CN110776747A - Heat-insulating waterproof material and preparation method thereof - Google Patents
Heat-insulating waterproof material and preparation method thereof Download PDFInfo
- Publication number
- CN110776747A CN110776747A CN201911082521.5A CN201911082521A CN110776747A CN 110776747 A CN110776747 A CN 110776747A CN 201911082521 A CN201911082521 A CN 201911082521A CN 110776747 A CN110776747 A CN 110776747A
- Authority
- CN
- China
- Prior art keywords
- parts
- weight
- waterproof material
- raw materials
- ethylene glycol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Sealing Material Composition (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention provides a heat-insulating waterproof material which is prepared from the following raw materials: compared with the prior art, the mica bonding silicon resin, the epoxy resin, the sodium stearate, the graphite powder, the N-dodecyl ethanolamine, the hydroxypropyl methyl cellulose, the titanate coupling agent, the aluminum silicate powder, the ethylene glycol and the xanthan gum have the following beneficial effects: the anti-seepage effect, the tensile strength and the like of the waterproof material are improved, and the waterproof material has a better waterproof effect, wide application range, low temperature resistance, good waterproof performance and good bonding performance when being used for waterproofing walls, floors and the like.
Description
Technical Field
The invention relates to a heat-insulating waterproof material and a preparation method thereof, belonging to the technical field of waterproof materials.
Background
Along with the development of the building industry, the waterproof material in China is rapidly developed, in recent years, on the basis of meeting the use function of a product, the development of a novel environment-friendly and energy-saving waterproof material is increasingly supported, the use of a hot-melt coiled material which has a large influence on the environment is limited, and the self-adhesive coiled material capable of being subjected to cold construction is greatly popularized and applied all over the world; the self-adhesive coiled material has a series of characteristics of good low-temperature flexibility, large elongation, adaptation to deformation of a base layer, good cracking resistance and self-healing property, long service life and the like, and is convenient, safe, simple and environment-friendly to construct; however, the existing self-adhesive waterproof material has a plurality of unsatisfactory places, wherein the most remarkable defect is that the self-adhesive waterproof material is not adhered at low temperature, the construction of the common self-adhesive waterproof coiled material generally requires that the self-adhesive waterproof material is stable above 10 ℃, if the temperature is too low, the adhesive force of the coiled material is reduced, the construction by heating is usually needed, and the cold construction characteristic of the coiled material is lost; meanwhile, if water is encountered during construction of the common self-adhesive full color, the adhesive property is seriously reduced, great difficulty is brought to construction, and the waterproof layer has great hidden danger of leakage; at present, the common self-adhesive waterproof material can not completely meet the requirements of waterproof engineering; for the reasons, the research and development of novel heat-insulating, waterproof and bondable self-adhesive materials are needed to meet the use requirements of the waterproof material industry in China.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide a heat-insulating waterproof material and a preparation method thereof, so as to solve the problems in the background technology.
In order to achieve the purpose, the invention is realized by the following technical scheme: a heat-insulating waterproof material is composed of the following raw materials: mica bonding silicon resin, epoxy resin, sodium stearate, graphite powder, N-dodecyl ethanolamine, hydroxypropyl methyl cellulose, titanate coupling agent, aluminum silicate powder, ethylene glycol and xanthan gum.
Further, the feed additive is composed of the following raw materials in parts by weight: 20-30 parts of mica bonded silicon resin, 10-15 parts of epoxy resin, 3-6 parts of sodium stearate, 2-4 parts of graphite powder, 2-4 parts of N-dodecyl ethanolamine, 1-3 parts of hydroxypropyl methyl cellulose, 5-7 parts of titanate coupling agent, 3-6 parts of aluminum silicate powder, 2-5 parts of ethylene glycol and 1-2 parts of xanthan gum.
Further, the feed additive is composed of the following raw materials in parts by weight: 20 parts of mica bonded silicon resin, 15 parts of epoxy resin, 3 parts of sodium stearate, 4 parts of graphite powder, 2 parts of N-dodecyl ethanolamine, 3 parts of hydroxypropyl methyl cellulose, 5 parts of titanate coupling agent, 6 parts of aluminum silicate powder, 5 parts of ethylene glycol and 1 part of xanthan gum.
Further, the feed additive is composed of the following raw materials in parts by weight: 30 parts of mica bonded silicon resin, 15 parts of epoxy resin, 6 parts of sodium stearate, 4 parts of graphite powder, 4 parts of N-dodecyl ethanolamine, 3 parts of hydroxypropyl methyl cellulose, 7 parts of titanate coupling agent, 6 parts of aluminum silicate powder, 5 parts of ethylene glycol and 2 parts of xanthan gum.
Further, ethylene oxide and water are hydrated in a liquid phase in a tubular reactor under the conditions of 2.23MPa and 190-200 ℃ to prepare ethylene glycol.
Further, adding stearic acid into the reaction kettle, heating to be molten, adding NaOH aqueous solution under stirring, heating at 65 ℃ for 2 hours, controlling the pH value to be 8.0-8.5, and spray-drying to obtain sodium stearate in the raw materials.
A preparation method of a heat-insulating waterproof material is characterized by comprising the following steps: prepared by the following steps: placing 30 parts by weight of mica bonding silicon resin, 15 parts by weight of epoxy resin and 4 parts by weight of N-dodecyl ethanolamine into an internal mixer for internal mixing for 7-8 minutes, adding 3 parts by weight of hydroxypropyl methyl cellulose and 7 parts by weight of titanate coupling agent, and continuously internal mixing until the temperature of rubber rises to 100 ℃; adding the raw materials in an internal mixer into a stirrer, sequentially adding 6 parts by weight of sodium stearate, 4 parts by weight of graphite powder, 6 parts by weight of aluminum silicate powder, 5 parts by weight of ethylene glycol and 2 parts by weight of xanthan gum while stirring, and uniformly stirring to obtain the finished product material.
The invention has the beneficial effects that: the heat-insulating waterproof material and the preparation method thereof improve the anti-seepage effect, tensile strength and the like of the waterproof material, have better waterproof effect when being used for waterproofing walls, floors and the like, and have wide application range, low temperature resistance, good waterproof performance and good bonding performance of products.
Detailed Description
In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the invention is further described with the specific embodiments.
The invention provides a technical scheme that: a heat-insulating waterproof material is composed of the following raw materials: mica bonding silicon resin, epoxy resin, sodium stearate, graphite powder, N-dodecyl ethanolamine, hydroxypropyl methyl cellulose, titanate coupling agent, aluminum silicate powder, ethylene glycol and xanthan gum.
As an embodiment of the present invention: the composite material is prepared from the following raw materials in parts by weight: 20-30 parts of mica bonded silicon resin, 10-15 parts of epoxy resin, 3-6 parts of sodium stearate, 2-4 parts of graphite powder, 2-4 parts of N-dodecyl ethanolamine, 1-3 parts of hydroxypropyl methyl cellulose, 5-7 parts of titanate coupling agent, 3-6 parts of aluminum silicate powder, 2-5 parts of ethylene glycol and 1-2 parts of xanthan gum.
As an embodiment of the present invention: the composite material is prepared from the following raw materials in parts by weight: 20 parts of mica bonded silicon resin, 15 parts of epoxy resin, 3 parts of sodium stearate, 4 parts of graphite powder, 2 parts of N-dodecyl ethanolamine, 3 parts of hydroxypropyl methyl cellulose, 5 parts of titanate coupling agent, 6 parts of aluminum silicate powder, 5 parts of ethylene glycol and 1 part of xanthan gum.
As an embodiment of the present invention: the composite material is prepared from the following raw materials in parts by weight: 30 parts of mica bonded silicon resin, 15 parts of epoxy resin, 6 parts of sodium stearate, 4 parts of graphite powder, 4 parts of N-dodecyl ethanolamine, 3 parts of hydroxypropyl methyl cellulose, 7 parts of titanate coupling agent, 6 parts of aluminum silicate powder, 5 parts of ethylene glycol and 2 parts of xanthan gum.
Ethylene oxide and water are hydrated in a liquid phase in a tubular reactor under the conditions of 2.23MPa and 190-200 ℃ to prepare ethylene glycol.
Adding stearic acid into a reaction kettle, heating to melt, adding NaOH aqueous solution under stirring, heating at 65 ℃ for 2 hours, controlling the pH value to be 8.0-8.5, and spray-drying to obtain sodium stearate in the raw materials.
A preparation method of a heat-insulating waterproof material is characterized by comprising the following steps: prepared by the following steps: placing 30 parts by weight of mica bonding silicon resin, 15 parts by weight of epoxy resin and 4 parts by weight of N-dodecyl ethanolamine into an internal mixer for internal mixing for 7-8 minutes, adding 3 parts by weight of hydroxypropyl methyl cellulose and 7 parts by weight of titanate coupling agent, and continuously internal mixing until the temperature of rubber rises to 100 ℃; adding the raw materials in an internal mixer into a stirrer, sequentially adding 6 parts by weight of sodium stearate, 4 parts by weight of graphite powder, 6 parts by weight of aluminum silicate powder, 5 parts by weight of ethylene glycol and 2 parts by weight of xanthan gum while stirring, and uniformly stirring to obtain the finished product material.
As an embodiment of the present invention: the heat-insulating waterproof material and the preparation method thereof improve the anti-seepage effect, tensile strength and the like of the waterproof material, have better waterproof effect when being used for waterproofing walls, floors and the like, and have wide application range, low temperature resistance, good waterproof performance and good bonding performance of products.
While there have been shown and described what are at present considered the fundamental principles and essential features of the invention and its advantages, it will be apparent to those skilled in the art that the invention is not limited to the details of the foregoing exemplary embodiments, but is capable of other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.
Claims (7)
1. The heat-insulating waterproof material is characterized in that: the material is composed of the following raw materials: mica bonding silicon resin, epoxy resin, sodium stearate, graphite powder, N-dodecyl ethanolamine, hydroxypropyl methyl cellulose, titanate coupling agent, aluminum silicate powder, ethylene glycol and xanthan gum.
2. A heat insulating and waterproof material according to claim 1, characterized in that: the composite material is prepared from the following raw materials in parts by weight: 20-30 parts of mica bonded silicon resin, 10-15 parts of epoxy resin, 3-6 parts of sodium stearate, 2-4 parts of graphite powder, 2-4 parts of N-dodecyl ethanolamine, 1-3 parts of hydroxypropyl methyl cellulose, 5-7 parts of titanate coupling agent, 3-6 parts of aluminum silicate powder, 2-5 parts of ethylene glycol and 1-2 parts of xanthan gum.
3. A heat insulating and waterproof material according to claim 1, characterized in that: the composite material is prepared from the following raw materials in parts by weight: 20 parts of mica bonded silicon resin, 15 parts of epoxy resin, 3 parts of sodium stearate, 4 parts of graphite powder, 2 parts of N-dodecyl ethanolamine, 3 parts of hydroxypropyl methyl cellulose, 5 parts of titanate coupling agent, 6 parts of aluminum silicate powder, 5 parts of ethylene glycol and 1 part of xanthan gum.
4. A heat insulating and waterproof material according to claim 1, characterized in that: the composite material is prepared from the following raw materials in parts by weight: 30 parts of mica bonded silicon resin, 15 parts of epoxy resin, 6 parts of sodium stearate, 4 parts of graphite powder, 4 parts of N-dodecyl ethanolamine, 3 parts of hydroxypropyl methyl cellulose, 7 parts of titanate coupling agent, 6 parts of aluminum silicate powder, 5 parts of ethylene glycol and 2 parts of xanthan gum.
5. A heat insulating and waterproof material according to claim 1, characterized in that: ethylene oxide and water are hydrated in a liquid phase in a tubular reactor under the conditions of 2.23MPa and 190-200 ℃ to prepare ethylene glycol.
6. A heat insulating and waterproof material according to claim 1, characterized in that: adding stearic acid into a reaction kettle, heating to melt, adding NaOH aqueous solution under stirring, heating at 65 ℃ for 2 hours, controlling the pH value to be 8.0-8.5, and spray-drying to obtain sodium stearate in the raw materials.
7. The preparation method of the heat-insulating waterproof material according to claim 1 or 5, characterized in that: prepared by the following steps: placing 30 parts by weight of mica bonding silicon resin, 15 parts by weight of epoxy resin and 4 parts by weight of N-dodecyl ethanolamine into an internal mixer for internal mixing for 7-8 minutes, adding 3 parts by weight of hydroxypropyl methyl cellulose and 7 parts by weight of titanate coupling agent, and continuously internal mixing until the temperature of rubber rises to 100 ℃; adding the raw materials in an internal mixer into a stirrer, sequentially adding 6 parts by weight of sodium stearate, 4 parts by weight of graphite powder, 6 parts by weight of aluminum silicate powder, 5 parts by weight of ethylene glycol and 2 parts by weight of xanthan gum while stirring, and uniformly stirring to obtain the finished product material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911082521.5A CN110776747A (en) | 2019-11-07 | 2019-11-07 | Heat-insulating waterproof material and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911082521.5A CN110776747A (en) | 2019-11-07 | 2019-11-07 | Heat-insulating waterproof material and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110776747A true CN110776747A (en) | 2020-02-11 |
Family
ID=69389515
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201911082521.5A Pending CN110776747A (en) | 2019-11-07 | 2019-11-07 | Heat-insulating waterproof material and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110776747A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112939532A (en) * | 2021-01-28 | 2021-06-11 | 浙江广成装饰工程有限公司 | Heat-insulating waterproof material for indoor decoration and construction method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20030127248A1 (en) * | 2002-01-07 | 2003-07-10 | Gorden Kuo | Protection outer layer for circuit boards and method for making the same |
| CN102690499A (en) * | 2012-06-15 | 2012-09-26 | 天津市赛朗科技发展有限公司 | Epoxy waterproof composition |
| CN106118311A (en) * | 2016-07-25 | 2016-11-16 | 张海棠 | A kind of waterproof silicone materials and preparation method thereof |
| CN106854055A (en) * | 2016-12-09 | 2017-06-16 | 广西北海浩邦新能源科技有限公司 | A kind of thermal-insulating waterproof material of good stability |
| CN107759973A (en) * | 2016-08-18 | 2018-03-06 | 四川美登家具有限公司 | A kind of epoxy resin composite material |
-
2019
- 2019-11-07 CN CN201911082521.5A patent/CN110776747A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20030127248A1 (en) * | 2002-01-07 | 2003-07-10 | Gorden Kuo | Protection outer layer for circuit boards and method for making the same |
| CN102690499A (en) * | 2012-06-15 | 2012-09-26 | 天津市赛朗科技发展有限公司 | Epoxy waterproof composition |
| CN106118311A (en) * | 2016-07-25 | 2016-11-16 | 张海棠 | A kind of waterproof silicone materials and preparation method thereof |
| CN107759973A (en) * | 2016-08-18 | 2018-03-06 | 四川美登家具有限公司 | A kind of epoxy resin composite material |
| CN106854055A (en) * | 2016-12-09 | 2017-06-16 | 广西北海浩邦新能源科技有限公司 | A kind of thermal-insulating waterproof material of good stability |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112939532A (en) * | 2021-01-28 | 2021-06-11 | 浙江广成装饰工程有限公司 | Heat-insulating waterproof material for indoor decoration and construction method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107337409B (en) | Special adhesive for foam glass heat insulation system and preparation method and use method thereof | |
| CN103289573B (en) | A kind of SBS modified waterproof asphalt material for building | |
| CN105985051A (en) | Efficient water reducing agent with additional modified starch and function of improving performance of concrete | |
| CN112960958B (en) | Sealing slurry for winter assembly type construction and preparation method thereof | |
| CN102533189A (en) | Wet-heat resisting automobile folding adhesive and preparation method thereof | |
| CN101113280A (en) | Method for producing water-proof, fire-proof, antiseptic, heat-insulation, heat-preservation, insulating waterproofing paint | |
| CN106519993A (en) | Silicate inorganic adhesive and preparation method thereof | |
| CN110776747A (en) | Heat-insulating waterproof material and preparation method thereof | |
| CN103254843A (en) | Waterproof chloroprene rubber sealant and preparation method thereof | |
| CN103254844B (en) | Light fixture neoprene packing waterproof glue and preparation method thereof | |
| CN104673087A (en) | Anti-flaking waterproof coating material for buildings and preparation method thereof | |
| CN108395865A (en) | A kind of photovoltaic back water-proof high-intensity heat-resistant adhesive and preparation method thereof | |
| CN105062416B (en) | A kind of modified pitch sealing compound and its production method | |
| CN107216577A (en) | A kind of novel PVC liquid Ca-Zn composite heat stabilizer and preparation method for adding modified Nano carbon ball | |
| CN104119716B (en) | A kind of automatically cleaning water-repellent paint | |
| CN103664120A (en) | Gypsum base phase change energy storing polymer thermal mortar | |
| CN103614017A (en) | Waterproof coating containing rosin water | |
| CN103436071A (en) | Air-conditioner pipeline wall-through sealing putty powder for and preparation method thereof | |
| CN103275619B (en) | A kind of styrene butadiene rubber modified asphalt waterproof paint for building | |
| CN105315961A (en) | Reaction type modified emulsified asphalt waterproof sealing paste and preparation method thereof | |
| CN113716893A (en) | Concrete waterproof compacting agent and preparation method thereof | |
| CN109337588B (en) | Ceramic high-temperature adhesive and preparation method thereof | |
| CN103805091A (en) | Waterproof adhesive for building | |
| CN105950062A (en) | Efficient waterproof binder and production method thereof | |
| CN104893454A (en) | Heat preservation material |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20200211 |