CN111057486A - Special adhesive for advertisements and preparation method thereof - Google Patents

Special adhesive for advertisements and preparation method thereof Download PDF

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Publication number
CN111057486A
CN111057486A CN201811233079.7A CN201811233079A CN111057486A CN 111057486 A CN111057486 A CN 111057486A CN 201811233079 A CN201811233079 A CN 201811233079A CN 111057486 A CN111057486 A CN 111057486A
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CN
China
Prior art keywords
colloid
parts
resin
stirring
turning
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811233079.7A
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Chinese (zh)
Inventor
朱呈利
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shandong Qichen New Building Materials Co ltd
Original Assignee
Shandong Qichen New Building Materials Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shandong Qichen New Building Materials Co ltd filed Critical Shandong Qichen New Building Materials Co ltd
Priority to CN201811233079.7A priority Critical patent/CN111057486A/en
Publication of CN111057486A publication Critical patent/CN111057486A/en
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J109/00—Adhesives based on homopolymers or copolymers of conjugated diene hydrocarbons
    • C09J109/06—Copolymers with styrene
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02—Non-macromolecular additives
    • C09J11/04—Non-macromolecular additives inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J157/00—Adhesives based on unspecified polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C09J157/02—Copolymers of mineral oil hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J191/00—Adhesives based on oils, fats or waxes; Adhesives based on derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J201/00—Adhesives based on unspecified macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Adhesives Or Adhesive Processes (AREA)

Abstract

The invention relates to the technical field of adhesives, in particular to an adhesive special for advertisements and a preparation method thereof, which comprises the following steps: (1) feeding: sequentially adding tackifying resin ga1100 and No. 0C 5 resin into a reaction kettle, then injecting cyclohexane and solvent oil, starting a motor to stir, after 30 minutes, adding thermoplastic styrene butadiene rubber after the tackifying resin ga1100 and No. 0C 5 resin are dissolved, and continuously stirring for 3 hours until colloid is completely dissolved; (2) and compounding: opening circulating cooling water of a machine, cooling the colloid obtained in the step (1) to below 30 ℃, opening a vacuum device, evacuating to-0.8 MPA, turning off the vacuum device, sucking silicon dioxide into a kettle, starting stirring, stirring at a constant speed for 30 minutes until the colloid is completely and uniformly mixed until the colloid is transparent, and turning off a stirring motor; (3) and (6) packaging. The invention has the beneficial effects that: the product has high solid content, good initial adhesion, less volatile matter and high environmental protection coefficient.

Description

Special adhesive for advertisements and preparation method thereof
Technical Field
The invention relates to the technical field of adhesives, in particular to an adhesive special for advertisements and a preparation method thereof.
Background
KT board bonding mode commonly used on the market at present is mostly double faced adhesive tape and glass and glues, adopts the double faced adhesive tape alone and meets under the higher environment of large tracts of land bonding and temperature, falls easily, and adopts the glass again to glue alone and can not play quick fixed effect, must assist the double faced adhesive tape and use. Therefore, the use is very inconvenient, the construction difficulty and the construction cost are increased, and a lot of glue of the quick-drying type has strong corrosion effect on the KT plate, so that the damage to the plate is caused.
Disclosure of Invention
In order to solve the problems in the prior art, the invention provides the special advertisement adhesive with good initial adhesion, less volatile matters and high environmental protection coefficient and the preparation method thereof.
The technical scheme of the invention is as follows:
the special adhesive for the advertisement comprises the following components, by weight, 20 parts of styrene butadiene rubber, 110020 parts of tackifying resin ga, 10 parts of hydrophobic silica, 20 parts of No. 0C 5 resin, 10 parts of cyclohexane and 20 parts of solvent oil.
A preparation method of a special adhesive for advertisements comprises the following specific steps:
(1) feeding the materials
Sequentially adding tackifying resin ga1100 and No. 0C 5 resin into a reaction kettle, then injecting cyclohexane and solvent oil, starting a motor to stir, after 30 minutes, adding thermoplastic styrene butadiene rubber after the tackifying resin ga1100 and No. 0C 5 resin are dissolved, and continuously stirring for 3 hours until colloid is completely dissolved;
(2) and compounding
Opening circulating cooling water of a machine, cooling the colloid obtained in the step (1) to below 30 ℃, opening a vacuum device, evacuating to-0.8 MPA, turning off the vacuum device, sucking silicon dioxide into a kettle, starting stirring, stirring at a constant speed for 30 minutes until the colloid is completely and uniformly mixed until the colloid is transparent, and turning off a stirring motor;
(3) package (I)
And (3) sleeving a 200-liter barrel into a 200-liter inner film, placing the inner film in a reaction kettle, placing the material into a discharging port, hermetically packaging, and then independently packaging and storing a 300-milliliter aluminum film paper tube by a material pressing machine.
The technical scheme provided by the invention has the beneficial effects that:
the product has high solid content, good initial adhesion, less volatile matter and high environmental protection coefficient, completely meets and is higher than the national standard, and is an ideal bonding product of KT board, UV board, polystyrene board and other materials.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, embodiments of the present invention will be described in further detail with reference to specific examples.
Example one
The special adhesive for the advertisement comprises the following components, by weight, 20 parts of styrene butadiene rubber, 110020 parts of tackifying resin ga, 10 parts of hydrophobic silica, 20 parts of No. 0C 5 resin, 10 parts of cyclohexane and 20 parts of solvent oil.
A preparation method of a special adhesive for advertisements comprises the following specific steps:
(1) feeding the materials
Sequentially adding tackifying resin ga1100 and No. 0C 5 resin into a reaction kettle, then injecting cyclohexane and solvent oil, starting a motor to stir, after 30 minutes, adding thermoplastic styrene butadiene rubber after the tackifying resin ga1100 and No. 0C 5 resin are dissolved, and continuously stirring for 3 hours until colloid is completely dissolved;
(2) and compounding
Opening circulating cooling water of a machine, cooling the colloid obtained in the step (1) to below 30 ℃, opening a vacuum device, evacuating to-0.8 MPA, turning off the vacuum device, sucking silicon dioxide into a kettle, starting stirring, stirring at a constant speed for 30 minutes until the colloid is completely and uniformly mixed until the colloid is transparent, and turning off a stirring motor;
(3) package (I)
And (3) sleeving a 200-liter barrel into a 200-liter inner film, placing the inner film in a reaction kettle, placing the material into a discharging port, hermetically packaging, and then independently packaging and storing a 300-milliliter aluminum film paper tube by a material pressing machine.
Example a test result for an adhesive is as follows:
Figure BSA0000172445370000021
the above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.

Claims (2)

1. The special adhesive for the advertisement is characterized by comprising the following raw materials in parts by weight: 20 parts of styrene butadiene rubber, 110020 parts of tackifying resin ga, 10 parts of hydrophobic silica, 20 parts of No. 0C 5 resin, 10 parts of cyclohexane and 20 parts of solvent oil.
2. A method for preparing the special adhesive for advertisement as claimed in claim 1, characterized in that: the method comprises the following specific steps:
(1) feeding the materials
Sequentially adding tackifying resin ga1100 and No. 0C 5 resin into a reaction kettle, then injecting cyclohexane and solvent oil, starting a motor to stir, after 30 minutes, adding thermoplastic styrene butadiene rubber after the tackifying resin ga1100 and No. 0C 5 resin are dissolved, and continuously stirring for 3 hours until colloid is completely dissolved;
(2) and compounding
Opening circulating cooling water of a machine, cooling the colloid obtained in the step (1) to below 30 ℃, opening a vacuum device, evacuating to-0.8 MPA, turning off the vacuum device, sucking silicon dioxide into a kettle, starting stirring, stirring at a constant speed for 30 minutes until the colloid is completely and uniformly mixed until the colloid is transparent, and turning off a stirring motor;
(3) package (I)
And (3) sleeving a 200-liter barrel into a 200-liter inner film, placing the inner film in a reaction kettle, placing the material into a discharging port, hermetically packaging, and then independently packaging and storing a 300-milliliter aluminum film paper tube by a material pressing machine.
CN201811233079.7A 2018-10-16 2018-10-16 Special adhesive for advertisements and preparation method thereof Pending CN111057486A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811233079.7A CN111057486A (en) 2018-10-16 2018-10-16 Special adhesive for advertisements and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811233079.7A CN111057486A (en) 2018-10-16 2018-10-16 Special adhesive for advertisements and preparation method thereof

Publications (1)

Publication Number Publication Date
CN111057486A true CN111057486A (en) 2020-04-24

Family

ID=70297200

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201811233079.7A Pending CN111057486A (en) 2018-10-16 2018-10-16 Special adhesive for advertisements and preparation method thereof

Country Status (1)

Country Link
CN (1) CN111057486A (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1337435A (en) * 2000-08-03 2002-02-27 李云山 Adhesive
CN1456626A (en) * 2002-05-10 2003-11-19 王增启 Solvent style quick drying universal adhesive without benzene and its preparation
JP2008127450A (en) * 2006-11-20 2008-06-05 Sunstar Engineering Inc One-pack type adhesive composition for precoat
CN102775938A (en) * 2011-05-11 2012-11-14 深圳市顾康力化工有限公司 Environment-friendly solvent universal glue and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1337435A (en) * 2000-08-03 2002-02-27 李云山 Adhesive
CN1456626A (en) * 2002-05-10 2003-11-19 王增启 Solvent style quick drying universal adhesive without benzene and its preparation
JP2008127450A (en) * 2006-11-20 2008-06-05 Sunstar Engineering Inc One-pack type adhesive composition for precoat
CN102775938A (en) * 2011-05-11 2012-11-14 深圳市顾康力化工有限公司 Environment-friendly solvent universal glue and preparation method thereof

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SE01 Entry into force of request for substantive examination
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Application publication date: 20200424