CN220367071U - Calcium fluoride content measuring device - Google Patents
Calcium fluoride content measuring device Download PDFInfo
- Publication number
- CN220367071U CN220367071U CN202321649251.3U CN202321649251U CN220367071U CN 220367071 U CN220367071 U CN 220367071U CN 202321649251 U CN202321649251 U CN 202321649251U CN 220367071 U CN220367071 U CN 220367071U
- Authority
- CN
- China
- Prior art keywords
- tank
- calcium fluoride
- stirring
- motor
- rod
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 title claims abstract description 34
- 229910001634 calcium fluoride Inorganic materials 0.000 title claims abstract description 34
- 238000003756 stirring Methods 0.000 claims abstract description 48
- 230000007246 mechanism Effects 0.000 claims abstract description 29
- 238000010438 heat treatment Methods 0.000 claims abstract description 14
- 238000004090 dissolution Methods 0.000 claims abstract description 13
- 230000007306 turnover Effects 0.000 claims abstract description 7
- 238000001914 filtration Methods 0.000 claims description 14
- 238000007599 discharging Methods 0.000 claims description 6
- 238000003466 welding Methods 0.000 claims description 6
- 230000002146 bilateral effect Effects 0.000 claims description 3
- 239000012535 impurity Substances 0.000 abstract description 9
- 238000000034 method Methods 0.000 abstract description 6
- 238000005259 measurement Methods 0.000 abstract description 4
- 239000003814 drug Substances 0.000 abstract description 3
- 230000008569 process Effects 0.000 abstract description 3
- 239000007787 solid Substances 0.000 abstract description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 9
- 239000000243 solution Substances 0.000 description 8
- 244000309464 bull Species 0.000 description 5
- 239000007788 liquid Substances 0.000 description 4
- 239000011259 mixed solution Substances 0.000 description 4
- 239000002245 particle Substances 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- IXAIKEKMZXIEKF-UHFFFAOYSA-N S(O)(O)(=O)=O.Cl.B(O)(O)O Chemical compound S(O)(O)(=O)=O.Cl.B(O)(O)O IXAIKEKMZXIEKF-UHFFFAOYSA-N 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- JGIATAMCQXIDNZ-UHFFFAOYSA-N calcium sulfide Chemical compound [Ca]=S JGIATAMCQXIDNZ-UHFFFAOYSA-N 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 230000000873 masking effect Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000012086 standard solution Substances 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The utility model discloses a calcium fluoride content measuring device, in particular to the field of sample measuring devices, which comprises a dissolving tank, wherein a bracket is welded at the top end of the dissolving tank, a stirring mechanism is arranged on the bracket, a first feed inlet and a second feed inlet are symmetrically arranged on two sides of the stirring mechanism, the top end of the stirring mechanism is connected with a heating wire, the heating wire is connected with a heater, a valve pipe is welded at the bottom end of the dissolving tank, a filter tank is arranged at the bottom end of the valve pipe, a turnover mechanism is arranged in the filter tank, a discharge pipe is connected at the middle of the bottom end of the filter tank, and a plurality of supporting legs are arranged at the bottom end of the filter tank. The method has the advantages that the dissolution efficiency of impurities in the calcium fluoride sample can be improved, the impurities are dissolved more thoroughly, the solid sample formed after dissolution is filtered and collected conveniently, meanwhile, the whole dissolution process is a closed reaction, scalding caused by manual operation and medicine splashing on the skin of an operator are avoided, and the measurement safety is improved.
Description
Technical Field
The utility model relates to the technical field of sample measuring devices, in particular to a calcium fluoride content measuring device.
Background
The method for measuring calcium fluoride includes such steps as treating specimen with calcium-contained acetic acid solution to dissolve calcium carbonate and calcium sulfide, filtering to obtain insoluble dregs, dissolving with boric acid-sulfuric acid hydrochloride mixture, filtering, adding potassium hydroxide solution to pH value of 13 or more, using glycol as masking agent, mixing with CMP indicator, titration with EDTA standard solution, and quantitatively calculating calcium fluoride content.
However, when the impurities in the calcium fluoride sample are dissolved, the existing reaction is generally carried out through a beaker, and the manual operation is carried out by manpower, so that the thoroughness of the dissolution is influenced, the accuracy of the content of the follow-up calcium fluoride is poor, and the operation safety is low.
Disclosure of Invention
The technical scheme of the utility model aims at solving the technical problem of overlarge singleness in the prior art and provides a solution which is obviously different from the prior art. In order to overcome the above-mentioned drawbacks of the prior art, the present utility model provides a calcium fluoride content measuring device, so as to solve the above-mentioned problems in the prior art.
In order to achieve the above purpose, the present utility model provides the following technical solutions: the utility model provides a calcium fluoride content measuring device, including dissolving the jar, it has the support to dissolve jar top welding, installs rabbling mechanism on the support, and rabbling mechanism bilateral symmetry is provided with first feed inlet and second feed inlet, and the rabbling mechanism top is connected with the heater strip, and the heater strip is connected with the heater, dissolves jar bottom welding and has the valve pipe, and the filter tank is installed to valve pipe bottom, and filter tank internally mounted has tilting mechanism, and filter tank bottom middle part is connected with the discharging pipe, and a plurality of landing legs are installed to filter tank bottom.
Preferably, a supporting plate is welded on one side of the filter tank, and the top end of the supporting plate is connected with one end of the turnover mechanism.
Preferably, the bottom end inside the filter tank is of a conical structure, and a valve is arranged on the connected discharging pipe.
Preferably, the stirring mechanism comprises a first motor, the first motor being mounted on the support.
The first bull stick, first bull stick top is connected with first motor.
The gear is arranged at the bottom end of the first rotating rod.
The toothed ring is connected to one side of the gear in a meshed mode, and the toothed ring is positioned in the middle of the top end of the dissolving tank.
Stirring rod, stirring rod welding is in the ring gear bottom, and the stirring rod is pegged graft inside the dissolving tank.
And each stirring blade is uniformly arranged on a stirring rod in the dissolving tank.
Preferably, the stirring rod is of a hollow structure, and the heating wires are inserted into the stirring rod and connected with each stirring blade.
Preferably, the tilting mechanism comprises a second motor mounted on the support plate.
And one end of the second rotating rod is connected with the second motor, and the other end of the second rotating rod is inserted into the filter tank.
The filter plate, the filter plate setting is in the filtration jar, and filter plate edge and filtration jar inner wall sliding engagement to and filter plate one end and second bull stick end connection.
And one end of the supporting rod is connected with the other end of the filter plate, and the other end of the supporting rod is movably inserted into the filter tank.
The utility model has the technical effects and advantages that:
1. through the arrangement of the first motor, the first rotating rod, the gear, the toothed ring, the stirring rod, the stirring blade, the heater and the heating wire, compared with the prior art, when sundries in a calcium fluoride sample are dissolved, the mixed solution can be heated and stirred at the same time, so that the calcium fluoride sample and the solution are fully mixed, the reaction rate is improved, impurities in the calcium fluoride sample react more thoroughly, the measurement accuracy of the calcium fluoride content is improved, meanwhile, the whole dissolution process is a closed reaction, scalding caused by manual operation is avoided, medicines are splashed on the skin of an operator, and the measurement safety is improved;
2. through the setting of second motor, second bull stick, filter plate and branch, compare with prior art, can filter the solution after the reaction to realize solid-liquid separation, thereby conveniently retrieve the granule after dissolving in the calcium oxide sample, thereby conveniently carry out follow-up survey operation.
Drawings
Fig. 1 is a schematic diagram of the overall structure of the present utility model.
Fig. 2 is a schematic side view of the present utility model.
Fig. 3 is a schematic structural view of the stirring mechanism of the present utility model.
Fig. 4 is a schematic structural view of the turnover mechanism of the present utility model.
The reference numerals are: 1. a dissolving tank; 2. a filter tank; 3. a support leg; 4. a bracket; 5. a stirring mechanism; 501. a first motor; 502. a first rotating lever; 503. a gear; 504. a toothed ring; 505. a stirring rod; 506. stirring the leaves; 6. a heater; 7. a heating wire; 8. a first feed port; 9. a valve tube; 10. a support plate; 11. a turnover mechanism; 1101. a second motor; 1102. a second rotating rod; 1103. a filter plate; 1104. a support rod; 12. a discharge pipe; 13. and a second feed inlet.
Detailed Description
The following description of the embodiments of the present utility model will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present utility model, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the utility model without making any inventive effort, are intended to be within the scope of the utility model.
The utility model provides a calcium fluoride content measuring device as shown in figures 1-4, including dissolving tank 1, dissolving tank 1 top welding has support 4, install rabbling mechanism 5 on the support 4, rabbling mechanism 5 bilateral symmetry is provided with first feed inlet 8 and second feed inlet 13, the rabbling mechanism 5 top is connected with heater strip 7, heater strip 7 is connected with heater 6, dissolving tank 1 bottom welding has valve pipe 9, filtration jar 2 is installed to valve pipe 9 bottom, filtration jar 2 internally mounted has tilting mechanism 11, filtration jar 2 bottom middle part is connected with discharging pipe 12, a plurality of landing legs 3 are installed to filtration jar 2 bottom.
As shown in fig. 1, a supporting plate 10 is welded on one side of the filter tank 2, and the top end of the supporting plate 10 is connected with one end of a turnover mechanism 11, so as to support and fix the second motor 1101.
As shown in figure 1, the bottom end of the interior of the filter tank 2 is in a conical structure, and a valve is arranged on a connected discharging pipe 12, so that liquid and solid in the filter tank 2 can be discharged more thoroughly, and residues are prevented from being generated.
As shown in fig. 3, the stirring mechanism 5 includes a first motor 501, where the first motor 501 is mounted on the support 4, and the first motor 501 operates to rotate back and forth, so that the toothed ring 504 rotates within an included angle of 135 ° to prevent the heating wire 7 from twisting, thereby improving the service life of the heating wire 7.
The first rotating rod 502, the top of the first rotating rod 502 is connected with the first motor 501.
The gear 503, the gear 503 is installed at the bottom end of the first rotating rod 502.
The toothed ring 504, the toothed ring 504 is connected with one side of the gear 503 in a meshing way, and the toothed ring 504 is positioned in the middle of the top end of the dissolution tank 1.
Stirring rod 505, stirring rod 505 welds in ring gear 504 bottom, and stirring rod 505 peg graft in dissolving tank 1 inside.
A plurality of stirring blades 506, each stirring blade 506 being uniformly mounted on a stirring rod 505 inside the dissolution tank 1.
As shown in fig. 2, the stirring rod 505 is in a hollow structure, and the heating wire 7 is inserted into the stirring rod 505 and connected with each stirring blade 506, so that the heating wire 7 is installed, and the heating wire 7 is connected with each stirring blade 506, so that the stirring blades 506 are stirred and simultaneously have a heating function, impurities in a calcium fluoride sample are improved, and calcium-containing acetic acid solution can fully react, so that impurities can be thoroughly dissolved.
As shown in fig. 4, the tilting mechanism 11 includes a second motor 1101, and the second motor 1101 is mounted on the support plate 10.
And one end of the second rotating rod 1102 is connected with the second motor 1101, and the other end of the second rotating rod 1102 is inserted into the filter tank 2.
The filter plate 1103, filter plate 1103 setting is in filtering jar 2, and filter plate 1103 edge and filter jar 2 inner wall sliding engagement to and filter plate 1103 one end and second bull stick 1102 end connection, so as to carry out solid-liquid separation, thereby retrieve the residual calcium fluoride granule in the calcium fluoride sample after dissolving, thereby make things convenient for follow-up survey.
And one end of the support rod 1104 is connected with the other end of the filter plate 1103, and the other end of the support rod 1104 is movably inserted into the filter tank 2.
The working principle of the utility model is as follows: when the calcium fluoride content measuring device is used for measuring the content of calcium fluoride, a quantitative calcium fluoride sample is poured into the dissolution tank 1 from the first feed inlet 8, meanwhile, a sample is poured into the dissolution tank 1 from the second feed inlet 13 by using a calcium-containing acetic acid solution, then the heater 6 is started, heat generated by the heating wire 7 conducts heat to the stirring blade 506 on the stirring rod 505, the first motor 501 operates, the first rotating rod 502 rotates back and forth, the gear 503 drives the toothed ring 504 to rotate back and forth, the stirring rod 505 welded at the bottom end of the toothed ring 504 rotates back and forth along with the rotation, the stirring blade 506 stirs the mixed solution, the state of stirring while heating is realized, the calcium fluoride sample is fully mixed in the solution, and impurities in the calcium fluoride sample fully react;
after the reaction is finished, the valve pipe 9 is opened, the mixed solution in the dissolving tank 1 enters the filter tank 2, the valve on the discharge pipe 12 is opened, the mixed solution is filtered through the filter plate 1103, the waste liquid is discharged from the discharge pipe 12, the calcium fluoride particles are positioned on the filter plate 1103, the second motor 1101 is started when the discharge pipe 12 does not flow out any more, the second rotating rod 1102 drives the filter plate 1103 to rotate, the filter plate 1103 is turned over, the calcium fluoride particles are poured out from the discharge pipe 12, the poured calcium fluoride particles are taken in, and the subsequent test operation is continued.
The method has the advantages that the dissolution efficiency of impurities in the calcium fluoride sample can be improved, the impurities are dissolved more thoroughly, the solid sample formed after dissolution is filtered and collected conveniently, meanwhile, the whole dissolution process is a closed reaction, scalding caused by manual operation and medicine splashing on the skin of an operator are avoided, and the measurement safety is improved.
The foregoing description of the preferred embodiments of the utility model is not intended to limit the utility model to the precise form disclosed, and any such modifications, equivalents, and alternatives falling within the spirit and principles of the utility model are intended to be included within the scope of the utility model.
Claims (6)
1. The utility model provides a calcium fluoride content measuring device, includes dissolving tank (1), its characterized in that: the utility model discloses a dissolving tank, including dissolving tank (1), support (4), stirring mechanism (5) are installed on support (4), stirring mechanism (5) bilateral symmetry is provided with first feed inlet (8) and second feed inlet (13), stirring mechanism (5) top is connected with heater strip (7), heater strip (7) are connected with heater (6), dissolving tank (1) bottom welding has valve pipe (9), filtration jar (2) are installed to valve pipe (9) bottom, filtration jar (2) internally mounted has tilting mechanism (11), filtration jar (2) bottom middle part is connected with discharging pipe (12), a plurality of landing legs (3) are installed to filtration jar (2) bottom.
2. The calcium fluoride content measuring apparatus according to claim 1, wherein: a supporting plate (10) is welded on one side of the filtering tank (2), and the top end of the supporting plate (10) is connected with one end of the turnover mechanism (11).
3. The calcium fluoride content measuring apparatus according to claim 1, wherein: the bottom end inside the filter tank (2) is of a conical structure, and a valve is arranged on a connected discharging pipe (12).
4. The calcium fluoride content measuring apparatus according to claim 1, wherein: the stirring mechanism (5) comprises a first motor (501), and the first motor (501) is arranged on the bracket (4);
the top end of the first rotating rod (502) is connected with the first motor (501);
the gear (503) is arranged at the bottom end of the first rotating rod (502);
the toothed ring (504) is connected to one side of the gear (503) in a meshing manner, and the toothed ring (504) is positioned in the middle of the top end of the dissolution tank (1);
the stirring rod (505) is welded at the bottom end of the toothed ring (504), and the stirring rod (505) is inserted into the dissolving tank (1);
and a plurality of stirring blades (506), wherein each stirring blade (506) is uniformly arranged on a stirring rod (505) positioned in the dissolving tank (1).
5. The calcium fluoride content measuring apparatus according to claim 4, wherein: the stirring rod (505) is of a hollow structure, and the heating wire (7) is inserted into the stirring rod (505) and connected with each stirring blade (506).
6. The calcium fluoride content measuring apparatus according to claim 1, wherein: the turnover mechanism (11) comprises a second motor (1101), and the second motor (1101) is arranged on the supporting plate (10);
one end of the second rotating rod (1102) is connected with the second motor (1101), and the other end of the second rotating rod (1102) is inserted into the filter tank (2);
the filter plate (1103) is arranged in the filter tank (2), the edge of the filter plate (1103) is in sliding connection with the inner wall of the filter tank (2), and one end of the filter plate (1103) is connected with the end of the second rotating rod (1102);
and one end of the supporting rod (1104) is connected with the other end of the filter plate (1103), and the other end of the supporting rod (1104) is movably inserted into the filter tank (2).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321649251.3U CN220367071U (en) | 2023-06-27 | 2023-06-27 | Calcium fluoride content measuring device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321649251.3U CN220367071U (en) | 2023-06-27 | 2023-06-27 | Calcium fluoride content measuring device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN220367071U true CN220367071U (en) | 2024-01-19 |
Family
ID=89517992
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321649251.3U Active CN220367071U (en) | 2023-06-27 | 2023-06-27 | Calcium fluoride content measuring device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN220367071U (en) |
-
2023
- 2023-06-27 CN CN202321649251.3U patent/CN220367071U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN114184416A (en) | Soil pollution detection handles integrative device | |
| CN220367071U (en) | Calcium fluoride content measuring device | |
| CN215995716U (en) | Sedimentation tank for sewage treatment | |
| CN110863116A (en) | Noble metal platinum purification device | |
| CN113184970A (en) | High waste liquid automated inspection classification device for chemistry experiments of security | |
| CN117269091B (en) | System and method for rapidly measuring iodine value of activated carbon | |
| CN209481355U (en) | A kind of liquid waste treating apparatus | |
| CN210635747U (en) | Waste liquid treatment device | |
| CN216629945U (en) | Solid-liquid separation device for mucosa extract | |
| CN111999414B (en) | Device and method for detecting pesticide and veterinary drug residues in food | |
| CN212067810U (en) | Traditional chinese medicine concentrator and traditional chinese medicine extraction system | |
| CN221148244U (en) | Soil detection dissolving equipment | |
| CN112535970B (en) | Waste liquid treatment device | |
| CN209061039U (en) | A kind of automatic material mixer | |
| CN215086547U (en) | High-efficient finish surge tank | |
| CN221572002U (en) | Soil detection is with dissolving equipment | |
| CN213913380U (en) | Automatic reagent feeding equipment for chemical production | |
| CN221412929U (en) | Raw material blending detection tank | |
| CN219777185U (en) | Sampling device for agricultural product detection | |
| CN220633904U (en) | Stirring mechanism capable of assisting dissolution | |
| CN218642582U (en) | Promote water softening treatment ware of medicament mixed effect | |
| CN218774639U (en) | In-vitro diagnostic reagent mixing equipment | |
| CN215640472U (en) | Soil detection dissolving equipment | |
| CN218774635U (en) | Automatic blending device for adding dissolved mother liquor in alumina production | |
| CN213761787U (en) | Heavy metal ion trapping agent proportioning device |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |