CN111084814A - Weishu capsule and preparation method thereof - Google Patents
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/66—Papaveraceae (Poppy family), e.g. bloodroot
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A—HUMAN NECESSITIES
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- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/56—Materials from animals other than mammals
- A61K35/57—Birds; Materials from birds, e.g. eggs, feathers, egg white, egg yolk or endothelium corneum gigeriae galli
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
- A61K36/233—Bupleurum
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
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- A61K36/54—Lauraceae (Laurel family), e.g. cinnamon or sassafras
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- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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Abstract
The invention discloses a Weishu capsule and a preparation method thereof. The Weishu capsule comprises the following components in parts by weight: 20-30 parts of vinegar rhizoma corydalis, 5-10 parts of endothelium corneum gigeriae galli, 10-20 parts of radix bupleuri, 10-20 parts of cinnamon, 5-10 parts of dried alum and 10-20 parts of fried egg shell. The preparation method comprises the following steps: step 1, weighing each component; step 2, mixing dried alum and fried egg shells, and crushing into fine powder A; step 3, mixing the vinegar-processed rhizoma corydalis and the radix bupleuri, performing reflux extraction by using 30% ethanol, filtering an extracting solution, recovering the ethanol, and concentrating a solution A for later use; and 4, mixing the vinegar rhizoma corydalis residue, the radix bupleuri residue, the cinnamon and the endothelium corneum gigeriae galli, adding water for decoction, filtering decoction, combining the decoction with the concentrated solution A, concentrating into thick paste, drying, crushing into fine powder, mixing with the fine powder A, granulating, drying, and encapsulating to obtain the traditional Chinese medicine composition. The capsule has good effect of treating chronic gastritis, low cost and good application prospect.
Description
Technical Field
The invention relates to the technical field of stomach-soothing capsules, in particular to a stomach-soothing capsule and a preparation method thereof.
Background
With the development of society, the pace of life of people is faster and faster, and especially, workers in cities are hurried to go to work in a hurry early every day, fast food is ordered at places where people go to work at noon, and irregular eating habits cause that most people have chronic gastritis.
The symptoms of chronic gastritis manifest as a certain number: (1) the pain symptoms are: epigastric pain is one of the main symptoms, and can be dull pain, distending pain, dull pain, burning pain, stabbing pain, hunger pain, food pain and the like, and according to statistics, the epigastric pain accounts for 87.9 percent of patients, wherein dull pain is the most common pain. (2) Heartburn, acid regurgitation, upset discomfort symptoms: heartburn with or without pantothenic acid is a symptom of burning sensation in the gastric cavity, which is manifested as gastric discomfort, dull sensation and abnormal pain. (3) Belching symptom: belching can be continuous, frequent and intermittent, and the attack is 80.4% after eating or emotional stimulation. (4) Dry mouth and bitter taste symptoms: it is dry and thirst, but the bitter taste is obvious in morning and accounts for 50%. (5) Symptoms in the stool: both loose stool and constipation occur, with loose stool being the most common, accounting for 17.8%, and patients with gastric diseases having rough stool, with the characteristic of dyspepsia, and a few patients with thin stools such as water, who may have an attack even with careless diet. (6) Symptoms of sleep disorders: it is manifested as difficulty in falling asleep, dreaminess, easy waking up or no fatigue after waking up, etc., and insomnia is a common complication of chronic gastritis. (7) Emotional symptoms: it is known that the state of illness changes with emotional changes, such as pessimism, boredom, irritability, anxiety and anxiety.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides a stomach-soothing capsule and a preparation method thereof.
A Weishu capsule comprises the following components in parts by weight: 20-30 parts of vinegar rhizoma corydalis, 5-10 parts of endothelium corneum gigeriae galli, 10-20 parts of radix bupleuri, 10-20 parts of cinnamon, 5-10 parts of dried alum and 10-20 parts of fried egg shell.
The improvement is that the stomach soothing capsule comprises the following components in parts by weight: 25 parts of vinegar rhizoma corydalis, 8 parts of endothelium corneum gigeriae galli, 14 parts of radix bupleuri, 15 parts of cinnamon, 8 parts of dried alum and 16 parts of fried egg shell.
Rhizoma corydalis (Corydalis yanhusuoW.T. Wang ex Z.Y. Su et C.Y. Wu), rhizoma corydalis, etc. Is a perennial herb of the family Papaveraceae, the genus corydalis, with a tuber spherical and petal purplish red, and a capsule cylindrical with two gradually narrowed ends. And blossoming in summer. Tuber is a famous common traditional Chinese medicine, contains more than 20 alkaloids, and is used for promoting qi circulation, relieving pain, promoting blood circulation, removing blood stasis, traumatic injury and the like.
Endothelium corneum Gigeriae Galli is the inner wall (muscular stomach) of dry gizzard of domestic chicken (Gallus garlus domesticus Brisson) belonging to Phasianidae of phylum of chordata. Produced all over the country. After killing the chicken, the gizzard is taken out, the inner wall of the gizzard is immediately taken down, cleaned, dried in the sun, unprocessed or fried for use.
Bupleurum chinense DC or Bupleurum scorzonerifolium Willd dried root of Bupleurum scorzonerifolium of Umbelliferae. The root of this herb is thin and conical, the top of which has many hairy dead leaves, and the lower part of which has no branches or a little branches. The surface is reddish brown or dark brown, and the part near the root has fine ring veins. Soft, easy to break, flat in cross section and not showing fiber. The oil gas is lost.
Cinnamon (the Latin scientific name: Cinnamomum cassia Presl), also called Yugui, Japanese cinnamon, caju, Cinnamomum cassia, and Chinese cinnamon, is the dry bark of Cinnamomum cassia of Lauraceae. The bark is aromatic and can be used as a spice, with a flavor similar to that of cinnamon produced from cinnamon of the srilanka type, but more pungent, less delicious than cinnamon and thicker than cinnamon. In North America, cinnamon powder is indiscriminately sold together with cinnamon from cinnamon of China.
The cinnamon bark is peeled from the stems and branches, laid aside to dry, and rolled into rolls. Some varieties are scraped. The scraped ones were thin and bright reddish brown, and the non-scraped ones were thick and grey. The cinnamon powder is light reddish brown. Cinnamon produced in China has a slightly weaker flavor than those produced in Vietnam and Indonesia, and all the cinnamon, the Vietnam and the Indonesia have fragrance, sweet and spicy taste. Immature fruits of chinese cinnamon and Japanese cinnamon (c. laureiri) are attached to hard, crinkled, grayish-brown cupped calyx, generally 11 mm long (0.4 inch including calyx cylinder), 6 mm (0.25 inch) in diameter at the top, and removed with the calyx cylinder and dried, and called cinnamon bud. Has cinnamon-like fragrance and sweet and spicy taste of cinnamon bark, and can be used for flavoring food.
Dried alum, also known as calcined alum, is prepared by collecting cleaned alum, heating and melting in a casserole, calcining to dry, taking out, and obtaining irregular crystals with different sizes, colorless, transparent or semitransparent, smooth or uneven surface, fine longitudinal edges and glass-like luster. Hard and crisp, easy to break, slight smell, slightly sweet and astringent taste, white, transparent, hard and crisp, free of impurities, easily soluble in water or glycerol, insoluble in alcohol, and water solution showing various reactions of aluminum salt, potassium salt and sulfate to produce Gansu, Anhui, Shanxi, Hubei, Zhejiang and other places.
The egg shell of a chicken egg laid by Gallus gallotus Brisson, a phasianidae animal. Collecting eggshells, and drying in the sun. The egg shell can relieve hyperacidity and pain, and can be ground into powder for external use to stop bleeding, astringe and astringe. The eggshell powder can be used for treating gastric ulcer, acid regurgitation, gastritis and pain, and is beneficial for calcium supplement.
The preparation method of the Weishu capsule comprises the following steps: step 1, weighing each component; step 2, mixing dried alum and fried egg shells, and crushing into fine powder A; step 3, mixing the vinegar-processed rhizoma corydalis and the radix bupleuri, performing reflux extraction by using 30% ethanol, filtering an extracting solution, recovering the ethanol, and concentrating a solution A for later use; and 4, mixing the vinegar rhizoma corydalis residue, the radix bupleuri residue, the cinnamon and the endothelium corneum gigeriae galli, adding water for decoction, filtering decoction, combining the decoction with the concentrated solution A, concentrating into thick paste, drying, crushing into fine powder, mixing with the fine powder A, granulating, drying, and encapsulating to obtain the traditional Chinese medicine composition.
Has the advantages that:
compared with the prior art, the stomach soothing capsule and the preparation method thereof have the following advantages: the components are natural, and the obtained Weishu capsule has good effect and low cost; has little side effect after long-term use. In addition, the components are treated step by step, so that the drug effect is improved while the amount is reduced, and the application prospect is good.
Drawings
FIG. 1 is a flow chart of the preparation of a Weishu capsule according to the present invention;
FIG. 2 is a system suitability test chromatogram;
FIG. 3 is a chromatogram of a control of rhizoma corydalis processed with vinegar;
FIG. 4 is a chromatogram of a sample of a medicinal material, rhizoma corydalis processed with vinegar.
Detailed Description
The invention is further described with reference to specific examples.
Example 1
A Weishu capsule comprises the following components in parts by weight: 20 parts of vinegar corydalis tuber, 5 parts of chicken's gizzard-membrane, 10 parts of radix bupleuri, 10 parts of cinnamon, 5 parts of dried alum and 10 parts of fried egg shell.
The preparation method of the Weishu capsule comprises the following steps: step 1, weighing each component; step 2, mixing dried alum and fried egg shells, and crushing into fine powder A; step 3, mixing the vinegar-processed rhizoma corydalis and the radix bupleuri, performing reflux extraction by using 30% ethanol, filtering an extracting solution, recovering the ethanol, and concentrating a solution A for later use; and 4, mixing the vinegar rhizoma corydalis residue, the radix bupleuri residue, the cinnamon and the endothelium corneum gigeriae galli, adding water for decoction, filtering decoction, combining the decoction with the concentrated solution A, concentrating into thick paste, drying, crushing into fine powder, mixing with the fine powder A, granulating, drying, and encapsulating to obtain the traditional Chinese medicine composition.
Measuring the content of rhizoma corydalis processed with vinegar in the obtained Weishu capsule,
chromatographic conditions and system applicability test: octadecylsilane chemically bonded silica is used as a filling agent; methanol-0.4% phosphoric acid solution (50: 50) as mobile phase; the detection wavelength was 348 nm. The number of theoretical plates is not less than 2500 calculated according to tetrahydropalmatine peak.
Preparation of control solutions: precisely weighing appropriate amount of tetrahydropalmatine control substance dried under reduced pressure for 12 hr, and adding 30% methanol to obtain control substance mixed solution containing 10 μ g and 20 μ g per 1 ml.
Preparation of a test solution: taking 20 granules of the product, taking about 2g, precisely weighing, placing in a conical flask with a plug, precisely adding 50ml of 30% methanol, sealing the plug, weighing, ultrasonically extracting for 30 minutes, cooling, weighing again, supplementing the lost weight with 30% methanol, shaking up, filtering, precisely weighing 25 ml of subsequent filtrate, adding 5 ml of hydrochloric acid, shaking up, placing in a water bath at 80-90 ℃ for refluxing for 0.5 hour, taking out, rapidly cooling, quantitatively transferring to a 50ml measuring flask, adding 80% methanol for diluting to a scale, and shaking up to obtain the product.
Precisely sucking 20 μ l of each of the reference solution and the sample solution, injecting into liquid chromatograph, and measuring.
According to detection, each tablet of the product contains no less than 0.1mg of rhizoma corydalis processed with vinegar based on tetrahydropalmatine.
Example 2
A Weishu capsule comprises the following components in parts by weight: 25 parts of vinegar rhizoma corydalis, 8 parts of endothelium corneum gigeriae galli, 14 parts of radix bupleuri, 15 parts of cinnamon, 8 parts of dried alum and 16 parts of fried egg shell.
The preparation method of the Weishu capsule comprises the following steps: step 1, weighing each component; step 2, mixing dried alum and fried egg shells, and crushing into fine powder A; step 3, mixing the vinegar-processed rhizoma corydalis and the radix bupleuri, performing reflux extraction by using 30% ethanol, filtering an extracting solution, recovering the ethanol, and concentrating a solution A for later use; and 4, mixing the vinegar rhizoma corydalis residue, the radix bupleuri residue, the cinnamon and the endothelium corneum gigeriae galli, adding water for decoction, filtering decoction, combining the decoction with the concentrated solution A, concentrating into thick paste, drying, crushing into fine powder, mixing with the fine powder A, granulating, drying, and encapsulating to obtain the traditional Chinese medicine composition.
Example 3
A Weishu capsule comprises the following components in parts by weight: 30 parts of rhizoma corydalis processed with vinegar, 10 parts of endothelium corneum gigeriae galli, 20 parts of radix bupleuri, 20 parts of cinnamon, 10 parts of dried alum and 20 parts of fried egg shells.
The preparation method of the Weishu capsule comprises the following steps: step 1, weighing each component; step 2, mixing dried alum and fried egg shells, and crushing into fine powder A; step 3, mixing the vinegar-processed rhizoma corydalis and the radix bupleuri, performing reflux extraction by using 30% ethanol, filtering an extracting solution, recovering the ethanol, and concentrating a solution A for later use; and 4, mixing the vinegar rhizoma corydalis residue, the radix bupleuri residue, the cinnamon and the endothelium corneum gigeriae galli, adding water for decoction, filtering decoction, combining the decoction with the concentrated solution A, concentrating into thick paste, drying, crushing into fine powder, mixing with the fine powder A, granulating, drying, and encapsulating to obtain the traditional Chinese medicine composition.
The capsules of examples 1-3 above were selected for efficacy assessment criteria:
the effect is shown: disappearance of symptoms; improvement: relief of symptoms; and (4) invalidation: the standard of improvement can not be achieved, and the symptoms are not relieved.
The results of the treatment (see table 1).
TABLE 1 therapeutic effect observation statistics table
Through 100 clinical observations, the dampness eliminating patch of the invention has the following results: 58 cases of remarkable effect (15 cases of male 35-45 years old, 20 cases of female, 10 cases of male 45-60 years old, 13 cases of female), 40 cases of improvement (10 cases of male 35-45 years old, 10 cases of female, 12 cases of male 45-60 years old, 8 cases of female), and 2 cases of no effect (2 cases of male 40-55 years old); the significant efficiency is 58%, the good conversion rate is 40%, and the total effective rate is 98%.
The above description is only a preferred embodiment of the present invention, and the scope of the present invention is not limited thereto, and any simple modifications or equivalent substitutions of the technical solutions that can be obviously obtained by those skilled in the art within the technical scope of the present invention are within the scope of the present invention.
Claims (3)
1. The stomach soothing capsule is characterized by comprising the following components in parts by weight: 20-30 parts of vinegar rhizoma corydalis, 5-10 parts of endothelium corneum gigeriae galli, 10-20 parts of radix bupleuri, 10-20 parts of cinnamon, 5-10 parts of dried alum and 10-20 parts of fried egg shell.
2. The weishu capsule according to claim 1, which comprises the following components in parts by weight: 25 parts of vinegar rhizoma corydalis, 8 parts of endothelium corneum gigeriae galli, 14 parts of radix bupleuri, 15 parts of cinnamon, 8 parts of dried alum and 16 parts of fried egg shell.
3. The method for preparing the Weishu capsule according to claim 1: the method is characterized by comprising the following steps of 1, weighing all components; step 2, mixing dried alum and fried egg shells, and crushing into fine powder A; step 3, mixing the vinegar-processed rhizoma corydalis and the radix bupleuri, performing reflux extraction by using 30% ethanol, filtering an extracting solution, recovering the ethanol, and concentrating a solution A for later use; and 4, mixing the vinegar rhizoma corydalis residue, the radix bupleuri residue, the cinnamon and the endothelium corneum gigeriae galli, adding water for decoction, filtering decoction, combining the decoction with the concentrated solution A, concentrating into thick paste, drying, crushing into fine powder, mixing with the fine powder A, granulating, drying, and encapsulating to obtain the traditional Chinese medicine composition.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101485754A (en) * | 2009-02-18 | 2009-07-22 | 孙保臣 | Medicament for treating gastropathy and preparation method |
| CN101721523A (en) * | 2008-10-29 | 2010-06-09 | 刘海松 | Medicine for treating gastropathy |
| CN109045116A (en) * | 2018-09-11 | 2018-12-21 | 江苏七0七天然制药有限公司 | A kind of Weiyang-an capsule and preparation method thereof |
-
2019
- 2019-12-16 CN CN201911291720.7A patent/CN111084814A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101721523A (en) * | 2008-10-29 | 2010-06-09 | 刘海松 | Medicine for treating gastropathy |
| CN101485754A (en) * | 2009-02-18 | 2009-07-22 | 孙保臣 | Medicament for treating gastropathy and preparation method |
| CN109045116A (en) * | 2018-09-11 | 2018-12-21 | 江苏七0七天然制药有限公司 | A kind of Weiyang-an capsule and preparation method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 吉林省药品检验所革命委员会编: "《吉林省常见中药手册》", 31 December 1969 * |
| 屠美编著: "《药用高分子材料及其应用》", 30 November 2006, 华南理工大学出版社 * |
| 赵守训主编: "《中药辞海 第3卷》", 31 October 1997, 中国医药科技出版社 * |
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