CN111034875A - Natural residue-free disease-resistant growth promoter for aquatic livestock and preparation method thereof - Google Patents
Natural residue-free disease-resistant growth promoter for aquatic livestock and preparation method thereof Download PDFInfo
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- CN111034875A CN111034875A CN201911410875.8A CN201911410875A CN111034875A CN 111034875 A CN111034875 A CN 111034875A CN 201911410875 A CN201911410875 A CN 201911410875A CN 111034875 A CN111034875 A CN 111034875A
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- 201000010099 disease Diseases 0.000 title claims abstract description 32
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 title claims abstract description 32
- 239000007952 growth promoter Substances 0.000 title claims abstract description 31
- 244000144972 livestock Species 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims description 7
- 239000003814 drug Substances 0.000 claims abstract description 22
- 239000000284 extract Substances 0.000 claims abstract description 19
- 241001092040 Crataegus Species 0.000 claims abstract description 17
- 235000009917 Crataegus X brevipes Nutrition 0.000 claims abstract description 17
- 235000013204 Crataegus X haemacarpa Nutrition 0.000 claims abstract description 17
- 235000009685 Crataegus X maligna Nutrition 0.000 claims abstract description 17
- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 claims abstract description 17
- 235000009486 Crataegus bullatus Nutrition 0.000 claims abstract description 17
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 claims abstract description 17
- 235000009682 Crataegus limnophila Nutrition 0.000 claims abstract description 17
- 235000004423 Crataegus monogyna Nutrition 0.000 claims abstract description 17
- 235000002313 Crataegus paludosa Nutrition 0.000 claims abstract description 17
- 235000009840 Crataegus x incaedua Nutrition 0.000 claims abstract description 17
- 241000893536 Epimedium Species 0.000 claims abstract description 15
- 241000245665 Taraxacum Species 0.000 claims abstract description 15
- 235000005187 Taraxacum officinale ssp. officinale Nutrition 0.000 claims abstract description 15
- 235000018905 epimedium Nutrition 0.000 claims abstract description 15
- 241000334160 Isatis Species 0.000 claims abstract description 13
- 239000002994 raw material Substances 0.000 claims abstract description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 54
- 239000002904 solvent Substances 0.000 claims description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 28
- 238000000498 ball milling Methods 0.000 claims description 27
- 239000012153 distilled water Substances 0.000 claims description 27
- 235000006533 astragalus Nutrition 0.000 claims description 19
- -1 polysaccharides compounds Chemical class 0.000 claims description 18
- 239000000243 solution Substances 0.000 claims description 18
- 241001061264 Astragalus Species 0.000 claims description 14
- 238000006243 chemical reaction Methods 0.000 claims description 14
- 210000004233 talus Anatomy 0.000 claims description 14
- 229930003935 flavonoid Natural products 0.000 claims description 12
- 235000017173 flavonoids Nutrition 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 11
- 239000000463 material Substances 0.000 claims description 11
- 241000208688 Eucommia Species 0.000 claims description 10
- 238000010790 dilution Methods 0.000 claims description 9
- 239000012895 dilution Substances 0.000 claims description 9
- 229920001282 polysaccharide Polymers 0.000 claims description 6
- 239000005017 polysaccharide Substances 0.000 claims description 6
- 241000045403 Astragalus propinquus Species 0.000 claims description 5
- CWVRJTMFETXNAD-JUHZACGLSA-N chlorogenic acid Chemical class O[C@@H]1[C@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-JUHZACGLSA-N 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 2
- 230000035484 reaction time Effects 0.000 claims description 2
- 241000287828 Gallus gallus Species 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 7
- 241001673966 Magnolia officinalis Species 0.000 abstract description 6
- 230000004083 survival effect Effects 0.000 abstract description 6
- 230000001737 promoting effect Effects 0.000 abstract description 5
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract description 4
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract description 4
- 239000003674 animal food additive Substances 0.000 abstract description 4
- 239000011575 calcium Substances 0.000 abstract description 4
- 229910052791 calcium Inorganic materials 0.000 abstract description 4
- 239000011574 phosphorus Substances 0.000 abstract description 4
- 229910052698 phosphorus Inorganic materials 0.000 abstract description 4
- 102000004169 proteins and genes Human genes 0.000 abstract description 4
- 108090000623 proteins and genes Proteins 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 4
- 208000035240 Disease Resistance Diseases 0.000 abstract description 3
- 230000029087 digestion Effects 0.000 abstract description 3
- 235000015097 nutrients Nutrition 0.000 abstract description 3
- 238000010521 absorption reaction Methods 0.000 abstract description 2
- 235000013330 chicken meat Nutrition 0.000 abstract description 2
- 210000003608 fece Anatomy 0.000 abstract description 2
- 239000010871 livestock manure Substances 0.000 abstract 1
- 238000003756 stirring Methods 0.000 description 7
- 238000001291 vacuum drying Methods 0.000 description 7
- 239000010231 banlangen Substances 0.000 description 4
- 241001465754 Metazoa Species 0.000 description 3
- 241000208689 Eucommia ulmoides Species 0.000 description 2
- 239000009636 Huang Qi Substances 0.000 description 2
- 235000001368 chlorogenic acid Nutrition 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 244000144977 poultry Species 0.000 description 2
- 235000013594 poultry meat Nutrition 0.000 description 2
- 235000019750 Crude protein Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000019726 broiler meat Nutrition 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000000378 dietary effect Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000015816 nutrient absorption Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 235000013613 poultry product Nutrition 0.000 description 1
- 238000003307 slaughter Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/70—Feeding-stuffs specially adapted for particular animals for birds
- A23K50/75—Feeding-stuffs specially adapted for particular animals for birds for poultry
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Animal Husbandry (AREA)
- Zoology (AREA)
- Birds (AREA)
- Molecular Biology (AREA)
- Mycology (AREA)
- Physiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Health & Medical Sciences (AREA)
- Medicines Containing Plant Substances (AREA)
- Fodder In General (AREA)
Abstract
The invention relates to the technical field of disease-resistant growth promoters, and discloses a natural residue-free disease-resistant growth promoter for aquatic livestock, which is prepared from the main raw materials of isatis root, dandelion, hawthorn, rhizoma atractylodis, magnolia officinalis, epimedium and 60-100 parts of traditional Chinese medicine extract, the natural residue-free disease-resistant growth promoter for aquatic livestock is used as a feed additive and a disease-resistant growth promoter by adding the traditional Chinese medicine components such as the isatis root, the hawthorn, the epimedium herb, the traditional Chinese medicine extract and the like, has low cost, and has obvious effect of improving the disease resistance rate and the survival rate of the broiler chickens, the survival rate can reach 92 to 96 percent, through detecting the content of the chicken manure, the contents of nutrient substances such as protein, phosphorus and calcium are all reduced, the dressing percentage is obviously improved, and the natural residue-free disease-resistant growth promoter for aquatic livestock can be inferred to have good digestion and absorption promoting effect and growth promoting effect on the broiler chickens.
Description
Technical Field
The invention relates to the technical field of disease-resistant growth promoters, in particular to a natural residue-free disease-resistant growth promoter for aquatic livestock and a preparation method thereof.
Background
With the continuous development of modern livestock and poultry, livestock and poultry products in China grow rapidly, broiler meat is delicious, taste is good, nutrition is rich, contents of nutrients such as protein and mineral substances are high, fat content is low, digestion is easy, and the feed has an important effect on improving dietary structure of people.
The feed additive is a small amount of or trace substances added in the production, processing and using processes of feeds, has an obvious growth promotion effect, is a raw material inevitably used in the modern feed industry, and has obvious effects on enhancing the nutritive value of basic feeds, improving the production performance of animals, ensuring the health of the animals, saving the feed cost, improving the quality of animal products and the like, but the existing feed additive is difficult to integrate disease resistance and growth promotion into a whole, so that the feed cost is greatly increased.
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a natural residue-free disease-resistant growth promoter for aquatic livestock and a preparation method thereof, and solves the problems that the disease-resistant growth promoter is difficult to dissolve in water, the dissolution rate of the medicine is slow, and the dissolution rate and the release rate are low.
(II) technical scheme
In order to achieve the purpose, the invention provides the following technical scheme: a natural residue-free disease-resistant growth promoter for aquatic livestock comprises the following formula raw materials in parts by weight: 140 parts of isatis root, 30-60 parts of dandelion, 250 parts of hawthorn, 8-15 parts of rhizoma atractylodis, 10-15 parts of mangnolia officinalis, 160 parts of epimedium and 60-100 parts of traditional Chinese medicine extract, wherein the medicinal materials comprise 100-140 parts of isatis root, 30-60 parts of dandelion, 150-250 parts of hawthorn, 8-15 parts of rhizoma atractylodis, 10-15 parts of mangnoli.
Preferably, the traditional Chinese medicine extract comprises astragalus polysaccharides compounds, astragalus flavonoids compounds, eucommia flavonoids compounds and eucommia chlorogenic acids compounds, and the mass ratio of the astragalus polysaccharides compounds, the astragalus flavonoids compounds, the eucommia flavonoids compounds and the eucommia chlorogenic acids compounds is 100:40-80:40-55: 20-30.
Preferably, the preparation method of the natural residue-free disease-resistant growth promoter for aquatic livestock comprises the following steps:
(1) adding ethanol solvent, 100-150 parts of astragalus mongholicus, 100-140 parts of isatis root, 30-60 parts of dandelion, 150-250 parts of hawthorn, 8-15 parts of rhizoma atractylodis, 10-15 parts of mangnolia officinalis, 100-160 parts of epimedium and 60-100 parts of traditional Chinese medicine extract into a planetary ball mill, performing ball milling until the materials pass through a 100-mesh 200-mesh screen at the revolution speed of 400-mesh 600rpm and the rotation speed of 200-mesh 300 rpm.
(2) Adding distilled water and an ethanol solvent into a reaction bottle, wherein the volume ratio of the distilled water to the ethanol solvent is 2-6:1, adding a ball-milling mixed product, placing the ball-milling mixed product into an oil bath pot, heating for reaction, drying the solution in vacuum to completely remove the solvent, adding distilled water for dilution, controlling the total mass fraction of the solution to be 35-60%, and preparing the natural residue-free disease-resistant growth promoter for aquatic livestock.
Preferably, the heating temperature of the oil bath kettle is 90-120 ℃, and the reaction time is 6-12 h.
(III) advantageous technical effects
Compared with the prior art, the invention has the following beneficial technical effects:
the natural residue-free disease-resistant growth promoter for the aquatic livestock is prepared by adding traditional Chinese medicine components such as isatis roots, hawthorn fruits, epimedium herbs and traditional Chinese medicine extracts to serve as a feed additive and the disease-resistant growth promoter, is low in cost, has an obvious effect of improving the disease resistance rate and the survival rate of broiler chickens, can reach the survival rate of 92-96%, reduces the contents of protein, phosphorus and calcium which are nutrient substances through detecting the content of excrement of chickens, obviously improves the slaughter rate, can be inferred, and has good digestion and absorption promoting effects and growth promoting effects on the broiler chickens.
Detailed Description
To achieve the above object, the present invention provides the following embodiments and examples: a natural residue-free disease-resistant growth promoter for aquatic livestock comprises the following formula raw materials in parts by weight: 140 parts of isatis root, 30-60 parts of dandelion, 250 parts of hawthorn, 8-15 parts of rhizoma atractylodis, 10-15 parts of mangnolia officinalis, 160 parts of epimedium and 60-100 parts of traditional Chinese medicine extracts, wherein the traditional Chinese medicine extracts comprise astragalus polysaccharide compounds, astragalus flavonoid compounds, eucommia flavonoid compounds and eucommia chlorogenic acid compounds in a mass ratio of 100:40-80:40-55: 20-30.
The preparation method of the natural residue-free disease-resistant growth promoter for aquatic livestock comprises the following steps:
(1) adding an ethanol solvent, 100-150 parts of astragalus mongholicus, 100-140 parts of isatis root, 30-60 parts of dandelion, 150-250 parts of hawthorn, 8-15 parts of rhizoma atractylodis, 10-15 parts of mangnolia officinalis, 100-160 parts of epimedium and 60-100 parts of a traditional Chinese medicine extract into a planetary ball mill, wherein the traditional Chinese medicine extract comprises astragalus polysaccharide compounds, astragalus mongholicus flavonoid compounds, eucommia ulmoides flavonoid compounds and eucommia ulmoides chlorogenic acid compounds, the mass ratio of the four is 100:40-80:40-55:20-30, the revolving speed of the ball mill is 400-300 rpm, the rotating speed of the ball mill is 200-300rpm, and ball milling is carried out until the materials pass through a 100-mesh 200-mesh screen.
(2) Adding distilled water and an ethanol solvent into a reaction bottle, wherein the volume ratio of the distilled water to the ethanol solvent is 2-6:1, adding a ball-milling mixed product, placing the ball-milling mixed product in an oil bath pot, heating to 90-120 ℃, and stirring at a constant speed for reacting for 6-12 hours. And completely removing the solvent by vacuum drying the solution, adding distilled water for dilution, controlling the total mass fraction of the solution to be 35-60%, and preparing the natural residue-free disease-resistant growth promoter for the aquatic livestock.
Example 1
(1) Adding ethanol solvent, 100 parts of astragalus, 100 parts of radix isatidis, 30 parts of dandelion, 150 parts of hawthorn, 8 parts of rhizoma atractylodis, 10 parts of magnolia officinalis, 100 parts of epimedium and 60 parts of traditional Chinese medicine extract into a planetary ball mill, performing ball milling at the revolution speed of 400rpm and the rotation speed of 200rpm of the ball mill until the materials pass through a 100-mesh 200-mesh screen.
(2) Adding distilled water and an ethanol solvent into a reaction bottle, wherein the volume ratio of the distilled water to the ethanol solvent is 2:1, adding a ball-milling mixed product, placing the ball-milling mixed product in an oil bath pot, heating to 90 ℃, and stirring at a constant speed for reacting for 6 hours. And completely removing the solvent by vacuum drying the solution, adding distilled water for dilution, controlling the total mass fraction of the solution to be 35-60%, and preparing the natural residue-free disease-resistant growth promoter 1 for the aquatic livestock.
Example 2
(1) Adding ethanol solvent, 110 parts of astragalus, 110 parts of isatis root, 60 parts of dandelion, 150 parts of hawthorn, 15 parts of rhizoma atractylodis, 10 parts of magnolia officinalis, 160 parts of epimedium and 65 traditional Chinese medicine extracts into a planetary ball mill, and performing ball milling until the materials pass through a 100-mesh 200-mesh screen when the revolution speed of the ball mill is 600rpm and the rotation speed is 300 rpm.
(2) Adding distilled water and an ethanol solvent into a reaction bottle, wherein the volume ratio of the distilled water to the ethanol solvent is 2:1, adding a ball-milling mixed product, placing the ball-milling mixed product in an oil bath pot, heating to 120 ℃, and stirring at a constant speed for reaction for 12 hours. And completely removing the solvent by vacuum drying the solution, adding distilled water for dilution, controlling the total mass fraction of the solution to be 35-60%, and preparing the natural residue-free disease-resistant growth promoter 2 for the aquatic livestock.
Example 3
(1) Adding an ethanol solvent, 130 parts of astragalus, 140 parts of isatis root, 40 parts of dandelion, 250 parts of hawthorn, 15 parts of rhizoma atractylodis, 10-15 parts of magnolia officinalis, 100 parts of epimedium and 80 parts of a traditional Chinese medicine extract into a planetary ball mill, performing ball milling at the revolution speed of 400-300 rpm and the rotation speed of 200-300rpm of the ball mill until the materials pass through a 200-mesh screen.
(2) Adding distilled water and an ethanol solvent into a reaction bottle, wherein the volume ratio of the distilled water to the ethanol solvent is 5:1, adding a ball-milling mixed product, placing the ball-milling mixed product in an oil bath pot, heating to 100 ℃, and stirring at a constant speed for reacting for 8 hours. And completely removing the solvent by vacuum drying the solution, adding distilled water for dilution, controlling the total mass fraction of the solution to be 40%, and preparing the natural residue-free disease-resistant growth promoter 3 for the aquatic livestock.
Example 4
(1) Adding an ethanol solvent, 125 parts of astragalus mongholicus, 120 parts of radix isatidis, 45 parts of dandelion, 200 parts of hawthorn, 11 parts of rhizoma atractylodis, 10-15 parts of mangnolia officinalis, 140 parts of epimedium and 80 parts of traditional Chinese medicine extract into a planetary ball mill, performing ball milling at the revolution speed of 500rpm and the rotation speed of 250rpm of the ball mill until the materials pass through a 200-mesh screen.
(2) Adding distilled water and an ethanol solvent into a reaction bottle, wherein the volume ratio of the distilled water to the ethanol solvent is 4:1, adding a ball-milling mixed product, placing the ball-milling mixed product in an oil bath pot, heating to 100 ℃, and stirring at a constant speed for reacting for 8 hours. And completely removing the solvent by vacuum drying the solution, adding distilled water for dilution, controlling the total mass fraction of the solution to be 50%, and preparing the natural residue-free disease-resistant growth promoter for the aquatic livestock 4.
Example 5
(1) Adding ethanol solvent, 150 parts of radix astragali, 100 parts of radix isatidis, 30-60 parts of dandelion, 210 parts of hawthorn, 12 parts of rhizoma atractylodis, 11 parts of magnolia officinalis, 160 parts of epimedium and 60-100 parts of traditional Chinese medicine extract into a planetary ball mill, performing ball milling at the revolution speed of 540rpm and the rotation speed of 270rpm of the ball mill until the materials pass through a 100-mesh and 200-mesh screen.
(2) Adding distilled water and an ethanol solvent into a reaction bottle, wherein the volume ratio of the distilled water to the ethanol solvent is 5:1, adding a ball-milling mixed product, placing the ball-milling mixed product in an oil bath pot, heating to 110 ℃, and stirring at a constant speed for reaction for 10 hours. And completely removing the solvent by vacuum drying the solution, adding distilled water for dilution, controlling the total mass fraction of the solution to be 35%, and preparing the natural residue-free disease-resistant growth promoter 5 for the aquatic livestock.
Example 6
(1) Adding ethanol solvent, 150 parts of radix astragali, 140 parts of radix isatidis, 60 parts of dandelion, 250 parts of hawthorn, 15 parts of rhizoma atractylodis, 15 parts of magnolia officinalis, 160 parts of epimedium and 100 parts of traditional Chinese medicine extract into a planetary ball mill, wherein the revolution speed of the ball mill is 400rpm, and the rotation speed is 300rpm, and carrying out ball milling until the materials pass through a 200-mesh screen.
(2) Adding distilled water and an ethanol solvent into a reaction bottle, wherein the volume ratio of the distilled water to the ethanol solvent is 6:1, adding a ball-milling mixed product, placing the ball-milling mixed product in an oil bath pot, heating to 120 ℃, and stirring at a constant speed for reaction for 12 hours. And completely removing the solvent by vacuum drying the solution, adding distilled water for dilution, controlling the total mass fraction of the solution to be 60%, and preparing the natural residue-free disease-resistant growth promoter 6 for the aquatic livestock.
The healthy laying cocks are randomly divided into a blank control group and an experimental group 1-6, each group comprises 50 cocks, the initial weight is weighed and recorded, the experimental group 1-6 is respectively fed with quantitative common feed and natural residue-free disease-resistant growth promoting agent 1-6 for aquatic poultry, the weight accounts for 5% of the weight of the common feed, the cocks are respectively fed three times in the morning, at noon and evening, the feeding temperature is 30 ℃, the feeding period is 30 days, excrement samples of the broilers in the blank control group and the experimental group are collected after the feeding period is finished, the content of crude protein, calcium and phosphorus is tested by a liquid chromatography-mass spectrometer, the nutrient absorption rate is compared, and the survival rate, the total weight and the average mass, the dressing percentage and the complete evisceration of the control group and the blank are.
Content of protein, calcium and phosphorus in feces
Survival rate, average quality, dressing percentage and total smoothbore percentage
Claims (4)
1. The natural residue-free disease-resistant growth promoter for aquatic livestock comprises the following formula raw materials and components in parts by weight, and is characterized in that: 140 parts of isatis root, 30-60 parts of dandelion, 250 parts of hawthorn, 8-15 parts of rhizoma atractylodis, 10-15 parts of mangnolia officinalis, 160 parts of epimedium and 60-100 parts of traditional Chinese medicine extract, wherein the medicinal materials comprise 100-140 parts of isatis root, 30-60 parts of dandelion, 150-250 parts of hawthorn, 8-15 parts of rhizoma atractylodis, 10-15 parts of mangnoli.
2. The natural residue-free disease-resistant growth promoter for aquatic livestock according to claim 1, which is characterized in that: the traditional Chinese medicine extract comprises astragalus polysaccharides compounds, astragalus flavonoids compounds, eucommia flavonoids compounds and eucommia chlorogenic acid compounds, and the mass ratio of the astragalus polysaccharides compounds, the astragalus flavonoids compounds, the eucommia flavonoids compounds and the eucommia chlorogenic acid compounds is 100:40-80:40-55: 20-30.
3. The natural residue-free disease-resistant growth promoter for aquatic livestock according to claim 1, which is characterized in that: the preparation method of the natural residue-free disease-resistant growth promoter for aquatic livestock comprises the following steps:
(1) adding ethanol solvent, 100-150 parts of astragalus mongholicus, 100-140 parts of isatis root, 30-60 parts of dandelion, 150-250 parts of hawthorn, 8-15 parts of rhizoma atractylodis, 10-15 parts of mangnolia officinalis, 100-160 parts of epimedium and 60-100 parts of traditional Chinese medicine extract into a planetary ball mill, performing ball milling until the materials pass through a 100-mesh 200-mesh screen at the revolution speed of 400-mesh 600rpm and the rotation speed of 200-mesh 300 rpm.
(2) Adding distilled water and an ethanol solvent into a reaction bottle, wherein the volume ratio of the distilled water to the ethanol solvent is 2-6:1, adding a ball-milling mixed product, placing the ball-milling mixed product into an oil bath pot, heating for reaction, drying the solution in vacuum to completely remove the solvent, adding distilled water for dilution, controlling the total mass fraction of the solution to be 35-60%, and preparing the natural residue-free disease-resistant growth promoter for aquatic livestock.
4. The natural residue-free disease-resistant growth promoter for aquatic livestock according to claim 2, which is characterized in that: the heating temperature of the oil bath kettle is 90-120 ℃, and the reaction time is 6-12 h.
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CN106852408A (en) * | 2015-12-07 | 2017-06-16 | 天津市中敖饲料有限公司 | Improve Chinese herb feed additive of meat chicken production performance and preparation method thereof |
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Application publication date: 20200421 |