CN110862806A - Electronic device cooling liquid and preparation method thereof - Google Patents
Electronic device cooling liquid and preparation method thereof Download PDFInfo
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Abstract
The invention discloses an electronic device cooling liquid and a preparation method thereof, wherein the electronic device cooling liquid comprises the following components in percentage by mass: 99.5 to 99.9 percent of base oil and 0.1 to 0.5 percent of antioxidant; base oil viscosity μ: mu is more than 30 and less than or equal to 40 cst. The cooling liquid for the electronic device comprises the following components in percentage by mass: 99.0 to 99.9 percent of base oil, 0.005 to 0.9 percent of dispersant and 0.005 to 0.5 percent of antioxidant; base oil viscosity μ: mu is more than or equal to 5 and less than or equal to 30cst, and mu is more than 40 and less than or equal to 50 cst. The cooling liquid with different formula ratios improves partial performance indexes of insulativity, fire resistance, fluidity, loss and corrosivity, and improves the overall comprehensive performance, namely the cooling liquid with different formula ratios has higher flash point and breakdown voltage, and the insulativity and the fire resistance are good; the viscosity is suitable, and the requirement of spraying liquid cooling flow is met; the evaporation loss is low, and the loss is small; has low acid value and low corrosivity.
Description
Technical Field
The invention relates to an electronic device cooling liquid and a preparation method thereof.
Background
With the rapid development of the information-oriented society of China and the rise of industries such as cloud computing and the Internet of things, the computer technology enters a rapid development stage, and the performance requirements of people on IT equipment are higher and higher. With the performance improvement of IT devices and the development trend of high integration and miniaturization of electronic devices, the power consumption of IT devices is increased, so that the heat dissipation problem is more prominent.
At present, the commonly used heat dissipation mode of the electronic device is air-cooled heat dissipation, namely air is used as a cooling medium to cool the electronic device, but the traditional air-cooled heat dissipation cannot meet the heat dissipation requirement along with the continuous rising of the power consumption and the integration level of the electronic device. Liquid cooling heat dissipation is mainly to take away waste heat generated by a heating element through direct contact of cooling liquid. The heat carrying capacity of the working medium, which is reflected by the product of the density and the specific heat of the cooling liquid, is nearly 2000 times higher than that of air-cooled heat dissipation, so the liquid-cooled heat dissipation becomes the mainstream technology of heat dissipation in the future.
The liquid cooling heat dissipation comprises an immersion type liquid cooling and a spraying type liquid cooling, wherein the spraying type liquid cooling adopts insulating cooling liquid to spray on the heating electronic device to take away waste heat of the electronic device, so that the purpose of quickly dissipating heat of the electronic device is achieved. Because the cooling liquid directly contacts with the electronic device and is suitable for a relatively open spraying liquid cooling system, higher requirements are provided for the insulativity, the liquidity, the volatility, the chemical stability and the like of the cooling liquid. At present, the IT equipment is cooled by commonly used organic fluoride, but the organic fluoride has high cost and high density, has a certain destructive effect on the environment and influences the popularization and the application of the organic fluoride. Common mineral oil is also used as the cooling liquid, but the common mineral oil has poor insulating effect, relatively high viscosity and poor fluidity.
Disclosure of Invention
The first object of the present invention is to provide a coolant for electronic devices, which is improved in some of the performance indexes of insulation, fire resistance, fluidity, wear and corrosion, and improved in the overall performance.
The first object of the invention is achieved by the following technical measures:
the electronic device cooling liquid is characterized by comprising the following components in percentage by mass: 99.5 to 99.9 percent of base oil and 0.1 to 0.5 percent of antioxidant; viscosity of base oil μ: mu is more than 30 and less than or equal to 40 cst.
The electronic device cooling liquid is characterized by comprising the following components in percentage by mass:
99.0 to 99.9 percent of base oil, 0.005 to 0.9 percent of dispersant and 0.005 to 0.5 percent of antioxidant; viscosity of base oil μ: mu is more than or equal to 5 and less than or equal to 30cst or mu is more than 40 and less than or equal to 50 cst;
the sum of the contents of the components is 100 percent.
The base oil is dimethyl silicone oil, natural ester oil or synthetic ester oil and the like.
The dispersant is polyethylene glycol or polyglycerol fatty acid ester and the like.
The antioxidant is one or the combination of more than two of 2, 6-di-tert-butyl-p-cresol, antioxidant 1076 and alkyl diphenylamine.
The second purpose of the invention is to provide a preparation method of the cooling liquid for the electronic device.
The second object of the invention is achieved by the following technical measures:
the preparation method of the cooling liquid for the electronic device is characterized by comprising the following steps:
s1, respectively weighing the following components in percentage by mass:
99.5 to 99.9 percent of base oil and 0.1 to 0.5 percent of antioxidant; viscosity of base oil μ: mu is more than 30 and less than or equal to 40 cst;
s2, mixing the base oil weighed in the step S1 and an antioxidant, heating and stirring the mixture until the mixture is transparent, and then cooling the mixture to room temperature;
and S3, filtering the solution obtained in the step S2 to obtain the electronic device cooling liquid.
The preparation method of the cooling liquid for the electronic device is characterized by comprising the following steps:
s1, respectively weighing the following components in percentage by mass:
99.0 to 99.9 percent of base oil, 0.005 to 0.9 percent of dispersant and 0.005 to 0.5 percent of antioxidant; viscosity of base oil μ: mu is more than or equal to 5 and less than or equal to 30cst or mu is more than 40 and less than or equal to 50 cst;
the sum of the contents of the components is 100 percent;
s2, mixing the base oil weighed in the step S1 and an antioxidant, heating and stirring the mixture until the mixture is transparent, and then cooling the mixture to room temperature;
s3, adding the dispersant weighed in the step S1 into the solution obtained in the step S2, and stirring until the dispersant is completely dissolved;
and S4, filtering the solution obtained in the step S3 to obtain the electronic device cooling liquid.
In the step S2, the heating temperature is 50-60 ℃.
Compared with the prior art, the invention has the following remarkable effects:
the base oil and the antioxidant or the base oil, the dispersant and the antioxidant are used as raw materials, wherein the base oil can provide a liquid cooling environment for an electronic device, and the requirements of insulation and heat conduction are met; the dispersing agent can improve the volatility of the cooling liquid, balance the fluidity, and fuse other components of the cooling liquid to form uniform liquid, thereby improving the stability; the antioxidant can improve the chemical stability of the cooling liquid. The cooling liquid with different formula ratios can improve partial performance indexes of insulating property, fireproof property, fluidity, loss and corrosivity, and improve the overall comprehensive performance, namely the cooling liquid with different formula ratios has higher flash point and breakdown voltage, and the insulating property and the fireproof property are good; the spraying liquid has proper viscosity, and can meet the flowing requirement of spraying liquid cooling; the evaporation loss is low, and the loss is small in the using process; has a low acid value, resulting in low corrosivity.
Detailed Description
The invention is further illustrated by the following specific examples and specific applications. For the person skilled in the art, without departing from the inventive concept, several changes, improvements and modifications can be made, which shall also be regarded as the protective scope of the invention.
Example 1
The cooling liquid for the electronic device comprises the following components in percentage by mass: 99.0 to 99.9 percent of base oil, 0.005 to 0.9 percent of dispersant and 0.005 to 0.5 percent of antioxidant; viscosity of base oil μ: mu is more than or equal to 5 and less than or equal to 30cst or mu is more than 40 and less than or equal to 50 cst; the sum of the contents of the components is 100 percent.
In the embodiment, the base oil is dimethyl silicone oil with the viscosity of 20cst, and the mass percent is 99.0 percent; the dispersant is polyethylene glycol, and the mass percent of the polyethylene glycol is 0.9%; the antioxidant adopts 2, 6-di-tert-butyl-p-cresol, and the mass percent of the antioxidant is 0.1 percent.
The preparation method of the electronic device cooling liquid specifically comprises the following steps:
s1, respectively weighing the following components in percentage by mass:
99.0 percent of dimethyl silicone oil, 0.9 percent of polyethylene glycol and 0.1 percent of 2, 6-di-tert-butyl-p-cresol;
s2, mixing the dimethyl silicone oil weighed in the step S1 and the 2, 6-di-tert-butyl-p-cresol, heating to 60 ℃, stirring until the mixture is transparent, and then cooling to room temperature of 25 ℃;
s3, adding the polyethylene glycol weighed in the step S1 into the solution obtained in the step S2, and stirring until the polyethylene glycol is completely dissolved;
and S4, filtering the solution obtained in the step S3 to obtain the electronic device cooling liquid.
Example 2
In this embodiment, the base oil is a natural ester oil with a viscosity of 30cst, the dispersant is a polyglycerol ester, the dispersant is 0.495% by mass, and the antioxidant is an antioxidant 1076, which is β - (3, 5-di-tert-butyl-4-hydroxyphenyl) n-octadecyl propionate, and the mass percentage of the antioxidant is 0.005%.
The preparation method of the electronic device cooling liquid in this example is the same as that in example 1 (the steps are the same, and only the specific raw materials and mass percentages are different), and details are not repeated. The subsequent steps of preparing the electronic device cooling liquid of examples 3 to 7 were the same as in example 1.
Example 1 and example 2 the cooling fluid and conventional mineral oil performance index tests were compared as follows:
performance index | Common mineral oil | Example 1 | Example 2 | Test standard |
Viscosity of the oil | 26.5 | 23.5 | 36 | GB/T 265 |
Flash point. C | 185 | 245 | 319 | GB/T |
Breakdown voltage KV | 25 | 71.8 | 54.4 | GB/T 507 |
Loss by weight of evaporation | 1.40% | 1.85% | 1.18% | GB/T 7325 |
Acid value mgKOH/g | 0.02 | 0.01 | 0.03 | GB/T7304 |
(Table 1)
As can be seen from Table 1, the cooling liquid in example 1 has a viscosity of 23.5, which meets the flow requirement of spraying liquid cooling, but the lower the viscosity, the higher the volatility, the higher the loss and the easy fire-fighting hazard; the flash point and the breakdown voltage of the cooling liquid in the embodiment 1 are much higher than those of common mineral oil, which shows that the insulating property and the fireproof property are greatly improved; the evaporation loss of the cooling liquid in the embodiment 1 is slightly larger than that of the common mineral oil, and the loss is slightly increased; the acid value of the cooling liquid of example 1 was lower than that of ordinary mineral oil, and the corrosiveness was reduced. As can be seen,
the overall performance of example 1 is better improved compared to conventional mineral oils.
The viscosity of the cooling liquid in the embodiment 2 is 36, the flowing requirement of spraying liquid cooling is met, compared with the embodiment 1, the viscosity is increased, the volatility is reduced, the loss is reduced, the fire-fighting hidden danger is not easy to generate, but if the viscosity is too high, the pumping power of the system needs to be improved, and thus the energy-saving and environment-friendly requirements are not met; in the embodiment 2, the flash point and the breakdown voltage of the cooling liquid are much higher than those of common mineral oil, which shows that the insulating property and the fireproof property are greatly improved; in the embodiment 2, the evaporation loss of the cooling liquid is less than that of common mineral oil, and the loss is reduced; the acid value of the cooling liquid of example 2 is slightly lower than that of the common mineral oil, and the corrosiveness is slightly higher. It can be seen that the overall performance of example 2 is better improved compared to conventional mineral oils.
Example 1 and example 2 coolant heat rejection parameters are as follows:
(Table 2)
As can be seen from table 2, when the cooling liquids of example 1 and example 2 are used to cool the electronic device, compared to the conventional air cooling mode, the cooling liquids of example 1 and example 2 can obtain a lower temperature difference, which indicates that the cooling liquid has a significantly higher ability to remove heat from the electronic device (e.g., GPU) than the conventional air cooling.
Example 3
The concrete raw materials used in the embodiment are the same as those used in the embodiment 1, and the mass percentages are different. In this example, the viscosity of 20cst dimethicone was 99.4% by mass, the polyethylene glycol was 0.595% by mass, and the 2, 6-di-t-butyl-p-cresol was 0.005% by mass.
Example 4
The example is the same as the example 1 in the specific raw materials used for the three components, the mass percentages are different, and the viscosity of the dimethyl silicone oil is 50 cst. In this example, the mass percent of the dimethylsilicone oil was 99.9%, the mass percent of the polyethylene glycol was 0.005%, and the mass percent of the 2, 6-di-tert-butyl-p-cresol was 0.005%.
Example 5
The specific raw materials used in this example are the same as those used in example 2, but the mass percentages are different. In this example, the viscosity of the natural ester oil was 30cst, and the mass percentages were 99.9%, 0.005%, and 0.005%, respectively, of the polyglycerin fatty acid ester and the antioxidant 1076, respectively.
Example 6
In the embodiment, the base oil is synthetic ester oil with the viscosity of 30cst, and the mass percent of the synthetic ester oil is 99.5%; the dispersant is polyglycerol fatty acid ester with the mass percent of 0.495%; the antioxidant adopts antioxidant 1076 and alkyl diphenylamine, and the mass percent is 0.005%.
Example 7
The present example was conducted using the same raw materials as those used in example 6, but in different mass percentages. In this example, the synthetic ester oil accounts for 99.9% by mass, the polyglycerin fatty acid ester accounts for 0.005% by mass, and the antioxidant 1076+ the alkyl diphenylamine accounts for 0.005% by mass.
Example 8
The cooling liquid for the electronic device comprises the following components in percentage by mass: 99.5 to 99.9 percent of base oil and 0.1 to 0.5 percent of antioxidant; viscosity of base oil μ: mu is more than 30 and less than or equal to 40 cst.
In this example, the base oil was dimethicone with a viscosity of 40cst of 99.5% by mass, and the antioxidant was 2, 6-di-tert-butyl-p-cresol of 0.5% by mass.
The preparation method of the electronic device cooling liquid specifically comprises the following steps:
s1, respectively weighing the following components in percentage by mass:
99.5 percent of dimethyl silicone oil with the viscosity of 40cst and 0.5 percent of 2, 6-di-tert-butyl-p-cresol;
s2, mixing the dimethyl silicone oil weighed in the step S1 and the 2, 6-di-tert-butyl-p-cresol, heating to 60 ℃, stirring until the mixture is transparent, and then cooling to room temperature of 25 ℃;
and S3, filtering the solution obtained in the step S2 to obtain the electronic device cooling liquid.
Example 8 comparison of coolant and common mineral oil performance index tests, the following table:
performance index | Common mineral oil | Example 8 | Test standard |
Viscosity of the oil | 26.5 | 39 | GB/T 265 |
Flash point. C | 185 | 310 | GB/T |
Breakdown voltage KV | 25 | 84.4 | GB/T 507 |
Loss by weight of evaporation | 1.40% | 1.05% | GB/T 7325 |
Acid value mgKOH/g | 0.02 | 0.01 | GB/T7304 |
(Table 3)
As can be seen from table 3, the viscosity 39 of the cooling liquid of example 8 satisfies the flow requirement of the spray liquid cooling; in example 8, the flash point and the breakdown voltage of the cooling liquid are much higher than those of common mineral oil, which shows that the insulating property and the fireproof property are greatly improved; example 8 the evaporation loss of the cooling liquid is less than that of the common mineral oil, and the loss is reduced; example 8 the acid value of the cooling fluid was lower than that of ordinary mineral oil and the corrosiveness was reduced. It can be seen that the overall performance of example 8 is better improved compared to conventional mineral oils.
Example 9
In the embodiment, the base oil is natural ester oil with the viscosity of 40cst, and the mass percent of the natural ester oil is 99.9%; the antioxidant adopts an antioxidant 1076, and the mass percent of the antioxidant is 0.1 percent.
The preparation method of the electronic device cooling liquid of this example (same steps, different specific raw materials and mass percentages) is the same as that of example 8, and is not repeated herein.
Example 10
In the embodiment, the base oil is synthetic ester oil with the viscosity of 40cst, and the mass percent of the synthetic ester oil is 99.5%; the antioxidant adopts antioxidant 1076 and alkyl diphenylamine, and the mass percent of the antioxidant is 0.5 percent.
The preparation method of the electronic device cooling liquid of this example is the same as that of example 8, and details thereof are omitted.
Claims (10)
1. The electronic device cooling liquid is characterized by comprising the following components in percentage by mass:
99.5 to 99.9 percent of base oil and 0.1 to 0.5 percent of antioxidant; viscosity of base oil μ: mu is more than 30 and less than or equal to 40 cst.
2. The electronic device cooling fluid of claim 1, wherein the base oil is a dimethylsilicone oil, a natural ester oil, or a synthetic ester oil.
3. The electronic device cooling liquid of claim 1 or 2, wherein the antioxidant is one or a combination of two or more of 2, 6-di-tert-butyl-p-cresol, antioxidant 1076, and alkyl diphenylamine.
4. The electronic device cooling liquid is characterized by comprising the following components in percentage by mass:
99.0 to 99.9 percent of base oil, 0.005 to 0.9 percent of dispersant and 0.005 to 0.5 percent of antioxidant; viscosity of base oil μ: mu is more than or equal to 5 and less than or equal to 30cst or mu is more than 40 and less than or equal to 50 cst;
the sum of the contents of the components is 100 percent.
5. The electronic device cooling fluid of claim 4, wherein the base oil is a dimethylsilicone oil, a natural ester oil, or a synthetic ester oil.
6. The electronic device coolant of claim 4 or 5, wherein the dispersant is polyethylene glycol or polyglyceryl esters.
7. The electronic device cooling liquid of claim 6, wherein the antioxidant is one or a combination of two or more of 2, 6-di-tert-butyl-p-cresol, antioxidant 1076 and alkyl diphenylamine.
8. A preparation method of the electronic device cooling liquid as claimed in any one of claims 1 to 3, characterized by comprising the following steps:
s1, respectively weighing the following components in percentage by mass:
99.5 to 99.9 percent of base oil and 0.1 to 0.5 percent of antioxidant; viscosity of base oil μ: mu is more than 30 and less than or equal to 40 cst;
s2, mixing the base oil weighed in the step S1 and an antioxidant, heating and stirring the mixture until the mixture is transparent, and then cooling the mixture to room temperature;
and S3, filtering the solution obtained in the step S2 to obtain the electronic device cooling liquid.
9. A preparation method of the electronic device cooling liquid as claimed in any one of claims 4 to 7, characterized by comprising the following steps:
s1, respectively weighing the following components in percentage by mass:
99.0 to 99.9 percent of base oil, 0.005 to 0.9 percent of dispersant and 0.005 to 0.5 percent of antioxidant; viscosity of base oil μ: mu is more than or equal to 5 and less than or equal to 30cst or mu is more than 40 and less than or equal to 50 cst;
the sum of the contents of the components is 100 percent;
s2, mixing the base oil weighed in the step S1 and an antioxidant, heating and stirring the mixture until the mixture is transparent, and then cooling the mixture to room temperature;
s3, adding the dispersant weighed in the step S1 into the solution obtained in the step S2, and stirring until the dispersant is completely dissolved;
and S4, filtering the solution obtained in the step S3 to obtain the electronic device cooling liquid.
10. The method for producing an electronic device cooling liquid according to claim 9, characterized in that: in the step S2, the heating temperature is 50-60 ℃.
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CN114106787A (en) * | 2021-12-02 | 2022-03-01 | 中国石油化工股份有限公司 | Cooling medium composition and preparation method thereof |
CN115160578A (en) * | 2022-06-24 | 2022-10-11 | 纯钧新材料(深圳)有限公司 | Solid-solid phase change material for data center, preparation method and cooling liquid thereof |
CN115181550A (en) * | 2022-06-09 | 2022-10-14 | 纯钧新材料(深圳)有限公司 | Solid-solid phase change cooling liquid applicable to data center and preparation method thereof |
CN115322753A (en) * | 2022-09-14 | 2022-11-11 | 杭州云酷智能科技有限公司 | Cooling liquid and preparation method and application thereof |
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