CN110863116A - Noble metal platinum purification device - Google Patents
Noble metal platinum purification device Download PDFInfo
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- CN110863116A CN110863116A CN201911046099.8A CN201911046099A CN110863116A CN 110863116 A CN110863116 A CN 110863116A CN 201911046099 A CN201911046099 A CN 201911046099A CN 110863116 A CN110863116 A CN 110863116A
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B11/00—Obtaining noble metals
- C22B11/04—Obtaining noble metals by wet processes
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/02—Apparatus therefor
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
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Abstract
The invention discloses a noble metal platinum purifying device which comprises a stirring cup, wherein a positioning clamping sheet is arranged on the inner side of the stirring cup, a baffle is placed on the positioning clamping sheet, a through hole is formed in the baffle, a stirrer is arranged on the baffle, a heating device is connected onto the stirring cup, a filter plate is arranged at the bottom of the stirring cup, a liquid outlet pipe is arranged at the bottom of the stirring cup, an adjusting control valve is arranged on the liquid outlet pipe, a sedimentation tank is arranged below the stirring cup, a sliding groove is formed in the sedimentation tank, a protection plate is arranged on the sedimentation tank, a liquid inlet hole is formed in the protection plate, a sampling hole is formed in the protection plate, and a groove is formed in the sedimentation tank. This noble metal platinum purification device dismantles comparatively conveniently, and the staff of being convenient for dismantles and clears up the device, and the equipment of being convenient for simultaneously uses, and can prevent dangerous solution spill to can control the velocity of flow of reaction liquid to a certain extent.
Description
Technical Field
The invention relates to the technical field of platinum purification, in particular to a noble metal platinum purification device.
Background
The platinum purification device is a kind of extraction equipment for extracting platinum from a material containing noble metal platinum, and the platinum-containing material is mostly dissolved by aqua regia during the extraction of the platinum, then precipitated by alkali liquor and finally burned.
In the extraction processes of gold and silver and the like, solid metal materials which are not easy to dissolve often contain a trace amount of noble metal platinum, and because the content of noble metals is rare, artificial purification is carried out frequently, various instruments are required to be used in the conventional artificial purification process, the purification device is not convenient to clean, the speed is low during dissolution, solution is required to be collected in the operation process for content detection, the added reaction solvent amount is determined, dangerous reagents are involved in the operation process, the operation is carried out by personnel with rich experience, and the solution is also inconvenient to transfer in the reaction process, so that the technology capable of improving the structure of the noble metal platinum purification device is urgently needed in the market, and the equipment is perfected.
Disclosure of Invention
The invention aims to provide a noble metal platinum purification device, which solves the problems that the existing purification device in the background art is inconvenient to clean by using various instruments, has low speed during dissolution, needs to collect solution for content detection in the operation process to determine the added reaction solvent amount, and needs to operate by personnel with rich experience because dangerous reagents are involved in the operation process, and is inconvenient to transfer the solution in the reaction process.
In order to achieve the purpose, the invention provides the following technical scheme: a noble metal platinum purification device comprises a stirring cup, a positioning card is arranged at the inner side of the stirring cup, a baffle is arranged on the positioning card, wherein,
the stirring cup is characterized in that a through hole is formed in the baffle plate, a stirrer is arranged on the baffle plate, a heating device is connected onto the stirring cup, a filter plate is arranged at the bottom of the stirring cup, a liquid outlet pipe is arranged at the bottom of the stirring cup, and an adjusting control valve is arranged on the liquid outlet pipe;
the stirring cup is characterized in that a sedimentation tank is arranged below the stirring cup, a sliding groove is formed in the sedimentation tank, a protection plate is arranged on the sedimentation tank, a liquid inlet hole is formed in the protection plate, a sampling hole is formed in the protection plate, a groove is formed in the sedimentation tank, a clamping strip is arranged on the sedimentation tank, a connecting block is arranged in the sedimentation tank, a buffer block is arranged in the sedimentation tank, and the buffer block is connected with the connecting block.
Preferably, the agitator includes connecting rod, first fixture block, second fixture block, bull stick, puddler, hand bull stick and gum cover, be provided with first fixture block on the connecting rod, be provided with the second fixture block on the connecting rod, be provided with the bull stick on the connecting rod, be connected through the bull stick between puddler and the connecting rod, the one end of connecting rod is provided with hand bull stick, be provided with the gum cover on the hand bull stick, and 75 contained angles are personally submitted with the level to the puddler.
Preferably, the first fixture block is located above the baffle, the second fixture block is located below the baffle, the radius of the connecting rod is smaller than that of the through hole, and the radii of the first fixture block and the second fixture block are both larger than that of the through hole.
Preferably, heating device is including heating urceolus, the connecting pipe of intaking, play water connecting pipe and connection card, one side of heating urceolus is provided with the connecting pipe of intaking, keeps away from the connecting pipe of intaking one side of heating urceolus is provided with the connecting pipe of going out water, the top of heating urceolus is connected with the connection card, and connects the card and be provided with altogether to individual connection card is about the connecting rod symmetry, and the size of connecting the card is identical with the size of stirring cup moreover, the internal diameter size of heating urceolus equals the external diameter size of stirring cup, the high sum of heating urceolus and connection card is less than the height of stirring cup.
Preferably, the adjusting control valve comprises a connecting outer sleeve, a flow hole, a connecting hole, a control rod, a control hole, an adjusting block, first threads, a fastening bolt and second threads, the flow hole is formed in the middle of the connecting outer sleeve, the connecting hole is formed in the connecting outer sleeve, the control rod is arranged in the connecting outer sleeve, the control hole is formed in the control rod, the adjusting block is arranged at one end of the control rod, the first threads are arranged on the control rod, the fastening bolt is connected onto the control rod, the second threads are arranged on the fastening bolt, and the control rod and the fastening bolt are in threaded connection through the first threads and the second threads.
Preferably, the radius of the control rod is equal to that of the connecting hole, the control hole and the outflow hole are correspondingly arranged, and the radius of the control hole is equal to that of the outflow hole.
Preferably, the protection plate and the sedimentation tank form sliding connection through the sliding groove, and the sum of the lengths of the protection plate and the connecting block is equal to the length of the sedimentation tank.
Compared with the prior art, the invention has the beneficial effects that: the noble metal platinum purification device is mainly designed for purifying platinum metal:
1. the stirring cup of the noble metal platinum purification device is provided with the baffle, and the baffle is connected with the stirrer, so that an operator can place the solution and the metal in the stirring cup during operation, and the dangerous solution is prevented from splashing to cause accidents by stirring through the stirrer, and the noble metal platinum purification device is suitable for being operated by personnel with less working experience;
2. the baffle plate of the noble metal platinum purification device is placed above the stirring cup, and the heating device is directly clamped on the stirring cup through the connecting clamping piece, so that the device is convenient to integrally disassemble, is convenient for workers to disassemble and clean, and is convenient to assemble and use;
3. the heating device connected through the connecting card is arranged outside the stirring cup of the noble metal platinum purification device, and the heating device realizes water bath heating by adding hot water from the water inlet connecting pipe, so that the reaction temperature can be effectively controlled, the reaction efficiency is accelerated, and the safety is ensured;
4. one side of the sedimentation tank of the precious metal platinum purification device, which is used for adding the precipitated alkali liquor, is provided with a connecting block and a buffer block, and meanwhile, the sedimentation tank is provided with a protection plate, so that the solution sputtering caused by adding the alkali liquor by an operator is prevented, and accidents are prevented;
5. a sampling hole is formed in the sedimentation tank of the precious metal platinum purification device, so that an operator can take out the solution in the sedimentation tank through the sampling hole before and after reaction for detection to determine the reaction condition and then determine the next operation;
6. the radius size of this noble metal platinum purification device's drain pipe equals with the feed liquor hole size on the sedimentation tank, can directly insert the drain pipe and put and operate on the feed liquor hole, prevents that solution from splashing, and the drain pipe is adjusted through the governing valve simultaneously, and the structure of governing valve is similar with current separating funnel governing valve structure, not only can control whether solution flows to can control the velocity of flow to a certain extent.
Drawings
FIG. 1 is a schematic cross-sectional view of the present invention;
FIG. 2 is a schematic view of a blender cup according to the present invention;
FIG. 3 is a schematic top view of the sedimentation tank without a clamping strip according to the present invention;
FIG. 4 is an enlarged view of part A of the present invention.
In the figure: 1. the stirring cup, 2, a positioning clamping piece, 3, a baffle, 4, a stirrer, 401, a connecting rod, 402, a first clamping block, 403, a second clamping block, 404, a rotating rod, 405, a stirring rod, 406, a hand-operated rotating rod, 407, a rubber sleeve, 5, a heating device, 501, a heating outer cylinder, 502, a water inlet connecting pipe, 503, a water outlet connecting pipe, 504, a connecting clamping block, 6, a filter plate, 7, a liquid outlet pipe, 8, a regulating valve, 801, a connecting outer sleeve, 802, a liquid outlet hole, 803, a connecting hole, 804, a control rod, 805, a control hole, 806, a regulating block, 807, a first thread, 808, a fastening bolt, 809, a second thread, 9, a sedimentation tank, 10, a sliding chute, 11, a protection plate, 12, a liquid inlet hole, 13, a sampling hole, 14, a groove, 15, a clamping strip, 16, a connecting block, 17, a buffering block, 18 and a.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-3, the present invention provides a technical solution: a precious metal platinum purification device comprises a stirring cup 1, a positioning card 2, a baffle 3, a stirrer 4, a heating device 5, a filter plate 6, a liquid outlet pipe 7, an adjusting valve 8, a sedimentation tank 9, a chute 10, a protection plate 11, a liquid inlet hole 12, a sampling hole 13, a groove 14, a card strip 15, a connecting block 16, a buffer block 17 and a perforation 18, wherein the positioning card 2 is arranged on the inner side of the stirring cup 1, the baffle 3 is placed on the positioning card 2,
the baffle plate 3 is provided with a through hole 18, the baffle plate 3 is provided with a stirrer 4, the stirrer 4 comprises a connecting rod 401, a first clamping block 402, a second clamping block 403, a rotating rod 404, a stirring rod 405, a hand-operated rotating rod 406 and a rubber sleeve 407, the connecting rod 401 is provided with the first clamping block 402, the connecting rod 401 is provided with the second clamping block 403, the connecting rod 401 is provided with the rotating rod 404, the stirring rod 405 and the connecting rod 401 are connected through the rotating rod 404, one end of the connecting rod 401 is provided with the hand-operated rotating rod 406, the hand-operated rotating rod 406 is provided with the rubber sleeve 407, the stirring rod 405 and the horizontal plane form an included angle of 75 degrees, so that the stirring is convenient to stir uniformly, the first clamping block 402 is positioned above the baffle plate 3, the second clamping block 403 is positioned below the baffle plate 3, the radius of the connecting rod 401 is smaller than that of the through hole 18, and the radii of the first clamping block 402 and the second clamping, be convenient for stirring and agitator 4 like this can reciprocate, be connected with heating device 5 on the stirring cup 1, heating device 5 is including heating urceolus 501, intake connecting pipe 502, play water connecting pipe 503 and connection card 504, one side of heating urceolus 501 is provided with intake connecting pipe 502, keeps away from intake connecting pipe 502 one side of heating urceolus 501 is provided with out water connecting pipe 503, the top of heating urceolus 501 is connected with connection card 504, and connects card 504 and be provided with 2 altogether to 2 connect card 504 are symmetrical about connecting rod 401, and the size of connecting card 504 is identical with the size of stirring cup 1 moreover, the internal diameter size of heating urceolus 501 equals the external diameter size of stirring cup 1, the height of heating urceolus 501 and connection card 504 with be less than the height of stirring cup 1, the loading and unloading of heating device 5 of being convenient for like this, the bottom of stirring cup 1 is provided with filter plate 6, the bottom of the stirring cup 1 is provided with a liquid outlet pipe 7, the liquid outlet pipe 7 is provided with an adjusting control valve 8, the adjusting control valve 8 comprises a connecting outer sleeve 801, an outflow hole 802, a connecting hole 803, a control rod 804, a control hole 805, an adjusting block 806, a first thread 807, a fastening bolt 808 and a second thread 809, the middle part of the connecting outer sleeve 801 is provided with the outflow hole 802, the connecting outer sleeve 801 is provided with the connecting hole 803, the connecting outer sleeve 801 is internally provided with the control rod 804, the control rod 804 is provided with the control hole 805, one end of the control rod 804 is provided with the adjusting block 806, the control rod 804 is provided with the first thread 807, the control rod 804 is connected with the fastening bolt 808, the fastening bolt 808 is provided with the second thread 809, and the control rod 804 and the fastening bolt 808 are in threaded connection through the first thread 807 and the second thread 809, the radius of the control rod 804 is equal to that of the connecting hole 803, the control hole 805 and the outflow hole 802 are correspondingly arranged, and the radius of the control hole 805 is equal to that of the outflow hole 802, so that the outflow of the stirring liquid can be adjusted;
the stirring cup 1's below is provided with sedimentation tank 9, spout 10 has been seted up on the sedimentation tank 9, be provided with guard plate 11 on the sedimentation tank 9, constitute sliding connection through spout 10 between guard plate 11 and the sedimentation tank 9, and the length sum of guard plate 11 and connecting block 16 equals the length of sedimentation tank 9, be convenient for like this to the inside clearance of sedimentation tank 9, and prevent solution sputtering when adding the solution, feed liquor hole 12 has been seted up on guard plate 11, sampling hole 13 has been seted up on guard plate 11, set up recess 14 on the sedimentation tank 9, be provided with card strip 15 on the sedimentation tank 9, be provided with connecting block 16 in the sedimentation tank 9, be provided with buffer block 17 in the sedimentation tank 9, just buffer block 17 and connecting block 16 are connected.
The working principle is as follows: before using the precious metal platinum purification device, firstly, an operator needs to simply know the structure of the whole precious metal platinum purification device, firstly, whether the device leaks liquid is checked, then, the dissolved liquid and the metal are put into the stirring cup 1, then, the baffle plate 3 is placed on the positioning clamping plate 2, then, the connecting clamping plate 504 is clamped on the stirring cup 1, hot water is led into the heating outer cylinder 501 from the water inlet connecting pipe 502, so that the heating device 5 heats the stirring cup 1, then, the rubber sleeve 407 on the hand-operated rotating rod 406 is held, the hand-operated rotating rod 406 is rotated to drive the connecting rod 401, the rotating rod 404 and the stirring rod 405 to rotate, the dissolved metal material is stirred, after the dissolution is completed, the adjusting block 806 is rotated, so that the control rod 804 rotates in the connecting hole 803, the control hole 805 is aligned with the outflow hole 802, the solution flows out from the filter plate 6 to the outflow pipe 7, the structure is similar to the outflow of, flow to sedimentation tank 9 from feed liquor hole 12 in, operating personnel accessible thief hole 13 sample detection this moment, after the detection is accomplished, pour into alkali lye from sedimentation tank 9 does not have protection board 11, alkali lye can flow into sedimentation tank 9 along connecting block 16 and buffer block 17, after the reaction, through thief hole 13 sample detection, can pour out the reactant in sedimentation tank 9, burn the processing to the sediment, the content of not making detailed description in this description belongs to the prior art that technical personnel known in the field.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (8)
1. A noble metal platinum purification device comprises a stirring cup (1), and is characterized in that: a positioning card (2) is arranged on the inner side of the stirring cup (1), a baffle (3) is arranged on the positioning card (2), wherein,
the stirring device is characterized in that a through hole (18) is formed in the baffle (3), a stirrer (4) is arranged on the baffle (3), a heating device (5) is connected to the stirring cup (1), a filter plate (6) is arranged at the bottom of the stirring cup (1), a liquid outlet pipe (7) is arranged at the bottom of the stirring cup (1), and an adjusting control valve (8) is arranged on the liquid outlet pipe (7);
the stirring cup is characterized in that a sedimentation tank (9) is arranged below the stirring cup (1), a sliding groove (10) is formed in the sedimentation tank (9), a protection plate (11) is arranged on the sedimentation tank (9), a liquid inlet hole (12) is formed in the protection plate (11), a sampling hole (13) is formed in the protection plate (11), a groove (14) is formed in the sedimentation tank (9), a clamping strip (15) is arranged on the sedimentation tank (9), a connecting block (16) is arranged in the sedimentation tank (9), a buffer block (17) is arranged in the sedimentation tank (9), and the buffer block (17) is connected with the connecting block (16).
2. The noble metal platinum purifying apparatus according to claim 1, wherein: agitator (4) are including connecting rod (401), first fixture block (402), second fixture block (403), bull stick (404), puddler (405), hand bull stick (406) and gum cover (407), be provided with first fixture block (402) on connecting rod (401), be provided with second fixture block (403) on connecting rod (401), be provided with bull stick (404) on connecting rod (401), be connected through bull stick (404) between puddler (405) and connecting rod (401), the one end of connecting rod (401) is provided with hand bull stick (406), be provided with gum cover (407) on hand bull stick (406), and puddler (405) personally submit 75 contained angles with the level.
3. The noble metal platinum purifying apparatus according to claim 2, wherein: the first fixture block (402) is located above the baffle (3), the second fixture block (403) is located below the baffle (3), the radius of the connecting rod (401) is smaller than that of the through hole (18), and the radii of the first fixture block (402) and the second fixture block (403) are larger than that of the through hole (18).
4. The noble metal platinum purifying apparatus according to claim 2, wherein: heating device (5) are including heating urceolus (501), connecting pipe (502) of intaking, go out water connecting pipe (503) and connection card (504), one side of heating urceolus (501) is provided with into water connecting pipe (502), keeps away from into water connecting pipe (502) one side of heating urceolus (501) is provided with out water connecting pipe (503), the top of heating urceolus (501) is connected with connection card (504), and connects card (504) and be provided with 2 altogether to 2 connect card (504) about connecting rod (401) symmetry, and the size of connecting card (504) is identical with the size of stirring cup (1), the internal diameter size of heating urceolus (501) equals the external diameter size of stirring cup (1), the sum of the height of heating urceolus (501) and connection card (504) is less than the height of stirring cup (1).
5. The noble metal platinum purifying apparatus according to claim 1, wherein: the adjusting control valve (8) comprises a connecting outer sleeve (801), an outflow hole (802), a connecting hole (803), a control rod (804), a control hole (805), an adjusting block (806), a first thread (807), a fastening bolt (808) and a second thread (809), the middle part of the connecting outer sleeve (801) is provided with an outflow hole (802), the connecting outer sleeve (801) is provided with a connecting hole (803), a control rod (804) is arranged in the connecting outer sleeve (801), a control hole (805) is arranged on the control rod (804), one end of the control rod (804) is provided with an adjusting block (806), the control rod (804) is provided with a first thread (807), the control rod (804) is connected with a fastening bolt (808), the fastening bolt (808) is provided with a second thread (809), and the control rod (804) and the fastening bolt (808) form a threaded connection through a first thread (807) and a second thread (809).
6. The noble metal platinum purifying apparatus according to claim 5, wherein: the radius of the control rod (804) is equal to that of the connecting hole (803), the positions of the control hole (805) and the outflow hole (802) are correspondingly arranged, and the radius of the control hole (805) is equal to that of the outflow hole (802).
7. The noble metal platinum purifying apparatus according to claim 1, wherein: the protection plate (11) and the sedimentation tank (9) are in sliding connection through the sliding groove (10), and the sum of the lengths of the protection plate (11) and the connecting block (16) is equal to the length of the sedimentation tank (9).
8. A method for purifying noble metal platinum is characterized by comprising the following steps: firstly, the whole precious metal platinum purification device needs to be simply understood in structure, an operator firstly checks whether the device leaks liquid, then the dissolved liquid and metal are put into the stirring cup 1, then the baffle plate 3 is placed on the positioning clamping plate 2, then the connecting clamping plate 504 is clamped on the stirring cup 1, hot water is led into the heating outer barrel 501 from the water inlet connecting pipe 502, the heating device 5 heats the stirring cup 1, then the rubber sleeve 407 on the hand-operated rotating rod 406 is held, the hand-operated rotating rod 406 is rotated to drive the connecting rod 401, the rotating rod 404 and the stirring rod 405 to rotate, the dissolved metal material is stirred, after the dissolution is completed, the adjusting block 806 is rotated to enable the control rod 804 to rotate in the connecting hole 803, the control hole 805 is aligned with the outflow hole 802, the solution flows out from the filter plate 6 to the outflow pipe 7, the structure is similar to the outflow of the solution control funnel, and flows into the sedimentation tank 9 from the liquid inlet hole 12 in, at this moment, the sampling hole 13 of operating personnel accessible sample detection, after the detection is accomplished, pour into alkali lye from the no protection plate 11 department of sedimentation tank 9, alkali lye can flow into sedimentation tank 9 along connecting block 16 and buffer block 17, after the reaction, through sampling hole 13 sample detection, can pour out the inside reactant of sedimentation tank 9, burn the processing to the sediment.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911046099.8A CN110863116B (en) | 2019-10-30 | 2019-10-30 | Noble metal platinum purification device |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911046099.8A CN110863116B (en) | 2019-10-30 | 2019-10-30 | Noble metal platinum purification device |
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| Publication Number | Publication Date |
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| CN110863116A true CN110863116A (en) | 2020-03-06 |
| CN110863116B CN110863116B (en) | 2022-02-15 |
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| CN201911046099.8A Active CN110863116B (en) | 2019-10-30 | 2019-10-30 | Noble metal platinum purification device |
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| CN114214697A (en) * | 2021-09-10 | 2022-03-22 | 安徽富乐德科技发展股份有限公司 | Aluminum alloy anodic oxidation electrolyte and anodic oxidation system process |
| CN115125398A (en) * | 2022-08-09 | 2022-09-30 | 顾秀华 | Preparation process of semi-metallic compound of metal platinum |
| CN115522062A (en) * | 2022-05-24 | 2022-12-27 | 范利华 | Metal solution gold refining processing device |
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| CN110863116B (en) | 2022-02-15 |
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