CN110772441A - Paeonol-containing multi-effect repairing sun-proof lipstick and preparation method thereof - Google Patents
Paeonol-containing multi-effect repairing sun-proof lipstick and preparation method thereof Download PDFInfo
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- CN110772441A CN110772441A CN201911284759.6A CN201911284759A CN110772441A CN 110772441 A CN110772441 A CN 110772441A CN 201911284759 A CN201911284759 A CN 201911284759A CN 110772441 A CN110772441 A CN 110772441A
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- paeonol
- lipstick
- containing multi
- oil
- sunscreen
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention belongs to the technical field of daily skin care products, and particularly relates to a paeonol-containing multi-effect repairing sun-proof lipstick and a preparation method thereof. According to the paeonol-containing multi-effect repair sunscreen lipstick, paeonol is applied to the preparation of the lipstick/lipstick for the first time, fine lines of lips can be obviously improved by the lipstick due to the addition of the paeonol, the lips are ruddy and glossy, and the purposes of moistening, protecting the lips and increasing the aesthetic feeling of the face are achieved; meanwhile, the paeonol has good antibacterial and ultraviolet-resistant effects, so that the lipstick does not need to be additionally provided with a preservative, has good sun-proof effect and is more suitable for daily outdoor use.
Description
Technical Field
The invention belongs to the technical field of daily skin care products, and particularly relates to a paeonol-containing multi-effect repairing sun-proof lipstick and a preparation method thereof.
Background
In recent years, with the improvement of living standard of people, more and more women who love beauty begin to use color cosmetics products, wherein the lipstick/lipstick is most widely used. The lip cream cosmetic has the main functions of moistening and protecting the skin of lips, giving the color tone to the lips, and emphasizing or changing the outline of the two lips so as to increase the aesthetic feeling of the face, and is one of the necessary cosmetic for women.
Since lipstick is a cosmetic product applied to the lips, and is easily ingested when eating or eating, the data show that 18.2% of young cancer patients abroad suffer from the usual use of lipstick or lipstick. In addition, since many conventional lipsticks contain many chemical components, skin allergy is likely to occur after long-term use, and lip allergy such as dry lip, swelling, itching, exfoliation of the skin, and slight pain occurs, and such a symptom is called "lipstick disease". Therefore, the development of the multi-effect lipstick with safe raw materials, good moistening degree and good repairing performance has important significance for wide application of the lipstick/lipstick.
Paeonol is an active ingredient extracted and separated from root bark of peony, has been found to have various medicinal effects, has main pharmacological effects of sedation, hypnosis, antioxidation, blood pressure reduction, antibiosis, anti-inflammation and the like, can reduce and fade pigment deposited in skin so as to whiten the skin, and is widely applied to cosmetics, toothpaste, gargle and tooth powder. However, the requirement of the lips on the efficacy of the cosmetics is different from that of other parts, and the application of paeonol in the lipstick is not reported.
Disclosure of Invention
Therefore, the technical problem to be solved by the invention is to provide a paeonol-containing multi-effect repair sunscreen lipstick which can obviously improve fine lines of lips, so that the lips are ruddy and glossy, and the aims of moistening, protecting the lips and increasing the aesthetic feeling of the face are fulfilled;
the second technical problem to be solved by the invention is to provide the preparation method of the lipstick.
In order to solve the technical problems, the invention provides a paeonol-containing multi-effect repairing sunscreen lipstick, which is prepared from the following raw materials:
specifically, the oil comprises olive oil and/or peony seed oil.
Specifically, the mass ratio of the olive oil to the peony seed oil is 3-5: 1-2.
Specifically, the wax includes soybean wax and beeswax.
Specifically, the mass ratio of the soybean wax to the beeswax is 1-2: 1-3.
Specifically, the natural perfume is at least one of rose essential oil, sweet orange essential oil, mint essential oil or sweet osmanthus essential oil.
Specifically, the natural pigment is at least one selected from lycopene, lutein ester or carotene.
The invention also discloses a method for preparing the paeonol-containing multi-effect repairing sunscreen lipstick, which comprises the following steps:
(1) heating and stirring selected amounts of the oil and the wax until the oil and the wax are completely dissolved and uniformly mixed;
(2) adding a selected amount of paeonol, natural perfume and natural pigment while the mixture is hot, and continuously stirring until the paeonol, the natural perfume and the natural pigment are completely dissolved to obtain a mixed material;
(3) and (3) injection molding the obtained mixed material while the mixed material is hot, and cooling and solidifying to obtain the material.
Preferably, the paeonol is prepared by extracting according to the following method:
(a) cleaning cortex moutan, air drying, slicing, naturally stacking the processed cortex moutan, uniformly spraying complex enzyme solution containing complex enzyme preparation, and performing pile fermentation at 25-32 deg.C for 8-12h to obtain pretreated cortex moutan;
the compound enzyme preparation comprises cellulase, α -amylase and glucose oxidase in a mass ratio of 1-3: 1-2: 1;
the amount of the complex enzyme preparation accounts for 3-8 wt% of the mass of the tree peony bark;
the mass concentration of the compound enzyme solution is 1-3 wt%;
(b) directly placing the pretreated cortex moutan into a steam distillation extractor, adding water 8-15 times of the mass of cortex moutan, performing steam distillation extraction for 6-12h, collecting distillate, crystallizing, filtering to obtain crystal, and drying.
The invention also discloses an application of paeonol in preparing the multi-effect repairing sun-proof lipstick.
According to the paeonol-containing multi-effect repair sunscreen lipstick, paeonol is applied to the preparation of the lipstick/lipstick for the first time, fine lines of lips can be obviously improved by the lipstick due to the addition of the paeonol, the lips are ruddy and glossy, and the purposes of moistening, protecting the lips and increasing the aesthetic feeling of the face are achieved; meanwhile, the paeonol has good antibacterial and ultraviolet-resistant effects, so that the lipstick does not need to be additionally provided with a preservative, has good sun-proof effect and is more suitable for daily outdoor use.
According to the extraction of the paeonol, the cortex moutan is effectively pretreated by spraying the selected complex enzyme preparation and carrying out pile fermentation, so that the transfer and diffusion of the paeonol components are accelerated, the distillation efficiency of subsequent paeonol is improved, the high-efficiency extraction of the paeonol is realized, and the subsequent practical application is facilitated.
Detailed Description
Preparation example 1
The method for extracting paeonol in the preparation example specifically comprises the following steps:
(1) cleaning, airing and slicing the tree peony bark, naturally stacking 200g of processed tree peony bark, mixing 2g of cellulase, 2g of α -amylase and 2g of glucose oxidase, dissolving in water to prepare a compound enzyme liquid with the mass concentration of 1 wt%, uniformly spraying the compound enzyme liquid in the tree peony bark, uniformly turning over in the spraying process to ensure that the enzyme liquid is uniformly sprayed, naturally stacking and fermentation the sprayed tree peony bark at 30 ℃ for 10 hours to obtain the pretreated tree peony bark for later use;
(2) directly placing the pretreated cortex moutan into a steam distillation extractor, adding water 8 times of the mass of cortex moutan, mixing, performing steam distillation extraction for 10h, collecting distillate, refrigerating for 12h, crystallizing, filtering to obtain crystal, and drying.
Preparation example 2
The method for extracting paeonol in the preparation example specifically comprises the following steps:
(1) cleaning, airing and slicing the tree peony bark, naturally stacking 200g of processed tree peony bark, mixing 6g of cellulase, 4g of α -amylase and 2g of glucose oxidase, dissolving in water to prepare a compound enzyme liquid with the mass concentration of 3 wt%, uniformly spraying the compound enzyme liquid in the tree peony bark, uniformly turning over in the spraying process to ensure that the enzyme liquid is uniformly sprayed, naturally stacking and fermentation the sprayed tree peony bark at 30 ℃ for 10 hours to obtain the pretreated tree peony bark for later use;
(2) directly placing the pretreated cortex moutan into a steam distillation extractor, adding water 15 times of the mass of cortex moutan, mixing, performing steam distillation extraction for 10h, collecting distillate, refrigerating for 12h, crystallizing, filtering to obtain crystal, and drying.
Preparation example 3
The method for extracting paeonol in the preparation example specifically comprises the following steps:
(1) cleaning, airing and slicing the tree peony bark, naturally stacking 200g of processed tree peony bark, mixing 4g of cellulase, 4g of α -amylase and 2g of glucose oxidase, dissolving in water to prepare a compound enzyme liquid with the mass concentration of 2 wt%, uniformly spraying the compound enzyme liquid in the tree peony bark, uniformly turning over in the spraying process to ensure that the enzyme liquid is uniformly sprayed, naturally stacking and fermentation the sprayed tree peony bark at 30 ℃ for 10 hours to obtain the pretreated tree peony bark for later use;
(2) directly placing the pretreated cortex moutan into a steam distillation extractor, adding water in an amount which is 12 times of the mass of the cortex moutan, mixing uniformly, performing steam distillation extraction for 10h, collecting distillate, refrigerating for 12h, crystallizing, filtering to obtain crystal, and drying to obtain the final product.
Preparation example 4
The method for extracting paeonol in the preparation example specifically comprises the following steps:
(1) cleaning, airing and slicing the tree peony bark, naturally stacking 200g of processed tree peony bark, mixing 8g of cellulase, 4g of α -amylase and 4g of glucose oxidase, and dissolving in water to prepare a compound enzyme liquid with the mass concentration of 3 wt%, uniformly spraying the compound enzyme liquid in the tree peony bark, uniformly turning over in the spraying process to ensure that the enzyme liquid is uniformly sprayed, naturally stacking and fermentation the sprayed tree peony bark at 30 ℃ for 10 hours to obtain the pretreated tree peony bark for later use;
(2) directly placing the pretreated cortex moutan into a steam distillation extractor, adding water in an amount which is 12 times of the mass of the cortex moutan, mixing uniformly, performing steam distillation extraction for 10h, collecting distillate, refrigerating for 12h, crystallizing, filtering to obtain crystal, and drying to obtain the final product.
Comparative example 1
The extraction method of paeonol in this comparative example is the same as that in preparation example 3, except that no pretreatment of moutan bark is performed in step (1).
Comparative example 2
The extraction method of paeonol described in this comparative example is the same as that of preparation example 3, except that no pretreatment of moutan bark is performed in step (1), and the same amount of complex enzyme is added to water before steam distillation is performed in step (2).
Comparative example 3
The extraction method of paeonol described in this comparative example is the same as that of preparation example 3 except that no pretreatment of moutan bark was performed in step (1), and cellulase in the same amount as the complex enzyme was added to water before steam distillation in step (2).
Comparative example 4
The extraction method of paeonol described in this comparative example is the same as that of preparation example 3 except that no pretreatment of moutan bark was performed in step (1), and α -amylase in the same amount as the complex enzyme was added to water before steam distillation in step (2).
Comparative example 5
The extraction method of paeonol described in this comparative example is the same as that of preparation example 3 except that no pretreatment of moutan bark was performed in step (1), and glucose oxidase in the same amount as the complex enzyme was added to water before steam distillation in step (2).
The paeonol crystals collected in the above preparation examples 1 to 4 and comparative examples 1 to 5 were collected, and the amount of the paeonol crystals and the content of the paeonol in each case were measured and recorded in the following table 1.
TABLE 1 Paeonol crystals and Paeonol content
| Numbering | Paeonol crystal mass/g | Content of paeonol/%) |
| Preparation example 1 | 3.01 | 90.98 |
| Preparation example 2 | 3.05 | 91.18 |
| Preparation example 3 | 3.11 | 92.17 |
| Preparation example 4 | 3.07 | 91.32 |
| Comparative example 1 | 2.75 | 89.05 |
| Comparative example 2 | 2.81 | 91.08 |
| Comparative example 3 | 2.88 | 90.35 |
| Comparative example 4 | 2.84 | 90.12 |
| Comparative example 5 | 2.74 | 87.96 |
Therefore, the method for extracting the paeonol adopts the mode of spraying the selected enzyme preparation on the tree peony bark and performing pile fermentation, effectively improves the surface dissolution performance of the tree peony bark, improves the dissolution efficiency and purity of the paeonol, and is beneficial to subsequent industrial utilization.
The paeonol described in the following examples of the present invention was selected from the group consisting of those prepared in preparation example 3.
Example 1
The paeonol-containing multi-effect repair sunscreen lipstick provided by the embodiment comprises the following preparation raw materials:
the preparation method of the paeonol-containing multi-effect repairing sunscreen lipstick comprises the following steps:
(1) heating selected amount of the oil and the wax to 85-90 ℃, and stirring until the oil and the wax are completely dissolved and uniformly mixed;
(2) adding a selected amount of paeonol while the mixture is hot, uniformly mixing, then cooling to 60-70 ℃, adding a selected amount of natural perfume and natural pigment, and continuously stirring until the natural perfume and the natural pigment are completely dissolved to obtain a mixed material;
(3) and (3) carrying out injection molding on the obtained mixed material while the mixed material is hot, and naturally cooling or cooling and solidifying to obtain the material.
Example 2
The paeonol-containing multi-effect repair sunscreen lipstick provided by the embodiment comprises the following preparation raw materials:
the preparation method of the paeonol-containing multi-effect repairing sunscreen lipstick comprises the following steps:
(1) heating selected amount of the oil and the wax to 85-90 ℃, and stirring until the oil and the wax are completely dissolved and uniformly mixed;
(2) adding a selected amount of paeonol while the mixture is hot, uniformly mixing, then cooling to 60-70 ℃, adding a selected amount of natural perfume and natural pigment, and continuously stirring until the natural perfume and the natural pigment are completely dissolved to obtain a mixed material;
(3) and (3) carrying out injection molding on the obtained mixed material while the mixed material is hot, and naturally cooling or cooling and solidifying to obtain the material.
Example 3
The paeonol-containing multi-effect repair sunscreen lipstick provided by the embodiment comprises the following preparation raw materials:
the preparation method of the paeonol-containing multi-effect repairing sunscreen lipstick comprises the following steps:
(1) heating selected amount of the oil and the wax to 85-90 ℃, and stirring until the oil and the wax are completely dissolved and uniformly mixed;
(2) adding a selected amount of paeonol while the mixture is hot, uniformly mixing, then cooling to 60-70 ℃, adding a selected amount of natural perfume and natural pigment, and continuously stirring until the natural perfume and the natural pigment are completely dissolved to obtain a mixed material;
(3) and (3) carrying out injection molding on the obtained mixed material while the mixed material is hot, and naturally cooling or cooling and solidifying to obtain the material.
Example 4
The paeonol-containing multi-effect repair sunscreen lipstick provided by the embodiment comprises the following preparation raw materials:
the preparation method of the paeonol-containing multi-effect repairing sunscreen lipstick comprises the following steps:
(1) heating selected amount of the oil and the wax to 85-90 ℃, and stirring until the oil and the wax are completely dissolved and uniformly mixed;
(2) adding a selected amount of paeonol while the mixture is hot, uniformly mixing, then cooling to 60-70 ℃, adding a selected amount of natural perfume and natural pigment, and continuously stirring until the natural perfume and the natural pigment are completely dissolved to obtain a mixed material;
(3) and (3) carrying out injection molding on the obtained mixed material while the mixed material is hot, and naturally cooling or cooling and solidifying to obtain the material.
Examples of the experiments
1. Safety test
20 persons with fine lines on lips were selected as volunteers, and the skin reaction on lips after 6h and 12h was recorded after applying the composition of each example once a day.
The results show that: after the composition in each example of the invention is coated for 6h and 12h, allergic reaction such as lip skin redness and the like is not seen, which indicates that the product of the invention is safe and has no adverse phenomenon.
2. Efficacy test for lightening fine lines
The test population: the test was performed by 20 persons with fine lip lines.
The test method comprises the following steps: the experimental part is provided with lips. The lips are applied for 14 days after the lips are insisted at 7 am and 7 pm every day, the situation that the lip fine lines fade after the 20 experimenters continuously use for 3 days, 7 days, 10 days and 14 days is tested, and the results of the people who are effective in fading the fine lines are recorded as shown in the following table 2.
TABLE 2 Effect of reducing Fine wrinkles (%)
| Day 3 | Day 7 | Day 10 | Day 14 |
| 20％ | 35％ | 45％ | 60％ |
3. Coloring ability and moisturizing degree test
The test population: 40 women who used lipstick frequently were selected to participate in the test and divided into 2 groups of 20 persons, and the lipstick prepared in example 1 was tested.
By adopting the practical use sensory evaluation, the score 5 shows good, the score 4 shows good, the score 3 shows general, the score 2 shows poor, and the score 1 shows poor; data were recorded after evaluation and averaged, the results of which are shown in table 3 below.
TABLE 3 coloring power and moisturizing degree test results
| Coloring ability | Moistening degree |
| 4.5 | 4.8 |
Therefore, the lipstick prepared by the invention has better coloring capability and moistening degree.
4. Test for Sun protection Properties
20 guinea pigs, each half of male and female, were depilated on the back, 1g (10) of the product of the present invention obtained in example 1 or 1g (10) of a commercially available lipstick product having no sunscreen effect were applied to skin having an area of 2cm × 2cm, irradiated with a straight tube type quartz ultraviolet germicidal lamp at an illumination distance of 8cm for 7min, the number of animals showing erythema on the irradiated part immediately after irradiation, 4h, and 24h was recorded, and the sunscreen effect was observed, and the test results were recorded as shown in table 4 below, with the highest control.
Table 4 sunscreen performance test results
Therefore, the paeonol lipstick has a certain sun-screening effect.
It should be understood that the above examples are only for clarity of illustration and are not intended to limit the embodiments. Other variations and modifications will be apparent to persons skilled in the art in light of the above description. And are neither required nor exhaustive of all embodiments. And obvious variations or modifications therefrom are within the scope of the invention.
Claims (10)
1. The paeonol-containing multi-effect repairing sun-blocking lipstick is characterized by comprising the following preparation raw materials:
2. the paeonol-containing multi-effect repairing sunscreen lipstick according to claim 1, wherein the oil comprises olive oil and/or peony seed oil.
3. The paeonol-containing multi-effect repairing sunscreen lipstick according to claim 2, wherein the mass ratio of the olive oil to the peony seed oil is 3-5: 1-2.
4. The paeonol-containing multi-effect repairing sun lipstick according to any one of claims 1-3, wherein the wax comprises soybean wax and beeswax.
5. The paeonol-containing multi-effect repairing sunscreen lipstick according to claim 4, wherein the mass ratio of the soybean wax to the beeswax is 1-2: 1-3.
6. The paeonol-containing multi-effect repairing sunscreen lipstick according to any one of claims 1-5, wherein the natural perfume is at least one selected from rose essential oil, sweet orange essential oil, mint essential oil or sweet osmanthus essential oil.
7. The paeonol-containing multipurpose repair sunscreen lipstick according to any one of claims 1-6, wherein the natural pigment is at least one selected from lycopene, lutein ester or carotene.
8. A method for preparing the paeonol-containing multi-effect repair sunscreen lipstick according to any one of claims 1-7, comprising the following steps:
(1) heating and stirring selected amounts of the oil and the wax until the oil and the wax are completely dissolved and uniformly mixed;
(2) adding a selected amount of paeonol, natural perfume and natural pigment while the mixture is hot, and continuously stirring until the paeonol, the natural perfume and the natural pigment are completely dissolved to obtain a mixed material;
(3) and (3) injection molding the obtained mixed material while the mixed material is hot, and cooling and solidifying to obtain the material.
9. The method for preparing the paeonol-containing multi-effect repairing sunscreen lipstick according to claim 8, wherein the paeonol is extracted according to the following method:
(a) cleaning cortex moutan, air drying, slicing, naturally stacking the processed cortex moutan, uniformly spraying complex enzyme solution containing complex enzyme preparation, and performing pile fermentation at 25-32 deg.C for 8-12h to obtain pretreated cortex moutan;
the compound enzyme preparation comprises cellulase, α -amylase and glucose oxidase in a mass ratio of 1-3: 1-2: 1;
the amount of the complex enzyme preparation accounts for 3-8 wt% of the mass of the tree peony bark;
the mass concentration of the compound enzyme solution is 1-3 wt%;
(b) directly placing the pretreated cortex moutan into a steam distillation extractor, adding water 8-15 times of the mass of cortex moutan, performing steam distillation extraction for 6-12h, collecting distillate, crystallizing, filtering to obtain crystal, and drying.
10. An application of paeonol in preparing multi-effect repairing sunscreen lipstick is provided.
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| CN201911284759.6A CN110772441A (en) | 2019-12-13 | 2019-12-13 | Paeonol-containing multi-effect repairing sun-proof lipstick and preparation method thereof |
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| CN201911284759.6A CN110772441A (en) | 2019-12-13 | 2019-12-13 | Paeonol-containing multi-effect repairing sun-proof lipstick and preparation method thereof |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101628866A (en) * | 2009-08-11 | 2010-01-20 | 张守力 | Extraction method of paeonol |
| CN103202782A (en) * | 2012-09-29 | 2013-07-17 | 广州环亚化妆品科技有限公司 | Lipstick with sun-screening and anti-free radical effects |
| CN105662923A (en) * | 2016-01-22 | 2016-06-15 | 武汉市农业科学技术研究院林业果树科学研究所 | Pure natural multi-effect repairing color-variable lip balm with peony seed oil and method for preparing pure natural multi-effect repairing color-variable lip balm |
| CN108815064A (en) * | 2018-09-28 | 2018-11-16 | 合肥满地金农业科技有限公司 | A kind of natural tree peony nourishing lipstick |
| CN110368318A (en) * | 2019-08-30 | 2019-10-25 | 杭州电子科技大学 | A kind of Paeonol lipstick and preparation method thereof |
-
2019
- 2019-12-13 CN CN201911284759.6A patent/CN110772441A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101628866A (en) * | 2009-08-11 | 2010-01-20 | 张守力 | Extraction method of paeonol |
| CN103202782A (en) * | 2012-09-29 | 2013-07-17 | 广州环亚化妆品科技有限公司 | Lipstick with sun-screening and anti-free radical effects |
| CN105662923A (en) * | 2016-01-22 | 2016-06-15 | 武汉市农业科学技术研究院林业果树科学研究所 | Pure natural multi-effect repairing color-variable lip balm with peony seed oil and method for preparing pure natural multi-effect repairing color-variable lip balm |
| CN108815064A (en) * | 2018-09-28 | 2018-11-16 | 合肥满地金农业科技有限公司 | A kind of natural tree peony nourishing lipstick |
| CN110368318A (en) * | 2019-08-30 | 2019-10-25 | 杭州电子科技大学 | A kind of Paeonol lipstick and preparation method thereof |
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Application publication date: 20200211 |