CN111040900B - Camellia oil scrub facial soap and preparation method thereof - Google Patents

Camellia oil scrub facial soap and preparation method thereof Download PDF

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Publication number
CN111040900B
CN111040900B CN201911181061.1A CN201911181061A CN111040900B CN 111040900 B CN111040900 B CN 111040900B CN 201911181061 A CN201911181061 A CN 201911181061A CN 111040900 B CN111040900 B CN 111040900B
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oil
camellia
parts
essential oil
soap
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CN111040900A (en
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杨旸
盛占武
郑丽丽
郑晓燕
校导
艾斌凌
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Haikou Experimental Station of Chinese Academy of Tropical Agricultural Sciences
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Haikou Experimental Station of Chinese Academy of Tropical Agricultural Sciences
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/38—Products in which the composition is not well defined
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/005—Synthetic soaps
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
    • C11D9/442—Perfumes

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention belongs to the technical field of face cleaning products, and particularly relates to camellia oil polishing face cleaning soap and a preparation method thereof. The invention discloses camellia oil scrub facial soap which comprises, by weight, 500 parts of grease 400, 12-18 parts of alkali metal hydroxide, 25-35 parts of camellia seed shell micro powder, 1-5 parts of plant essential oil and 38-50 parts of water. The camellia seed husk micro powder used in the invention has smooth surface and no sharp edges and corners after being ground by a ball mill, and the minimum size can reach 100nm, so that the camellia seed husk micro powder can effectively clean skin dirt on the premise of not causing mechanical damage to the skin, and can effectively improve the problems of black heads and white heads after being used for 6 weeks. The camellia oil used in the invention is rich in unsaturated fatty acid, squalene, tea polyphenol and the like, and has good skin care effect. The camellia oil and camellia oil seed shells are fully utilized, the preparation process is simple, mild and non-irritant, the safety is high, the camellia oil seed shells are suitable for sensitive people, and meanwhile, the economic benefit of camellia oil by-products can be improved.

Description

Camellia oil scrub facial soap and preparation method thereof
Technical Field
The invention belongs to the technical field of face cleaning products, and particularly relates to camellia oil polishing face cleaning soap and a preparation method thereof.
Background
Cleansing of facial skin may refer to cleansing of the superficial skin, which is a function that is realized by common cleansing products, and also to cleansing of the deep skin, which is a deep cleansing of the skin and adjustment of the skin texture. The abrasive materials in some of the currently available abrasive cleansing products are generally inexpensive plastic particles that provide some removal of skin keratin materials by physical abrasion. However, because the plastic is hard in texture and inconsistent in surface flatness, mechanical damage can be caused to the skin when force is improperly applied in use, the sensitivity and the inflammation of the skin are increased, and certain limitations exist.
In addition, in the preparation process of the scrub cleansing product, cheap fatty acid is often used as grease, so that a certain burden is caused on the skin after long-term use, and the sensitivity and the sensitization of the skin are increased.
The scrub facial cleanser disclosed in CN106983680A adopts traditional Chinese medicine collagen particles as abrasive, which is a collagen solution prepared from collagen, chitosan and glacial acetic acid, and various traditional Chinese medicine extracts are added into the prepared collagen solution, and the scrub facial cleanser is vacuum-dried, sprayed, solidified and molded to obtain traditional Chinese medicine collagen fibers, and then pulverized to obtain traditional Chinese medicine collagen particles. Because the abrasive contains various traditional Chinese medicine extracts, the application range of the skin is limited, and the collagen particles have certain solubility, the sanding and cleaning effects are limited.
Disclosure of Invention
In order to solve the technical problems, the first aspect of the invention provides camellia oil scrub facial soap which comprises, by weight, 500 parts of grease 400-19 parts, 12-18 parts of alkali metal hydroxide, 25-35 parts of camellia seed shell micro powder, 1-5 parts of plant essential oil and 38-50 parts of water.
As a preferable technical scheme, the grease comprises at least one of camellia oil, olive oil, avocado oil, palm oil and coconut oil.
As a preferable technical scheme, the weight of the coconut oil accounts for 0-20% of the total weight of the grease.
In a preferable technical scheme, the weight of the palm oil accounts for 0-30% of the total weight of the grease.
As a preferable technical scheme, the total weight of the coconut oil and the palm oil accounts for 0-30% of the total weight of the grease.
As a preferable technical scheme, the weight ratio of the camellia oil, the olive oil, the avocado oil and the palm oil to the coconut oil is (3-6): 1: 1: 1: (0-2).
As a preferred embodiment, the alkali metal hydroxide is sodium hydroxide.
As a preferable technical scheme, the preparation method of the camellia seed shell micro powder comprises the following steps: ball milling the camellia seed shells by using a ball mill for 2-8 hours at the rotation speed of 500-1200r/min to obtain the camellia seed shells.
As a preferable technical solution, the plant essential oil is at least one selected from the group consisting of peppermint essential oil, lavender essential oil, chamomile essential oil, tea tree essential oil, cypress essential oil, patchouli essential oil, rose essential oil, eucalyptus essential oil, thyme essential oil, sandalwood essential oil, rosemary oil, lemon oil, clove oil, cinnamon oil, basil oil, chamomile oil, caraway oil, coriander oil, tarragon oil, wormwood oil, hyssop oil, sage oil, chrysanthemum indicum oil, pine needle oil, and frankincense oil.
The second aspect of the invention provides a preparation method of the camellia oil scrub facial soap, which comprises the following steps:
(1) heating oil at 38-45 deg.C;
(2) adding alkali metal hydroxide into water to prepare a solution, dropwise adding the solution into the grease obtained in the step (1), and stirring and reacting at 35-45 ℃ for 1-4 hours to obtain a thick soap solution;
(3) sequentially adding camellia seed shell micro powder and plant essential oil into the thick soap liquid obtained in the step (2), and uniformly stirring;
(4) and (4) pouring the product obtained in the step (3) into a mold, standing for 46-50 hours at room temperature, then demolding, and saponifying for 10-14 weeks at room temperature to obtain the product.
Has the advantages that: the camellia oil and camellia oil seed shells are fully utilized, the preparation process is simple, the safety is high, the camellia oil seed shells are suitable for sensitive people, and meanwhile, the economic benefit of camellia oil byproducts can be improved. Meanwhile, the camellia oil used in the facial soap disclosed by the invention is rich in antioxidant components, is mild, has no stimulation and high safety, and camellia seed shells are ground by a ball mill to be smooth in surface and free of sharp edges and corners, and the minimum size can reach 100nm, so that the facial soap can effectively clean skin dirt on the premise of not causing mechanical damage to the skin, and can effectively improve the problems of blackheads and whiteheads after being used for 6 weeks.
Detailed Description
For purposes of the following detailed description, it is to be understood that the invention may assume various alternative variations and step sequences, except where expressly specified to the contrary. Moreover, other than in any operating examples, or where otherwise indicated, all numbers expressing, for example, quantities of ingredients used in the specification and claims are to be understood as being modified in all instances by the term "about". Accordingly, unless indicated to the contrary, the numerical parameters set forth in the following specification and attached claims are approximations that may vary depending upon the desired properties to be obtained by the present invention. At the very least, and not as an attempt to limit the application of the doctrine of equivalents to the scope of the claims, each numerical parameter should at least be construed in light of the number of reported significant digits and by applying ordinary rounding techniques.
Notwithstanding that the numerical ranges and parameters setting forth the broad scope of the invention are approximations, the numerical values set forth in the specific examples are reported as precisely as possible. Any numerical value, however, inherently contains certain errors necessarily resulting from the standard deviation found in their respective testing measurements.
When a range of values is disclosed herein, the range is considered to be continuous and includes both the minimum and maximum values of the range, as well as each value between such minimum and maximum values. Further, when a range refers to an integer, each integer between the minimum and maximum values of the range is included. Further, when multiple range-describing features or characteristics are provided, the ranges may be combined. In other words, unless otherwise indicated, all ranges disclosed herein are to be understood to encompass any and all subranges subsumed therein. For example, a stated range from "1 to 10" should be considered to include any and all subranges between the minimum value of 1 and the maximum value of 10. Exemplary subranges of the range 1 to 10 include, but are not limited to, 1 to 6.1, 3.5 to 7.8, 5.5 to 10, and the like.
In order to solve the problems, the invention provides camellia oil scrub facial soap which comprises, by weight, 400-500 parts of grease, 10-18 parts of alkali metal hydroxide, 25-35 parts of camellia seed shell micro powder, 1-5 parts of plant essential oil and 38-50 parts of water.
As a preferred embodiment, the camellia oil scrub facial soap is prepared from 450 parts by weight of grease, 15.1 parts by weight of alkali metal hydroxide, 30 parts by weight of camellia seed shell micro powder, 2 parts by weight of plant essential oil and 45 parts by weight of water.
Oil and fat
As a preferred embodiment, the oil comprises at least one of camellia oil, olive oil, shea butter, palm oil, and coconut oil.
As a preferred embodiment, the weight ratio of the camellia oil, the olive oil, the shea butter and the palm oil is (3-6): 1: 1: 1: (0-2).
Preferably, the weight ratio of the camellia oil, the olive oil, the avocado oil and the palm oil is 6: 1: 1: 1: 2.
in a preferred embodiment, the coconut oil accounts for 0-20% of the total weight of the grease.
In a preferred embodiment, the palm oil is present in an amount of 0 to 30% by weight based on the total weight of the fat.
In a more preferred embodiment, the palm oil is present in an amount of 8-15% by weight based on the total weight of the fat.
Preferably, the total weight of the coconut oil and the palm oil accounts for 0-35% of the total weight of the grease.
More preferably, the total weight of the coconut oil and the palm oil accounts for 0-30% of the total weight of the grease.
More preferably, the total weight of the coconut oil and the palm oil accounts for 10-30% of the total weight of the grease.
The oil and fat may also comprise cacao butter, Plukenetia volubilis oil, shea butter, and jojoba oil.
The Camellia oil is fatty oil obtained by squeezing mature seeds of Camellia oleifera Camellia oleifera Abel or Camellia oleifera Camellia meiocarpa Hu.
The camellia oil is a light yellow clear liquid, contains rich unsaturated fatty acid, squalene and tea polyphenol, has strong capacity of removing free radicals, and can play a certain role in resisting oxidation and preserving moisture when being used in cosmetics.
The olive oil has CAS number 8001-25-0.
The avocado oil is fatty oil obtained by squeezing avocado (scientific name: Butyrum mumparkii Kotschy) kernels.
The shea butter is also called shea butter and deciduous tree, the height is 10-15 m, and the diameter at breast is 1-1.5 m; the tree crown is developed, branches are many and dense, stems and branches are thick, and multiple knots are often bent; the bark was thick, irregular and cracked, milky. The leaves are long and round, the tips are round or blunt, the bases are round or blunt, the upper surface of the young; the petiole is round. The flower stalks are rusted and soft; the calyx cleft pieces are in a needle shape, and the outside is coated with hair; the flower has sweet taste, and the flower crown is split into oval and full-edged. Berry is spherical, has a diameter of 3-4 cm, and is edible and tastes like persimmon; the seeds are oval, yellow brown, glossy, laterally grown and long round. The flowering period is 6 months, and the fruit period is 10 months.
The CAS number of the palm oil is 8002-75-3.
The CAS number of the coconut oil is 8001-31-8.
The applicant finds that by adding a certain proportion of compounded oil and plant essential oil for mutual cooperation, the scrub facial soap which is mild, non-irritant, high in safety and strong in cleaning capacity is obtained. Wherein said olive oil has the effect of smoothing and tenderizing the skin and increasing its elasticity; but also can accelerate the metabolism of epidermal cells and keep the skin young for a longer time; flattening the skin micro-folds; the avocado oil supplements abundant protein and vitamins for skin, plays a role in nourishing and tendering skin, can accelerate the regeneration and metabolism of skin cells, can improve the activity of the skin cells, delays skin aging and reduces the generation of wrinkles.
Moreover, the applicant has found that the skin is damaged by using too much coconut oil, and the skin is not easy to foam and has poor cleaning capability by using too much palm oil. The weight ratio of the camellia oil, the olive oil, the avocado oil and the palm oil is (3-6): 1: 1: 1: (0-2), the synergistic effect can be well played, the better play function of each other is promoted, and the effect that 1+1 is greater than 2 is achieved. This is probably because: the active ingredients in the facial soap can increase the hydration of skin tissues and the fluidity of stratum corneum lipid ingredients, and meanwhile, the acting force between the substance tissues is weaker due to a certain proportion, so that the substance tissues are easier to absorb by the skin; moreover, the avocado oil can form a protective layer on the surface layer of the skin, so that the water loss is prevented, and the moisturizing function of the skin is effectively improved. The fatty acids with various carbon chain lengths cooperate to achieve good cleaning capability after saponification.
Alkali metal hydroxides
As a preferred embodiment, the alkali metal hydroxide is sodium hydroxide.
Mountain tea seed shell micro powder
The camellia seed hulls are also called camellia seeds, and contain tea saponin, camellia seed polysaccharide, camellia seed protein, lignin, cellulose and the like.
The cleaning and skin-care effects of the facial soap are further improved by adding the camellia seed shell micro powder. The reason may be that the camellia seed shells contain tea saponin, which is a natural nonionic surfactant and is a glycoside compound with good functions of emulsification, dispersion, foaming, wetting and the like; in addition, the tea saponin also has the functions of scavenging free radicals, inhibiting bacteria and calming; cellulose and lignin contained in the camellia seed shell micro powder are insoluble in water, and can form microsphere particles with smooth surfaces after being ground by a planetary ball mill, the surfaces of the microsphere particles are smooth, sharp edges and corners do not exist, mechanical damage to skin can not be caused, and skin aging cutin can be removed mildly through physical friction. Meanwhile, the cellulose in the camellia oil seed shell micro powder can absorb redundant oil in the skin, so that the effects of removing aged horny layer of the skin and cleaning the skin are achieved.
The preparation method of the camellia seed shell micro powder comprises the following steps: ball milling the camellia seed shells by using a ball mill for 2-8 hours at the rotation speed of 500-1200r/min to obtain the camellia seed shells.
Preferably, the preparation method of the camellia seed husk micropowder comprises the following steps: ball milling the camellia seed shells for 5-8 hours by using a ball mill at the rotating speed of 900r/min to obtain the camellia seed shells.
Plant essential oil
The plant essential oil is at least one selected from peppermint essential oil, lavender essential oil, chamomile essential oil, tea tree essential oil, cypress essential oil, patchouli essential oil, rose essential oil, eucalyptus essential oil, thyme essential oil, sandalwood essential oil, rosemary oil, lemon oil, clove oil, cinnamon oil, basil oil, chamomile oil, caraway oil, coriander oil, tarragon oil, wormwood oil, hyssop oil, sage oil, wild chrysanthemum oil, pine needle oil and mastic oil.
As a preferred embodiment, the plant essential oil is a mint essential oil.
The mint essential oil is a component extracted from mint by water distillation or subcritical low-temperature extraction. The herba Menthae is dried aerial part of Mentha haphallocalyxBriq.
The main chemical components in the mint essential oil are alcohol, ketone, ester, terpene and terpene compounds, and the content and the properties of the compounds can be changed to a certain extent according to the variety, the collection part, the collection time and the production place of the mint. The oil content in the mint new leaves is about 0.8-1%, and the volatile oil content in the dry stems and leaves is about 1.3-2%. The mint volatile oil mainly comprises: l-menthone (menthone) with a content of about 77-87% and L-menthol (menthol) with a content of about 10%. Further, it contains pulegone (pulegone), neomint (neomenthone), menthyl acetate (menthyl acetate), camphene (camphene), pinene (pinene), limonene (limonene), menthenone (menthenone), methyl benzoate (methylbenzoate), decyl acetate (decyl acetate), 3-pentanol (3-pentol), β -thujene (β -thujene), 3-octanol (3-octanol), 2-hexene (2-hexanol), d-myrcene (myrcene), cineol (cineole), carvone (carvone), α -terpineol (α -terpineol) and the like.
The non-volatile components of the mint mainly comprise: amino acids, flavonoids, organic acids, fatty acids, and the like. In addition, ursolic acid, various inorganic elements, various vitamins, beta-carotene and the like are also included. The flavonoids extracted from the lotus essential oil comprise: luteolin, peppermint isoflavone glycoside, and isoprofuryl. Thin rosmarinic acid and caffeic acid are organic acid components present in peppermint essential oil.
The mint essential oil can be prepared by self or purchased.
The peppermint essential oil is purchased from Jiangxin Xinsen Natural plant oil, Inc.
The second aspect of the invention provides a preparation method of the scrub facial soap, which comprises the following steps:
(1) heating oil at 38-45 deg.C;
(2) adding alkali metal hydroxide into water to prepare a solution, dropwise adding the solution into the grease obtained in the step (1), and stirring and reacting at 35-45 ℃ for 1-4 hours to obtain a thick soap solution;
(3) sequentially adding camellia seed shell micro powder and plant essential oil into the thick soap liquid obtained in the step (2), and uniformly stirring;
(4) and (4) pouring the product obtained in the step (3) into a mold, standing for 46-50 hours at room temperature, then demolding, and saponifying for 10-14 weeks at room temperature to obtain the product.
The present invention will be specifically described below by way of examples. It should be noted that the following examples are only for illustrating the present invention and should not be construed as limiting the scope of the present invention, and that the insubstantial modifications and adaptations of the present invention by those skilled in the art based on the above disclosure are still within the scope of the present invention.
In addition, the starting materials used are all commercially available, unless otherwise specified.
Examples
Example 1
The camellia oil scrub facial soap comprises, by weight, 450 parts of grease, 15 parts of alkali metal hydroxide, 30 parts of camellia seed shell micro powder, 2 parts of plant essential oil and 45 parts of water.
The oil comprises camellia oil, olive oil, avocado oil, palm oil and coconut oil.
The weight ratio of the camellia oil, the olive oil, the avocado oil, the palm oil and the coconut oil is 6: 1: 1: 1: 2.
The alkali metal compound is sodium hydroxide.
The preparation method of the tea seed shell micro powder comprises the following steps: ball milling the tea seed shells for 8 hours by using a ball mill at the rotating speed of 900r/min to obtain the tea seed shells.
The plant essential oil is mint essential oil. The peppermint essential oil is purchased from Jiangxin Xinsen Natural plant oil, Inc.
The preparation method of the scrub facial soap comprises the following steps:
(1) heating oil at 40 deg.C;
(2) adding alkali metal hydroxide into water to prepare a solution, dropwise adding the solution into the grease obtained in the step (1), and stirring and reacting for 3 hours at 40 ℃ to obtain a thick soap solution;
(3) sequentially adding camellia seed shell micro powder and plant essential oil into the thick soap liquid obtained in the step (2), and uniformly stirring;
(4) and (4) pouring the product obtained in the step (3) into a mold, standing for 48 hours at room temperature, then demolding, and saponifying for 14 weeks at normal temperature to obtain the product.
Example 2
The camellia oil scrub facial soap comprises, by weight, 400 parts of grease, 12 parts of alkali metal hydroxide, 25 parts of camellia seed shell micro powder, 2 parts of plant essential oil and 38 parts of water.
The oil comprises camellia oil, olive oil, avocado oil, palm oil and coconut oil.
The weight ratio of the camellia oil, the olive oil, the avocado oil, the palm oil and the coconut oil is 5: 1: 1: 1: 1.
The alkali metal compound is sodium hydroxide.
The preparation method of the camellia seed shell micro powder comprises the following steps: ball milling the camellia seed shells for 5 hours by using a ball mill at the rotating speed of 900r/min to obtain the camellia seed shells.
The plant essential oil is mint essential oil. The peppermint essential oil is purchased from Jiangxin Xinsen Natural plant oil, Inc.
The preparation method of the scrub facial soap comprises the specific steps of example 1.
Example 3
The camellia oil scrub facial soap comprises, by weight, 500 parts of grease, 18 parts of alkali metal hydroxide, 35 parts of camellia seed shell micro powder, 5 parts of plant essential oil and 50 parts of water.
The oil comprises camellia oil, olive oil, avocado oil, palm oil and coconut oil.
The weight ratio of the camellia oil, the olive oil, the avocado oil, the palm oil and the coconut oil is 5: 1: 1: 1: 2.
The alkali metal compound is sodium hydroxide.
The preparation method of the camellia seed shell micro powder comprises the following steps: ball milling the camellia seed shells for 6 hours by using a ball mill at the rotating speed of 900r/min to obtain the camellia seed shells.
The plant essential oil is mint essential oil. The peppermint essential oil is purchased from Jiangxin Xinsen Natural plant oil, Inc.
The preparation method of the scrub facial soap comprises the specific steps of example 1.
Example 4
The camellia oil scrub facial soap comprises, by weight, 450 parts of grease, 15 parts of alkali metal hydroxide, 30 parts of camellia seed shell micro powder, 2 parts of plant essential oil and 45 parts of water.
The oil comprises camellia oil, olive oil, avocado oil, palm oil and coconut oil.
The weight ratio of the camellia oil, the olive oil, the avocado oil, the palm oil and the coconut oil is 3: 1: 1: 2: 2.
The alkali metal compound is sodium hydroxide.
The preparation method of the camellia seed shell micro powder has the specific steps as in example 1.
The plant essential oil is mint essential oil. The peppermint essential oil is purchased from Jiangxin Xinsen Natural plant oil, Inc.
The preparation method of the scrub facial soap comprises the specific steps of example 1.
Example 5
The camellia oil scrub facial soap comprises, by weight, 450 parts of grease, 15 parts of alkali metal hydroxide, 30 parts of camellia seed shell micro powder, 2 parts of plant essential oil and 45 parts of water.
The oil comprises camellia oil, olive oil, avocado oil, palm oil and coconut oil.
The weight ratio of the camellia oil, the olive oil, the avocado oil, the palm oil and the coconut oil is 3: 1: 1: 1: 3.
The alkali metal compound is sodium hydroxide.
The preparation method of the camellia seed shell micro powder has the specific steps as in example 1.
The plant essential oil is mint essential oil. The peppermint essential oil is purchased from Jiangxin Xinsen Natural plant oil, Inc.
The preparation method of the scrub facial soap comprises the specific steps of example 1.
Example 6
The camellia oil scrub facial soap comprises the following specific components in parts by weight in the same manner as in example 1. The difference lies in that the preparation method of the camellia seed shell micro powder comprises the following steps: ball milling the camellia seed hulls for 1 hour by using a ball mill at the rotating speed of 900r/min to obtain the camellia seed hulls.
The preparation method of the scrub facial soap comprises the specific steps of example 1.
Example 7
The camellia oil scrub facial soap comprises, by weight, 450 parts of grease, 15 parts of alkali metal hydroxide, 30 parts of camellia seed shell micro powder, 2 parts of plant essential oil and 45 parts of water.
The oil comprises camellia oil, olive oil, avocado oil, palm oil and coconut oil.
The weight ratio of the camellia oil, the olive oil, the avocado oil, the palm oil and the coconut oil is 5: 1: 1: 0: 2.
The alkali metal compound is sodium hydroxide.
The preparation method of the camellia seed shell micro powder has the specific steps as in example 1.
The plant essential oil is mint essential oil. The peppermint essential oil is purchased from Jiangxin Xinsen Natural plant oil, Inc.
The preparation method of the scrub facial soap comprises the specific steps of example 1.
Performance testing
The evaluation method comprises the following steps: young people (age 22-26 years, 21 people in total) with skin easy to produce oil and obvious blackheads at nose are selected as test objects, and then a cleaning test is carried out by using the camellia oil scrub facial soap, and the skin state is observed after gentle rubbing for 20 seconds. 3 individuals were selected for each example.
Table 1 shows the effect of the camellia oil scrub facial soap of example 1 after 2-8 weeks of use. Table 2 shows the effect of the camellia oil scrub cleansing soap of examples 2-7 after 6 weeks of use. (use 1 time each morning and evening)
Wherein. + represents cleaning power, the more + the number, the stronger the cleaning power, -the general or no apparent cleaning power.
TABLE 1 Effect of the Camellia oil scrub facial soap of example 1 after 2-8 weeks of use
Time of use Skin fouling Aged stratum corneum Black head White head
2 weeks + + － －
4 weeks ++ + + +
6 weeks ++ ++ +++ ++
8 weeks ++ ++ +++ ++
TABLE 2 Effect of Camellia oil scrub facial soap of examples 2-7 after 6 weeks of use
Examples Skin fouling Aged stratum corneum Black head White head
Example 2 ++ ++ + +
Example 3 ++ + + ++
Example 4 + + － －
Example 5 ++ + － －
Example 6 ++ － － －
Example 7 + + － +
Test results show that the camellia oil frosted soap has obvious cleaning effect on skin dirt, white heads and aged cuticles after being used for 4 weeks, has obvious effect on removing black heads and aged cuticles after being used for 6 weeks, and has obvious effect on removing black heads and aged cuticles after being used for 8 weeks.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in other forms, and any person skilled in the art may modify or change the technical content of the above disclosed embodiment into equivalent embodiments with equivalent changes, but all those simple modifications, equivalent changes and modifications made to the above embodiments according to the technical spirit of the present invention still belong to the technical solution of the present invention.

Claims (4)

1. The camellia oil scrub facial soap is characterized in that the preparation raw materials comprise, by weight, 400-500 parts of grease, 12-18 parts of alkali metal hydroxide, 25-35 parts of camellia seed shell micro powder, 1-5 parts of plant essential oil and 38-50 parts of water;
the oil comprises camellia oil, olive oil, avocado oil, palm oil and coconut oil;
the camellia oil, the olive oil, the avocado oil, the palm oil and the coconut oil are in a weight ratio of (3-6): 1: 1: 1: (1-2);
the preparation method of the camellia seed shell micro powder comprises the following steps: ball milling the camellia seed shells by using a ball mill for 2-8 hours at the rotation speed of 500-1200r/min to obtain the camellia seed shells.
2. The camellia oil scrub facial soap of claim 1, wherein the alkali metal hydroxide is sodium hydroxide.
3. The camellia oil facial scrub soap of claim 1, wherein the plant essential oil is at least one selected from the group consisting of peppermint essential oil, lavender essential oil, chamomile essential oil, tea tree essential oil, cypress essential oil, patchouli essential oil, rose essential oil, eucalyptus essential oil, thyme essential oil, sandalwood essential oil, rosemary oil, lemon oil, clove oil, cinnamon oil, basil oil, chamomile oil, caraway oil, coriander oil, tarragon oil, wormwood oil, hyssop oil, sage oil, chrysanthemum indicum oil, pine needle oil, and frankincense oil.
4. A method of making the camellia oil scrub facial soap of any of claims 1-3, comprising the steps of:
(1) heating oil at 38-45 deg.C;
(2) adding alkali metal hydroxide into water to prepare a solution, dropwise adding the solution into the grease obtained in the step (1), and stirring and reacting at 35-45 ℃ for 1-4 hours to obtain a thick soap solution;
(3) sequentially adding camellia seed shell micro powder and plant essential oil into the thick soap liquid obtained in the step (2), and uniformly stirring;
(4) and (4) pouring the product obtained in the step (3) into a mold, standing for 46-50 hours at room temperature, then demolding, and saponifying for 10-14 weeks at room temperature to obtain the product.
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CN104694302A (en) * 2013-12-09 2015-06-10 东莞市立普利化工科技有限公司 Oil stain removing cleaning perfumed soap and preparing method thereof

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JP5616188B2 (en) * 2010-10-04 2014-10-29 横浜油脂工業株式会社 Washing soap
KR102504196B1 (en) * 2015-11-26 2023-02-28 주식회사 엘지생활건강 Composition for skin cleansing
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CN1087942A (en) * 1992-12-07 1994-06-15 田地 Soap with abrasive
CN102041205A (en) * 2009-10-10 2011-05-04 王世范 Scrub soap and preparation process and formula thereof
CN103666793A (en) * 2013-09-27 2014-03-26 红河五里冲生态茶业有限公司 Tea soap powder and use thereof
CN104694302A (en) * 2013-12-09 2015-06-10 东莞市立普利化工科技有限公司 Oil stain removing cleaning perfumed soap and preparing method thereof

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