CN110771899A - Composite nano calcium composition and preparation method thereof - Google Patents
Composite nano calcium composition and preparation method thereof Download PDFInfo
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- CN110771899A CN110771899A CN201911188755.8A CN201911188755A CN110771899A CN 110771899 A CN110771899 A CN 110771899A CN 201911188755 A CN201911188755 A CN 201911188755A CN 110771899 A CN110771899 A CN 110771899A
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- 239000011575 calcium Substances 0.000 title claims abstract description 58
- 229910052791 calcium Inorganic materials 0.000 title claims abstract description 57
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 title claims abstract description 37
- 239000000203 mixture Substances 0.000 title claims abstract description 23
- 239000002131 composite material Substances 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 239000000843 powder Substances 0.000 claims abstract description 85
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 69
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 35
- 108010076119 Caseins Proteins 0.000 claims abstract description 32
- 239000005018 casein Substances 0.000 claims abstract description 32
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 claims abstract description 32
- 235000021240 caseins Nutrition 0.000 claims abstract description 32
- SQDAZGGFXASXDW-UHFFFAOYSA-N 5-bromo-2-(trifluoromethoxy)pyridine Chemical compound FC(F)(F)OC1=CC=C(Br)C=N1 SQDAZGGFXASXDW-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229920001287 Chondroitin sulfate Polymers 0.000 claims abstract description 19
- 108010001441 Phosphopeptides Proteins 0.000 claims abstract description 19
- 229940059329 chondroitin sulfate Drugs 0.000 claims abstract description 19
- 108090000765 processed proteins & peptides Proteins 0.000 claims abstract description 19
- NRHMKIHPTBHXPF-TUJRSCDTSA-M sodium cholate Chemical compound [Na+].C([C@H]1C[C@H]2O)[C@H](O)CC[C@]1(C)[C@@H]1[C@@H]2[C@@H]2CC[C@H]([C@@H](CCC([O-])=O)C)[C@@]2(C)[C@@H](O)C1 NRHMKIHPTBHXPF-TUJRSCDTSA-M 0.000 claims abstract description 19
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims abstract description 18
- 239000005715 Fructose Substances 0.000 claims abstract description 18
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims abstract description 18
- 229930091371 Fructose Natural products 0.000 claims abstract description 18
- 244000068988 Glycine max Species 0.000 claims abstract description 18
- 235000010469 Glycine max Nutrition 0.000 claims abstract description 18
- 240000002605 Lactobacillus helveticus Species 0.000 claims abstract description 18
- 235000013967 Lactobacillus helveticus Nutrition 0.000 claims abstract description 18
- GOMNOOKGLZYEJT-UHFFFAOYSA-N isoflavone Chemical compound C=1OC2=CC=CC=C2C(=O)C=1C1=CC=CC=C1 GOMNOOKGLZYEJT-UHFFFAOYSA-N 0.000 claims abstract description 18
- CJWQYWQDLBZGPD-UHFFFAOYSA-N isoflavone Natural products C1=C(OC)C(OC)=CC(OC)=C1C1=COC2=C(C=CC(C)(C)O3)C3=C(OC)C=C2C1=O CJWQYWQDLBZGPD-UHFFFAOYSA-N 0.000 claims abstract description 18
- 235000008696 isoflavones Nutrition 0.000 claims abstract description 18
- 229940054346 lactobacillus helveticus Drugs 0.000 claims abstract description 18
- 239000000600 sorbitol Substances 0.000 claims abstract description 18
- 238000003756 stirring Methods 0.000 claims abstract description 16
- 238000011049 filling Methods 0.000 claims abstract description 14
- 241000237502 Ostreidae Species 0.000 claims abstract description 12
- 235000020636 oyster Nutrition 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 12
- 244000293323 Cosmos caudatus Species 0.000 claims abstract description 6
- 235000005956 Cosmos caudatus Nutrition 0.000 claims abstract description 6
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims abstract description 6
- 108010033929 calcium caseinate Proteins 0.000 claims abstract description 6
- 238000002156 mixing Methods 0.000 claims abstract description 6
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims description 30
- 239000000292 calcium oxide Substances 0.000 claims description 30
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 30
- 239000000725 suspension Substances 0.000 claims description 15
- 230000029087 digestion Effects 0.000 claims description 11
- 238000001035 drying Methods 0.000 claims description 10
- 230000001804 emulsifying effect Effects 0.000 claims description 10
- 239000002245 particle Substances 0.000 claims description 10
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 5
- 239000000920 calcium hydroxide Substances 0.000 claims description 5
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims description 5
- 238000003763 carbonization Methods 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 230000018044 dehydration Effects 0.000 claims description 5
- 238000006297 dehydration reaction Methods 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 5
- 238000004806 packaging method and process Methods 0.000 claims description 5
- 239000008213 purified water Substances 0.000 claims description 5
- 238000010008 shearing Methods 0.000 claims description 5
- 239000002002 slurry Substances 0.000 claims description 5
- 238000005979 thermal decomposition reaction Methods 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000010521 absorption reaction Methods 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 3
- 230000002195 synergetic effect Effects 0.000 abstract description 2
- 239000000047 product Substances 0.000 description 7
- 210000000988 bone and bone Anatomy 0.000 description 6
- 230000009286 beneficial effect Effects 0.000 description 3
- 208000008035 Back Pain Diseases 0.000 description 2
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 2
- 230000037180 bone health Effects 0.000 description 2
- 229910001424 calcium ion Inorganic materials 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 230000035790 physiological processes and functions Effects 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- 208000006820 Arthralgia Diseases 0.000 description 1
- 230000005653 Brownian motion process Effects 0.000 description 1
- 206010058314 Dysplasia Diseases 0.000 description 1
- 208000001132 Osteoporosis Diseases 0.000 description 1
- 206010034464 Periarthritis Diseases 0.000 description 1
- 208000007502 anemia Diseases 0.000 description 1
- 206010003246 arthritis Diseases 0.000 description 1
- 208000019804 backache Diseases 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 230000003851 biochemical process Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000023555 blood coagulation Effects 0.000 description 1
- 230000037182 bone density Effects 0.000 description 1
- 238000005537 brownian motion Methods 0.000 description 1
- 229940069978 calcium supplement Drugs 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000004087 circulation Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000002124 endocrine Effects 0.000 description 1
- 235000021321 essential mineral Nutrition 0.000 description 1
- 230000012010 growth Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 208000024765 knee pain Diseases 0.000 description 1
- 208000018944 leg cramp Diseases 0.000 description 1
- 230000033001 locomotion Effects 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 230000004118 muscle contraction Effects 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 208000004296 neuralgia Diseases 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000003488 releasing hormone Substances 0.000 description 1
- 230000033458 reproduction Effects 0.000 description 1
- 230000033764 rhythmic process Effects 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 230000001502 supplementing effect Effects 0.000 description 1
- 210000001694 thigh bone Anatomy 0.000 description 1
- 210000000515 tooth Anatomy 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/16—Inorganic salts, minerals or trace elements
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/15—Vitamins
- A23L33/155—Vitamins A or D
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/17—Amino acids, peptides or proteins
- A23L33/18—Peptides; Protein hydrolysates
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Polymers & Plastics (AREA)
- Molecular Biology (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
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- Coloring Foods And Improving Nutritive Qualities (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention discloses a composite nano-calcium composition, which comprises the following raw materials in parts by mass: 10-20 parts of nano calcium carbonate powder; 15-20 parts of pearl powder; 5-10 parts of oyster powder; 3-7 parts of lactobacillus helveticus; 15-20 parts of casein calcium peptide; 5-10 parts of sodium cholate; 5-10 parts of casein phosphopeptide; 10-15 parts of chondroitin sulfate; 0.5-1 part of VD3 powder; 0.5-1 part of soybean isoflavone; 3-5 parts of sorbitol; 5-10 parts of fructose. The preparation method comprises the following steps: (1) preparing nano calcium carbonate; (2) mixing nanometer calcium carbonate powder, Margarita powder, Concha Ostreae powder, Lactobacillus helveticus, calcium caseinate peptide, sodium cholate, casein phosphopeptide, chondroitin sulfate, VD3 powder, and soybean isoflavone, adding sorbitol and fructose, and stirring; (3) and (3) quantitatively filling the powder obtained in the step (2) to obtain a finished product. The invention combines a plurality of components together, has synergistic effect and mutual gain, obviously improves the absorption utilization rate of calcium, and has wide application range and good effect.
Description
Technical Field
The invention relates to the technical field of food-grade nano calcium preparation, in particular to a composite nano calcium composition and a preparation method thereof.
Background
Calcium is an essential structural component in the formation of bones, teeth and cell walls, and these structures also have important physiological functions of supporting, protecting, exercising, feeding and the like, and are also essential mineral nutrients for human bodies, and all cells require calcium. Calcium ion (Ca)
2+) In living organisms are triggers for many biochemical and physiological processes, such as triggering muscle contractions, releasing hormones, delivering pulses, promoting blood clotting, regulating heart rhythm and lactating, among others. Modern medical research shows that calcium nutrition is closely related to the functions of more than ten systems in vivo, such as immunity, nerves, endocrine, digestion, circulation, movement, reproduction and the like. Basic, clinical medicine studies have demonstrated that calcium ions have a great impact on life, that is, human health is not isolated from calcium.
The nano calcium is manufactured by adopting a fine and accurate grinding method through an advanced laser technology, is more fine and accurate than a common grinding method, has very fine particles, and scientific tests prove that the nano technology can break calcium molecules into very fine molecules, can be quickly absorbed into blood by a body, and can be more effectively stored in bone through Brownian motion of the fine particles, thereby effectively supplementing lost calcium, improving bone health and improving bone problems. Clinical trials in university prove that the nano calcium has very high absorption rate compared with common calcium, and the nano calcium obviously increases the bone density. A number of clinical test reports also show that nano-calcium is beneficial for improving bone health. The nano calcium is a product which is commonly used for improving and strengthening the growth of bones and teeth, supplements lost calcium in time, is suitable for middle-aged and elderly people to eat, and is beneficial to the health of bones.
At present, various nano-calcium products are developed by high technology, but the cost is high, and the defects of poor taste, unsatisfactory calcium supplement effect and insufficient suitable range exist, so that a new nano-calcium product needs to be developed.
Disclosure of Invention
In order to solve the existing problems, the invention provides a composite nano-calcium composition and a preparation method thereof. The invention is realized by the following technical scheme.
The formula of the composite nano calcium composition comprises the following raw materials in parts by mass:
10-20 parts of nano calcium carbonate powder; 15-20 parts of pearl powder; 5-10 parts of oyster powder; 3-7 parts of lactobacillus helveticus; 15-20 parts of casein calcium peptide; 5-10 parts of sodium cholate; 5-10 parts of casein phosphopeptide; 10-15 parts of chondroitin sulfate; 0.5-1 part of VD3 powder; 0.5-1 part of soybean isoflavone; 3-5 parts of sorbitol; 5-10 parts of fructose.
Preferably, the formula comprises the following raw materials in parts by mass:
15 parts of nano calcium carbonate powder; 18 parts of pearl powder; 8 parts of oyster powder; 6 parts of lactobacillus helveticus; 18 parts of casein calcium peptide; 8 parts of sodium cholate; 6 parts of casein phosphopeptide; 15 parts of chondroitin sulfate; 0.8 part of VD3 powder; soybean isoflavone 0.9 weight portions; 4 parts of sorbitol; and 8 parts of fructose.
Preferably, the formula comprises the following raw materials in parts by mass:
19 parts of nano calcium carbonate powder; 15 parts of pearl powder; 7 parts of oyster powder; 4 parts of lactobacillus helveticus; 18 parts of casein calcium peptide; 8 parts of sodium cholate; 5 parts of casein phosphopeptide; 12 parts of chondroitin sulfate; 0.7 part of VD3 powder; soybean isoflavone 0.9 weight portions; 5 parts of sorbitol; and 8 parts of fructose.
A preparation method of the composite nano-calcium composition comprises the following steps:
(1) preparing nano calcium carbonate: carrying out thermal decomposition treatment on calcium carbonate powder with the purity of more than 98% by adopting plasma flame to prepare particle calcium oxide with the particle size of 2500 meshes; digesting the particulate calcium oxide, feeding the particulate calcium oxide into a groove type continuous digester, simultaneously adding purified water with the weight being five times that of the particulate calcium oxide, stirring for 10 minutes to 15 minutes by a stirring device in the digester to ensure that calcium hydroxide suspension produced by digestion flows out from a slurry overflow outlet after digestion reaction is finished, then putting the generated calcium oxide suspension into a high-shear emulsifying machine, and shearing and emulsifying for 20 minutes to 30 minutes to ensure that the calcium oxide suspension is fully refined and uniform; then dehydrating, drying and surface treating are carried out, H2O2 in the second stage of carbonization liquid is discharged along with dehydration and drying, and nano calcium carbonate with the average grain diameter of 1-10nm is obtained;
(2) mixing nanometer calcium carbonate powder, Margarita powder, Concha Ostreae powder, Lactobacillus helveticus, calcium caseinate peptide, sodium cholate, casein phosphopeptide, chondroitin sulfate, VD3 powder, and soybean isoflavone, adding sorbitol and fructose, and stirring;
(3) and (3) quantitatively filling the powder obtained in the step (2) to obtain a finished product.
Preferably, the step (3) is carried out by a quantitative packaging machine with the speed of 40-60 bags/minute and the filling amount of 5 g/bag.
The invention has the beneficial effects that:
the composite nano-calcium composition adopts pearl powder and nano-calcium carbonate as calcium sources, adopts casein calcium peptide, sodium cholate, casein phosphopeptide and chondroitin sulfate which are mutually matched as absorption promoting agents, and has synergistic effect and mutual gain, so that the absorption utilization rate of calcium is obviously improved; the addition of VD3 further enhances the absorption and utilization of calcium. The invention also provides a preparation method for preparing the nano-calcium composition, which is simple in process and convenient for industrial batch production.
In conclusion, the nano-calcium composition can improve the texture of thighbone and vertebra, regulate the content of calcium in bone, and improve the functional state of a body; the composite nano calcium powder also has obvious improvement effect on neuralgia, knee pain, scapulohumeral periarthritis and waist and back pain; can be used for preventing and treating osteoporosis, arthritis, soreness of waist, backache, leg cramp, children dysplasia, anemia, etc.
Detailed Description
The technical solution of the present invention will be described in more detail and fully with reference to the following embodiments.
The formula of the composite nano calcium composition comprises the following raw materials in parts by mass:
10-20 parts of nano calcium carbonate powder; 15-20 parts of pearl powder; 5-10 parts of oyster powder; 3-7 parts of lactobacillus helveticus; 15-20 parts of casein calcium peptide; 5-10 parts of sodium cholate; 5-10 parts of casein phosphopeptide; 10-15 parts of chondroitin sulfate; 0.5-1 part of VD3 powder; 0.5-1 part of soybean isoflavone; 3-5 parts of sorbitol; 5-10 parts of fructose.
Preferably, the formula comprises the following raw materials in parts by mass:
15 parts of nano calcium carbonate powder; 18 parts of pearl powder; 8 parts of oyster powder; 6 parts of lactobacillus helveticus; 18 parts of casein calcium peptide; 8 parts of sodium cholate; 6 parts of casein phosphopeptide; 15 parts of chondroitin sulfate; 0.8 part of VD3 powder; soybean isoflavone 0.9 weight portions; 4 parts of sorbitol; and 8 parts of fructose.
Preferably, the formula comprises the following raw materials in parts by mass:
19 parts of nano calcium carbonate powder; 15 parts of pearl powder; 7 parts of oyster powder; 4 parts of lactobacillus helveticus; 18 parts of casein calcium peptide; 8 parts of sodium cholate; 5 parts of casein phosphopeptide; 12 parts of chondroitin sulfate; 0.7 part of VD3 powder; soybean isoflavone 0.9 weight portions; 5 parts of sorbitol; and 8 parts of fructose.
A preparation method of the composite nano-calcium composition comprises the following steps:
(1) preparing nano calcium carbonate: carrying out thermal decomposition treatment on calcium carbonate powder with the purity of more than 98% by adopting plasma flame to prepare particle calcium oxide with the particle size of 2500 meshes; digesting the particulate calcium oxide, feeding the particulate calcium oxide into a groove type continuous digester, simultaneously adding purified water with the weight being five times that of the particulate calcium oxide, stirring for 10 minutes to 15 minutes by a stirring device in the digester to ensure that calcium hydroxide suspension produced by digestion flows out from a slurry overflow outlet after digestion reaction is finished, then putting the generated calcium oxide suspension into a high-shear emulsifying machine, and shearing and emulsifying for 20 minutes to 30 minutes to ensure that the calcium oxide suspension is fully refined and uniform; then dehydrating, drying and surface treating are carried out, H2O2 in the second stage of carbonization liquid is discharged along with dehydration and drying, and nano calcium carbonate with the average grain diameter of 1-10nm is obtained;
(2) mixing nanometer calcium carbonate powder, Margarita powder, Concha Ostreae powder, Lactobacillus helveticus, calcium caseinate peptide, sodium cholate, casein phosphopeptide, chondroitin sulfate, VD3 powder, and soybean isoflavone, adding sorbitol and fructose, and stirring;
(3) and (3) quantitatively filling the powder obtained in the step (2) to obtain a finished product.
Preferably, the step (3) is carried out by a quantitative packaging machine with the speed of 40-60 bags/minute and the filling amount of 5 g/bag.
In specific embodiment 1, a composite nano-calcium composition comprises the following raw materials in parts by mass: 15 parts of nano calcium carbonate powder; 18 parts of pearl powder; 8 parts of oyster powder; 6 parts of lactobacillus helveticus; 18 parts of casein calcium peptide; 8 parts of sodium cholate; 6 parts of casein phosphopeptide; 15 parts of chondroitin sulfate; 0.8 part of VD3 powder; soybean isoflavone 0.9 weight portions; 4 parts of sorbitol; and 8 parts of fructose.
The preparation method comprises the following steps:
(1) preparing nano calcium carbonate: carrying out thermal decomposition treatment on calcium carbonate powder with the purity of more than 98% by adopting plasma flame to prepare particle calcium oxide with the particle size of 2500 meshes; digesting the particulate calcium oxide, feeding the particulate calcium oxide into a groove type continuous digester, simultaneously adding purified water with the weight being five times that of the particulate calcium oxide, stirring for 10 minutes to 15 minutes by a stirring device in the digester to ensure that calcium hydroxide suspension produced by digestion flows out from a slurry overflow outlet after digestion reaction is finished, then putting the generated calcium oxide suspension into a high-shear emulsifying machine, and shearing and emulsifying for 20 minutes to 30 minutes to ensure that the calcium oxide suspension is fully refined and uniform; then dehydrating, drying and surface treating are carried out, H2O2 in the second stage of carbonization liquid is discharged along with dehydration and drying, and nano calcium carbonate with the average grain diameter of 1-10nm is obtained;
(2) mixing nanometer calcium carbonate powder, Margarita powder, Concha Ostreae powder, Lactobacillus helveticus, calcium caseinate peptide, sodium cholate, casein phosphopeptide, chondroitin sulfate, VD3 powder, and soybean isoflavone, adding sorbitol and fructose, and stirring;
(3) quantitatively filling the powder obtained in the step (2) to obtain a finished product; and (4) filling by adopting a quantitative packaging machine at the speed of 40-60 bags/minute and the filling amount of 5 g/bag. .
Embodiment 2, a composite nano-calcium composition, the formula of which comprises the following raw materials in parts by mass:
19 parts of nano calcium carbonate powder; 15 parts of pearl powder; 7 parts of oyster powder; 4 parts of lactobacillus helveticus; 18 parts of casein calcium peptide; 8 parts of sodium cholate; 5 parts of casein phosphopeptide; 12 parts of chondroitin sulfate; 0.7 part of VD3 powder; soybean isoflavone 0.9 weight portions; 5 parts of sorbitol; and 8 parts of fructose.
A preparation method of the composite nano-calcium composition comprises the following steps:
(1) preparing nano calcium carbonate: carrying out thermal decomposition treatment on calcium carbonate powder with the purity of more than 98% by adopting plasma flame to prepare particle calcium oxide with the particle size of 2500 meshes; digesting the particulate calcium oxide, feeding the particulate calcium oxide into a groove type continuous digester, simultaneously adding purified water with the weight being five times that of the particulate calcium oxide, stirring for 10 minutes to 15 minutes by a stirring device in the digester to ensure that calcium hydroxide suspension produced by digestion flows out from a slurry overflow outlet after digestion reaction is finished, then putting the generated calcium oxide suspension into a high-shear emulsifying machine, and shearing and emulsifying for 20 minutes to 30 minutes to ensure that the calcium oxide suspension is fully refined and uniform; then dehydrating, drying and surface treating are carried out, H2O2 in the second stage of carbonization liquid is discharged along with dehydration and drying, and nano calcium carbonate with the average grain diameter of 1-10nm is obtained;
(2) mixing nanometer calcium carbonate powder, Margarita powder, Concha Ostreae powder, Lactobacillus helveticus, calcium caseinate peptide, sodium cholate, casein phosphopeptide, chondroitin sulfate, VD3 powder, and soybean isoflavone, adding sorbitol and fructose, and stirring;
(3) quantitatively filling the powder obtained in the step (2) to obtain a finished product; and (4) filling by adopting a quantitative packaging machine at the speed of 40-60 bags/minute and the filling amount of 5 g/bag.
It is to be understood that the described embodiments are merely individual embodiments of the invention, rather than all embodiments. All other implementations made by those skilled in the art without any inventive step based on the embodiments of the present invention belong to the protection scope of the present invention.
Claims (5)
1. A composite nanocalcium composition characterized by: the formula comprises the following raw materials in parts by mass:
10-20 parts of nano calcium carbonate powder; 15-20 parts of pearl powder; 5-10 parts of oyster powder; 3-7 parts of lactobacillus helveticus; 15-20 parts of casein calcium peptide; 5-10 parts of sodium cholate; 5-10 parts of casein phosphopeptide; 10-15 parts of chondroitin sulfate; 0.5-1 part of VD3 powder; 0.5-1 part of soybean isoflavone; 3-5 parts of sorbitol; 5-10 parts of fructose.
2. The composite nano-calcium composition and the preparation method thereof according to claim 1, wherein the composite nano-calcium composition comprises: the formula comprises the following raw materials in parts by mass:
15 parts of nano calcium carbonate powder; 18 parts of pearl powder; 8 parts of oyster powder; 6 parts of lactobacillus helveticus; 18 parts of casein calcium peptide; 8 parts of sodium cholate; 6 parts of casein phosphopeptide; 15 parts of chondroitin sulfate; 0.8 part of VD3 powder; soybean isoflavone 0.9 weight portions; 4 parts of sorbitol; and 8 parts of fructose.
3. The composite nano-calcium composition and the preparation method thereof according to claim 1, wherein the composite nano-calcium composition comprises: the formula comprises the following raw materials in parts by mass:
19 parts of nano calcium carbonate powder; 15 parts of pearl powder; 7 parts of oyster powder; 4 parts of lactobacillus helveticus; 18 parts of casein calcium peptide; 8 parts of sodium cholate; 5 parts of casein phosphopeptide; 12 parts of chondroitin sulfate; 0.7 part of VD3 powder; soybean isoflavone 0.9 weight portions; 5 parts of sorbitol; and 8 parts of fructose.
4. A method for preparing the composite nano-calcium composition of claim 1, which is characterized by comprising the following steps: the method comprises the following steps:
(1) preparing nano calcium carbonate: carrying out thermal decomposition treatment on calcium carbonate powder with the purity of more than 98% by adopting plasma flame to prepare particle calcium oxide with the particle size of 2500 meshes; digesting the particulate calcium oxide, feeding the particulate calcium oxide into a groove type continuous digester, simultaneously adding purified water with the weight being five times that of the particulate calcium oxide, stirring for 10 minutes to 15 minutes by a stirring device in the digester to ensure that calcium hydroxide suspension produced by digestion flows out from a slurry overflow outlet after digestion reaction is finished, then putting the generated calcium oxide suspension into a high-shear emulsifying machine, and shearing and emulsifying for 20 minutes to 30 minutes to ensure that the calcium oxide suspension is fully refined and uniform; then dehydrating, drying and surface treating are carried out, H2O2 in the second stage of carbonization liquid is discharged along with dehydration and drying, and nano calcium carbonate with the average grain diameter of 1-10nm is obtained;
(2) mixing nanometer calcium carbonate powder, Margarita powder, Concha Ostreae powder, Lactobacillus helveticus, calcium caseinate peptide, sodium cholate, casein phosphopeptide, chondroitin sulfate, VD3 powder, and soybean isoflavone, adding sorbitol and fructose, and stirring;
(3) and (3) quantitatively filling the powder obtained in the step (2) to obtain a finished product.
5. The composite nano-calcium composition and the preparation method thereof according to claim 4, wherein the composite nano-calcium composition comprises: and (4) filling by adopting a quantitative packaging machine in the step (3), wherein the speed is 40-60 bags per minute, and the filling amount is 5g per bag.
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