CN111020608A - Train wheel pair bearing lubricating grease spray cleaning agent and preparation method thereof - Google Patents

Train wheel pair bearing lubricating grease spray cleaning agent and preparation method thereof Download PDF

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Publication number
CN111020608A
CN111020608A CN201911334351.5A CN201911334351A CN111020608A CN 111020608 A CN111020608 A CN 111020608A CN 201911334351 A CN201911334351 A CN 201911334351A CN 111020608 A CN111020608 A CN 111020608A
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CN
China
Prior art keywords
low
train wheel
nonionic surfactant
lubricating grease
cleaning agent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201911334351.5A
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Chinese (zh)
Inventor
柴明峰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dalian Sandaaoke Chemistry Co Ltd
Original Assignee
Dalian Sandaaoke Chemistry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dalian Sandaaoke Chemistry Co Ltd filed Critical Dalian Sandaaoke Chemistry Co Ltd
Priority to CN201911334351.5A priority Critical patent/CN111020608A/en
Publication of CN111020608A publication Critical patent/CN111020608A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23GCLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
    • C23G1/00Cleaning or pickling metallic material with solutions or molten salts
    • C23G1/14Cleaning or pickling metallic material with solutions or molten salts with alkaline solutions
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23GCLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
    • C23G1/00Cleaning or pickling metallic material with solutions or molten salts
    • C23G1/14Cleaning or pickling metallic material with solutions or molten salts with alkaline solutions
    • C23G1/19Iron or steel
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23GCLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
    • C23G5/00Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents
    • C23G5/06Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using emulsions

Abstract

The invention discloses a spray cleaning agent for bearing lubricating grease of a train wheel, which is water-based, free of ecological pollution, high in cleaning efficiency, free of corrosion to steel and low in cost, and a preparation method thereof. The raw materials and the mass percentage are as follows: 2-15% of potassium hydroxide or sodium hydroxide, 2-5% of a nonionic surfactant Plurafac LF-9000.5-5%, 11-10% of a nonionic surfactant Plurafac LF-9011%, 5-32% of a low-foaming wetting agent Marlox FK-860.5%, 10% of an alkaline low-foaming surfactant Berol LFG-611%, 26-15% of alkyl glycoside AG 62060.5%, 0.1-10% of N, N-diacetyl-3-hydroxypropyl amine and the balance of water.

Description

Train wheel pair bearing lubricating grease spray cleaning agent and preparation method thereof
Technical Field
The invention relates to a cleaning agent for removing lubricating grease on a bearing of a train wheel, in particular to a spray cleaning agent for the lubricating grease on the bearing of the train wheel, which is water-based, has no ecological pollution, high cleaning efficiency, no corrosion to steel and low cost, and a preparation method thereof.
Background
In order to ensure the running safety of the railway train and prolong the service life of the train, the railway train must be regularly checked and repaired, including the maintenance work of cleaning bearing lubricating grease by the train wheels. The grease cleaning agent applied to the surface of a common metal workpiece at present is basically divided into an organic solvent cleaning agent and a water-based cleaning agent. The organic solvent cleaning agent generally adopts kerosene, gasoline, diesel oil and other halogenated hydrocarbon organic solvents, has high cost, can cause serious damage to the ecological environment and harm the health of operators. The water-based cleaning agent is composed of a surfactant, an emulsifier, a penetrant and the like, realizes the cleaning of oil stains and grease through the actions of wetting, emulsifying, permeating, dispersing, solubilizing and the like, is safe to use and does not pollute the environment. However, the prior art
The water base is not suitable for cleaning lubricating grease on the bearing of the train wheel pair, and a large amount of lubricating grease can still be adsorbed on the surface of the workpiece of the train wheel pair even if the bearing is cleaned at the high temperature of 60 ℃ and the high pressure of 1MPa for about 10 minutes.
Disclosure of Invention
The invention aims to solve the technical problems in the prior art and provides a spray cleaning agent for bearing lubricating grease of train wheels, which is water-based, free of ecological pollution, high in cleaning efficiency, free of corrosion to steel and low in cost, and a preparation method thereof.
The technical solution of the invention is as follows: the spray cleaning agent for the lubricating grease of the bearing of the train wheel is characterized by comprising the following raw materials in percentage by mass: 2-15% of potassium hydroxide or sodium hydroxide, 2-5% of a nonionic surfactant Plurafac LF-9000.5-5%, 11-10% of a nonionic surfactant Plurafac LF-9011%, 5-32% of a low-foaming wetting agent Marlox FK-860.5%, 10% of an alkaline low-foaming surfactant Berol LFG-611%, 26-15% of alkyl glycoside AG 62060.5%, 0.1-10% of N, N-diacetyl-3-hydroxypropyl amine and the balance of water.
The preparation method of the spray cleaning agent for the bearing lubricating grease of the train wheel sequentially comprises the following steps:
(1) adding reaction water into a reaction kettle, adding potassium hydroxide or sodium hydroxide at normal temperature, and stirring until the reaction water is completely dissolved;
(2) sequentially adding a nonionic surfactant Plurafac LF-900, a nonionic surfactant Plurafac LF-901, a low-foam wetting agent Marlox FK-86 and an alkaline low-foam surfactant Berol LFG-61 into a reaction kettle, and stirring at a shear speed of 500-800 rpm for 4-6 minutes;
(3) adding alkyl glycoside AG6206, and stirring for 3-5 minutes at a shearing speed of 500-800 rpm;
(4) adding N, N-diacetyl-3-hydroxy propylamine, stirring until the product is transparent, and naturally cooling.
The water-based cleaning agent is a water-based product, overcomes the problems of environmental pollution and the like of an organic solvent cleaning agent, simultaneously keeps high penetration, emulsification and stripping capabilities on lubricating grease on a bearing of a train wheel, has spraying cleaning pressure of only 0.3-0.5 Mpa, temperature of only 25-30 ℃ and time of only 3-5 minutes, and is simple to operate, good in cleaning effect, capable of saving energy, improving efficiency and reducing cost compared with the existing water-based cleaning agent.
Detailed Description
Example 1:
the spray cleaning agent for the lubricating grease of the train wheel pair bearing is prepared from the following raw materials in percentage by mass: 2% of sodium hydroxide, 2% of a nonionic surfactant Plurafac LF-9003%, a nonionic surfactant Plurafac LF-9017%, a low-foaming wetting agent Marlox FK-862%, a basic low-foaming surfactant Berol LFG-612.5%, an alkyl glycoside AG 62063.5%, N-diacetyl-3-hydroxypropyl amine 1.8% and the balance of water.
The preparation method comprises the following steps in sequence:
(1) adding reaction water into a reaction kettle, adding sodium hydroxide at normal temperature, and stirring until the sodium hydroxide is completely dissolved;
(2) sequentially adding a nonionic surfactant Plurafac LF-900, a nonionic surfactant Plurafac LF-901, a low-foaming wetting agent Marlox FK-86 and an alkaline low-foaming surfactant Berol LFG-61 into a reaction kettle, and stirring at a shear speed of 600 revolutions per minute for 5 minutes;
(3) adding the alkyl glycoside AG6206, and stirring for 4 minutes at a shear rate of 600 revolutions per minute;
(4) adding N, N-diacetyl-3-hydroxy propylamine, stirring until the product is transparent, and naturally cooling.
The nonionic surfactant Plurafac LF-900 and the nonionic surfactant Plurafac LF-901 are products of Pasteur, the low-foaming wetting agent Marlox FK-86 is a product of Sasol, and the alkaline low-foaming surfactant BerollFG-61 and the alkyl glycoside AG6206 are products of Acksonobel.
Application example 1:
the volume ratio of the spray cleaning agent for the lubricating grease of the train wheel pair bearing prepared according to the embodiment 1 of the invention to water in the first tank is 1: 20, placing the train wheel pair bearing to be cleaned in spraying cleaning equipment, adjusting the spraying pressure to be 0.5MPa, controlling the cleaning temperature to be 25 ℃, adjusting the running speed of a production line of the spraying cleaning equipment to start spraying cleaning, and controlling the effective spraying time of the train wheel pair bearing to be 5 minutes; tap water is added into the second tank, and the second tank is sprayed and rinsed for 1 minute and then dried by hot air. The cleaned train wheel has no grease stain residue on the bearing, and is bright and free of corrosion.
Example 2:
the spray cleaning agent for the lubricating grease of the train wheel pair bearing is prepared from the following raw materials in percentage by mass: 3% of potassium hydroxide, 3% of nonionic surfactant Plurafac LF-9003%, Plurafac LF-9016%, low foaming wetting agent Marlox FK-861.5%, alkaline low foaming surfactant Berol LFG-613.5%, alkyl glycoside AG 62064%, N-diacetyl-3-hydroxy propylamine 2.2%, and the balance of water.
The preparation method comprises the following steps in sequence:
(1) adding reaction water into a reaction kettle, adding sodium hydroxide at normal temperature, and stirring until the sodium hydroxide is completely dissolved;
(2) sequentially adding a nonionic surfactant Plurafac LF-900, a nonionic surfactant Plurafac LF-901, a low-foaming wetting agent Marlox FK-86 and an alkaline low-foaming surfactant Berol LFG-61 into a reaction kettle, and stirring at a shear speed of 500 revolutions per minute for 5 minutes;
(3) adding the alkyl glycoside AG6206, and stirring for 5 minutes at a shear rate of 600 revolutions per minute;
(4) adding N, N-diacetyl-3-hydroxy propylamine, stirring until the product is transparent, and naturally cooling.
The starting materials used were the same as in example 1.
Application example 2:
the volume ratio of the spray cleaning agent for the lubricating grease of the train wheel pair bearing prepared according to the embodiment 1 of the invention to water in the first tank is 1: 25, placing the train wheel pair bearing to be cleaned in spraying cleaning equipment, adjusting the spraying pressure to be 0.3MPa, controlling the cleaning temperature to be 30 ℃, adjusting the running speed of a production line of the spraying cleaning equipment to start spraying cleaning, and controlling the effective spraying time of the train wheel pair bearing to be 5 minutes; tap water is added into the second tank, and the second tank is sprayed and rinsed for 1 minute and then dried by hot air. The cleaned train wheel has no grease stain residue on the bearing, and is bright and free of corrosion.

Claims (2)

1. The spray cleaning agent for the lubricating grease of the bearing of the train wheel is characterized by comprising the following raw materials in percentage by mass: 2-15% of potassium hydroxide or sodium hydroxide, 2-5% of a nonionic surfactant Plurafac LF-9000.5-5%, 11-10% of a nonionic surfactant Plurafac LF-9011%, 5-32% of a low-foaming wetting agent Marlox FK-860.5%, 10% of an alkaline low-foaming surfactant Berol LFG-611%, 26-15% of alkyl glycoside AG 62060.5%, 0.1-10% of N, N-diacetyl-3-hydroxypropyl amine and the balance of water.
2. The preparation method of the spray cleaning agent for the lubricating grease of the train wheel pair bearing as claimed in claim 1 is characterized by comprising the following steps in sequence:
(1) adding reaction water into a reaction kettle, adding potassium hydroxide or sodium hydroxide at normal temperature, and stirring until the reaction water is completely dissolved;
(2) sequentially adding a nonionic surfactant Plurafac LF-900, a nonionic surfactant Plurafac LF-901, a low-foam wetting agent Marlox FK-86 and an alkaline low-foam surfactant Berol LFG-61 into a reaction kettle, and stirring at a shear speed of 500-800 rpm for 4-6 minutes;
(3) adding alkyl glycoside AG6206, and stirring for 3-5 minutes at a shearing speed of 500-800 rpm;
(4) adding N, N-diacetyl-3-hydroxy propylamine, stirring until the product is transparent, and naturally cooling.
CN201911334351.5A 2019-12-23 2019-12-23 Train wheel pair bearing lubricating grease spray cleaning agent and preparation method thereof Pending CN111020608A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201911334351.5A CN111020608A (en) 2019-12-23 2019-12-23 Train wheel pair bearing lubricating grease spray cleaning agent and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201911334351.5A CN111020608A (en) 2019-12-23 2019-12-23 Train wheel pair bearing lubricating grease spray cleaning agent and preparation method thereof

Publications (1)

Publication Number Publication Date
CN111020608A true CN111020608A (en) 2020-04-17

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113122396A (en) * 2021-03-12 2021-07-16 大连传奇化工有限公司 Fabric surface porphyrin and conjugated double bond structure type stain remover and preparation method thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102399642A (en) * 2011-09-27 2012-04-04 英特沃斯(北京)科技有限公司 Neutral cleaning agent and preparation method thereof
CN103046059A (en) * 2012-12-17 2013-04-17 厦门科珑精细化工有限公司 Environment-friendly concentrated multifunctional metal cleaning agent and preparation method thereof
CN105419957A (en) * 2015-12-16 2016-03-23 广州立白企业集团有限公司 Glass cleaner composition added with cationic polymers
CN105802757A (en) * 2016-04-11 2016-07-27 广州立白企业集团有限公司 Method for enabling detergent composition to have small-range viscosity change in wide temperature range and detergent composition
CN108754521A (en) * 2018-05-09 2018-11-06 苏州捷德瑞精密机械有限公司 A kind of high-effective low foam rust-proof type metal cleaner and preparation method thereof
CN110592605A (en) * 2018-12-17 2019-12-20 江苏斯尔邦石化有限公司 Heavy oil stain cleaning agent for metal surface

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102399642A (en) * 2011-09-27 2012-04-04 英特沃斯(北京)科技有限公司 Neutral cleaning agent and preparation method thereof
CN103046059A (en) * 2012-12-17 2013-04-17 厦门科珑精细化工有限公司 Environment-friendly concentrated multifunctional metal cleaning agent and preparation method thereof
CN105419957A (en) * 2015-12-16 2016-03-23 广州立白企业集团有限公司 Glass cleaner composition added with cationic polymers
CN105802757A (en) * 2016-04-11 2016-07-27 广州立白企业集团有限公司 Method for enabling detergent composition to have small-range viscosity change in wide temperature range and detergent composition
CN108754521A (en) * 2018-05-09 2018-11-06 苏州捷德瑞精密机械有限公司 A kind of high-effective low foam rust-proof type metal cleaner and preparation method thereof
CN110592605A (en) * 2018-12-17 2019-12-20 江苏斯尔邦石化有限公司 Heavy oil stain cleaning agent for metal surface

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113122396A (en) * 2021-03-12 2021-07-16 大连传奇化工有限公司 Fabric surface porphyrin and conjugated double bond structure type stain remover and preparation method thereof

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Application publication date: 20200417

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