CN110791404A - Preparation method of Chinese toon white spirit - Google Patents
Preparation method of Chinese toon white spirit Download PDFInfo
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- CN110791404A CN110791404A CN201911230454.7A CN201911230454A CN110791404A CN 110791404 A CN110791404 A CN 110791404A CN 201911230454 A CN201911230454 A CN 201911230454A CN 110791404 A CN110791404 A CN 110791404A
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- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
- C12G3/05—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with health-improving ingredients, e.g. flavonoids, flavones, polyphenols or polysaccharides
- C12G3/055—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with health-improving ingredients, e.g. flavonoids, flavones, polyphenols or polysaccharides extracted from plants
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Abstract
The invention discloses a preparation method of a Chinese toon white spirit, which comprises the steps of raw material selection and pretreatment, freeze drying and crushing, Chinese toon active ingredient extraction, concentration and freeze drying, Chinese toon wine preparation, post-filtration treatment and packaging, and the finished Chinese toon white spirit is prepared. By adopting the Chinese toon white spirit process, the extraction rate is high, the Chinese toon and the white spirit are organically fused, the health care function of the white spirit is obviously improved, the Chinese toon of the white spirit is endowed with a special flavor, and the Chinese toon white spirit can play the roles of resisting oxidation, reducing blood sugar, inhibiting bacteria and viruses, preventing cardiovascular and cerebrovascular diseases, enhancing resistance and resisting aging, and achieves the effect of prolonging life; increases the deep processing way of the cedrela sinensis, improves the utilization rate and increases the economic income of farmers. The product of the invention is light yellow in color, has unique taste of the Chinese toon, and has fine, soft and soft mouthfeel; the product has wide application objects; the invention adopts vacuum freeze drying, microwave and rotary steaming technologies, and the operation process is simple; the raw materials are low in price and wide in source, and are suitable for industrial large-scale production.
Description
Technical Field
The invention relates to a preparation method of white spirit, in particular to a preparation method of white spirit by adding vegetable extracts, and also relates to a preparation method of a toona sinensis food, which is applied to the technical field of preparation of alcoholic beverages and toona sinensis nutritional functional health-care foods.
Background
Chinese toon is a unique woody vegetable in China, the origin is located in the middle and south of China, but due to the development of science and technology, the current planting area is distributed all over the country. The cedrela sinensis has rich fragrance and high nutritive value, so the cedrela sinensis is known as 'vegetables on trees'. The cedrela sinensis is not only edible, but also can be used as a medicine, and is rich in polyphenol, flavone, polysaccharide, terpenoid and other substances, so that the cedrela sinensis has high medicinal values of resisting virus, resisting cancer, resisting oxidation and the like.
In recent years, the eating of the cedrela sinensis is more and more popular. The cedrela sinensis is rich in nutrition and wide in source, but is seasonal and not easy to store, so that the price of the cedrela sinensis is greatly increased. Therefore, the research on the nutrition and health care functions and the research and development of the related natural health care food have great market prospect and economic benefit.
At present, white spirit in the market has various fragrance types, and the alcoholic strength, the fragrance type and the fragrance are different. When a certain amount of white spirit is drunk, the functions of appetizing and helping digestion, and promoting appetite, stimulation and pancreatic secretion of people can be realized. The premise of the health benefiting of the wine is 'reasonable drinking', otherwise the wine is harmful to the body.
Therefore, the Chinese toon and the white spirit are taken as raw materials to prepare the Chinese toon white spirit. Firstly, the active ingredients in the Chinese toon are extracted to prepare dry powder, and then the dry powder is fully mixed with a proper amount of white spirit, so that the active ingredients can be promoted to be completely dissolved.
The traditional extraction processes of the active ingredients comprise an immersion method, a decoction method and the like, but the methods have long time consumption and low extraction efficiency and are not suitable for the production of high-efficiency operation in modern factories. The vacuum freeze drying avoids the defects of color change, taste change, large loss of nutrient components, poor rehydration property and the like caused by high temperature and normal pressure in the traditional drying method, has the advantages of keeping the shape, color, aroma, taste, nutrient components, good rehydration property and the like of vegetables, but has not ideal extraction efficiency in the prior art.
At present, the production process of the Chinese toon products in the market is single, and the Chinese toon products are mostly in the form of Chinese toon tea and Chinese toon sauce. The cedrela sinensis tea keeps the unique aroma substances of the cedrela sinensis, the content of active substances is reduced, and the effects of reducing blood sugar, resisting oxidation and the like of the cedrela sinensis cannot be well achieved. Although the shelf life of the cedrela sinensis is prolonged, the pickles belong to high-salt food, nitrite is easily generated in the pickling process, the cedrela sinensis sauce is not suitable for eating more and long-term eating, otherwise cardiovascular and cerebrovascular diseases and osteoporosis are easily caused, and therefore the health application value of the cedrela sinensis is yet to be further developed.
Disclosure of Invention
In order to solve the problems of the prior art, the invention aims to overcome the defects in the prior art, and provides a preparation method of a toona sinensis baijiu, which is used for preparing a functional health-care drink of the baijiu, has the characteristic of high-alcohol content baijiu, increases various active ingredients such as natural flavonoids, polyphenols and the like rich in the toona sinensis, endows the baijiu with a new unique mixed fragrance type, and has pharmacological effects of reducing blood sugar, reducing blood fat, resisting aging, resisting tumors and the like. The method improves the preparation efficiency, reduces the production cost and is suitable for large-scale high-efficiency production.
In order to achieve the purpose, the invention adopts the following technical scheme:
a preparation method of a Chinese toon white spirit comprises the following steps:
a. raw material selection and pretreatment:
selecting fresh, disease-free and tender Chinese toon sprouts which are 10-15 cm long and are not lignified as initial raw materials, washing pollutants on the surfaces of the Chinese toon sprouts with clear water, and not excessively kneading the Chinese toon sprouts during cleaning so as to avoid tissue damage; using sodium bicarbonate with the mass fraction of 0.2% as a blanching liquid to blanch clean Chinese toon sprouts for 30s to complete the de-enzyming treatment of the Chinese toon leaves; immediately taking out the Chinese toon sprouts after blanching treatment, putting the Chinese toon sprouts into a sodium bicarbonate solution for cooling, and meanwhile, adopting a plurality of containers for containing cooling liquid for accelerating cooling to carry out graded cooling; then, controlling the dry moisture of the cooled Chinese toon sprouts, putting the cooled Chinese toon sprouts into a sterilized plastic bag according to the filling amount of 0.5 kg/bag, and placing, wherein the heads and the tails of the Chinese toon sprouts are arranged orderly, and the openings of the bags are folded; then placing the packaged toona sinensis into a freezer at the temperature of minus 80 ℃, quickly freezing for at least 24 hours, and transferring the quickly frozen bagged toona sinensis buds to the environment at the temperature of minus 18 ℃ for low-temperature storage for later use; taking base wine with the alcoholic strength of 40-60 degrees (v/v) as raw wine for later use; preferably, base wine with the alcoholic strength of 42-53 degrees (v/v) is used as raw wine;
b. freeze drying and crushing:
taking out the Chinese toon sprouts preserved at the low temperature in the step a from the bag, tiling until the tiling thickness is not more than 5cm, and then putting the tiled Chinese toon sprouts into a freezing vacuum drying machine at the temperature of between 50 ℃ below zero and 40 ℃ below zero for vacuum drying treatment to obtain dried Chinese toon sprouts; then taking out the dried Chinese toon sprouts, putting the dried Chinese toon sprouts into a grinder for grinding, sieving the ground Chinese toon sprouts through a 100-mesh sieve, bagging the Chinese toon sprout powder, and storing the bagged Chinese toon sprout powder for later use; as a preferred technical scheme of the invention, when the toona sinensis buds are dried in vacuum, the drying time is at least 36h, and the vacuum degree is controlled to be 20-50 Pa;
c. extracting the active ingredients of the Chinese toon:
transferring the toona sinensis powder prepared in the step b into an extraction device, adding an ethanol water solution with the concentration of 70% (v/v) into the toona sinensis powder to obtain a mixed solution, putting the mixed solution into an ultrasonic instrument, performing ultrasonic-assisted extraction, filtering, taking a supernatant, extracting for at least three times, performing extraction treatment for at least 0.5h each time, and combining the supernatants to obtain an active ingredient solution of the toona sinensis; when the extraction of the active ingredients of the cedrela sinensis is carried out, the solid-to-liquid ratio (w/v) of the cedrela sinensis powder and the ethanol water solution is preferably 1 g: 30 ml;
d. concentration and freeze drying:
c, concentrating the toona sinensis active ingredient solution prepared in the step c at 46 ℃ by using a rotary evaporator for at least 1h to the required concentration, and freezing and storing; freezing at-80 deg.C for 24 hr, vacuum freeze drying to obtain dry powder of the ethanol extract of Toona sinensis, and sealing for storage;
e. preparing, filtering, post-treating and packaging the cedrela sinensis wine:
adding the dry powder of the toona sinensis alcohol extract prepared in the step d into base liquor according to the mixing proportion of adding not less than 0.3g of dry powder of the toona sinensis alcohol extract into 500ml of raw liquor to obtain toona sinensis liquor, filtering the toona sinensis liquor by adopting a vacuum filtering method, carrying out high-pressure sterilization, and carrying out glass bottle filling on the toona sinensis liquor to obtain the finished product of the toona sinensis liquor. As a preferred technical scheme of the invention, the preparation of the toona sinensis wine is carried out according to the mixing proportion of 0.5g of toona sinensis alcohol extract dry powder added in every 500ml of raw material wine, and the material-liquid ratio is 0.5g of alcohol extract dry powder: 500ml of Chinese toon white spirit. Preferably, the dry extract content of the finished product of the Chinese toon white spirit is not less than 1.0 g/L. As the preferred technical scheme of the invention, the finished Chinese toon white spirit has uniform and consistent color, is clear and transparent, is light yellow, and has no suspended matters and precipitates. As a preferred technical scheme of the invention, in the preparation process of the cedrela sinensis wine, the dry powder of the cedrela sinensis alcohol extract is added into the base wine according to the proportion of the mixing proportion of at least 0.5g +/-0.2 g of the dry powder of the cedrela sinensis alcohol extract added into 500ml of raw material wine.
1. The Chinese toon white spirit prepared by the method has the characteristic of high-degree white spirit, and various active ingredients such as natural flavonoids, polyphenols and the like which are rich in Chinese toon are added in the white spirit, so that the white spirit has a new fragrance, and has pharmacological actions such as blood sugar reduction, blood fat reduction, aging resistance, tumor resistance and the like;
2. the white spirit product prepared by the method has uniform and consistent color, is in a light yellow transparent shape, has specific and attractive flavor, embodies the unique aroma of the cedrela sinensis, is pure and elegant, is harmonious and pleasant, and has full taste. The integral characteristics are as follows: the wine is typical and clear, the style is obvious, and the wine body is perfect;
3. the cedrela sinensis wine prepared by the method has long shelf life, is convenient to carry and is easy to eat; with the improvement of living standard and the enhancement of health consciousness, the cedrela sinensis wine product meets the public love to cedrela sinensis and white spirit, and the cedrela sinensis wine product and the white spirit are organically combined together, so that the problem of seasonal insufficiency of the cedrela sinensis is solved.
Detailed Description
The above-described scheme is further illustrated below with reference to specific embodiments, which are detailed below:
the first embodiment is as follows:
in this embodiment, a preparation method of cedrela sinensis-flavored maotai liquor comprises the following steps:
a. raw material selection and pretreatment:
selecting fresh and disease-free tender cedrela sinensis buds which are 10-15 cm long and are not lignified as initial raw materials, wherein fresh and tender cedrela sinensis leaves are fresh, rot-free and pollution-free;
cleaning pollutants on the surfaces of the Chinese toon buds by using clear water, wherein excessive rubbing is not needed during cleaning so as to avoid tissue damage;
then, using sodium bicarbonate with the mass fraction of 0.2% as a blanching liquid to blanch clean Chinese toon sprouts for 30s, and completing the de-enzyming treatment of the Chinese toon leaves;
immediately taking out the Chinese toon sprouts after blanching treatment, putting the Chinese toon sprouts into a sodium bicarbonate solution for cooling, and meanwhile, adopting a plurality of containers for containing cooling liquid for accelerating cooling to carry out graded cooling;
then draining the cooled Chinese toon sprouts, putting the cooled Chinese toon sprouts into a sterilized plastic bag according to the loading amount of 0.5 kg/bag, and placing, wherein the heads and the tails of the Chinese toon sprouts are arranged orderly, and the bag openings are folded;
then placing the packaged toona sinensis into a freezer at the temperature of minus 80 ℃, quickly freezing for 24 hours, and transferring the quickly frozen bagged toona sinensis buds to the environment at the temperature of minus 18 ℃ for low-temperature storage for later use;
selecting 500ml of 53-degree Maotai liquor as base liquor and raw liquor for later use, wherein the liquor is unique in flavor of Maotai, cellar bottom and mellow, sweet and fragrant, perfect in liquor body, elegant in fragrance, full in liquor flavor and mellow;
b. freeze drying and crushing:
taking out the Chinese toon sprouts preserved at the low temperature in the step a from the bag, tiling until the tiling thickness is not more than 5cm, then putting the tiled Chinese toon sprouts into a freezing vacuum drying machine at the temperature of between 50 ℃ below zero and 40 ℃ below zero for vacuum drying treatment for 36 hours, and controlling the vacuum degree to be 20 to 50 Pa; obtaining dried Chinese toon sprouts;
then taking out the dried Chinese toon sprouts, putting the dried Chinese toon sprouts into a grinder for grinding, sieving the ground Chinese toon sprouts through a 100-mesh sieve, bagging the Chinese toon sprout powder, and storing the bagged Chinese toon sprout powder to prepare ultramicro Chinese toon for later use;
c. extracting the active ingredients of the Chinese toon:
transferring the toona sinensis powder prepared in the step b to an extraction device, wherein the solid-to-liquid ratio (w/v) of the toona sinensis powder to an ethanol aqueous solution is 1 g: adding ethanol aqueous solution with the concentration of 70% (v/v) into the toona sinensis powder according to the proportion of 30ml to obtain mixed solution, putting the mixed solution into an ultrasonic instrument, carrying out ultrasonic-assisted extraction, filtering, taking supernatant, extracting for at least three times, carrying out extraction treatment for 0.5h each time, and combining the supernatants to obtain toona sinensis active ingredient solution;
d. concentration and freeze drying:
c, concentrating the toona sinensis active ingredient solution prepared in the step c at 46 ℃ by using a rotary evaporator for at least 1h to the required concentration, and freezing and storing;
transferring the frozen toona sinensis extract into a vacuum freeze dryer, freezing at-80 ℃ for 36h to obtain toona sinensis alcohol extract dry powder, and sealing and storing;
e. modulation, filtration, post-treatment and packaging of the cedrela sinensis wine:
adding the dry powder of the toona sinensis alcohol extract prepared in the step d into the base liquor according to the mixing ratio of 0.5g of dry powder of the toona sinensis alcohol extract added into 500ml of raw liquor to obtain toona sinensis white liquor, filtering the toona sinensis white liquor by adopting a vacuum filtration method, carrying out high-pressure sterilization, and carrying out glass bottle filling on the toona sinensis white liquor to obtain the finished product of the toona sinensis white liquor.
In this embodiment, the cedrela sinensis wine is prepared according to the mixing ratio of 0.5g of dry powder of the cedrela sinensis alcohol extract added to 500ml of raw material wine, and the material-liquid ratio is 0.5g of dry powder of the alcohol extract: 500ml of Chinese toon white spirit.
The cedrela sinensis and typhoon resistant wine prepared by the embodiment has the characteristics that:
alcohol content: 53 degrees; net content: 500 ml; the dry extract (g/L) is more than or equal to 1.0;
sensory indexes are as follows: the color is uniform, clear and transparent, is light yellow, and has no suspended matters and precipitates;
taste and flavor: the wine has strong cedrela sinensis fruit flavor and sauce flavor, is mellow and full, and has pure and elegant fragrance;
and (3) integration: the wine is typically clear, remarkable in style and perfect in body.
In the embodiment, the active ingredients of the toona sinensis leaves are extracted and prepared into dry powder integrating treatment, adjustment and health care through technologies such as ultrasonic-assisted extraction and vacuum freeze drying. The white spirit product prepared by the embodiment is positioned to have the functions of appetizing, reducing blood sugar, reducing pressure and the like, is suitable for middle-aged and elderly people, and has high nutritive value, pleasant aroma and higher medical health-care effect.
Example two:
this embodiment is substantially the same as the first embodiment, and is characterized in that:
in this embodiment, a preparation method of a toona sinensis-flavor wuliangye wine includes the following steps:
a. raw material selection and pretreatment:
selecting fresh and disease-free tender cedrela sinensis buds which are 10-15 cm long and are not lignified as initial raw materials, wherein fresh and tender cedrela sinensis leaves are fresh, rot-free and pollution-free;
cleaning pollutants on the surfaces of the Chinese toon buds by using clear water, wherein excessive rubbing is not needed during cleaning so as to avoid tissue damage;
then, using sodium bicarbonate with the mass fraction of 0.2% as a blanching liquid to blanch clean Chinese toon sprouts for 30s, and completing the de-enzyming treatment of the Chinese toon leaves;
immediately taking out the Chinese toon sprouts after blanching treatment, putting the Chinese toon sprouts into a sodium bicarbonate solution for cooling, and meanwhile, adopting a plurality of containers for containing cooling liquid for accelerating cooling to carry out graded cooling;
then draining the cooled Chinese toon sprouts, putting the cooled Chinese toon sprouts into a sterilized plastic bag according to the loading amount of 0.5 kg/bag, and placing, wherein the heads and the tails of the Chinese toon sprouts are arranged orderly, and the bag openings are folded;
then placing the packaged toona sinensis into a freezer at the temperature of minus 80 ℃, quickly freezing for 24 hours, and transferring the quickly frozen bagged toona sinensis buds to the environment at the temperature of minus 18 ℃ for low-temperature storage for later use;
500ml of five-grain liquor with 52 degrees is selected as base liquor and is used as raw material liquor for standby, the liquor body is strong-flavor, and after long-term aging and elaborate blending, the taste is fresh and sweet and endless in aftertaste;
b. freeze drying and crushing:
taking out the Chinese toon sprouts preserved at the low temperature in the step a from the bag, tiling until the tiling thickness is not more than 5cm, then putting the tiled Chinese toon sprouts into a freezing vacuum drying machine at the temperature of between 50 ℃ below zero and 40 ℃ below zero for vacuum drying treatment for 36 hours, and controlling the vacuum degree to be 20 to 50 Pa; obtaining dried Chinese toon sprouts;
then taking out the dried Chinese toon sprouts, putting the dried Chinese toon sprouts into a grinder for grinding, sieving the ground Chinese toon sprouts through a 100-mesh sieve, bagging the Chinese toon sprout powder, and storing the bagged Chinese toon sprout powder to prepare ultramicro Chinese toon for later use;
c. extracting the active ingredients of the Chinese toon:
transferring the toona sinensis powder prepared in the step b to an extraction device, wherein the solid-to-liquid ratio (w/v) of the toona sinensis powder to an ethanol aqueous solution is 1 g: adding ethanol aqueous solution with the concentration of 70% (v/v) into the toona sinensis powder according to the proportion of 30ml to obtain mixed solution, putting the mixed solution into an ultrasonic instrument, carrying out ultrasonic-assisted extraction, filtering, taking supernatant, extracting for at least three times, carrying out extraction treatment for 0.5h each time, and combining the supernatants to obtain toona sinensis active ingredient solution;
d. concentration and freeze drying:
c, concentrating the toona sinensis active ingredient solution prepared in the step c at 46 ℃ by using a rotary evaporator for at least 1h to the required concentration, and freezing and storing;
transferring the frozen toona sinensis extract into a vacuum freeze dryer, freezing at-80 ℃ for 36h to obtain toona sinensis alcohol extract dry powder, and sealing and storing;
e. modulation, filtration, post-treatment and packaging of the cedrela sinensis wine:
adding the dry powder of the toona sinensis alcohol extract prepared in the step d into the base liquor according to the mixing ratio of 0.5g of dry powder of the toona sinensis alcohol extract added into 500ml of raw liquor to obtain toona sinensis white liquor, filtering the toona sinensis white liquor by adopting a vacuum filtration method, carrying out high-pressure sterilization, and carrying out glass bottle filling on the toona sinensis white liquor to obtain the finished product of the toona sinensis white liquor.
In this embodiment, the cedrela sinensis wine is prepared according to the mixing ratio of 0.5g of dry powder of the cedrela sinensis alcohol extract added to 500ml of raw material wine, and the material-liquid ratio is 0.5g of dry powder of the alcohol extract: 500ml of Chinese toon white spirit.
The toona sinensis five-grain liquor prepared by the embodiment has the characteristics that:
alcohol content: 52 degrees; net content: 500 ml; the dry extract (g/L) is more than or equal to 1.0;
sensory indexes are as follows: uniform color, clear and transparent, light yellow color, no suspended matter and precipitate
Taste and flavor: has strong cedrela sinensis fruit fragrance, lingering dizzy and soft mouthfeel and slightly sweet
And (3) integration: the wine is typically clear, remarkable in style and perfect in body.
In the embodiment, the active ingredients of the toona sinensis leaves are extracted and prepared into dry powder integrating treatment, adjustment and health care through technologies such as ultrasonic-assisted extraction and vacuum freeze drying. The white spirit product prepared by the embodiment is positioned to have the functions of appetizing, reducing blood sugar, reducing pressure and the like, is suitable for middle-aged and elderly people, and has high nutritive value, pleasant aroma and higher medical health-care effect.
Example three:
this embodiment is substantially the same as the previous embodiment, and is characterized in that:
in this embodiment, a method for preparing toona sinensis-flavor gujinggong wine includes the following steps:
a. raw material selection and pretreatment:
selecting fresh and disease-free tender cedrela sinensis buds which are 10-15 cm long and are not lignified as initial raw materials, wherein fresh and tender cedrela sinensis leaves are fresh, rot-free and pollution-free;
cleaning pollutants on the surfaces of the Chinese toon buds by using clear water, wherein excessive rubbing is not needed during cleaning so as to avoid tissue damage;
then, using sodium bicarbonate with the mass fraction of 0.2% as a blanching liquid to blanch clean Chinese toon sprouts for 30s, and completing the de-enzyming treatment of the Chinese toon leaves;
immediately taking out the Chinese toon sprouts after blanching treatment, putting the Chinese toon sprouts into a sodium bicarbonate solution for cooling, and meanwhile, adopting a plurality of containers for containing cooling liquid for accelerating cooling to carry out graded cooling;
then draining the cooled Chinese toon sprouts, putting the cooled Chinese toon sprouts into a sterilized plastic bag according to the loading amount of 0.5 kg/bag, and placing, wherein the heads and the tails of the Chinese toon sprouts are arranged orderly, and the bag openings are folded;
then placing the packaged toona sinensis into a freezer at the temperature of minus 80 ℃, quickly freezing for 24 hours, and transferring the quickly frozen bagged toona sinensis buds to the environment at the temperature of minus 18 ℃ for low-temperature storage for later use;
500ml of 50-degree Gujing tribute wine is selected as base wine and is used as raw material wine for standby, the wine body is strong-flavor, and after long-term aging, the wine body is carefully blended, and the taste is fresh and sweet and endless in aftertaste;
b. freeze drying and crushing:
taking out the Chinese toon sprouts preserved at the low temperature in the step a from the bag, tiling until the tiling thickness is not more than 5cm, then putting the tiled Chinese toon sprouts into a freezing vacuum drying machine at the temperature of between 50 ℃ below zero and 40 ℃ below zero for vacuum drying treatment for 36 hours, and controlling the vacuum degree to be 20 to 50 Pa; obtaining dried Chinese toon sprouts;
then taking out the dried Chinese toon sprouts, putting the dried Chinese toon sprouts into a grinder for grinding, sieving the ground Chinese toon sprouts through a 100-mesh sieve, bagging the Chinese toon sprout powder, and storing the bagged Chinese toon sprout powder to prepare ultramicro Chinese toon for later use;
c. extracting the active ingredients of the Chinese toon:
transferring the toona sinensis powder prepared in the step b to an extraction device, wherein the solid-to-liquid ratio (w/v) of the toona sinensis powder to an ethanol aqueous solution is 1 g: adding ethanol aqueous solution with the concentration of 70% (v/v) into the toona sinensis powder according to the proportion of 30ml to obtain mixed solution, putting the mixed solution into an ultrasonic instrument, carrying out ultrasonic-assisted extraction, filtering, taking supernatant, extracting for at least three times, carrying out extraction treatment for 0.5h each time, and combining the supernatants to obtain toona sinensis active ingredient solution;
d. concentration and freeze drying:
c, concentrating the toona sinensis active ingredient solution prepared in the step c at 46 ℃ by using a rotary evaporator for at least 1h to the required concentration, and freezing and storing;
transferring the frozen toona sinensis extract into a vacuum freeze dryer, freezing at-80 ℃ for 36h to obtain toona sinensis alcohol extract dry powder, and sealing and storing;
e. modulation, filtration, post-treatment and packaging of the cedrela sinensis wine:
adding the dry powder of the toona sinensis alcohol extract prepared in the step d into the base liquor according to the mixing ratio of 0.5g of dry powder of the toona sinensis alcohol extract added into 500ml of raw liquor to obtain toona sinensis white liquor, filtering the toona sinensis white liquor by adopting a vacuum filtration method, carrying out high-pressure sterilization, and carrying out glass bottle filling on the toona sinensis white liquor to obtain the finished product of the toona sinensis white liquor.
In this embodiment, the cedrela sinensis wine is prepared according to the mixing ratio of 0.5g of dry powder of the cedrela sinensis alcohol extract added to 500ml of raw material wine, and the material-liquid ratio is 0.5g of dry powder of the alcohol extract: 500ml of Chinese toon white spirit.
The Chinese toon gujing tribute wine prepared by the embodiment has the characteristics that:
alcohol content: 50 degrees; net content: 500 ml; the dry extract (g/L) is more than or equal to 1.0;
sensory indexes are as follows: uniform color, clear and transparent, light yellow color, no suspended matter and precipitate
Taste and flavor: has strong cedrela sinensis fruit fragrance, mellow and full wine body, fresh and sweet taste and proper sour and sweet taste
And (3) integration: the wine is typically clear, remarkable in style and perfect in body.
In the embodiment, the active ingredients of the toona sinensis leaves are extracted and prepared into dry powder integrating treatment, adjustment and health care through technologies such as ultrasonic-assisted extraction and vacuum freeze drying. The white spirit product prepared by the embodiment is positioned to have the functions of appetizing, reducing blood sugar, reducing pressure and the like, is suitable for middle-aged and elderly people, and has high nutritive value, pleasant aroma and higher medical health-care effect.
Example four:
this embodiment is substantially the same as the previous embodiment, and is characterized in that:
in this embodiment, a method for preparing a toona sinensis-flavor Yingjia tribute wine includes the following steps:
a. raw material selection and pretreatment:
selecting fresh and disease-free tender cedrela sinensis buds which are 10-15 cm long and are not lignified as initial raw materials, wherein fresh and tender cedrela sinensis leaves are fresh, rot-free and pollution-free;
cleaning pollutants on the surfaces of the Chinese toon buds by using clear water, wherein excessive rubbing is not needed during cleaning so as to avoid tissue damage;
then, using sodium bicarbonate with the mass fraction of 0.2% as a blanching liquid to blanch clean Chinese toon sprouts for 30s, and completing the de-enzyming treatment of the Chinese toon leaves;
immediately taking out the Chinese toon sprouts after blanching treatment, putting the Chinese toon sprouts into a sodium bicarbonate solution for cooling, and meanwhile, adopting a plurality of containers for containing cooling liquid for accelerating cooling to carry out graded cooling;
then draining the cooled Chinese toon sprouts, putting the cooled Chinese toon sprouts into a sterilized plastic bag according to the loading amount of 0.5 kg/bag, and placing, wherein the heads and the tails of the Chinese toon sprouts are arranged orderly, and the bag openings are folded;
then placing the packaged toona sinensis into a freezer at the temperature of minus 80 ℃, quickly freezing for 24 hours, and transferring the quickly frozen bagged toona sinensis buds to the environment at the temperature of minus 18 ℃ for low-temperature storage for later use;
500ml of 42-degree Yingjia tribute wine is selected as base wine and is used as raw material wine for standby, the wine body is clear and transparent, the cellar aroma is strong, and the taste is sweet and sweet;
b. freeze drying and crushing:
taking out the Chinese toon sprouts preserved at the low temperature in the step a from the bag, tiling until the tiling thickness is not more than 5cm, then putting the tiled Chinese toon sprouts into a freezing vacuum drying machine at the temperature of between 50 ℃ below zero and 40 ℃ below zero for vacuum drying treatment for 36 hours, and controlling the vacuum degree to be 20 to 50 Pa; obtaining dried Chinese toon sprouts;
then taking out the dried Chinese toon sprouts, putting the dried Chinese toon sprouts into a grinder for grinding, sieving the ground Chinese toon sprouts through a 100-mesh sieve, bagging the Chinese toon sprout powder, and storing the bagged Chinese toon sprout powder to prepare ultramicro Chinese toon for later use;
c. extracting the active ingredients of the Chinese toon:
transferring the toona sinensis powder prepared in the step b to an extraction device, wherein the solid-to-liquid ratio (w/v) of the toona sinensis powder to an ethanol aqueous solution is 1 g: adding ethanol aqueous solution with the concentration of 70% (v/v) into the toona sinensis powder according to the proportion of 30ml to obtain mixed solution, putting the mixed solution into an ultrasonic instrument, carrying out ultrasonic-assisted extraction, filtering, taking supernatant, extracting for at least three times, carrying out extraction treatment for 0.5h each time, and combining the supernatants to obtain toona sinensis active ingredient solution;
d. concentration and freeze drying:
c, concentrating the toona sinensis active ingredient solution prepared in the step c at 46 ℃ by using a rotary evaporator for at least 1h to the required concentration, and freezing and storing;
transferring the frozen toona sinensis extract into a vacuum freeze dryer, freezing at-80 ℃ for 36h to obtain toona sinensis alcohol extract dry powder, and sealing and storing;
e. modulation, filtration, post-treatment and packaging of the cedrela sinensis wine:
adding the dry powder of the toona sinensis alcohol extract prepared in the step d into the base liquor according to the mixing ratio of 0.5g of dry powder of the toona sinensis alcohol extract added into 500ml of raw liquor to obtain toona sinensis white liquor, filtering the toona sinensis white liquor by adopting a vacuum filtration method, carrying out high-pressure sterilization, and carrying out glass bottle filling on the toona sinensis white liquor to obtain the finished product of the toona sinensis white liquor.
In this embodiment, the cedrela sinensis wine is prepared according to the mixing ratio of 0.5g of dry powder of the cedrela sinensis alcohol extract added to 500ml of raw material wine, and the material-liquid ratio is 0.5g of dry powder of the alcohol extract: 500ml of Chinese toon white spirit.
The cedrela sinensis Yingjia tribute wine prepared by the embodiment has the characteristics that:
alcohol content: 42 degrees; net content: 500 ml; dry extract (g/L) is more than or equal to 1.0
Sensory indexes are as follows: uniform color, clear and transparent, light yellow color, no suspended matter and precipitate
Taste and flavor: the wine body is clear and transparent, the cellar fragrance is strong, the taste is sweet and sweet, the wine body is full, and typical strong aromatic white spirit is whole: the wine is typically clear, remarkable in style and perfect in body.
In the embodiment, the active ingredients of the toona sinensis leaves are extracted and prepared into dry powder integrating treatment, adjustment and health care through technologies such as ultrasonic-assisted extraction and vacuum freeze drying. The white spirit product prepared by the embodiment is positioned to have the functions of appetizing, reducing blood sugar, reducing pressure and the like, is suitable for middle-aged and elderly people, and has high nutritive value, pleasant aroma and higher medical health-care effect.
In conclusion, the cedrela sinensis belongs to a medicine-food homologous food, has no toxic or side effect, contains a large amount of biological active ingredients such as flavonoids, polyphenol compounds and polysaccharides, and has pharmacological effects of reducing blood sugar, reducing blood fat, resisting aging, resisting tumors and the like. The liquor has a long history in China, is an indispensable part of dining table culture, and is beneficial to health when being drunk properly. By adopting the toona sinensis liquor process in the technical scheme of the embodiment of the invention, the extraction rate is high, the toona sinensis and the liquor are organically fused, the health care function of the liquor can be obviously increased, the liquor is endowed with the special flavor of the toona sinensis, and the effects of resisting oxidation, reducing blood sugar, inhibiting bacteria and viruses, preventing cardiovascular and cerebrovascular diseases, enhancing resistance, resisting aging and the like can be achieved, so that the effect of prolonging life is achieved; in addition, the deep processing way of the cedrela sinensis is increased, the utilization rate is improved, and the economic income of farmers is increased. The product produced by the raw materials in the embodiment is light yellow, has the unique fresh taste of the Chinese toon, and has fine, soft and smooth mouthfeel; the product has wide application objects. The novel white spirit product prepared by the embodiment adopts the technologies of vacuum freeze drying, microwave, rotary steaming and the like, and the operation process is simple; the raw materials are low in price and wide in source, and are suitable for industrial large-scale production.
The above embodiments of the present invention have been described, but the present invention is not limited to the above embodiments, and various changes and modifications can be made according to the purpose of the invention, and any changes, modifications, substitutions, combinations or simplifications made according to the spirit and principle of the technical solution of the present invention shall be equivalent substitutions, as long as the purpose of the present invention is met, and the present invention shall fall within the protection scope of the present invention as long as the technical principle and the inventive concept of the method for preparing the toona sinensis spirit of the present invention are not departed.
Claims (8)
1. A preparation method of a Chinese toon white spirit is characterized by comprising the following steps:
a. raw material selection and pretreatment:
selecting fresh, disease-free and tender Chinese toon sprouts which are 10-15 cm long and are not lignified as initial raw materials, washing pollutants on the surfaces of the Chinese toon sprouts with clear water, and not excessively kneading the Chinese toon sprouts during cleaning so as to avoid tissue damage; using sodium bicarbonate with the mass fraction of 0.2% as a blanching liquid to blanch clean Chinese toon sprouts for 30s to complete the de-enzyming treatment of the Chinese toon leaves; immediately taking out the Chinese toon sprouts after blanching treatment, putting the Chinese toon sprouts into a sodium bicarbonate solution for cooling, and meanwhile, adopting a plurality of containers for containing cooling liquid for accelerating cooling to carry out graded cooling; then, controlling the dry moisture of the cooled Chinese toon sprouts, putting the cooled Chinese toon sprouts into a sterilized plastic bag according to the filling amount of 0.5 kg/bag, and placing, wherein the heads and the tails of the Chinese toon sprouts are arranged orderly, and the openings of the bags are folded; then placing the packaged toona sinensis into a freezer at the temperature of minus 80 ℃, quickly freezing for at least 24 hours, and transferring the quickly frozen bagged toona sinensis buds to the environment at the temperature of minus 18 ℃ for low-temperature storage for later use; taking base wine with the alcoholic strength of 40-60 degrees (v/v) as raw wine for later use;
b. freeze drying and crushing:
taking out the Chinese toon sprouts preserved at the low temperature in the step a from the bag, tiling until the tiling thickness is not more than 5cm, and then putting the tiled Chinese toon sprouts into a freezing vacuum drying machine at the temperature of between 50 ℃ below zero and 40 ℃ below zero for vacuum drying treatment to obtain dried Chinese toon sprouts; then taking out the dried Chinese toon sprouts, putting the dried Chinese toon sprouts into a grinder for grinding, sieving the ground Chinese toon sprouts through a 100-mesh sieve, bagging the Chinese toon sprout powder, and storing the bagged Chinese toon sprout powder for later use;
c. extracting the active ingredients of the Chinese toon:
transferring the toona sinensis powder prepared in the step b into an extraction device, adding an ethanol water solution with the concentration of 70% (v/v) into the toona sinensis powder to obtain a mixed solution, putting the mixed solution into an ultrasonic instrument, performing ultrasonic-assisted extraction, filtering, taking a supernatant, extracting for at least three times, performing extraction treatment for at least 0.5h each time, and combining the supernatants to obtain an active ingredient solution of the toona sinensis;
d. concentration and freeze drying:
c, concentrating the toona sinensis active ingredient solution prepared in the step c at 46 ℃ by using a rotary evaporator for at least 1h to the required concentration, and freezing and storing; freezing at-80 deg.C for 24 hr, vacuum freeze drying to obtain dry powder of the ethanol extract of Toona sinensis, and sealing for storage;
e. preparing, filtering, post-treating and packaging the cedrela sinensis wine:
adding the dry powder of the toona sinensis alcohol extract prepared in the step d into base liquor according to the mixing proportion of adding not less than 0.3g of dry powder of the toona sinensis alcohol extract into 500ml of raw liquor to obtain toona sinensis liquor, filtering the toona sinensis liquor by adopting a vacuum filtering method, carrying out high-pressure sterilization, and carrying out glass bottle filling on the toona sinensis liquor to obtain the finished product of the toona sinensis liquor.
2. The preparation method of the toona sinensis baijiu according to claim 1, which is characterized by comprising the following steps: in the step e, the cedrela sinensis wine is prepared according to the mixing proportion of 0.5g of dry powder of the cedrela sinensis alcohol extract added into 500ml of raw material wine, and the material-liquid ratio is 0.5g of dry powder of the alcohol extract: 500ml of Chinese toon white spirit.
3. The preparation method of the toona sinensis baijiu according to claim 1, which is characterized by comprising the following steps: in the step e, the content of the dry extract of the finished product of the Chinese toon white spirit is not less than 1.0 g/L.
4. The preparation method of the toona sinensis baijiu according to claim 1, which is characterized by comprising the following steps: in the step e, the finished product of the Chinese toon white spirit is uniform in color, clear, transparent and light yellow, and has no suspended matters and precipitates.
5. The preparation method of the toona sinensis baijiu according to claim 1, which is characterized by comprising the following steps: in the step a, the base wine with the alcoholic strength of 42-53 degrees (v/v) is used as the raw wine.
6. The preparation method of the toona sinensis baijiu according to claim 1, which is characterized by comprising the following steps: in the step b, when the Chinese toon sprouts are dried in vacuum, the drying time is at least 36h, and the vacuum degree is controlled to be 20-50 Pa.
7. The preparation method of the toona sinensis baijiu according to claim 1, which is characterized by comprising the following steps: in the step c, when the active ingredients of the cedrela sinensis are extracted, the solid-to-liquid ratio (w/v) of the cedrela sinensis powder to the ethanol water solution is 1 g: 30 ml.
8. The preparation method of the toona sinensis baijiu according to claim 1, which is characterized by comprising the following steps: in the step e, in the preparation process of the cedrela sinensis wine, adding the dried powder of the cedrela sinensis alcohol extract into the base wine according to the proportion of the mixing proportion of adding at least 0.5g +/-0.2 g of the dried powder of the cedrela sinensis alcohol extract into 500ml of the raw material wine.
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