3-ol Chemical compound CC(C)(C)C(O)(C(C)(C)C)C1=CC=CC=C1 KNENSDLFTGIERH-UHFFFAOYSA-N 0.000 claims description 2
- 239000005632 Capric acid (CAS 334-48-5) Substances 0.000 claims description 2
- 239000005635 Caprylic acid (CAS 124-07-2) Substances 0.000 claims description 2
- 229920002472 Starch Polymers 0.000 claims description 2
- 150000008442 polyphenolic compounds Chemical class 0.000 claims description 2
- 235000013824 polyphenols Nutrition 0.000 claims description 2
- 235000019698 starch Nutrition 0.000 claims description 2
- 239000008107 starch Substances 0.000 claims description 2
- 241000209094 Oryza Species 0.000 claims 8
- 235000013312 flour Nutrition 0.000 claims 1
- 235000013616 tea Nutrition 0.000 claims 1
- 235000016709 nutrition Nutrition 0.000 abstract description 9
- 230000035764 nutrition Effects 0.000 abstract description 8
- 235000019197 fats Nutrition 0.000 description 55
- 230000000052 comparative effect Effects 0.000 description 32
- 239000000463 material Substances 0.000 description 21
- 206010012735 Diarrhoea Diseases 0.000 description 14
- 235000006708 antioxidants Nutrition 0.000 description 11
- 150000004665 fatty acids Chemical class 0.000 description 10
- 238000010008 shearing Methods 0.000 description 10
- 230000000694 effects Effects 0.000 description 8
- 239000003094 microcapsule Substances 0.000 description 8
- 238000012545 processing Methods 0.000 description 8
- 230000002354 daily effect Effects 0.000 description 7
- 239000004519 grease Substances 0.000 description 7
- 239000002994 raw material Substances 0.000 description 7
- 239000002253 acid Substances 0.000 description 6
- 150000002978 peroxides Chemical class 0.000 description 6
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 6
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 6
- 102000004190 Enzymes Human genes 0.000 description 5
- 108090000790 Enzymes Proteins 0.000 description 5
- 240000007594 Oryza sativa Species 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 230000009471 action Effects 0.000 description 4
- 230000003712 anti-aging effect Effects 0.000 description 4
- 230000001804 emulsifying effect Effects 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 231100000331 toxic Toxicity 0.000 description 4
- 230000002588 toxic effect Effects 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 244000223014 Syzygium aromaticum Species 0.000 description 3
- 235000016639 Syzygium aromaticum Nutrition 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 210000003608 fece Anatomy 0.000 description 3
- 235000021050 feed intake Nutrition 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 235000021588 free fatty acids Nutrition 0.000 description 3
- 238000011056 performance test Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000003860 storage Methods 0.000 description 3
- 125000005457 triglyceride group Chemical group 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- 229930195730 Aflatoxin Natural products 0.000 description 2
- XWIYFDMXXLINPU-UHFFFAOYSA-N Aflatoxin G Chemical compound O=C1OCCC2=C1C(=O)OC1=C2C(OC)=CC2=C1C1C=COC1O2 XWIYFDMXXLINPU-UHFFFAOYSA-N 0.000 description 2
- 231100000678 Mycotoxin Toxicity 0.000 description 2
- 239000005409 aflatoxin Substances 0.000 description 2
- 235000021053 average weight gain Nutrition 0.000 description 2
- 238000009395 breeding Methods 0.000 description 2
- 230000001488 breeding effect Effects 0.000 description 2
- 239000003240 coconut oil Substances 0.000 description 2
- 235000019864 coconut oil Nutrition 0.000 description 2
- 230000009849 deactivation Effects 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000008157 edible vegetable oil Substances 0.000 description 2
- 230000003203 everyday effect Effects 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 230000002366 lipolytic effect Effects 0.000 description 2
- 244000144972 livestock Species 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002636 mycotoxin Substances 0.000 description 2
- 244000144977 poultry Species 0.000 description 2
- 230000008569 process Effects 0.000 description 2
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- 238000000926 separation method Methods 0.000 description 2
- 230000000087 stabilizing effect Effects 0.000 description 2
- 210000000130 stem cell Anatomy 0.000 description 2
- 238000005809 transesterification reaction Methods 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- 235000019786 weight gain Nutrition 0.000 description 2
- 230000004584 weight gain Effects 0.000 description 2
- YYGNTYWPHWGJRM-UHFFFAOYSA-N (6E,10E,14E,18E)-2,6,10,15,19,23-hexamethyltetracosa-2,6,10,14,18,22-hexaene Chemical compound CC(C)=CCCC(C)=CCCC(C)=CCCC=C(C)CCC=C(C)CCC=C(C)C YYGNTYWPHWGJRM-UHFFFAOYSA-N 0.000 description 1
- GYSCBCSGKXNZRH-UHFFFAOYSA-N 1-benzothiophene-2-carboxamide Chemical compound C1=CC=C2SC(C(=O)N)=CC2=C1 GYSCBCSGKXNZRH-UHFFFAOYSA-N 0.000 description 1
- GJJVAFUKOBZPCB-UHFFFAOYSA-N 2-methyl-2-(4,8,12-trimethyltrideca-3,7,11-trienyl)-3,4-dihydrochromen-6-ol Chemical compound OC1=CC=C2OC(CCC=C(C)CCC=C(C)CCC=C(C)C)(C)CCC2=C1 GJJVAFUKOBZPCB-UHFFFAOYSA-N 0.000 description 1
- 241001346334 Amomum tsao-ko Species 0.000 description 1
- 235000019737 Animal fat Nutrition 0.000 description 1
- 241000758794 Asarum Species 0.000 description 1
- 244000068645 Carya illinoensis Species 0.000 description 1
- 235000009025 Carya illinoensis Nutrition 0.000 description 1
- 244000223760 Cinnamomum zeylanicum Species 0.000 description 1
- 244000000626 Daucus carota Species 0.000 description 1
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- 244000303040 Glycyrrhiza glabra Species 0.000 description 1
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 description 1
- 240000006509 Gynostemma pentaphyllum Species 0.000 description 1
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- 235000017784 Mespilus germanica Nutrition 0.000 description 1
- 244000182216 Mimusops elengi Species 0.000 description 1
- 235000000560 Mimusops elengi Nutrition 0.000 description 1
- 244000178231 Rosmarinus officinalis Species 0.000 description 1
- 244000297179 Syringa vulgaris Species 0.000 description 1
- 235000004338 Syringa vulgaris Nutrition 0.000 description 1
- BHEOSNUKNHRBNM-UHFFFAOYSA-N Tetramethylsqualene Natural products CC(=C)C(C)CCC(=C)C(C)CCC(C)=CCCC=C(C)CCC(C)C(=C)CCC(C)C(C)=C BHEOSNUKNHRBNM-UHFFFAOYSA-N 0.000 description 1
- 235000007837 Vangueria infausta Nutrition 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 235000009754 Vitis X bourquina Nutrition 0.000 description 1
- 235000012333 Vitis X labruscana Nutrition 0.000 description 1
- 240000006365 Vitis vinifera Species 0.000 description 1
- 235000014787 Vitis vinifera Nutrition 0.000 description 1
- 210000001015 abdomen Anatomy 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- OBETXYAYXDNJHR-UHFFFAOYSA-N alpha-ethylcaproic acid Natural products CCCCC(CC)C(O)=O OBETXYAYXDNJHR-UHFFFAOYSA-N 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 235000017803 cinnamon Nutrition 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000006027 corn-soybean meal Substances 0.000 description 1
- 235000021316 daily nutritional intake Nutrition 0.000 description 1
- 235000019621 digestibility Nutrition 0.000 description 1
- 239000013070 direct material Substances 0.000 description 1
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N dodecahydrosqualene Natural products CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 1
- 235000004626 essential fatty acids Nutrition 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 230000002068 genetic effect Effects 0.000 description 1
- LPLVUJXQOOQHMX-QWBHMCJMSA-N glycyrrhizinic acid Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@@H]1C([C@H]2[C@]([C@@H]3[C@@]([C@@]4(CC[C@@]5(C)CC[C@@](C)(C[C@H]5C4=CC3=O)C(O)=O)C)(C)CC2)(C)CC1)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O LPLVUJXQOOQHMX-QWBHMCJMSA-N 0.000 description 1
- 239000008172 hydrogenated vegetable oil Substances 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 238000011221 initial treatment Methods 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 235000011477 liquorice Nutrition 0.000 description 1
- 210000001161 mammalian embryo Anatomy 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
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- 238000007670 refining Methods 0.000 description 1
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- 229940031439 squalene Drugs 0.000 description 1
- TUHBEKDERLKLEC-UHFFFAOYSA-N squalene Natural products CC(=CCCC(=CCCC(=CCCC=C(/C)CCC=C(/C)CC=C(C)C)C)C)C TUHBEKDERLKLEC-UHFFFAOYSA-N 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000009210 therapy by ultrasound Methods 0.000 description 1
- 229930003802 tocotrienol Natural products 0.000 description 1
- 239000011731 tocotrienol Substances 0.000 description 1
- 235000019148 tocotrienols Nutrition 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/158—Fatty acids; Fats; Products containing oils or fats
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
- A23K10/37—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/105—Aliphatic or alicyclic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/116—Heterocyclic compounds
- A23K20/132—Heterocyclic compounds containing only one nitrogen as hetero atom
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/163—Sugars; Polysaccharides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
- A23K20/22—Compounds of alkali metals
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K40/00—Shaping or working-up of animal feeding-stuffs
- A23K40/30—Shaping or working-up of animal feeding-stuffs by encapsulating; by coating
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/30—Feeding-stuffs specially adapted for particular animals for swines
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/60—Feeding-stuffs specially adapted for particular animals for weanlings
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3472—Compounds of undetermined constitution obtained from animals or plants
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
Abstract
The invention provides rice bran oil fat powder and a preparation method and application thereof, and the rice bran oil fat powder comprises the following components in parts by weight: 5-25 parts of structural ester; 24-50 parts of raw rice bran oil; 15-30 parts of phospholipid oil; 1-10 parts of an emulsifier; 4-10 parts of flos caryophyllata extract; 0.1-1 part of sodium sulfite; 1-7 parts of an antioxidant; 30-50 parts of a carrier. The rice bran oil fat powder provided by the invention utilizes the raw rice bran oil with lower cost, and is compounded with the structural ester for use, so that the fat powder provided by the invention can meet the fat nutrition requirement of an animal body, improve the growth performance of the animal, and improve the use value of the raw rice bran oil.
Description
Technical Field
The invention belongs to the technical field of animal feed, and relates to rice bran oil fat powder and a preparation method and application thereof.
Background
The grease is a main source of essential fatty acid in livestock and poultry breeding, is also a preferred additive for improving the energy concentration of feed, and has an important function in the livestock and poultry breeding. The oil and fat are very easily oxidized, so that the flavor and the product quality of the oil and fat are damaged. At present, the grease processing technology at home and abroad mainly adopts a grease hydrogenation technology or a grease powdering technology. The oil and fat powdering technology is to coat oil and fat with a coating wall material to prepare microencapsulated powder. The fat powder is powder prepared by taking refined hydrogenated vegetable oil and various food auxiliary materials as raw materials and performing blending, emulsification, sterilization and spray drying. The fat powder has good dispersibility, water solubility and stability.
The rice bran oil is obtained from rice cortex and embryo with most concentrated rice nutrition, and is rich in nutrition, and unsaturated fatty acid reaches 80%. The rice bran oil has balanced fatty acid composition, contains dozens of natural bioactive components such as vitamin E, compound lipid, phospholipid, tocotrienol, squalene, phytosterol (5%), oryzanol (0.5%) and the like, and has the content of unsaturated fatty acid of more than 80%. The rice bran oil has good use effect in the feed, but the rice bran oil has high acid value and is easy to deteriorate, and the rice bran oil is basically not applied at present. The raw rice bran oil, the raw coconut oil and the like are cheap and rich in domestic resources, but the food-grade oil has high refining cost, high threshold and high requirement, so that the production cost is extremely high, and the raw rice bran oil, the raw coconut oil and the like are not suitable for feed enterprises.
CN104997026A discloses a highly unsaturated fatty acid rice bran oil microcapsule and a preparation method thereof, wherein the raw materials comprise a material A, a material B, a microcapsule wall material and an emulsifier; the preparation method comprises the following steps: treating the material A to obtain a mixed material, spraying water to moisten the mixed material, and standing to obtain a first material; carrying out steam enzyme deactivation treatment on the first material to obtain a second material; carrying out primary treatment on the second material to obtain free oil 1, the second material and waste residues; putting the second material into second processing equipment, raising the temperature of the second processing equipment and the temperature of the content of the second processing equipment, preserving the heat, and performing centrifugal separation to obtain free oil 2; putting the free oil 1 and the free oil 2 into a third processing device, dewaxing, degumming, deacidifying and decoloring to obtain the highly unsaturated fatty acid rice bran oil; and then mixing and shearing the highly unsaturated fatty acid rice bran oil, the material B and the microcapsule, and drying to obtain the highly unsaturated fatty acid rice bran oil microcapsule. CN105124594A discloses a multi-nutrient anti-aging rice bran oil microcapsule and a preparation method thereof, wherein the raw materials comprise rice bran, tea seeds, grape seeds, pecan kernels, corn germs, carrots, tea leaves, rosemary, medlar, asarum, gynostemma pentaphylla, acanthopanax, amomum tsao-ko, liquorice, cortex acanthopanacis, cinnamon, microcapsule wall materials and an emulsifier; the preparation method comprises the following steps: the raw materials are subjected to raw material treatment and steam enzyme deactivation treatment and then are put into first processing equipment for ultrasonic treatment and enzymolysis to obtain free oil 1, a fourth material and waste residues; putting the fourth material into second processing equipment, heating, preserving heat and performing centrifugal separation to obtain free oil 2; then putting the free oil 1 and the free oil 2 into a third processing device, dewaxing, degumming, deacidifying and decoloring to obtain the multi-nutrient anti-aging rice bran oil; then mixing, shearing and drying the multi-nutrient anti-aging rice bran oil, the microcapsule wall material and the emulsifier to obtain multi-nutrient anti-aging rice bran oil microcapsules; the fat capsule provided by the patent application has the effects of eliminating free radicals of a human body and resisting aging, enriches the application of rice bran oil, but does not perform performance research on animal fat powder.
Therefore, it is desirable to provide a rice bran oil fat powder to meet the fat demand of animals, while reducing the cost of the fat powder for animals and enriching the application range of rice bran oil.
Disclosure of Invention
The invention aims to provide rice bran oil fat powder and a preparation method and application thereof. The rice bran oil fat powder provided by the invention utilizes the raw rice bran oil with lower cost, and is compounded with the structural ester for use, so that the fat powder provided by the invention can meet the fat nutrition requirement of an animal body, improve the growth performance of the animal, and improve the use value of the raw rice bran oil.
In order to achieve the purpose, the invention adopts the following technical scheme:
in a first aspect, the invention provides rice bran oil fat powder, which comprises the following components in parts by weight:
in the invention, the fatty acid which is lacked by the rice bran oil can be supplemented by matching the structural ester with the rice bran oil, so that the fatty acid is balanced to the maximum extent. Meanwhile, the clove extract can prevent feed from mildewing, reduce the toxic effect of mycotoxin on organisms, particularly the toxic effect of aflatoxin on stem cells, and effectively improve the storage period of the fat powder; furthermore, the addition of sodium sulfite can inhibit the activity of lipolytic enzyme in the rice bran oil, effectively prevent rancidity and play a role in stabilizing the rice bran oil fat powder.
Therefore, the rice bran oil fat powder provided by the invention can improve the use value of the rice bran oil, reduce the production cost of the rice bran oil and improve the storage stability of the fat powder by adjusting the proportion of each component; on the other hand, the fat nutrition requirement of animal organisms can be met, and the growth performance of animals is improved.
In the present invention, the structural ester is 5 to 25 parts, for example, 8 parts, 10 parts, 12 parts, 15 parts, 18 parts, 20 parts, 22 parts, etc.
In the present invention, the raw rice bran oil is 24-50 parts, such as 26 parts, 31 parts, 38 parts, 42 parts, 46 parts, 49 parts and the like.
In the present invention, the phospholipid oil is 15 to 30 parts, for example, 16 parts, 19 parts, 22 parts, 25 parts, 27 parts, 29 parts, etc.
In the present invention, the emulsifier is 1 to 10 parts, for example, 2 parts, 4 parts, 5 parts, 7 parts, 8 parts, 9 parts, etc.
In the present invention, the flos caryophylli extract is 4-10 parts, such as 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, etc.
In the present invention, the sodium sulfite is 0.1 to 1 part, for example, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.8 part, 0.9 part, etc.
In the present invention, the antioxidant is 1 to 7 parts, for example, 2 parts, 3 parts, 5 parts, etc.
In the present invention, the carrier is 30 to 50 parts, for example, 33 parts, 38 parts, 40 parts, 41 parts, 44 parts, 48 parts, etc.
In the invention, the preparation method of the structural ester comprises the following steps:
carrying out ester exchange reaction on vegetable oil, caprylic acid (C8:0) and capric acid (C10:0) to obtain the structured fat.
Preferably, the vegetable oil comprises any one of soybean oil, palm oil or rapeseed oil or a combination of at least two thereof.
The invention does not limit the specific reaction conditions of ester exchange, such as temperature, time and the like, and any ester exchange reaction which can achieve the purpose of the invention in the prior art can be adopted, such as the preparation method mentioned in the research on preparing MLM structured fat by using Yang hongli, Yang Tian Qu, muying.
The structural ester provided by the invention is MLM structural ester, the MLM structural ester is triglyceride with high digestibility, the Sn-2 position of the triglyceride is long-carbon-chain fatty acid (L), and the Sn-1 and 3 positions of the triglyceride are medium-carbon-chain fatty acid (M); the new structure lipid can exert physiological functions and nutritional values of various fatty acids to the maximum extent.
Preferably, the emulsifier is selected from any one of or a combination of at least two of refined lecithin, sucrose fatty acid ester, chitosan, sodium stearoyl lactylate or esterified porous starch.
Preferably, the antioxidant is selected from any one of Ethoxyquinoline (EQ), di-tert-Butylhydroxytoluene (BHT), tert-Butylhydroxyanisole (BHA), tert-butylhydroquinone (TBHQ), Propyl Gallate (PG), or tea polyphenol, or a combination of at least two thereof.
Preferably, the carrier comprises any one of rice bran meal, coconut meal, cottonseed meal, rapeseed meal or corn meal or a combination of at least two of the above.
In a second aspect, the present invention provides a method for producing rice bran oil fat powder according to the first aspect, wherein the method comprises the steps of:
(1) sequentially degumming, deacidifying, decolorizing and deodorizing the raw rice bran oil to obtain rice bran oil;
(2) dissolving and mixing rice bran oil and phospholipid oil to obtain an oil phase, performing first-stage homogenization treatment, then mixing with an emulsifier and an antioxidant, performing second-stage emulsification treatment, and finally adding a structural fat and a flos caryophylli extract, mixing and performing third-stage emulsification treatment to obtain an emulsion;
(3) mixing a carrier with sodium sulfite to obtain a solid phase;
(4) mixing the emulsion and the solid phase for adsorption to obtain the rice bran oil fat powder.
Preferably, the degumming method comprises mixing water with crude rice bran oil, and filtering; the water and the hydrophilic phospholipid in the raw rice bran oil are combined to form floccule and precipitate, and the floccule is separated from the oil to achieve the purpose of degumming.
Preferably, the deacidification method is acid-base neutralization, and free fatty acid is removed by acid-base neutralization.
Preferably, the decolorization method is to mix deacidified raw rice bran oil with clay, stir at 90-100 deg.C (e.g. 92 deg.C, 95 deg.C, 98 deg.C, etc.) for 20-30min (e.g. 22min, 25min, 28min, etc.), and then filter.
Preferably, the deodorization method is a method using steam stripping, the temperature is 190-200 ℃, such as 192 ℃, 195 ℃, 198 ℃ and the like, and the time is 120-130min, such as 122min, 124min, 125min, 126min, 128min and the like.
The invention adopts a special treatment process to treat the raw rice bran oil, and can solve the problems of high acid value and high free fatty acid; the treatment process of the raw rice bran oil needs to be carried out according to the sequence provided by the invention, otherwise, the technical effect of the invention cannot be achieved.
Preferably, the temperature of the dissolving and mixing is 40-70 ℃, such as 45 ℃, 50 ℃, 55 ℃, 60 ℃, 65 ℃ and the like.
Preferably, the pressure of the first stage homogenization treatment is 10-30MPa, such as 12MPa, 15MPa, 18MPa, 22MPa, 25MPa, 29MPa, etc., and the rotation speed is 1500-3000rpm, such as 1600rpm, 1900rpm, 2300rpm, 2700rpm, 2900rpm, etc.
Preferably, the pressure of the second stage emulsification treatment is 0.1-1.0MPa, such as 0.2MPa, 0.3MPa, 0.5MPa, 0.8MPa, 0.9MPa, etc., and the rotation speed is 5000-15000rpm, such as 6000rpm, 7000rpm, 9000rpm, 12000rpm, 13000rpm, 14000rpm, etc.
Preferably, the pressure of the third stage emulsification treatment is 10 to 50MPa, such as 14MPa, 19MPa, 23MPa, 28MPa, 31MPa, 40MPa, 47MPa and the like.
Preferably, the mixing is performed in a spray mixer.
Preferably, the pressure of the mixed adsorption is 5-20MPa, such as 7MPa, 8MPa, 9MPa, 12MPa, 15MPa, 18MPa and the like, and the spraying speed is 20L/min.
In a third aspect, the present invention provides use of the rice bran oil fat powder according to the first aspect in animal feed.
Preferably, the rice bran oil fat powder is added in an amount of 2.5 to 7.5%, for example, 3%, 4%, 5%, 6%, 7%, etc., in the animal feed.
Compared with the prior art, the invention has the following beneficial effects:
(1) the fatty acid lacking in the rice bran oil can be supplemented by matching the structural ester with the rice bran oil, so that the fatty acid is balanced to the maximum extent; meanwhile, the clove extract can prevent feed from mildewing, reduce the toxic effect of mycotoxin on organisms, particularly the toxic effect of aflatoxin on stem cells, and effectively improve the storage period of the fat powder; furthermore, the addition of sodium sulfite can inhibit the activity of the lipolytic enzyme in the rice bran oil, and play a role in stabilizing the rice bran oil fat powder;
(2) the rice bran oil fat powder provided by the invention is low in production cost, low in fatty acid value and peroxide value, capable of meeting the fat nutrition requirement of animal bodies and improving the growth performance of animals. Wherein the acid value is below 2mgKOH/g, the peroxide value is below 4mmol/kg, the cost is below 4000 yuan/ton, the weight gain of the piglets is above 11.9kg within 30 days, the average daily gain is above 0.673kg, the feed-meat ratio is below 1.28, and the probability of diarrhea of the piglets is extremely low.
Detailed Description
The technical solution of the present invention is further explained by the following embodiments. It should be understood by those skilled in the art that the examples are only for the understanding of the present invention and should not be construed as the specific limitations of the present invention.
Preparation example 1
A structural ester is prepared from soybean oil, octanoic acid (C8:0) and decanoic acid (C10:0) by transesterification, and is prepared by the following steps: chinese oil and fat for preparing MLM structural fat by enzyme catalysis transesterification, 2013,38(4):39-42.
Preparation example 2
The difference from preparation example 1 is that structural esters were prepared using palm oil.
Preparation example 3
The difference from preparation example 1 is that rapeseed oil is used to prepare structural esters.
Example 1
The rice bran oil fat powder comprises the following components in parts by weight:
wherein the structural ester is the structural ester provided in preparation example 1, the raw rice bran oil and the phospholipid oil are provided by grease Co., Ltd, the flos Caryophylli extract is provided by bioscience Co., Ltd, Xianchang Yue, the emulsifier is refined lecithin, the antioxidant is ethoxyquinoline, and the carrier is rice bran meal.
The preparation method comprises the following steps:
(1) sequentially treating raw rice bran oil to obtain rice bran oil, wherein the treatment method comprises the following steps:
mixing water and crude rice bran oil, filtering, degumming, and then adding sodium hydroxide to react with free fatty acid to perform deacidification treatment; mixing deacidified raw rice bran oil with clay, stirring at 90 deg.C for 30min for decolorizing, and filtering; and finally, removing the odor in the grease by using direct steam stripping, and deodorizing for 120min at the temperature of 190 ℃.
(2) Heating rice bran oil and phospholipid oil to 55 ℃ for dissolving and mixing to obtain an oil phase, then performing first-stage homogenization treatment at the pressure of 15MPa and the rotating speed of 2200rpm, and then performing high-speed shearing, homogenizing and emulsifying with an emulsifier and an antioxidant under the action of a high-speed shearing homogenizer at the pressure of 0.5MPa and the rotating speed of 10000 rpm; finally, adding the structure fat and the flos caryophylli extract to carry out high-pressure homogenizing emulsification in a high-pressure homogenizer under the pressure of 30 MPa;
(3) mixing a carrier with sodium sulfite to obtain a solid phase;
(4) mixing the emulsion with solid phase by spray mixer, and adsorbing under 5-20MPa at 20L/min to obtain rice bran oil fat powder.
Examples 2 to 3
The difference from preparation example 1 is that in this example, the structural ester provided in preparation example 1 was replaced with the structural esters provided in preparation examples 2 to 3.
Example 4
The rice bran oil fat powder comprises the following components in parts by weight:
wherein the structural ester is the structural ester provided in preparation example 1, the raw rice bran oil and the phospholipid oil are provided by grease Co Ltd in east of Hubei province, the flos Caryophylli extract is provided by bioscience Co., Ltd of Xianchang Yue, the emulsifier is sucrose fatty acid ester, the antioxidant is a combination of tert-butyl hydroxyanisole and tert-butyl hydroquinone in a mass ratio of 1:1, and the carrier is cottonseed meal.
The preparation method comprises the following steps:
(1) referring to example 1, raw rice bran oil was sequentially subjected to degumming, deacidification, decoloration, and deodorization to obtain rice bran oil;
(2) heating rice bran oil and phospholipid oil to 55 ℃ for dissolving and mixing to obtain an oil phase, then performing first-stage homogenization treatment at the pressure of 10MPa and the rotating speed of 1500rpm, and then performing high-speed shearing, homogenizing and emulsifying with an emulsifier and an antioxidant under the action of a high-speed shearing homogenizer at the pressure of 0.1MPa and the rotating speed of 5000 rpm; finally, adding the structure fat and the flos caryophylli extract to carry out high-pressure homogenizing emulsification in a high-pressure homogenizer under the pressure of 10 MPa;
(3) mixing a carrier with sodium sulfite to obtain a solid phase;
(4) mixing and adsorbing the emulsion with the solid phase by a spray mixer at a pressure of 5MPa and a spray speed of 20L/min to obtain the rice bran oil fat powder.
Example 5
The rice bran oil fat powder comprises the following components in parts by weight:
wherein the structural ester is the structural ester provided in preparation example 1, the raw rice bran oil and the phospholipid oil are provided by grease limited of east of Hubei province, the flos caryophyllata extract is provided by biotechnology limited of Xianchang Yue, the emulsifier is chitosan, the antioxidant is tert-butyl hydroxy anisole, and the carrier is rapeseed meal.
The preparation method comprises the following steps:
(1) sequentially carrying out dewaxing, degumming, decoloring, deodorizing and deacidifying treatment on the raw rice bran oil to obtain rice bran oil;
(2) heating rice bran oil and phospholipid oil to 55 ℃ for dissolving and mixing to obtain an oil phase, then carrying out first-stage homogenization treatment at the pressure of 30MPa and the rotating speed of 3000rpm, and then carrying out high-speed shearing, homogenizing and emulsifying with an emulsifier and an antioxidant under the action of a high-speed shearing homogenizer at the pressure of 1.0MPa and the rotating speed of 15000 rpm; finally, adding the structure fat and the flos caryophylli extract to carry out high-pressure homogenizing emulsification in a high-pressure homogenizer under the pressure of 50 MPa;
(3) mixing a carrier with sodium sulfite to obtain a solid phase;
(4) mixing and adsorbing the emulsion with the solid phase by a spray mixer at a pressure of 20MPa and a spray speed of 20L/min to obtain the rice bran oil fat powder.
Example 6
The rice bran oil fat powder comprises the following components in parts by weight:
wherein the structural ester is provided in preparation example 1, the raw rice bran oil and the phospholipid oil are provided by grease Co., Ltd, the flos Caryophylli extract is provided by bioscience Co., Ltd, Xianchang Yue, the emulsifier is a composition comprising chitosan and sodium stearoyl lactylate in a mass ratio of 1:2, the antioxidant is tert-butyl hydroquinone, and the carrier is coconut meal.
The preparation method comprises the following steps:
(1) sequentially carrying out dewaxing, degumming, decoloring, deodorizing and deacidifying treatment on the raw rice bran oil to obtain rice bran oil;
(2) heating rice bran oil and phospholipid oil to 55 ℃ for dissolving and mixing to obtain an oil phase, then carrying out first-stage homogenization treatment at the pressure of 17MPa and the rotating speed of 2000rpm, and then carrying out high-speed shearing, homogenizing and emulsifying with an emulsifier and an antioxidant under the action of a high-speed shearing homogenizer at the pressure of 0.3MPa and the rotating speed of 11000 rpm; finally, adding the structure fat and the flos caryophylli extract to carry out high-pressure homogenizing emulsification in a high-pressure homogenizer, wherein the pressure is 35 MPa;
(3) mixing a carrier with sodium sulfite to obtain a solid phase;
(4) mixing and adsorbing the emulsion with the solid phase by a spray mixer at a pressure of 18MPa and a spray speed of 20L/min to obtain the rice bran oil fat powder.
Comparative example 1
The difference from example 1 is that in this comparative example, no sodium sulfite was added.
Comparative example 2
The difference from example 1 is that in this comparative example, no lilac extract was added.
Comparative example 3
The difference from example 1 is that in this comparative example the structural ester provided in preparation example 1 was replaced by an OPO structural ester.
Comparative example 4
The difference from example 1 is that, in this comparative example, step (1) was not performed.
Comparative example 5
The difference from example 1 is that in this comparative example, the raw rice bran oil was treated by deacidification, decolorization, degumming and deodorization in this order.
Comparative example 6
The difference from example 1 is that in this comparative example, the raw rice bran oil was treated by decoloring, deacidifying, degumming and deodorizing in this order.
Comparative examples 7 to 8
The difference from example 1 is that in this comparative example, the addition amount of the structural ester was 1 part (comparative example 7) and 30 parts (comparative example 8).
Comparative examples 9 to 10
The difference from example 1 is that, in this comparative example, the addition amounts of raw rice bran oil were 20 parts (comparative example 9) and 60 parts (comparative example 10).
Comparative examples 11 to 12
The difference from example 1 is that in this comparative example, the addition amount of the phospholipid oil was 8 parts (comparative example 11) and 36 parts (comparative example 12).
And (3) performance testing:
the fat powders provided in examples 1 to 6 and comparative examples 1 to 12 were subjected to a performance test as follows:
(1) acid value: detecting according to an acid value detection method recorded in the Chinese food quality standard GB/T5009.37-2003 edible oil sanitary standard;
(2) peroxide number: detecting according to a peroxide value detection method recorded in the Chinese food quality standard GB/T5009.37-2003 edible oil sanitary standard;
(3) the product cost is as follows: the sum of direct materials (raw materials), labor costs and manufacturing costs;
(4) animal experiments: animal experiments were performed as follows;
experimental materials: 190 weaned piglets with 25 days old and similar genetic background and gestation times are randomly divided into 19 treatment groups, wherein 1-6 groups are used as an example group, and 7-19 groups are used as a comparative example group;
the feeding method comprises the following steps: the piglets of the example group and the comparative example group are fed at 8:00 am and 4:00 pm every day, are fed freely, are fed and drink freely, 5 percent of the fat powder provided by the examples 1-6 and the comparative examples 1-13 is added into the feed, and the basic ration is corn-soybean meal type ration; the test was performed for a total of 30 days.
Test items:
a) total average weight gain: weighing on empty stomach before feeding on the day of formal start as initial average weight, weighing on the 30 th sky belly in the formal period, and calculating average weight gain;
b) average daily gain: calculating Average Daily Gain (ADG) using "total average gain/day";
c) average daily food intake: calculating Average Daily Feed Intake (ADFI) using "feed intake/days";
d) the ratio of the materials to the meat is as follows: calculating the Feed Conversion Ratio (FCR) by using the average daily feed intake/average daily gain;
e) diarrhea condition: and (3) observing and recording the diarrhea condition of the piglets every day during the experiment, scoring the diarrhea, and counting the diarrhea rate of the piglets, wherein the diarrhea index of the piglets is as follows:
0 min-no diarrhea, normal shaping of feces, and water content less than 70%;
1 minute-mild diarrhea, soft feces, can be shaped, and has a water content of 70-75%;
2-moderate diarrhea, pasty and unformed, and the water content is 75-80%;
3 min-severe diarrhea, separating water sample and liquid dung, and leading the water content to be more than 80 percent;
the diarrhea rate is the number of diarrhea piglets/total number of experimental piglets multiplied by 100%;
diarrhea index is the sum of diarrhea index scores and/total number of experimental piglets;
the test results are shown in tables 1 and 2:
TABLE 1
According to the embodiment and the performance test, the rice bran oil fat powder provided by the invention is low in production cost, low in fatty acid value and low in peroxide value, can meet the fat nutrition requirement of an animal body, and improves the growth performance of animals; wherein the acid value is below 2mgKOH/g, the peroxide value is below 4mmol/kg, and the cost is below 4000 yuan/ton.
TABLE 2
According to the embodiment and the performance test, the rice bran oil fat powder provided by the invention can meet the fat nutrition requirement of animal organisms and improve the growth performance of animals; wherein the weight gain of the piglets is more than 11.9kg within 30 days, the average daily gain is more than 0.673kg, the feed-meat ratio is less than 1.28, and the probability of the piglets suffering from diarrhea is extremely low.
As can be seen from the comparison of example 1 and comparative examples 1-2, both the clove extract and sodium sulfite of the present invention are indispensable; as can be seen from the comparison between example 1 and comparative example 3, the structural ester provided by the present invention needs to be selected to have a good effect in the present invention; as can be seen from the comparison of example 1 with comparative examples 4 to 6, the preparation method of the present invention has the technical effect of optimizing the fat powder of the present invention; as is clear from comparison of example 1 and comparative examples 7 to 12, the amounts of the components of the present invention to be added need to be within the limits of the present invention in order to achieve the advantageous effects of the present invention.
The applicant states that the rice bran oil fat powder of the present invention and the preparation method and application thereof are illustrated by the above examples, but the present invention is not limited to the above detailed methods, i.e., it is not meant that the present invention must be implemented by the above detailed methods. It should be understood by those skilled in the art that any modification of the present invention, equivalent substitutions of the raw materials of the product of the present invention, addition of auxiliary components, selection of specific modes, etc., are within the scope and disclosure of the present invention.
Claims (10)
1. The rice bran oil fat powder is characterized by comprising the following components in parts by weight:
2. the rice oil fat powder of claim 1, wherein the method of making the structural ester comprises the steps of:
and carrying out ester exchange reaction on the vegetable oil, the caprylic acid and the capric acid to obtain the structural fat.
3. The rice oil fat powder of claim 2, wherein the vegetable oil comprises any one of soybean oil, palm oil, or rapeseed oil, or a combination of at least two thereof.
4. Rice oil fat powder according to any of claims 1-3, characterized in that the emulsifier is selected from any one or a combination of at least two of refined lecithin, sucrose fatty acid ester, chitosan, sodium stearoyl lactylate or esterified porous starch.
5. The rice oil fat powder according to any one of claims 1 to 4, wherein the antioxidant is selected from any one or a combination of at least two of ethoxyquinoline, di-tert-butylhydroxytoluene, tert-butylhydroxyanisole, tert-butylhydroquinone, propyl gallate, and tea polyphenols.
6. The rice oil fat powder according to any one of claims 1 to 5, wherein the carrier comprises any one of or a combination of at least two of rice bran meal, coconut meal, cottonseed meal, rapeseed meal, or corn meal.
7. A method of producing rice oil fat powder as claimed in any one of claims 1 to 6 comprising the steps of:
(1) sequentially degumming, deacidifying, decolorizing and deodorizing the raw rice bran oil to obtain rice bran oil;
(2) dissolving and mixing rice bran oil and phospholipid oil to obtain an oil phase, performing first-stage homogenization treatment, then mixing with an emulsifier and an antioxidant, performing second-stage emulsification treatment, and finally adding a structural fat and a flos caryophylli extract, mixing and performing third-stage emulsification treatment to obtain an emulsion;
(3) mixing a carrier with sodium sulfite to obtain a solid phase;
(4) mixing the emulsion and the solid phase for adsorption to obtain the rice bran oil fat powder.
8. The method of claim 7, wherein the degumming is carried out by mixing water with crude rice bran oil, filtering;
preferably, the deacidification method is acid-base neutralization;
preferably, the decolorization method comprises the steps of mixing deacidified raw rice bran oil with clay, stirring at 90-100 ℃ for 20-30min, and then filtering;
preferably, the deodorization method is a method utilizing steam stripping, the temperature is 190-.
9. The method of claim 7 or 8, wherein the temperature of the dissolving and mixing is 40-70 ℃;
preferably, the pressure of the first-stage homogenization treatment is 10-30MPa, and the rotating speed is 1500-3000 rpm;
preferably, the pressure of the second-stage emulsification treatment is 0.1-1.0MPa, and the rotating speed is 5000-;
preferably, the pressure of the third-stage emulsification treatment is 10-50 MPa;
preferably, the mixing is performed in a spray mixer;
preferably, the pressure of the mixed adsorption is 5-20MPa, and the spraying speed is 20L/min.
10. Use of rice oil fat flour according to any one of claims 1-6 in animal feed;
preferably, in the animal feed, the rice bran oil fat powder is added in an amount of 2.5 to 7.5%.
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| CN114223803A (en) * | 2021-12-28 | 2022-03-25 | 湖北优百特生物工程有限公司 | Fat powder for promoting weight gain of rejected laying hens and preparation method and application thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104839450A (en) * | 2015-04-15 | 2015-08-19 | 嘉兴学院南湖学院 | Extract and application thereof as feed additive |
| CN105076723A (en) * | 2015-08-27 | 2015-11-25 | 广州市优百特饲料科技有限公司 | Microencapsulation fatty powder feed additives and preparation method thereof |
| CN105831414A (en) * | 2016-04-26 | 2016-08-10 | 广州市优百特饲料科技有限公司 | High fat puffed soybean meal/cake feed raw material |
| CN108077586A (en) * | 2018-02-26 | 2018-05-29 | 山东省滨州畜牧兽医研究院 | It is a kind of suitable for emulsification equilibrium fat powder product of fur-bearing animal and preparation method thereof |
| CN109566876A (en) * | 2019-01-22 | 2019-04-05 | 广州市优百特饲料科技有限公司 | A kind of aquatic livestock fatty powder and its preparation method and application |
-
2020
- 2020-03-13 CN CN202010176500.6A patent/CN111280310A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104839450A (en) * | 2015-04-15 | 2015-08-19 | 嘉兴学院南湖学院 | Extract and application thereof as feed additive |
| CN105076723A (en) * | 2015-08-27 | 2015-11-25 | 广州市优百特饲料科技有限公司 | Microencapsulation fatty powder feed additives and preparation method thereof |
| CN105831414A (en) * | 2016-04-26 | 2016-08-10 | 广州市优百特饲料科技有限公司 | High fat puffed soybean meal/cake feed raw material |
| CN108077586A (en) * | 2018-02-26 | 2018-05-29 | 山东省滨州畜牧兽医研究院 | It is a kind of suitable for emulsification equilibrium fat powder product of fur-bearing animal and preparation method thereof |
| CN109566876A (en) * | 2019-01-22 | 2019-04-05 | 广州市优百特饲料科技有限公司 | A kind of aquatic livestock fatty powder and its preparation method and application |
Non-Patent Citations (1)
| Title |
|---|
| G.AZEEMODDIN等: "偏酸性亚硫酸钠对米糠的安定作用", 《中国油脂》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114223803A (en) * | 2021-12-28 | 2022-03-25 | 湖北优百特生物工程有限公司 | Fat powder for promoting weight gain of rejected laying hens and preparation method and application thereof |
| CN114223803B (en) * | 2021-12-28 | 2023-10-31 | 湖北优百特生物工程有限公司 | Fat powder for promoting fattening of obsolete laying hens and preparation method and application thereof |
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Application publication date: 20200616 |