CN111224639B - Resonant frequency self-adaptive control system based on two-dimensional heterogeneous thin film - Google Patents

Resonant frequency self-adaptive control system based on two-dimensional heterogeneous thin film Download PDF

Info

Publication number
CN111224639B
CN111224639B CN202010058523.7A CN202010058523A CN111224639B CN 111224639 B CN111224639 B CN 111224639B CN 202010058523 A CN202010058523 A CN 202010058523A CN 111224639 B CN111224639 B CN 111224639B
Authority
CN
China
Prior art keywords
dimensional heterogeneous
thin film
heterogeneous thin
dimensional
vibration
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN202010058523.7A
Other languages
Chinese (zh)
Other versions
CN111224639A (en
Inventor
王兴华
刘红卫
范光腾
覃江毅
冉德超
胡粲彬
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
National Defense Technology Innovation Institute PLA Academy of Military Science
Original Assignee
National Defense Technology Innovation Institute PLA Academy of Military Science
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by National Defense Technology Innovation Institute PLA Academy of Military Science filed Critical National Defense Technology Innovation Institute PLA Academy of Military Science
Priority to CN202010058523.7A priority Critical patent/CN111224639B/en
Publication of CN111224639A publication Critical patent/CN111224639A/en
Application granted granted Critical
Publication of CN111224639B publication Critical patent/CN111224639B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • HELECTRICITY
    • H03ELECTRONIC CIRCUITRY
    • H03HIMPEDANCE NETWORKS, e.g. RESONANT CIRCUITS; RESONATORS
    • H03H9/00Networks comprising electromechanical or electro-acoustic devices; Electromechanical resonators
    • H03H9/15Constructional features of resonators consisting of piezoelectric or electrostrictive material
    • H03H9/17Constructional features of resonators consisting of piezoelectric or electrostrictive material having a single resonator
    • H03H9/171Constructional features of resonators consisting of piezoelectric or electrostrictive material having a single resonator implemented with thin-film techniques, i.e. of the film bulk acoustic resonator [FBAR] type
    • HELECTRICITY
    • H03ELECTRONIC CIRCUITRY
    • H03HIMPEDANCE NETWORKS, e.g. RESONANT CIRCUITS; RESONATORS
    • H03H9/00Networks comprising electromechanical or electro-acoustic devices; Electromechanical resonators
    • H03H9/15Constructional features of resonators consisting of piezoelectric or electrostrictive material
    • H03H9/17Constructional features of resonators consisting of piezoelectric or electrostrictive material having a single resonator
    • H03H9/176Constructional features of resonators consisting of piezoelectric or electrostrictive material having a single resonator consisting of ceramic material

Landscapes

  • Physics & Mathematics (AREA)
  • Acoustics & Sound (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Optical Modulation, Optical Deflection, Nonlinear Optics, Optical Demodulation, Optical Logic Elements (AREA)

Abstract

The invention relates to a resonant frequency self-adaptive control system based on a two-dimensional heterogeneous film, which comprises the two-dimensional heterogeneous film, a supporting substrate, a piezoelectric ceramic driver, an external adjustable light source, a vibration detector and a signal conditioning circuit, wherein nano metal particles on the heterogeneous film can generate a plasma resonance effect, the two-dimensional heterogeneous film is arranged on the supporting substrate, the supporting substrate is fixedly connected with the piezoelectric ceramic driver, the external adjustable light source irradiates the two-dimensional heterogeneous film, the piezoelectric ceramic driver drives the two-dimensional heterogeneous film to vibrate, the vibration detector senses the vibration of the two-dimensional heterogeneous film and generates corresponding electric signals, and the signal conditioning circuit processes the electric signals generated by the vibration detector and converts the electric signals into driving control signals, so that the vibration control of the piezoelectric ceramic driver is realized. The invention has the characteristics of non-contact, large range and self-adaption, and can realize flexible regulation and control and high-precision detection.

Description

Resonant frequency self-adaptive control system based on two-dimensional heterogeneous thin film
Technical Field
The invention belongs to the technical field of micro-electro-mechanical control, and particularly relates to a resonant frequency self-adaptive control system based on a two-dimensional heterogeneous film.
Background
Adaptive adjustment of structural resonant frequency is a typical evolutionary mechanism, which is mainly manifested by sensing external environment, communicating with peers, or recognizing external risks, defending predators, and the like. The bat carries out echo positioning based on ultrasonic waves, and after potential prey is detected, the ultrasonic frequency of the bat is subjected to self-adaptive control according to the position information of the prey, so that accurate predation is realized; the moth thoracic cavity is provided with a drum membrane-like structure, the eardrum state is changed by regulating and controlling the pretension, a sensitive area of a moth auditory system can be adaptively adjusted from a low-frequency signal to a high frequency when facing a predator, and a defense mechanism for resisting the predator is made on the basis of the high-frequency signal; the blowholes of the dolphin will sound a "click" to track a prey or identify an obstacle, and through adaptive control of the forehead soft tissue structure, a signal of frequency variation is generated in a larger range for high-bandwidth detection.
The two-dimensional system nano-particles are widely concerned by researchers due to unique properties, and when two materials with different properties are self-assembled into a two-dimensional heterogeneous lattice structure, the two-dimensional system nano-particles often show unique optical, electrical, thermal, magnetic and other characteristics different from micro-particles and macro-substances, and simultaneously, the materials generate unique macro physical properties and functions. The nanoparticles can couple incident electromagnetic wave energy during plasmon resonance, show strong absorption and scattering enhancement effects, convert into heat energy through nonradiative transition with great efficiency, and obviously improve the temperature of the nanoparticles. Nanoparticles in heterogeneous nano-lattices efficiently absorb incident light and convert it to heat on a picosecond time scale through electron-electron, electron-phonon interactions. When incident light and nano-particle interact, the photo-thermal coupling effect in the resonant crystal lattice can be obviously enhanced, and generated heat is accumulated along with time and conducted to surrounding media, so that the thermal stress state in the nano-crystal lattice is changed, and the modal frequency of the resonator is further influenced.
The rigidity and mass deep coupling of the traditional resonator are difficult to independently regulate and control, and the problems of low efficiency, poor flexibility and the like exist at the same time.
Disclosure of Invention
Aiming at the problems, the invention aims to provide a resonant frequency adaptive control system with typical bionic adaptive control characteristics.
When incident light irradiates the heterogeneous composite resonance film, the photothermal coupling effect caused by metal (gold/silver) nanoparticle plasma resonance is remarkable, and the generated heat is transferred to a surrounding medium by taking the metal particles as the center and is gradually accumulated along with time to cause the macroscopic temperature of the film to change. The heterogeneous thin film has smaller equivalent mass and vibration rigidity, and the temperature fluctuation can generate obvious disturbance on the vibration characteristic of the thin film resonator, so that the change of the micro-scale key size or the change of the mechanical characteristic is caused, and the change of the resonance frequency of the heterogeneous composite thin film is caused.
When incident light parameters (such as light intensity and wavelength) are changed, the temperature and the stress of the resonant structure are changed, so that the resonant frequency is adapted and matched with environmental parameters, and the non-contact and large-range flexible regulation and control of the resonant frequency of the heterogeneous composite film can be realized in a non-contact manner.
In order to achieve the purpose, the invention adopts the following technical scheme:
the utility model provides a resonant frequency self-adaptation control system based on two-dimensional heterogeneous film, including two-dimensional heterogeneous film, supporting substrate, piezoceramics driver, outside adjustable light source, vibration detector and signal conditioning circuit, nanometer metal particle on the two-dimensional heterogeneous film can produce plasma resonance effect, two-dimensional heterogeneous film is unsettled to be arranged in on the supporting substrate, supporting substrate and piezoceramics driver realize fixed connection, outside adjustable light source shines two-dimensional heterogeneous film, piezoceramics driver drive two-dimensional heterogeneous film vibrates, the vibration of vibration detector perception two-dimensional heterogeneous film produces corresponding signal of telecommunication, signal conditioning circuit handles the signal of telecommunication that vibration detector generated and converts into drive control signal, thereby realize the vibration control to piezoceramics driver.
Preferably, the two-dimensional heterogeneous thin film is prepared based on a surface critical self-assembly process and is formed by connecting nano metal particles through organic polymer, and the structural form and the critical dimension of the metal nano particles can be selected.
Preferably, the support substrate is prepared on the basis of a silicon wafer, obtained by means of a dry etching or wet etching process.
Preferably, when the two-dimensional heterogeneous thin film is irradiated by an external adjustable light source, the wavelength and the intensity of incident light can be adjusted.
Preferably, the signal conditioning circuit comprises a phase-locked amplifying circuit, a filtering processing circuit and a phase adjusting circuit.
Preferably, the vibration detector is a doppler laser interferometer.
Due to the adoption of the technical scheme, the invention has the following advantages:
1. and (4) non-contact regulation. Compared with other modes, the light control has the remarkable characteristics of non-contact, flexible control and the like by changing the parameters of the far-field light source. The structural resonance frequency regulation has two important indexes, namely the frequency regulation range and the required energy.
2. And (4) regulating and controlling in a large range. The self-adaptive tuner needs to have a self-adaptive internal working mechanism, and flexible and large-range regulation and control of the natural frequency of the structure are realized. The size of the metal particles can be flexibly regulated and controlled, and the sensitive wavelength selection is realized. The structural form and the key size of the metal nano particles can obviously influence the position of a resonance peak of the two-dimensional heterogeneous film, and the optical absorption peak of the two-dimensional heterogeneous film can be regulated and controlled by reasonably selecting the metal particles and controlling a self-assembly mode.
3. And (4) self-adaptive control. The self-adaptive control technology based on the nano-particle system has wide application prospect in the civil field, and the research result plays an important role in the field of bionic self-adaptive control, thereby having important significance for improving the research level in the field of China.
4. Integrates perception and regulation. Can be used for flexible regulation and control and can also be used for high-sensitivity detection. The adjacent nodes of the two-dimensional heterogeneous film are linked through flexible polymer, the temperature changes rapidly when surface plasma resonance occurs, the difference of thermal expansion coefficients between materials and the parameters of the materials can change, and key parameters influencing the performance of the device are changed.
Drawings
FIG. 1 is a schematic view of an embodiment of the present invention;
fig. 2 is a working principle diagram of the present invention.
Detailed Description
The invention is described in detail below with reference to the figures and examples. In this embodiment, an adaptive control system includes a two-dimensional heterogeneous thin film, a piezoelectric ceramic driver, an external adjustable light source, a vibration detector, a signal conditioning circuit, and the like, where the two-dimensional heterogeneous thin film is prepared based on a surface self-assembly process, the light intensity and wavelength generated by the external adjustable light source can be flexibly adjusted and controlled, the vibration detector detects a vibration signal of a resonator based on a doppler effect, and the signal conditioning circuit includes functions of filtering, phase-locked amplification, phase adjustment, and the like. The components of the invention are shown in fig. 1, and the working principle is shown in fig. 2.
The two-dimensional heterogeneous thin film is suspended above the substrate, and the substrate is fixedly connected with the PZT piezoelectric ceramic piece.
The two-dimensional heterogeneous film is prepared based on a surface critical autonomous assembly process, the nano metal particles are connected through organic polymer and suspended on the substrate, and the structural form and the key size of the metal nano particles can be selected.
The supporting substrate is prepared on the basis of silicon wafers through dry etching or wet etching, and the suspended size is regulated and controlled according to the size requirement of the thin film.
The incident light is guided to the surface of the two-dimensional heterogeneous thin film resonator through a specific light path and the like, incident light parameters (wavelength and intensity) are the key for regulating and controlling the resonant frequency of the two-dimensional heterogeneous thin film resonator, and flexible regulation and control in a certain range can be realized by changing the parameters of the incident light.
The vibration detector can extract vibration signals (displacement and speed) within a certain frequency and range, and converts the vibration signals into electric signals for a subsequent signal conditioning circuit. The vibration detector adopts a Doppler laser interferometer to test the vibration characteristics of the two-dimensional heterogeneous thin film structure in time domain and frequency domain.
The signal conditioning circuit specifically comprises a phase-locked amplifying circuit, a filtering processing circuit and a phase adjusting circuit. The phase-locked amplifier can amplify the vibration signal, and the vibration signal is used as a driving signal to drive the piezoelectric resonator after filtering and phase change conditioning. Different resonance sensitivity peaks can be achieved by adjusting the size.
In this embodiment, the two-dimensional heterogeneous thin film is prepared based on a surface critical self-assembly process, such that a plurality of metal nanoparticle individuals are spontaneously associated and integrated to form a compact and ordered two-dimensional multi-particle mesostructure.
In the embodiment, the self-driving circuit and the closed-loop feedback circuit are designed, so that the two-dimensional heterogeneous film works in a closed-loop mode, and the dynamic characteristic of the system is obviously improved. When the environment changes, the closed-loop control makes the output frequency of the resonator correspondingly adjusted, and the structural vibration is always maintained in a resonance state; and the frequency meter monitors the frequency signal of the system to reflect the vibration information in real time.
The foregoing is merely a preferred embodiment of the invention and is not intended to limit the invention in any manner. Although the present invention has been described with reference to the preferred embodiments, it is not intended to be limited thereto. Those skilled in the art can make many possible variations and modifications to the disclosed embodiments, or equivalent modifications, without departing from the spirit and scope of the invention, using the methods and techniques disclosed above. Therefore, any simple modification, equivalent replacement, equivalent change and modification made to the above embodiments according to the technical essence of the present invention are still within the scope of the protection of the technical solution of the present invention.

Claims (6)

1. A resonant frequency self-adaptive control system based on a two-dimensional heterogeneous thin film is characterized by comprising a supporting substrate (1), the two-dimensional heterogeneous thin film (2), a piezoelectric ceramic driver (3), a vibration detector (4), a signal conditioning circuit and an external adjustable light source (8), wherein the two-dimensional heterogeneous thin film (2) is formed by connecting nano metal particles through a flexible organic polymer and is self-assembled into a two-dimensional heterogeneous lattice structure, the structural form and the size of the two-dimensional heterogeneous lattice structure formed by connecting the nano metal particles on the flexible organic polymer can obviously influence the position of a resonant peak of the two-dimensional heterogeneous thin film, the microstructure of the two-dimensional heterogeneous lattice structure can be changed under the influence of illumination, so that the resonant frequency of the two-dimensional heterogeneous thin film is changed, the two-dimensional heterogeneous thin film (2) is suspended on the supporting substrate (1), support substrate (1) and piezoceramics driver (3) and realize fixed connection, outside adjustable light source (8) shine two-dimentional heterogeneous membrane (2), piezoceramics driver (3) drive two-dimentional heterogeneous membrane (2) vibration, the vibration of vibration detector (4) perception two-dimentional heterogeneous membrane (2) produces corresponding signal of telecommunication, signal conditioning circuit handles the signal of telecommunication that vibration detector (4) generated and converts into drive control signal, thereby realize the vibration control to piezoceramics driver (3).
2. The adaptive control system for the resonant frequency based on the two-dimensional heterogeneous thin film according to claim 1 is characterized in that the two-dimensional heterogeneous thin film (2) is prepared based on a critical self-assembly process of a surface and is formed by connecting nano metal particles through organic polymer, and the structural form and the critical dimension of the metal nano particles can be selected.
3. The adaptive control system of resonant frequency based on two-dimensional heterogeneous thin film according to claim 2, characterized in that the support substrate (1) is prepared based on silicon wafer, obtained by dry etching or wet etching process.
4. The adaptive control system for resonant frequency based on two-dimensional heterogeneous thin film according to claim 3, characterized in that when the external tunable light source (8) irradiates the two-dimensional heterogeneous thin film (2), the wavelength and intensity of incident light can be adjusted.
5. The adaptive control system for the resonant frequency based on the two-dimensional heterogeneous thin film according to claim 4, wherein the signal conditioning circuit comprises a phase-locked amplifying circuit (5), a filtering processing circuit (6) and a phase adjusting circuit (7).
6. The adaptive control system for resonance frequency based on two-dimensional heterogeneous thin films according to claim 4, characterized in that the vibration detector (4) is a Doppler laser interferometer.
CN202010058523.7A 2020-01-19 2020-01-19 Resonant frequency self-adaptive control system based on two-dimensional heterogeneous thin film Expired - Fee Related CN111224639B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202010058523.7A CN111224639B (en) 2020-01-19 2020-01-19 Resonant frequency self-adaptive control system based on two-dimensional heterogeneous thin film

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202010058523.7A CN111224639B (en) 2020-01-19 2020-01-19 Resonant frequency self-adaptive control system based on two-dimensional heterogeneous thin film

Publications (2)

Publication Number Publication Date
CN111224639A CN111224639A (en) 2020-06-02
CN111224639B true CN111224639B (en) 2020-11-27

Family

ID=70828205

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202010058523.7A Expired - Fee Related CN111224639B (en) 2020-01-19 2020-01-19 Resonant frequency self-adaptive control system based on two-dimensional heterogeneous thin film

Country Status (1)

Country Link
CN (1) CN111224639B (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111811426B (en) * 2020-06-29 2021-07-30 中国人民解放军军事科学院国防科技创新研究院 Method and device for regulating and controlling micro-electromechanical system structure

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1606233A (en) * 2004-09-20 2005-04-13 南京大学 Bulk acoustic wave device composed of multilayer heterostructure and method for making same
CN102946236A (en) * 2012-10-22 2013-02-27 华中科技大学 Adjustable film bulk acoustic wave resonator and preparation method thereof
CN104124938A (en) * 2014-07-18 2014-10-29 天津大学 Resonator and resonant frequency regulate and control method thereof
KR20160028564A (en) * 2014-09-03 2016-03-14 한국광기술원 Plasmonic sensor with multilayer thin film and nano-structures
CN106949914A (en) * 2017-03-23 2017-07-14 山东大学 A kind of utilization local phasmon structure improves the method that photo-thermal excites micro-cantilever vibrational energy conversion efficiency
CN207300884U (en) * 2017-05-15 2018-05-01 安徽大学 Embedded nanogold array surface plasma resonance sensor substrate
CN108709629A (en) * 2018-06-25 2018-10-26 华南理工大学 Film square vibration detection control device and method based on laser displacement sensor
CN110231095A (en) * 2019-05-23 2019-09-13 武汉大学 A kind of phasmon surface acoustic wave resonance infrared sensor

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1959568A1 (en) * 2007-02-19 2008-08-20 Consejo Superior de Investigaciones Cientificas Thin-film bulk acoustic ware resonator and method for performing heterogeneous integration of the same with complementary-metal-oxide-semiconductor integrated circuit
KR100991563B1 (en) * 2008-06-30 2010-11-04 재단법인서울대학교산학협력재단 Surface plasmon resonance sensor chip, method for manufacturing the same, surface plasmon resonance sensor system, and method for detecting analyzed material with surface plasmon resonance sensor system
KR20100061603A (en) * 2008-11-29 2010-06-08 한국전자통신연구원 Nano-particles for detecting bio materials and biosensor by using the nano-particles
JP5222835B2 (en) * 2009-12-16 2013-06-26 日本電信電話株式会社 Qualitative quantitative analysis method and qualitative quantitative analysis system
US10291203B2 (en) * 2016-07-12 2019-05-14 Murata Manufacturing Co., Ltd. Piezoelectric MEMS resonator with a high quality factor
CN106525669B (en) * 2016-10-28 2018-10-26 山东理工大学 Light momentum excited nano beam nano-particle apparatus for measuring quality and method
CN107749433B (en) * 2017-08-30 2023-07-04 中国科学院上海技术物理研究所 Two-dimensional van der Waals heterojunction photoelectric detector and preparation method thereof

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1606233A (en) * 2004-09-20 2005-04-13 南京大学 Bulk acoustic wave device composed of multilayer heterostructure and method for making same
CN102946236A (en) * 2012-10-22 2013-02-27 华中科技大学 Adjustable film bulk acoustic wave resonator and preparation method thereof
CN104124938A (en) * 2014-07-18 2014-10-29 天津大学 Resonator and resonant frequency regulate and control method thereof
KR20160028564A (en) * 2014-09-03 2016-03-14 한국광기술원 Plasmonic sensor with multilayer thin film and nano-structures
CN106949914A (en) * 2017-03-23 2017-07-14 山东大学 A kind of utilization local phasmon structure improves the method that photo-thermal excites micro-cantilever vibrational energy conversion efficiency
CN207300884U (en) * 2017-05-15 2018-05-01 安徽大学 Embedded nanogold array surface plasma resonance sensor substrate
CN108709629A (en) * 2018-06-25 2018-10-26 华南理工大学 Film square vibration detection control device and method based on laser displacement sensor
CN110231095A (en) * 2019-05-23 2019-09-13 武汉大学 A kind of phasmon surface acoustic wave resonance infrared sensor

Also Published As

Publication number Publication date
CN111224639A (en) 2020-06-02

Similar Documents

Publication Publication Date Title
Choi et al. A brief review of sound energy harvesting
US5569968A (en) Microfabricated acoustic source and receiver
CN111224639B (en) Resonant frequency self-adaptive control system based on two-dimensional heterogeneous thin film
US7292740B1 (en) Apparatus and method for controlling transmission through a photonic band gap crystal
CN107132210B (en) A kind of substrate manufacturing method of the surface-enhanced Raman based on dynamic control
Khan et al. Contributed Review: Recent developments in acoustic energy harvesting for autonomous wireless sensor nodes applications
CN113514179B (en) Force field gradient measuring device and method based on double-vibrator suspension optomechanics system
Peng et al. Enhanced acoustoelectric coupling in acoustic energy harvester using dual helmholtz resonators
KR20180019415A (en) Acoustic energy harvester using meta-materials
CN104501842A (en) Optical sensing device and optical sensing method based on micro-electromechanical system
Cui et al. Piezoelectric nanofiber/polymer composite membrane for noise harvesting and active acoustic wave detection
Reger et al. Aluminum nitride piezoelectric microphones as zero-power passive acoustic filters
Yuan et al. Integrated acoustic metamaterial triboelectric nanogenerator for joint low-frequency acoustic insulation and energy harvesting
Karanja et al. Femtosecond laser ablated FBG multitrenches for magnetic field sensor application
Lee et al. Vibroacoustic Characteristics of a Specific Patterned Polymer with Graphene for an Electrostatic Speaker
Wang et al. An adaptive soft plasmonic nanosheet resonator
Zhang et al. Control of vortex-induced non-resonance vibration using piezo-ceramic actuators embedded in a structure
CN112727876B (en) Controllable-strength adhesion device and control method thereof
CN1023873C (en) Resonance tracking system of sound suspending device
Gieva et al. Analyses of energy harvesting methods and devices for use in transport noise harvesting
CN109225788B (en) High-efficiency broadband air-medium ultrasonic transducer with double-phonon crystal composite structure
CN110790217A (en) Micro-electro-mechanical system infrared detector and manufacturing method thereof
Aksyuk et al. Plasmonic Nano-Electro-Mechanical Systems: from Local Motion Sensing to Powering Mechanical Oscillation
Wang et al. Ultra-sensitive photon sensor based on self-assembled nanoparticle plasmonic membrane resonator
Fan et al. MEMS piezoelectric bionic directional sound sensor based on ZnO thin film

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20201127

CF01 Termination of patent right due to non-payment of annual fee