CN110761088A - Wax printing dye and wax printing method - Google Patents
Wax printing dye and wax printing method Download PDFInfo
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- CN110761088A CN110761088A CN201911194112.4A CN201911194112A CN110761088A CN 110761088 A CN110761088 A CN 110761088A CN 201911194112 A CN201911194112 A CN 201911194112A CN 110761088 A CN110761088 A CN 110761088A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65118—Compounds containing hydroxyl groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/6515—Hydrocarbons
- D06P1/65162—Hydrocarbons without halogen
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
- D06P3/66—Natural or regenerated cellulose using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/12—Reserving parts of the material before dyeing or printing ; Locally decreasing dye affinity by chemical means
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/20—Physical treatments affecting dyeing, e.g. ultrasonic or electric
- D06P5/2011—Application of vibrations, pulses or waves for non-thermic purposes
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Abstract
The invention discloses a wax printing dye and a wax printing method, wherein a substance containing a bis-monochlorotriazine active group or a monochlorodiazine active group is used as a coloring agent, a mixed wax liquid is adopted, the color fastness of dyeing is changed through the proportion of the wax liquid and the coloring agent, and meanwhile, in order to improve the light aging resistance of the dyeing color, tea polyphenol is added into the dye; the fabric is subjected to softening pretreatment in the dyeing process to provide a material basis for natural and fine wax patterns in the subsequent wax printing process, and then the pretreated fabric is placed in a dye and is dyed under the action of ultrasound, so that the movement of dye molecules is facilitated under the action of the ultrasound, the dyeing speed is accelerated, and the color fastness and uniformity of dyeing are improved.
Description
Technical Field
The invention relates to the technical field of wax printing, in particular to wax printing dye and a wax printing method.
Background
The wax printing is an ancient art which summarizes a concise shape, has pure and plain colors, exaggerates a deformed decorative pattern and adapts to the requirements of modern life and modern aesthetic requirements. Wax printing is a method for obtaining a pattern fabric by using wax as a dye inhibitor, coating the wax in a heating melting state on the fabric, carrying out crack treatment and carrying out low-temperature dyeing and dewaxing. It features that its natural irregular wax pattern is formed. The reason is that after the wax liquid coated on the fabric is condensed, a plurality of irregular cracks can be formed by rubbing or turning before dyeing or during dyeing, and the cracks are different in color depth during dyeing to form natural and fine wax patterns.
Dyeing is an extremely important step in the wax printing process, and different dyes have greatly different performances and processes and different dyeing effects. In the past, X-type reactive dyes, insoluble azo dyes and vat dyes have been mainly used.
The research of the applicant finds that the X-type reactive dye is mainly medium-light color and has low washing fastness; the vat dye lacks deep color, and most of the vat dyes are expensive; the color of the dyed ice dye is dark and thick, but the color spectrum is not complete, and most of the ice dye is forbidden.
Disclosure of Invention
In view of the above, the present invention is directed to a wax printing dye and a wax printing method, which can improve the color fastness of wax printing by combining the dye and the wax printing process.
The wax printing dye comprises 8-10% of dye (owf), 20-45 g/L of anhydrous sodium sulphate, 25-50 g/L of soda ash and 40-60 g/L of tea polyphenol, wherein the mass percentage of wax liquid in the dye is 65-85%.
Optionally, the dye comprises 5-6.5% (owf) of the dye, 30-40 g/L of anhydrous sodium sulphate, 35-45 g/L of soda ash and 45-50 g/L of tea polyphenol, and the mass percentage of the wax liquid in the dye is 75-80%.
Optionally, the dye comprises 6% of dye (owf), 37g/L of anhydrous sodium sulphate, 41g/L of soda ash and 47g/L of tea polyphenol, and the mass percentage of the wax liquid in the dye is 78%.
Optionally, the wax liquid is a mixture of paraffin, white wax and beeswax in a mass ratio of 1-2: 1: 1.
Optionally, the dyeing component in the dye contains a bis-monochlorotriazine active group or a monochlorodiazine active group.
From the above, the wax printing dye provided by the invention adopts the substance containing the bis-monochlorotriazine active group or the monochlorodiazine active group as the dyeing agent, and adopts the mixed wax liquid at the same time, the color fastness of the dyeing is changed through the proportion of the wax liquid and the dyeing agent, and meanwhile, in order to improve the light aging resistance of the dyed color, the tea polyphenol is added into the dye, and the color fastness of the dye is improved through the reasonable proportion and the coordination effect of the components.
A wax printing method comprises the following steps,
pretreatment of the fabric: soaking the fabric in water at normal temperature for 10-20 min, then adding a softener into the water, heating the water to 40-70 ℃, boiling for 10-20 min, taking out, and drying in the air;
dyeing: adding water into the dye at a bath ratio of 1: 40-60, heating to 45-60 ℃, stirring until the dye is completely dissolved, putting the pretreated fabric into the dye solution, dip-dyeing for 35-45 min, then carrying out ultrasonic treatment for 5-10 min, taking out, sealing, standing at room temperature for 8-14 h, taking out, washing with water, and removing wax.
Optionally, the power of the ultrasonic treatment is 2-10 KHz.
From the above, the wax printing method provided by the invention has the advantages that the fabric is subjected to softening pretreatment to provide a material basis for natural and fine wax patterns in the subsequent wax printing process, and then the pretreated fabric is placed in the dye and is dyed under the action of ultrasound, so that the movement of dye molecules is facilitated under the action of ultrasound, the dyeing speed is accelerated, and the color fastness and uniformity of dyeing are improved.
Detailed Description
In the following description of the embodiments, the detailed description of the present invention, such as the manufacturing processes and the operation and use methods, will be further described in detail to help those skilled in the art to more fully, accurately and deeply understand the inventive concept and technical solutions of the present invention.
In order to solve the problems of poor color fastness and uneven dyeing of the dye in the prior art, the invention provides a wax printing dye which comprises 8-10% of dye (owf), 20-45 g/L of anhydrous sodium sulphate, 25-50 g/L of soda ash and 40-60 g/L of tea polyphenol, wherein the mass percentage of wax liquid in the dye is 65-85%.
Simultaneously provides a wax printing method, which comprises the following steps,
pretreatment of the fabric: soaking the fabric in water at normal temperature for 10-20 min, then adding a softener into the water, heating the water to 40-70 ℃, boiling for 10-20 min, taking out, and drying in the air;
dyeing: adding water into the dye at a bath ratio of 1: 40-60, heating to 45-60 ℃, stirring until the dye is completely dissolved, putting the pretreated fabric into the dye solution, dip-dyeing for 35-45 min, then carrying out ultrasonic treatment for 5-10 min, taking out, sealing, standing at room temperature for 8-14 h, taking out, washing with water, and removing wax.
The method adopts a substance containing a bis-monochlorotriazine active group or a monochlorodiazine active group as a coloring agent, adopts mixed wax liquid, changes the color fastness of dyeing through the mixture ratio of the wax liquid and the coloring agent, and simultaneously adds tea polyphenol into the dye in order to improve the light aging resistance of the dyeing color, so that the color fastness of the dye is improved through the reasonable mixture ratio and the coordination action of all components. The fabric is subjected to softening pretreatment in the dyeing process to provide a material basis for natural and fine wax patterns in the subsequent wax printing process, and then the pretreated fabric is placed in a dye and is dyed under the action of ultrasound, so that the movement of dye molecules is facilitated under the action of the ultrasound, the dyeing speed is accelerated, and the color fastness and uniformity of dyeing are improved.
In order to improve the color fastness of the dye, the dye comprises 5-6.5% (owf) of the dye, 30-40 g/L of anhydrous sodium sulphate, 35-45 g/L of soda ash and 45-50 g/L of tea polyphenol, wherein the mass percentage of wax liquid in the dye is 75-80%.
More specifically, the dye comprises 6% of dye (owf), 37g/L of anhydrous sodium sulphate, 41g/L of soda ash and 47g/L of tea polyphenol, wherein the mass percentage of wax liquid in the dye is 78%.
In order to improve the color fastness of the dye, the wax liquid is a mixture of paraffin, white wax and beeswax in a mass ratio of 1-2: 1: 1.
In order to improve the color fastness of the dye, the dyeing component in the dye contains a bis-monochlorotriazine active group or a monochlorodiazine active group, especially the KE type and the ME type.
In order to improve the dyeing speed and the dyeing uniformity, the power of ultrasonic treatment is 2-10 KHz.
Specifically, the wax printing method provided in embodiment 1 of the present invention includes the following steps,
the dye comprises 6% of dye (owf), 37g/L of anhydrous sodium sulphate, 41g/L of soda ash and 47g/L of tea polyphenol, wherein the mass percentage of wax liquid in the dye is 78%. Wherein the coloring agent is KE type, and the liquid wax is a mixture of paraffin, white wax and beeswax in a mass ratio of 1:1: 1.
The wax printing steps are as follows: soaking the bleached cotton fabric in normal-temperature water for 10-20 min, adding a softener sold on the market into the water according to the using amount of the softener, heating the water to 55 ℃, boiling for 15min, taking out, and airing by natural wind;
dyeing: adding water into the dye at a bath ratio of 1:50, heating to 50 ℃, stirring until the dye is completely dissolved, putting the pretreated bleached cotton fabric into the dye solution, dip-dyeing for 40min, then carrying out ultrasonic treatment for 6min, taking out, sealing, standing at room temperature for 10h, taking out, washing with water, and removing wax.
Specifically, the wax printing method provided in embodiment 2 of the present invention includes the following steps,
the dye comprises 5% of dye (owf), 30g/L of anhydrous sodium sulphate, 35g/L of soda ash and 45g/L of tea polyphenol, wherein the mass percentage of wax liquid in the dye is 75%. Wherein the coloring agent is KE type, and the liquid wax is a mixture of paraffin, white wax and beeswax in a mass ratio of 1:1: 1.
The wax printing steps are as follows: soaking the bleached cotton fabric in normal-temperature water for 10-20 min, adding a softener sold on the market into the water according to the using amount of the softener, heating the water to 55 ℃, boiling for 15min, taking out, and airing by natural wind;
dyeing: adding water into the dye at a bath ratio of 1:50, heating to 50 ℃, stirring until the dye is completely dissolved, putting the pretreated bleached cotton fabric into the dye solution, dip-dyeing for 40min, then carrying out ultrasonic treatment for 6min, taking out, sealing, standing at room temperature for 10h, taking out, washing with water, and removing wax.
Specifically, the wax printing method provided in embodiment 3 of the present invention includes the following steps,
the dye comprises 6.5 percent of dye (owf), 40g/L of anhydrous sodium sulphate, 45g/L of soda ash and 50g/L of tea polyphenol, wherein the mass percent of wax liquid in the dye is 80 percent. Wherein the coloring agent is KE type, and the liquid wax is a mixture of paraffin, white wax and beeswax in a mass ratio of 1:1: 1.
The wax printing steps are as follows: soaking the bleached cotton fabric in normal-temperature water for 10-20 min, adding a softener sold on the market into the water according to the using amount of the softener, heating the water to 55 ℃, boiling for 15min, taking out, and airing by natural wind;
dyeing: adding water into the dye at a bath ratio of 1:50, heating to 50 ℃, stirring until the dye is completely dissolved, putting the pretreated bleached cotton fabric into the dye solution, dip-dyeing for 40min, then carrying out ultrasonic treatment for 6min, taking out, sealing, standing at room temperature for 10h, taking out, washing with water, and removing wax.
Specifically, the wax printing method provided in embodiment 4 of the present invention includes the following steps,
the dye comprises 8% of dye (owf), 20g/L of anhydrous sodium sulphate, 25g/L of soda ash and 40g/L of tea polyphenol, wherein the mass percentage of wax liquid in the dye is 65%. Wherein the coloring agent is ME type, and the liquid wax is a mixture of paraffin, white wax and beeswax in a mass ratio of 2:1: 1.
The wax printing steps are as follows: soaking the bleached cotton fabric in normal-temperature water for 10-20 min, adding a softener sold on the market into the water according to the using amount of the softener, heating the water to 55 ℃, boiling for 15min, taking out, and airing by natural wind;
dyeing: adding water into the dye at a bath ratio of 1:50, heating to 50 ℃, stirring until the dye is completely dissolved, putting the pretreated bleached cotton fabric into the dye solution, dip-dyeing for 40min, then carrying out ultrasonic treatment for 6min, taking out, sealing, standing at room temperature for 10h, taking out, washing with water, and removing wax.
Specifically, the wax printing method provided in embodiment 5 of the present invention includes the following steps,
the dye comprises the following components, by mass, 10% of dye (owf), 45g/L of anhydrous sodium sulphate, 50g/L of soda ash and 60g/L of tea polyphenol, wherein the wax liquid in the dye accounts for 85%. Wherein the coloring agent is ME type, and the liquid wax is a mixture of paraffin, white wax and beeswax in a mass ratio of 2:1: 1.
The wax printing steps are as follows: soaking the bleached cotton fabric in normal-temperature water for 10-20 min, adding a softener sold on the market into the water according to the using amount of the softener, heating the water to 55 ℃, boiling for 15min, taking out, and airing by natural wind;
dyeing: adding water into the dye at a bath ratio of 1:50, heating to 50 ℃, stirring until the dye is completely dissolved, putting the pretreated bleached cotton fabric into the dye solution, dip-dyeing for 40min, then carrying out ultrasonic treatment for 6min, taking out, sealing, standing at room temperature for 10h, taking out, washing with water, and removing wax.
Examples 1 to 5 were measured in accordance with GB/T3921-2008 "soaping color fastness for textile color fastness test", and in accordance with GB/T3920-2008 "rubbing color fastness for textile color fastness test". The results of the measurements are shown in the following table.
The data show that the dye prepared by the embodiment of the invention has good color fastness effect and stronger color fastness.
Those of ordinary skill in the art will understand that: the discussion of any embodiment above is meant to be exemplary only, and is not intended to intimate that the scope of the disclosure, including the claims, is limited to these examples; within the idea of the invention, also features in the above embodiments or in different embodiments may be combined, steps may be implemented in any order, and there are many other variations of the different aspects of the invention as described above, which are not provided in detail for the sake of brevity.
The embodiments of the invention are intended to embrace all such alternatives, modifications and variances that fall within the broad scope of the appended claims. Therefore, any omissions, modifications, substitutions, improvements and the like that may be made without departing from the spirit and principles of the invention are intended to be included within the scope of the invention.
Claims (7)
1. The batik dye is characterized by comprising 8-10% of dye (owf), 20-45 g/L of anhydrous sodium sulphate, 25-50 g/L of soda ash and 40-60 g/L of tea polyphenol, wherein the mass percentage of wax liquid in the dye is 65-85%.
2. The batik dye according to claim 1, wherein the dye comprises 5-6.5% (owf) of dye, 30-40 g/L of anhydrous sodium sulphate, 35-45 g/L of soda ash and 45-50 g/L of tea polyphenol, and the mass percentage of the wax liquid in the dye is 75-80%.
3. The batik dye according to claim 1, wherein the dye comprises 6% of dye (owf), 37g/L of anhydrous sodium sulphate, 41g/L of soda ash and 47g/L of tea polyphenol, and the mass percentage of the wax liquid in the dye is 78%.
4. The batik dye according to claim 1, wherein the wax liquid is a mixture of paraffin, white wax and beeswax in a mass ratio of 1-2: 1: 1.
5. The batik dye according to claim 1, wherein the dyeing component in the dye comprises a bis-monochlorotriazine reactive group or a monochlorodiazine reactive group.
6. A wax printing method using the wax printing dye according to any one of claims 1 to 5, comprising the steps of,
pretreatment of the fabric: soaking the fabric in water at normal temperature for 10-20 min, then adding a softener into the water, heating the water to 40-70 ℃, boiling for 10-20 min, taking out, and drying in the air;
dyeing: adding water into the dye at a bath ratio of 1: 40-60, heating to 45-60 ℃, stirring until the dye is completely dissolved, putting the pretreated fabric into the dye solution, dip-dyeing for 35-45 min, then carrying out ultrasonic treatment for 5-10 min, taking out, sealing, standing at room temperature for 8-14 h, taking out, washing with water, and removing wax.
7. The batik process according to claim 6, wherein the power of the ultrasonic treatment is 2-10 KHz.
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| CN201911194112.4A CN110761088A (en) | 2019-11-28 | 2019-11-28 | Wax printing dye and wax printing method |
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| CN201911194112.4A CN110761088A (en) | 2019-11-28 | 2019-11-28 | Wax printing dye and wax printing method |
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Cited By (1)
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| CN112227088A (en) * | 2020-10-22 | 2021-01-15 | 安顺市西秀区星月苗族蜡染工艺品有限公司 | Wax printing auxiliary agent suitable for cotton cloth and preparation method thereof |
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| CN112227088A (en) * | 2020-10-22 | 2021-01-15 | 安顺市西秀区星月苗族蜡染工艺品有限公司 | Wax printing auxiliary agent suitable for cotton cloth and preparation method thereof |
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