CN110813204B - A biochemical industry reaction vessel for liquid phase contact - Google Patents
A biochemical industry reaction vessel for liquid phase contact Download PDFInfo
- Publication number
- CN110813204B CN110813204B CN201911192960.1A CN201911192960A CN110813204B CN 110813204 B CN110813204 B CN 110813204B CN 201911192960 A CN201911192960 A CN 201911192960A CN 110813204 B CN110813204 B CN 110813204B
- Authority
- CN
- China
- Prior art keywords
- female
- male
- joint
- tank
- baffle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000007791 liquid phase Substances 0.000 title claims abstract description 61
- 238000006243 chemical reaction Methods 0.000 title abstract description 42
- 238000007789 sealing Methods 0.000 claims description 78
- 238000005842 biochemical reaction Methods 0.000 claims description 40
- 230000000903 blocking effect Effects 0.000 claims description 26
- 230000008878 coupling Effects 0.000 claims description 9
- 238000010168 coupling process Methods 0.000 claims description 9
- 238000005859 coupling reaction Methods 0.000 claims description 9
- 239000002994 raw material Substances 0.000 abstract description 17
- 239000007788 liquid Substances 0.000 abstract description 12
- 238000002156 mixing Methods 0.000 abstract description 10
- 238000000034 method Methods 0.000 abstract description 9
- 239000002086 nanomaterial Substances 0.000 abstract description 8
- 238000002360 preparation method Methods 0.000 abstract description 6
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 210000002445 nipple Anatomy 0.000 description 13
- 239000000047 product Substances 0.000 description 11
- 229910052751 metal Inorganic materials 0.000 description 5
- 239000002184 metal Substances 0.000 description 5
- 238000004891 communication Methods 0.000 description 4
- 239000000376 reactant Substances 0.000 description 4
- 230000009471 action Effects 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- 230000006835 compression Effects 0.000 description 3
- 238000007906 compression Methods 0.000 description 3
- 238000005086 pumping Methods 0.000 description 3
- 239000003638 chemical reducing agent Substances 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 230000013011 mating Effects 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 101710134784 Agnoprotein Proteins 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000010364 biochemical engineering Methods 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000003911 water pollution Methods 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
- B01F31/80—Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model provides a biochemical industry reaction vessel for liquid phase contact, includes positive jar and cloudy jar, the bottom of positive jar and cloudy jar is connected through the device that switches on, the device that switches on includes positive conduction mouth and negative conduction mouth, a biochemical industry reaction vessel for liquid phase contact still including respectively with positive jar and the cooperation of cloudy jar are used negative and are connected with positive. This a biochemical industry reaction vessel for liquid phase contact can be fast with the required product of two kinds of liquid phase reaction raw material liquid mixings preparation in the reaction vessel, has realized two kinds of reaction vessel's quick intercommunication through set up the device that switches on in reaction vessel's bottom, is particularly suitable for liquid phase reaction method to prepare micro-nano material, uses in the industrial aspect such as biochemical industry, environmental protection, electronic circuit.
Description
Technical Field
The invention belongs to the technical field of biochemical engineering, and particularly relates to a biochemical reaction container for liquid phase contact, which can be used for connecting and connecting reaction liquid in biological or chemical liquid phase reaction, and is particularly suitable for preparing micro-nano materials by a liquid phase reaction method.
Background
The liquid phase reaction means that different reactants are uniformly dispersed in a solution for reaction, most of the reactants are soluble, and many reactions in the biochemical industry belong to the liquid phase reaction, for example, a liquid phase reduction method, a template method and the like are adopted to prepare a metal micro-nano material commonly used in biology, chemistry or medicine, and the metal micro-nano material is often required to react in a liquid phase.
The raw materials for the liquid phase reaction are generally mixed in three ways, one is that different raw materials are already present in different solutions and the different solutions are directly mixed, the other is that several raw materials are already present in the solutions and the other raw materials are directly added in a solid and/or gaseous manner to the solution in which the former raw materials are dissolved, and the other is that all raw materials are already present in a solid and/or gaseous manner and are added to a common solution (which may be generally referred to as a solvent at this time) during the reaction.
The operation of mixing the latter two raw materials is simple, the application does not pay much attention, the preparation of the micro-nano material generally requires that the reaction raw materials are fully dispersed in the solution before mixing, therefore, the most common method in laboratories and industrial production is the first mixing method, namely, different raw materials are already in different solutions, different solutions are directly mixed, but the method is a relatively difficult operation method, different solutions are in different containers, generally a pumping device is needed to introduce one solution into another solution, or a plurality of solutions are introduced into a new container, the equipment operation is very complicated, the cost is high, the cleaning and maintenance are inconvenient, if different containers are directly communicated, the contact time and the contact speed of the solutions cannot be controlled, because many raw materials have sufficient standing time before the solution mixing to ensure self full dispersion or early pre-reaction, in addition, many solutions cannot be mixed too fast, otherwise reactant control targets cannot be achieved, for example, in many cases, in liquid phase preparation of metal micro-nano materials, the reactants are contacted slowly, and the product particle size is finer and more uniform. Therefore, both laboratories and manufacturing enterprises need a biochemical reaction container which can facilitate the rapid conduction of different solution containers and control the contact time and contact speed of the solution.
Disclosure of Invention
In order to solve the problems, the invention provides a biochemical reaction vessel for liquid phase contact, which can quickly conduct two or more raw material liquids in the reaction vessel when needed, reasonably control the liquid phase contact speed, and realize the quick communication of the two reaction vessels by arranging a conducting device at the bottom of the reaction vessel.
The purpose of the invention is realized by the following technical scheme.
A biochemical reaction vessel for liquid phase contact comprises a positive tank and a negative tank, wherein the bottoms of the positive tank and the negative tank are connected through a conduction device; the conduction device comprises a positive conduction port and a negative conduction port;
the positive conduction opening comprises a positive nozzle, a baffle table I, a positive tank plug and a positive tank spring, the positive nozzle is arranged at the bottom of a positive tank body, a central hole of the positive nozzle is communicated with the inside of the positive tank body, the baffle table I is arranged in the middle of the central hole of the positive nozzle, the positive tank plug penetrates through a middle hole of the baffle table I, the baffle table I is provided with a baffle table hole I, the positive tank plug is a columnar object with bosses at two ends, the right side of the boss at the left end of the positive tank plug is provided with a conical surface matched with the left end of the central hole of the positive nozzle, and the positive tank spring is arranged between the boss at the right end of the positive tank plug and the baffle table I; the outer circle of the right end of the male nozzle is provided with a sealing pipe thread;
the negative conduction opening comprises a negative nozzle, a baffle table II, a baffle table hole II, a clamping table, a straight sealing section, a negative tank plug, a negative tank spring, a negative tank nut and a negative tank gasket; the negative nozzle is arranged at the bottom of the negative tank body, a central hole of the negative nozzle is communicated with the inside of the negative tank body, a baffle table II is arranged in the middle of the central hole of the negative nozzle, a negative tank plug penetrates through a middle hole of the baffle table II, a baffle table hole II is arranged on the baffle table II, the negative tank plug is a columnar object with bosses at two ends, the boss at the right end of the negative tank plug is a stepped boss, a conical surface matched with the right end of the central hole of the negative nozzle is arranged between the stepped bosses, the left end of the stepped boss is a straight sealing section, and the straight sealing section is sealed with the right end hole of the central hole of the negative nozzle through a sealing ring; a boss at the left end of the female tank plug and the baffle table II are provided with female tank springs; the left end of the female nozzle is provided with a clamping table, the clamping table and the right end of the female can nut are sealed through a sealing ring, and the internal thread of the female can nut is a sealing pipe thread; a female tank gasket is arranged on the end surface of the female nozzle;
if the maximum compressible length of the male can spring is x1c, the maximum matching thread length of the female can nut and the sealing pipe thread at the right end of the male nozzle is x2d, and the length of the straight sealing section is L1, the following conditions should be satisfied between the two sections:
x2d＞x1c+L1
the biochemical reaction container for liquid phase contact also comprises a female joint and a male joint which are respectively matched with the male tank and the female tank;
the female joint comprises a joint body I, a female joint plug, a female joint nut, a female joint washer and a female joint spring; the female joint plug penetrates through a center hole of the joint body I, a female joint baffle table is arranged in the middle of the center hole of the joint body I, a female joint baffle table hole is formed in the female joint baffle table, a female joint spring is arranged between the female joint baffle table and a right end bulge of the female joint plug, and a straight cylinder sealing surface and a conical sealing surface which are matched with an inner hole of the joint body I are arranged at the left end of the female joint plug; a female joint clamping table is arranged on the right side of the joint body I, and the female joint clamping table and the left side of the female joint nut are sealed through a sealing ring; the internal thread of the female joint nut is a sealing pipe thread; a female joint gasket is arranged at the right end of the joint body I;
if the maximum compressible length of the male can spring is x1c, the maximum matching thread length of the female joint nut and the sealing pipe thread at the right end of the male nozzle is x4c, and the length of the straight cylinder sealing surface matched with the inner hole of the joint body I at the left end of the female joint plug is L4, the following conditions should be satisfied between the two parts:
x4c＞x1c+L4
the male joint comprises a joint body II, a male joint plug and a male joint spring; the male joint plug penetrates through a center hole of the joint body II, a male joint blocking platform is arranged in the middle of the center hole of the joint body II, a male joint blocking platform hole is formed in the male joint blocking platform, the right end of the male joint plug is in sealing fit with the conical surface of the right end of the center hole of the joint body II, and a male joint spring is arranged between the left end of the male joint plug and the male joint blocking platform; the outer circle of the left end of the joint body II is provided with a sealing pipe thread;
the maximum compressible length of the male joint spring is set to be x5c, the maximum matching thread length of the sealing pipe thread on the outer circles of the left ends of the female tank nut and the joint body II is set to be x2d, and the length of the straight sealing section is set to be L1, so that the following conditions are met between the straight sealing section and the joint body II:
x2d＞x1c+L1。
in the biochemical reaction vessel for liquid phase contact, the male vessel body and the female vessel body are both hollow structures with open upper parts, the upper parts of the male vessel body and the female vessel body are vessel openings, and the covers are in threaded connection with the vessel openings; the middle of the top of the inner side of the cover is provided with a conical platform matched with the tank opening hole.
The biochemical reaction vessel for liquid phase contact is characterized in that two anode conduction ports or one anode conduction port and one cathode conduction port are arranged at the bottom of the anode tank, and two cathode conduction ports or one cathode conduction port and one anode conduction port are arranged at the bottom of the cathode tank;
the bottom of the male tank is provided with two male conduction ports which are matched with the female tank and the female joint for use;
the bottom of the male tank is provided with a male conduction port and a female conduction port which are matched with the female tank and the male joint;
the bottom of the female tank is provided with two female conduction ports which are matched with the male tank and the male joint for use;
the bottom of the female tank is provided with a female conduction port and a male conduction port which are matched with the male tank and the female joint for use.
In the biochemical reaction vessel for liquid phase contact as described above, assuming that the elastic modulus of the male tank spring is k1c, the elastic modulus of the female tank spring is k2c, the elastic modulus of the female coupling spring is k4e, and the elastic modulus of the male coupling spring is k5c, they satisfy the following conditions:
k2c＞k1c；
k4e＞k1c；
k2c＞k5c。
the biochemical reaction vessel for liquid phase contact is characterized in that the bottom of the anode tank is provided with an anode conducting port, and the bottom of the cathode tank is provided with a cathode conducting port; the male tank and the female tank are inserted together, are separated after full reaction and are respectively matched with the female joint and the male joint for use.
According to the biochemical reaction vessel for liquid phase contact, the plurality of conducting devices are vertically arranged on the side surfaces of the male tank and the female tank from low to high correspondingly.
In the biochemical reaction vessel for liquid phase contact, the number of the baffle table holes I is at least 1; when the number of the baffle table holes I is larger than 1, the baffle table holes I are preferably and uniformly distributed on the baffle table I.
The biochemical reaction container for liquid phase contact is characterized in that the number of the baffle table holes II is at least 1; when the number of the baffle table holes II is larger than 1, the baffle table holes II are preferably uniformly distributed on the baffle table II.
The biochemical reaction vessel for liquid phase contact as described above, wherein the number of the female joint baffle plate holes is at least 1; when the number of the female joint blocking platform holes is more than 1, the female joint blocking platform holes are preferably uniformly distributed on the female joint blocking platform.
The biochemical reaction vessel for liquid phase contact is characterized in that the number of the male joint baffle table holes is at least 1; when the number of the male joint blocking table holes is more than 1, the male joint blocking table holes are preferably uniformly distributed on the male joint blocking table.
The invention has the beneficial effects that:
1. according to the biochemical reaction container for liquid phase contact, the conduction device is arranged at the bottom of the reaction container, so that the two reaction containers are quickly communicated when needed to mix two liquid phase reaction raw material liquids in the reaction containers, the two liquid phase reaction raw material liquids are reacted to prepare a needed product, the mixing speed is not too high in the mixing process of the two solutions, and the biochemical reaction container is very suitable for occasions with certain control requirements on the mixing speed, such as micro-nano metal sol preparation.
2. According to the biochemical reaction vessel for liquid phase contact, the two reaction vessels are quickly communicated to mix the two liquid phase reaction raw material liquids in the reaction vessels when needed by arranging the conducting device at the bottom of the reaction vessel, so that a complex pumping system and a complex stirring device are not needed, and auxiliary dispersion during mixing can be very easily realized only by placing the vessel on an ultrasonic vibration table when necessary.
3. According to the biochemical reaction vessel for liquid phase contact, the conducting device at the bottom of the reaction vessel and the joint used in cooperation can be combined in various using modes, so that the operations of mixing and taking raw material solutions of all parts in liquid phase reaction are facilitated, and the biochemical reaction vessel for liquid phase contact can be used for realizing the rapid preparation of products by arranging a plurality of groups of conducting devices on the reaction vessel.
4. The biochemical reaction container for liquid phase contact has the advantages of universal structure and wide applicability, can be used for preparing various easily soluble and easily extracted chemical products, sol, micro-nano materials and the like, is mainly applied to the field of biochemical industry, and has the same application prospect in the aspects of environment protection, electronic circuits and other industries.
Drawings
The aspects and advantages of the present application will become apparent to those of ordinary skill in the art upon reading the following detailed description of the preferred embodiments. The drawings are only for purposes of illustrating the preferred embodiments and are not to be construed as limiting the invention. In the drawings:
fig. 1 is a schematic structural view of a biochemical reaction vessel for liquid phase contact according to example 1 of the present invention.
Fig. 2 is an enlarged view of a portion a of fig. 1.
Fig. 3 is an enlarged view of portion B of fig. 1.
Fig. 4 is a schematic structural view of a male can body.
Fig. 5 is an enlarged view of the portion C of fig. 4.
Fig. 6 is a schematic structural view of a female can body.
Fig. 7 is an enlarged view of the portion D in fig. 6.
Fig. 8 is a schematic view of the structure of the female joint.
Fig. 9 is a schematic structural view of the male connector.
FIG. 10 is a view showing the conducting operation of a biochemical reaction vessel for liquid phase contact.
The components represented by the reference numerals in the figures are:
the positive tank comprises a positive tank 1, a positive tank body 1a, a positive nozzle 1a1, a baffle table I1 a2, a baffle table hole I1 a3, a positive tank plug 1b, a positive tank spring 1c, a negative tank 2, a negative tank body 2a, a negative nozzle 2a1, a baffle table II 2a2, a baffle table hole II 2a3, a clamping table 2a4, a straight sealing section 2a5, a negative tank plug 2b, a negative tank spring 2c, a negative tank nut 2d, a negative tank gasket 2e, a cover 3, a negative joint 4, a joint body I4 a, a negative joint plug 4b, a negative joint nut 4c, a negative joint gasket 4d, a negative joint spring 4e, a positive joint 5, a joint body II 5a, a positive joint plug 5b and a positive joint spring 5 c.
Detailed Description
Exemplary embodiments of the present disclosure will be described in more detail below with reference to the accompanying drawings. While exemplary embodiments of the present disclosure are shown in the drawings, it should be understood that the present disclosure may be embodied in various forms and should not be limited to the embodiments set forth herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete, and will fully convey the scope of the disclosure to those skilled in the art.
Example 1
Referring to fig. 1, fig. 1 is a schematic structural view of a biochemical reaction vessel for liquid phase contact according to embodiment 1 of the present invention, and includes a positive tank 1 and a negative tank 2, wherein bottoms of the positive tank 1 and the negative tank 2 are connected by a conducting device; the anode tank 1 and the cathode tank 2 are used together to mix and react two raw materials in liquid phase to prepare a desired product such as micro-nano metal sol, for example, if AgNO is prepared in the anode tank 13The solution containing the chemical reducing agent or the biological reducing agent is prepared in the cathode tank 2, and the two solutions can be mixed to prepare the micro-nano silver sol with different particle sizes or shapes by regulating and controlling reaction conditions (concentration, auxiliary agents, biological template agents and the like), so that the micro-nano silver sol can be used in the fields of medical disinfection and sterilization, water pollution prevention and control, biological marking, environmental protection, electronic circuits and the like.
Referring to fig. 2, the conduction device includes a male conduction port and a female conduction port, as shown in fig. 4 and 5, the male conduction port includes a male nipple 1a1, a baffle i 1a2, a male can plug 1b and a male can spring 1c, the male nipple 1a1 is arranged at the bottom of the male can body 1a, a central hole of the male nipple 1a1 is communicated with the inside of the male can body 1a, a baffle i 1a2 is arranged in the middle of the central hole of the male nipple 1a1, the male can plug 1b passes through the central hole of the baffle i 1a2, the baffle i 1a2 is provided with a baffle hole i 1a3, the male plug 1b is a column with bosses at both ends, the right side of the left-end boss of the male can plug 1b is provided with a conical surface matched with the left end of the central hole of the male nipple 1a1, and a male can spring 1c is arranged between the right-end boss of the male can plug 1b and the baffle 1a 2; a sealing pipe thread is arranged on the outer circle of the right end of the male nozzle 1a1, a male can plug 1b compresses a male can spring 1c to move leftwards under the action of external force, so that a conical surface matched with the left end of the central hole of the male nozzle 1a1 is arranged on the right side of the boss at the left end of the male can plug 1b to jack, liquid in the male can 1 can flow out through the central hole of the male nozzle 1a1, and the baffle hole I1 a3 is used for the liquid to flow in the central hole of the male nozzle 1a 1; as shown in fig. 6 and 7, the female conduction port includes a female nipple 2a1, a stop ii 2a2, a stop hole ii 2a3, a catch 2a4, a straight sealing section 2a5, a female can plug 2b, a female can spring 2c, a female can nut 2d, and a female can washer 2 e; the negative nozzle 2a1 is arranged at the bottom of the negative tank body 2a, the center hole of the negative nozzle 2a1 is communicated with the inside of the negative tank body 2a, the middle of the center hole of the negative nozzle 2a1 is provided with a baffle table II 2a2, a negative tank plug 2b penetrates through the middle hole of the baffle table II 2a2, the baffle table II 2a2 is provided with a baffle table hole II 2a3, the negative tank plug 2b is a column with bosses at two ends, the right end boss of the negative tank plug 2b is a stepped boss, a conical surface matched with the right end of the center hole of the negative nozzle 2a1 is arranged between the stepped bosses, the left end of the stepped boss is a straight sealing section 2a5, and the straight sealing section 2a5 is sealed with the right end hole of the center hole of the negative nozzle 2a1 through a sealing ring; a female tank spring 2c is arranged on the left end boss of the female tank plug 2b and the baffle table II 2a 2; a clamping table 2a4 is arranged at the left end of the female nozzle 2a1, the clamping table 2a4 and the right end of the female can nut 2d are sealed through a sealing ring, and the internal thread of the female can nut 2d is a sealing pipe thread; a female can gasket 2e is arranged on the end surface of the female mouth 2a 1; the female can plug 2b compresses the female can spring 2c under the action of external force, so that the female can plug 2b moves rightwards, a conical surface which is matched with the right end of the central hole of the female nozzle 2a1 is arranged between the step bosses and is pushed open firstly, the part, sealed by a sealing ring, between the straight sealing section 2a5 and the right end hole of the central hole of the female nozzle 2a1 can allow liquid in the female can 2 to flow out through the central hole of the female nozzle 2a1 after the liquid is completely separated, and the baffle hole II 2a3 is used for enabling the liquid in the central hole of the female nozzle 2a1 to flow; the internal thread of the female tank nut 2d is a sealing pipe thread and is in threaded fit with a sealing pipe thread on the outer circle of the right end of the male nozzle 1a1, the male tank plug 1b and the female tank plug 2b interact with each other along with the gradual screwing of the female tank nut 2d until the male tank 1 and the female tank 2 are communicated with each other through a conduction device, and as the internal thread of the female tank nut 2d is a sealing pipe thread and is in threaded fit with a sealing pipe thread on the outer circle of the right end of the male nozzle 1a1 and the clamping table 2a4 is sealed with the right end of the female tank nut 2d through a sealing ring, the conduction device cannot leak liquid once the female tank nut 2d is screwed up.
In the following embodiment, the clamping table 2a4 and the right end of the female can nut 2d are sealed by a sealing ring, that is, a sealing groove is formed in the clamping table 2a4, an O-shaped sealing ring is sleeved on the sealing groove, and the female can nut 2d is sleeved on the sealing groove to realize a sealing function. In the prior art, there are many other types of seals, such as Y-shaped seal rings, O-shaped seal rings and retainer ring combinations, which can achieve the sealing function. The sealing structure at other places in the patent can also adopt the mode.
In order to ensure that the female can nut 2d is screwed on, the male can 1 and the female can 2 can communicate with each other through a communication means. A clear specification is required for the relationship of the maximum compressible length of the male can spring 1c, the distance the female can nut 2d is tightened and the length of the straight seal segment 2a 5.
Assuming that the maximum compressible length of the male can spring 1c is x1c, the maximum matching thread length of the female can nut 2d and the sealing pipe thread at the right end of the male nozzle 1a1 is x2d, and the length of the straight sealing section 2a5 is L1, the following conditions should be satisfied between them:
x2d＞x1c+L1
after the reaction product is prepared by communicating the anode tank 1 and the cathode tank 2 through a conducting device, a device capable of taking the reaction product from the anode tank 1 and the cathode tank 2 is also arranged; the biochemical reaction container for liquid phase contact also comprises a female joint 4 and a male joint 5 which are respectively matched with the male tank 1 and the female tank 2;
referring to fig. 8, the female joint 4 includes a joint body i 4a, a female joint plug 4b, a female joint nut 4c, a female joint washer 4d, a female joint spring 4 e; the female joint plug 4b penetrates through a center hole of the joint body I4 a, a female joint baffle table is arranged in the middle of the center hole of the joint body I4 a, a female joint baffle table hole is formed in the female joint baffle table, a female joint spring 4e is arranged between the female joint baffle table and a right end bulge of the female joint plug 4b, and a straight cylinder sealing surface and a conical sealing surface which are matched with an inner hole of the joint body I4 a are arranged at the left end of the female joint plug 4 b; a female joint clamping table is arranged on the right side of the joint body I4 a, and the female joint clamping table and the left side of the female joint nut 4c are sealed through a sealing ring; the internal thread of the female joint nut 4c is a seal pipe thread; a female joint gasket 4d is arranged at the right end of the joint body I4 a; the working principle of the female joint 4 is the same as that of the female conduction port, and the left side of the joint body I4 a can be used for taking samples of reaction solution or product solution or leading prepared products dispersed in the solution out or taking the products as required.
As above, in order to ensure the communication between the female connector 4 and the male can 1, the maximum compressible length of the male can spring 1c is x1c, the maximum mating thread length of the female connector nut 4c and the sealing pipe thread at the right end of the male nipple 1a1 is x4c, and the length of the straight sealing surface at the left end of the female connector plug 4b, which is mated with the inner hole of the connector body i 4a, is L4, so that the following conditions should be satisfied:
x4c＞x1c+L4
as shown in fig. 9, the male connector 5 includes a connector body ii 5a, a male connector plug 5b, a male connector spring 5 c; the male joint plug 5b penetrates through the center hole of the joint body II 5a, a male joint blocking platform is arranged in the middle of the center hole of the joint body II 5a, a male joint blocking platform hole is formed in the male joint blocking platform, the right end of the male joint plug 5b is in conical surface sealing fit with the right end of the center hole of the joint body II 5a, and a male joint spring 5c is arranged between the left end of the male joint plug 5b and the male joint blocking platform; the outer circle of the left end of the joint body II 5a is provided with a sealing pipe thread; the working principle of the male joint 5 is the same as that of the male conduction port, and the right side of the joint body II 5a can be connected to sample and analyze a reaction solution or a product solution or lead out a prepared product dispersed in the solution or take the product as required.
As above, in order to ensure the communication between the male coupling 5 and the female coupling 2, the maximum compressible length of the male coupling spring 5c is x5c, the maximum mating thread length of the female coupling nut 2d and the outer circumference of the left end of the coupling body ii 5a having the sealing pipe thread is x2d, and the length of the straight sealing segment 2a5 is L1, which should satisfy the following conditions:
x2d＞x1c+L1。
referring to fig. 2, the male can body 1a and the female can body 2a are both hollow structures with open upper portions, the upper portions of the male can body 1a and the female can body 2a are can openings, a cover 3 is in threaded connection with the can openings, and the cover 3 is in fastening connection with the can openings to prevent leakage; the middle of the top of the inner side of the cover 3 is provided with a conical table matched with the tank opening hole, and the conical table is used for ensuring the tight sealing of the cover 3 and the tank opening.
In the embodiment, the anode can 1 has an anode conduction port and a cathode conduction port, and the bottom of the cathode can 2 is provided with a cathode conduction port and an anode conduction port; the bottom of the male tank 1 is provided with a male conducting port and a female conducting port which are matched with the female tank 2 and the male joint 5; the bottom of the female tank 2 is provided with a female conduction port and a male conduction port which are matched with the male tank 1 and the female joint 4 for use.
Preferably, in order to allow the end having the nut to be connected after being connected and sealed before being separated, the elastic modulus of the male tank spring 1c is k1c, the elastic modulus of the female tank spring 2c is k2c, the elastic modulus of the female joint spring 4e is k4e, and the elastic modulus of the male joint spring 5c is k5c, which satisfy the following conditions:
k2c＞k1c；
k4e＞k1c；
k2c＞k5c；
that is, the spring force of the side with the nut is larger than that of the other side, and under the same compression distance, the side without the nut can be firstly pushed open, and the spring force is the elastic coefficient of the spring multiplied by the compression amount.
In the present embodiment, it is preferred that,
k2c＞2k1c；
k4e＞2k1c；
k2c＞2k5c。
FIG. 10 is a view showing the conducting operation of a biochemical reaction vessel for liquid phase contact. As shown in the left drawing of fig. 10, in the initial state, the female can nut 2d is not screwed into the sealing pipe thread of the right end outer circle of the male nipple 1a1, the male can plug 1b and the female can spring 2c are both in the sealing state with the male can body 1a and the female can body 2a under the action of the springs, the liquid in the can does not flow into the male nipple 1a1 and the female nipple 2a1, as the female can nut 2d is screwed into the sealing pipe thread of the right end outer circle of the male nipple 1a1, the male can plug 1b is pushed open first due to the spring force of the male can spring 1c being smaller than that of the female can spring 2c until the male can spring 1c reaches the maximum compression amount, the female can plug 2b is pushed open until the male nipple 1a1 and the female nipple 2a1 are connected after being disengaged from the straight sealing section 2a5, and this operation is most effective when a solution containing a reaction product is taken up with the male and female joint, one side can be disconnected at first when the separation is carried out, and the leakage can be better prevented.
Preferably, a plurality of conducting devices are vertically arranged on the same side surface of the anode tank 1 and the cathode tank 2 from low to high, and the structure enables the anode tank 1 and the cathode tank 2 to be communicated through the conducting devices, so that the contact time and speed of liquid phases are regulated and controlled, and the reaction process is accelerated or inhibited.
In the biochemical reaction container for liquid phase contact, the number of the baffle table holes I1 a3 is at least 1; when the number of the baffle table holes I1 a3 is more than 1, the baffle table holes I1 a3 are uniformly distributed on the baffle table I1 a 2.
The biochemical reaction container for liquid phase contact is characterized in that the number of the baffle table holes II 2a3 is at least 1; when the number of the baffle table holes II 2a3 is more than 1, the baffle table holes II 2a3 are uniformly distributed on the baffle table II 2a 2.
The biochemical reaction vessel for liquid phase contact as described above, wherein the number of the female joint baffle plate holes is at least 1; and when the number of the female joint blocking platform holes is more than 1, the female joint blocking platform holes are uniformly distributed on the female joint blocking platform.
The biochemical reaction vessel for liquid phase contact is characterized in that the number of the male joint baffle table holes is at least 1; when the number of the male joint blocking table holes is larger than 1, the male joint blocking table holes are uniformly distributed on the male joint blocking table.
The reaction vessel of this embodiment can cooperate ultrasonic vibration to use when being used for the micro-nano material of liquid phase preparation, for example can directly place two jar bodies of reaction vessel on the ultrasonic vibration platform, on the basis of having left out complicated pumping system like this, also need not connect complicated agitating unit for container self, further improved convenience and the flexibility of using, practiced thrift the cost.
Example 2
The names of the male tank 1 and the female tank 2 are only used for easily expressing the technical scheme, and the essence of the invention is the matching use of the male connection port, the female joint 4 and the male joint 5; they can be used in various modes by permutation and combination.
Examples are as follows:
the bottom of the male tank 1 is provided with two male conduction ports which are matched with the female tank 2 and the female joint 4 for use; the bottom of the female tank 2 is provided with two female conduction ports which are matched with the male tank 1 and the male joint 5 for use.
The following combination schemes may also be employed: the bottom of the male tank 1 is provided with a male conduction port, and the bottom of the female tank 2 is provided with a female conduction port; the male tank 1 and the female tank 2 are inserted together, fully reacted, separated and then respectively matched with the female joint 4 and the male joint 5 for use.
Other technical contents not mentioned in this embodiment may be the same as those in embodiment 1, and are not described again.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any changes or substitutions that can be easily conceived by those skilled in the art within the technical scope of the present invention are included in the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the appended claims.
Claims (10)
1. A biochemical reaction vessel for liquid phase contact comprises a positive tank (1) and a negative tank (2), and is characterized in that the bottoms of the positive tank (1) and the negative tank (2) are connected through a conduction device; the conduction device comprises a positive conduction port and a negative conduction port;
the positive conduction port comprises a positive nozzle (1a1), a baffle table I (1a2), a positive tank plug (1b) and a positive tank spring (1c), the positive nozzle (1a1) is arranged at the bottom of the positive tank body (1a), a central hole of the positive nozzle (1a1) is communicated with the interior of the positive tank body (1a), a baffle table I (1a2) is arranged in the middle of the central hole of the positive nozzle (1a1), the positive tank plug (1b) penetrates through the central hole of the baffle table I (1a2), the baffle table I (1a2) is provided with a baffle table hole I (1a3), the tank positive plug (1b) is a column with bosses at two ends, the right side of the boss at the left end of the positive tank plug (1b) is provided with a conical surface matched with the left end of the positive nozzle (1a1), and the positive tank spring (1c) is arranged between the boss at the right end of the positive tank plug (1b) and the baffle table I (1a 2); the outer circle of the right end of the male nozzle (1a1) is provided with a sealing pipe thread;
the cathode conducting opening comprises a cathode nozzle (2a1), a baffle II (2a2), a baffle hole II (2a3), a clamping table (2a4), a straight sealing section (2a5), a cathode tank plug (2b), a cathode tank spring (2c), a cathode tank nut (2d) and a cathode tank gasket (2 e); the negative nozzle (2a1) is arranged at the bottom of a negative tank body (2a), the central hole of the negative nozzle (2a1) is communicated with the inside of the negative tank body (2a), the middle of the central hole of the negative nozzle (2a1) is provided with a baffle II (2a2), a negative tank plug (2b) penetrates through the middle hole of the baffle II (2a2), the baffle II (2a2) is provided with a baffle hole II (2a3), the negative tank plug (2b) is a column with bosses at two ends, the boss at the right end of the negative tank plug (2b) is a stepped boss, a conical surface matched with the right end of the central hole of the negative nozzle (2a1) is arranged between the stepped bosses, the left end of the stepped boss is a straight sealing section (2a5), and the straight sealing section (2a5) and the right end hole of the central hole of the negative nozzle (2a1) are sealed through a sealing ring; a left end boss of the female tank plug (2b) and the baffle II (2a2) are provided with a female tank spring (2 c); the left end of the female nozzle (2a1) is provided with a clamping table (2a4), the clamping table (2a4) and the right end of the female can nut (2d) are sealed through a sealing ring, and the internal thread of the female can nut (2d) is a sealing pipe thread; a female can gasket (2e) is arranged on the end surface of the female nozzle (2a 1);
the maximum compressible length of the male can spring (1c) is x1c, the maximum matching thread length of the female can nut (2d) and the sealing pipe thread at the right end of the male nozzle (1a1) is x2d, and the length of the straight sealing section (2a5) is L1, so that the following conditions are met between the two sections:
x2d＞x1c+L1
the biochemical reaction container for liquid phase contact also comprises a female joint (4) and a male joint (5) which are respectively matched with the male tank (1) and the female tank (2);
the female joint (4) comprises a joint body I (4a), a female joint plug (4b), a female joint nut (4c), a female joint washer (4d) and a female joint spring (4 e); the female joint plug (4b) penetrates through a center hole of the joint body I (4a), a female joint baffle table is arranged in the middle of the center hole of the joint body I (4a), a female joint baffle table hole is formed in the female joint baffle table, a female joint spring (4e) is installed between the female joint baffle table and a right end bulge of the female joint plug (4b), and a straight cylinder sealing surface and a conical sealing surface which are matched with an inner hole of the joint body I (4a) are arranged at the left end of the female joint plug (4 b); a female joint clamping table is arranged on the right side of the joint body I (4a), and the female joint clamping table and the left side of the female joint nut (4c) are sealed through a sealing ring; the internal thread of the female joint nut (4c) is a sealing pipe thread; a female joint gasket (4d) is arranged at the right end of the joint body I (4 a);
the maximum compressible length of the male can spring (1c) is set to be x1c, the maximum matching thread length of the female joint nut (4c) and the sealing pipe thread at the right end of the male nozzle (1a1) is set to be x4c, and the length of a straight-tube sealing surface matched with the inner hole of the joint body I (4a) at the left end of the female joint plug (4b) is set to be L4, so that the following conditions are met between the two parts:
x4c＞x1c+L4
the male joint (5) comprises a joint body II (5a), a male joint plug (5b) and a male joint spring (5 c); the male joint plug (5b) penetrates through the center hole of the joint body II (5a), a male joint baffle table is arranged in the middle of the center hole of the joint body II (5a), a male joint baffle table hole is formed in the male joint baffle table, the right end of the male joint plug (5b) is in sealing fit with the conical surface of the right end of the center hole of the joint body II (5a), and a male joint spring (5c) is arranged between the left end of the male joint plug (5b) and the male joint baffle table; the excircle of the left end of the joint body II (5a) is provided with a sealing pipe thread;
setting the maximum compressible length of the male joint spring (5c) as x5c, setting the maximum matching thread length of the sealing pipe thread on the excircle of the left ends of the female joint nut (2d) and the joint body II (5a) as x2d, and setting the length of the straight sealing section (2a5) as L1, the following conditions should be satisfied between the two sections:
x2d＞x1c+L1。
2. the biochemical reaction vessel for liquid phase contact according to claim 1, wherein the male vessel body (1a) and the female vessel body (2a) are both hollow structures with open upper portions, the upper portions of the male vessel body (1a) and the female vessel body (2a) are vessel openings, and a cover (3) is screwed to the vessel openings; the middle of the top of the inner side of the cover (3) is provided with a conical platform matched with the tank mouth hole.
3. The biochemical reaction vessel for liquid phase contact according to claim 2, wherein the bottom of the male tank (1) is provided with two male conduction ports or one male conduction port and one female conduction port, and the bottom of the female tank (2) is provided with two female conduction ports or one female conduction port and one male conduction port;
the bottom of the male tank (1) is provided with two male conduction ports which are matched with the female tank (2) and the female joint (4) for use;
the bottom of the male tank (1) is provided with a male conducting port and a female conducting port which are matched with the female tank (2) and the male joint (5) for use;
the bottom of the female tank (2) is provided with two female conduction ports which are matched with the male tank (1) and the male joint (5) for use;
the bottom of the female tank (2) is provided with a female conduction port and a male conduction port which are matched with the male tank (1) and the female joint (4) for use.
4. A biochemical reaction vessel for liquid phase contact according to claim 3, wherein assuming that the elastic modulus of the male tank spring (1c) is k1c, assuming that the elastic modulus of the female tank spring (2c) is k2c, assuming that the elastic modulus of the female coupling spring (4e) is k4e, assuming that the elastic modulus of the male coupling spring (5c) is k5c, they satisfy the following conditions:
k2c＞k1c；
k4e＞k1c；
k2c＞k5c。
5. the biochemical reaction vessel for liquid phase contact according to claim 1, wherein the bottom of the male tank (1) is provided with a male conducting port, and the bottom of the female tank (2) is provided with a female conducting port; the male tank (1) and the female tank (2) are inserted together, fully reacted, separated and then respectively matched with the female joint (4) and the male joint (5) for use.
6. The biochemical reaction vessel for liquid phase contact according to claim 1, wherein a plurality of conducting devices are arranged on the side surfaces of the male tank (1) and the female tank (2) from low to high in the same vertical corresponding manner.
7. The biochemical reaction vessel for liquid phase contact according to claim 1, wherein the number of the baffle holes i (1a3) is at least 1; when the number of the baffle table holes I (1a3) is more than 1, the baffle table holes I (1a3) are uniformly distributed on the baffle table I (1a 2).
8. The biochemical reaction vessel for liquid phase contact according to claim 1, wherein the number of the baffle holes ii (2a3) is at least 1; when the number of the baffle table holes II (2a3) is more than 1, the baffle table holes II (2a3) are uniformly distributed on the baffle table II (2a 2).
9. The biochemical reaction vessel for liquid phase contact according to claim 1, wherein the number of the female joint block holes is at least 1; and when the number of the female joint blocking platform holes is more than 1, the female joint blocking platform holes are uniformly distributed on the female joint blocking platform.
10. The biochemical reaction vessel for liquid phase contact according to claim 1, wherein the number of the male connector boss holes is at least 1; when the number of the male joint blocking table holes is larger than 1, the male joint blocking table holes are uniformly distributed on the male joint blocking table.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911192960.1A CN110813204B (en) | 2019-11-28 | 2019-11-28 | A biochemical industry reaction vessel for liquid phase contact |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911192960.1A CN110813204B (en) | 2019-11-28 | 2019-11-28 | A biochemical industry reaction vessel for liquid phase contact |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN110813204A CN110813204A (en) | 2020-02-21 |
| CN110813204B true CN110813204B (en) | 2021-09-21 |
Family
ID=69542941
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201911192960.1A Expired - Fee Related CN110813204B (en) | 2019-11-28 | 2019-11-28 | A biochemical industry reaction vessel for liquid phase contact |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110813204B (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3245393A1 (en) * | 1982-12-08 | 1984-06-14 | Degussa Ag, 6000 Frankfurt | Process and equipment for mixing and reacting liquid components with liquid, gaseous or solid components |
| JP2009226261A (en) * | 2008-03-19 | 2009-10-08 | Fujifilm Corp | Liquid mixing method and liquid mixing apparatus |
| CN102378776A (en) * | 2009-02-02 | 2012-03-14 | 巴斯夫欧洲公司 | Method for producing polymers and reactor for carrying out said method |
| CN202845022U (en) * | 2012-09-13 | 2013-04-03 | 成都益友科技发展有限公司 | Duplex cyclone liquid mixing system |
| CN202962442U (en) * | 2012-12-13 | 2013-06-05 | 北京东方红升新能源应用技术研究院有限公司 | Liquid phase reaction device for synthesizing polymethoxy dialkyl ether |
| CN104971673A (en) * | 2014-04-08 | 2015-10-14 | 中国石油大学(华东) | Liquid-liquid heterogeneous mixing-reaction-separation integrated short-contact cyclone reactor |
| CN107362751A (en) * | 2017-09-05 | 2017-11-21 | 蔡素真 | A kind of liquid reactions kettle material feed unit |
-
2019
- 2019-11-28 CN CN201911192960.1A patent/CN110813204B/en not_active Expired - Fee Related
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3245393A1 (en) * | 1982-12-08 | 1984-06-14 | Degussa Ag, 6000 Frankfurt | Process and equipment for mixing and reacting liquid components with liquid, gaseous or solid components |
| JP2009226261A (en) * | 2008-03-19 | 2009-10-08 | Fujifilm Corp | Liquid mixing method and liquid mixing apparatus |
| CN102378776A (en) * | 2009-02-02 | 2012-03-14 | 巴斯夫欧洲公司 | Method for producing polymers and reactor for carrying out said method |
| CN202845022U (en) * | 2012-09-13 | 2013-04-03 | 成都益友科技发展有限公司 | Duplex cyclone liquid mixing system |
| CN202962442U (en) * | 2012-12-13 | 2013-06-05 | 北京东方红升新能源应用技术研究院有限公司 | Liquid phase reaction device for synthesizing polymethoxy dialkyl ether |
| CN104971673A (en) * | 2014-04-08 | 2015-10-14 | 中国石油大学(华东) | Liquid-liquid heterogeneous mixing-reaction-separation integrated short-contact cyclone reactor |
| CN107362751A (en) * | 2017-09-05 | 2017-11-21 | 蔡素真 | A kind of liquid reactions kettle material feed unit |
Also Published As
| Publication number | Publication date |
|---|---|
| CN110813204A (en) | 2020-02-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP5055283B2 (en) | Drain connector for material processing containers | |
| US20130167960A1 (en) | Drain connector for fluid processing and storage containers | |
| CN101130264A (en) | Device at bone cement mixer | |
| CN110813204B (en) | A biochemical industry reaction vessel for liquid phase contact | |
| CN201669095U (en) | Device for strengthening gas distribution in strengthen | |
| CN204973865U (en) | Chemical reaction kettle | |
| CN104815600A (en) | Coaxial emulsification mixing reaction kettle | |
| CN104785188A (en) | Coaxial stirring reaction kettle | |
| CN205815703U (en) | A kind of reactor liquid premixing structure | |
| CN108854894A (en) | A kind of stainless steel cauldron | |
| CN208381318U (en) | A kind of reaction kettle axis sealing device | |
| CN212632625U (en) | Vibration feeding device | |
| CN213611439U (en) | Solvent transfer joint and solvent transfer system | |
| CN2636968Y (en) | Pipeline type solid-liquid dispersing mixer | |
| CN217527279U (en) | Liquid medicine connecting assembly | |
| CN203886572U (en) | Syringe connector | |
| CN217939800U (en) | Gilding raw materials mixing arrangement of misce bene | |
| CN218924336U (en) | Large-scale industrial liquid-alkali solution preparing device | |
| CN205517534U (en) | Kneading machine | |
| CN205164621U (en) | Chemical industry agitator | |
| CN205127873U (en) | Agitator with two hoppers down | |
| CH381200A (en) | Reaction vessel equipped with a stirrer | |
| CN204503061U (en) | A kind of reactor Split type device | |
| CN2636967Y (en) | Intermittent solid-liquid dispersing mixer | |
| CN220194806U (en) | Solid feeding device |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20210921 |