CN110693731A - High-hardness and long-lasting-foaming explosive salt and preparation method thereof - Google Patents

High-hardness and long-lasting-foaming explosive salt and preparation method thereof Download PDF

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Publication number
CN110693731A
CN110693731A CN201910990840.XA CN201910990840A CN110693731A CN 110693731 A CN110693731 A CN 110693731A CN 201910990840 A CN201910990840 A CN 201910990840A CN 110693731 A CN110693731 A CN 110693731A
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CN
China
Prior art keywords
sodium
salt
mixture
magnesium stearate
foaming
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Pending
Application number
CN201910990840.XA
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Chinese (zh)
Inventor
邹博龙
黄青海
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HUIZHOU ZHAOTING COSMETIC CO Ltd
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HUIZHOU ZHAOTING COSMETIC CO Ltd
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Priority to CN201910990840.XA priority Critical patent/CN110693731A/en
Publication of CN110693731A publication Critical patent/CN110693731A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/20Halogens; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/23Sulfur; Selenium; Tellurium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/361Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Emergency Medicine (AREA)
  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Cosmetics (AREA)

Abstract

The invention belongs to the field of daily chemicals. A high hardness and long-lasting foaming explosive salt comprises the following components in percentage by weight: 10-40% of sodium bicarbonate, 10-35% of alpha-hydroxy acid, 0.1-3% of grease and emulsifier, 5-30% of sodium sulfate or sodium chloride or a mixture of sodium sulfate and sodium chloride, and 0.1-5% of magnesium carbonate or magnesium stearate or a mixture of magnesium carbonate and magnesium stearate. The bath foam has the advantages of higher hardness and hydrophobicity, lasting foaming time, stable foaming effect, rich and fine foam, and can effectively relieve skin, eliminate fatigue, promote blood circulation and increase interestingness and joyful feeling during bathing.

Description

High-hardness and long-lasting-foaming explosive salt and preparation method thereof
Technical Field
The invention belongs to the field of daily chemicals, and relates to high-hardness and durable-foaming explosive salt and a preparation method thereof.
Background
The explosive salt is a bathing product, is put in water before bathing, can emit a large amount of bubbles on the water surface and generate a large amount of foam, and can increase the interestingness and the pleasure feeling during bathing compared with other bathing products. Current explosive salts have a short foaming time when dissolved, reducing consumer expectations for foaming effectiveness.
Disclosure of Invention
The technical problem to be solved by the invention is to provide the high-hardness and lasting-foaming explosive salt which has higher hardness and hydrophobicity, lasting foaming time, stable foaming effect and rich and fine foam, can effectively relieve skin, eliminate fatigue and promote blood circulation, and simultaneously increases the interestingness and joyful feeling during bathing.
The technical scheme of the invention is as follows:
1. a high hardness and long-lasting foaming explosive salt comprises the following components in percentage by weight: 0-40% of sodium bicarbonate, 10-35% of alpha-hydroxy acid, 0.1-3% of grease and emulsifier, 5-30% of sodium sulfate or sodium chloride or a mixture of sodium sulfate and sodium chloride, and 0.1-5% of magnesium carbonate or magnesium stearate or a mixture of magnesium carbonate and magnesium stearate.
Further, the alpha-hydroxy acid is at least one of anhydrous citric acid, tartaric acid and fumaric acid.
Further, the tower powder is 1-10% and the light sodium carbonate is 5-30%.
Further, at least one of essence, pigment and plant extract is contained in the composition at a content of 1.5% or less.
A method for preparing the high hardness and long-lasting foaming explosive salt, which comprises the following steps: adding oil and fat and an emulsifier into sodium sulfate or sodium chloride or a mixture of the sodium sulfate and the sodium chloride, uniformly mixing, adding alpha-hydroxy acid and sodium bicarbonate, uniformly mixing, finally adding magnesium carbonate or magnesium stearate or a mixture of the magnesium carbonate and the magnesium stearate, uniformly mixing, sieving by using a screen, pressing and molding by using a mold, and dehumidifying and drying. If tower powder, light sodium carbonate or plant extract is required to be added into the formula, the tower powder, the light sodium carbonate or the plant extract, grease and an emulsifier are added into sodium sulfate or sodium chloride or a mixture of the sodium sulfate and the sodium chloride; if essence is required to be added in the formula, the essence is added into the alpha-hydroxy acid in advance; if the pigment is required to be added into the formula, the pigment is required to be added into the sodium bicarbonate in advance.
The invention has the following beneficial effects:
the inventor finds that the hardness of the explosive salt in the forming process can be increased and the hydrophobicity of the explosive salt can be improved by adding magnesium carbonate or magnesium stearate into the material.
The citric acid selected by the invention can react with light sodium carbonate or sodium bicarbonate to generate sodium citrate, generate carbon dioxide and generate bubbles when being dissolved in water. The addition of magnesium carbonate or magnesium stearate can absorb water molecules participating in the reaction into the magnesium carbonate or magnesium stearate to delay the reaction process, thereby prolonging the foaming time, having stable foaming effect and rich and fine foam.
The tower powder and the light sodium carbonate selected by the invention have the density lower than that of water, good water solubility and good compatibility with other components, and the specific gravity of the explosive salt can be adjusted by limiting the using amount of the tower powder and the light sodium carbonate in the explosive salt, so that the selection of the floating explosive salt and the non-floating explosive salt is controllable. The tower powder and the light sodium carbonate react with other components more quickly, so that the volume of the explosive salt is fluffy, the explosive salt floats on the water surface, and rich and durable foam is generated.
The essence, the pigment and the plant extract selected by the invention can endow the explosive salt with rich color, fragrance and nourishing effect, and when the bath foam is applied to bath, the bath foam can effectively relieve skin, eliminate fatigue and promote blood circulation, and simultaneously increases the interestingness and joyful feeling during bath.
Detailed Description
The present invention will be described in detail with reference to examples, which are only preferred embodiments of the present invention and are not intended to limit the present invention.
Non-floating explosive salt
The following table is a table of formulations (in%) of examples 1 to 3 and comparative example 1 of the high hardness long lasting foaming explosive salt of the present invention.
Raw materials Example 1 Example 2 Example 3 Comparative example 1
Sodium bicarbonate 37 37 37 37
Alpha-hydroxy acids Anhydrous citric acid 25% Tartaric acid 25% Fumaric acid 25% Anhydrous citric acid 25%
Sodium sulfate 35 33 15 36
Sodium chloride / / 16 /
Oil and fat 0.7 0.7 0.7 0.7
Emulsifier 0.5 0.5 0.5 0.5
Magnesium stearate 1.0 / 3.0 /
Magnesium carbonate / 3.0 2.0 /
Rose essence 0.1 0.1 0.1 0.1
Red pigment 0.1 0.1 0.1 0.1
Lavender extract 0.6 0.6 0.6 0.6。
A method for preparing the high hardness and long-lasting foaming explosive salt, which comprises the following steps: adding oil and fat, emulsifier and plant extract into sodium sulfate or sodium chloride or mixture of sodium sulfate and sodium chloride, mixing, sequentially adding alpha-hydroxy acid (essence is added into alpha-hydroxy acid in advance) and sodium bicarbonate (essence is added into alpha-hydroxy acid in advance), mixing, adding magnesium carbonate or magnesium stearate or mixture of magnesium carbonate and magnesium stearate, mixing, sieving with a screen, press-molding with a mold, and drying.
The hardness of examples 1-3 and comparative example 1 after moisture extraction was tested using a GS-701N durometer. The samples of equal mass were dissolved in 50L of water at 38-40 deg.C, the change was observed after contact with water, and dissolution test was carried out to test the time required for complete dissolution, with the test results shown in the following table.
Item Example 1 Example 2 Example 3 Comparative example 1
Change after encountering water Sink to the water bottom to generate a large amount of bubbles Sinking to the water bottom to generate a large amount of gasBubble Sink to the water bottom to generate a large amount of bubbles Sink to the water bottom to generate a large amount of bubbles
Time/s required for complete dissolution 195 343 487 130
hardness/N 75 97 107 58。
Therefore, the high-hardness and long-foaming explosive salt has high hardness and hydrophobicity, long foaming time, stable foaming effect and rich and fine foam.
Floating explosive salt
The following table is a table of formulations (in%) of examples 4 to 6 and comparative example 2 of the high hardness long lasting foaming explosive salt of the present invention.
Raw materials Example 4 Example 5 Example 6 Comparative example 2
Sodium bicarbonate 22 22 22 22
Alpha-hydroxy acids Anhydrous citric acid and tartaric acid 25% Tartaric acid and fumaric acid 25% Fumaric acid, citric acid anhydrous 25% Anhydrous citric acid and tartaric acid 25%
Light sodium carbonate 30 30 30 30
Tower powder 10 10 10 10
Sodium chloride 10 / 3 11
Sodium sulfate / 8 3 /
Oil and fat 0.7 0.7 0.7 0.7
Emulsifier 0.5 0.5 0.5 0.5
Magnesium stearate 1.0 / 3.0 /
Magnesium carbonate / 3.0 2.0 /
Rose essence 0.1 0.1 0.1 0.1
Red pigment 0.1 0.1 0.1 0.1
Fumigating clothesGrass extract 0.6 0.6 0.6 0.6。
A method for preparing the high hardness and long-lasting foaming explosive salt, which comprises the following steps: adding oil and fat, emulsifier, tower powder, light sodium carbonate and plant extract into sodium sulfate or sodium chloride or a mixture of sodium sulfate and sodium chloride, mixing uniformly, sequentially adding alpha-hydroxy acid (essence is added into alpha-hydroxy acid in advance) and sodium bicarbonate (essence is added into alpha-hydroxy acid in advance), mixing uniformly, finally adding magnesium carbonate or magnesium stearate or a mixture of magnesium carbonate and magnesium stearate, sieving uniformly by using a screen, pressing and molding by using a mold, dehumidifying and drying.
The hardness of examples 4-6 and comparative example 2 after moisture extraction was tested using a GS-701N durometer. The samples of equal mass were dissolved in 50L of water at 38-40 deg.C, the change was observed after contact with water, and dissolution test was carried out to test the time required for complete dissolution, with the test results shown in the following table.
Item Example 1 Example 2 Example 3 Comparative example 1
Change after encountering water Float on the water surface and generate a large amount of bubbles Float on the water surface and generate a large amount of bubbles Float on the water surface and generate a large amount of bubbles Float on the water surface and generate a large amount of bubbles
Time/s required for complete dissolution 175 325 432 73
hardness/N 73 89 102 55。
Therefore, the explosive salt with high hardness and lasting foaming of the invention realizes the controllable selection of the floating explosive salt and the non-floating explosive salt, and the addition of the tower powder and the light sodium carbonate can ensure that the volume of the explosive salt is fluffy and floats on the water surface, the foaming time is lasting, the foaming effect is stable, and the foam is rich and fine.
The invention is used in a conventional bathtub bathing mode and mainly comprises the following steps:
(1) firstly, adding water with a proper temperature into a bathtub;
(2) putting a proper amount of the explosive salt of the product into a bathtub, and soaking the skin in the bathtub for 10-20 minutes;
(3) the skin was rinsed clean of foam with water.
The daily use is recommended to make the skin relax nerves, eliminate fatigue and promote the blood circulation of the body.
The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.

Claims (5)

1. A high hardness and long-lasting foaming explosive salt is characterized by comprising the following components in percentage by weight: 10-40% of sodium bicarbonate, 10-35% of alpha-hydroxy acid, 0.1-3% of grease and emulsifier, 5-30% of sodium sulfate or sodium chloride or a mixture of sodium sulfate and sodium chloride, and 0.1-5% of magnesium carbonate or magnesium stearate or a mixture of magnesium carbonate and magnesium stearate.
2. The high hardness, long lasting effervescent explosive salt of claim 1, wherein the α -hydroxy acid is at least one of anhydrous citric acid, tartaric acid, fumaric acid.
3. The high hardness long lasting effervescent blast salt of claim 1 further comprising 1-10% tower dust, 5-30% light sodium carbonate.
4. The high hardness long lasting effervescent blast salt of claim 1, further comprising at least one of essence, pigment, plant extract at 1.5% or less.
5. A method of preparing a high hardness long lasting effervescent blast salt of claim 1, comprising the steps of: adding oil and fat and an emulsifier into sodium sulfate or sodium chloride or a mixture of the sodium sulfate and the sodium chloride, uniformly mixing, adding alpha-hydroxy acid and sodium bicarbonate, uniformly mixing, finally adding magnesium carbonate or magnesium stearate or a mixture of the magnesium carbonate and the magnesium stearate, uniformly mixing, sieving by using a screen, pressing and molding by using a mold, and dehumidifying and drying.
CN201910990840.XA 2019-10-18 2019-10-18 High-hardness and long-lasting-foaming explosive salt and preparation method thereof Pending CN110693731A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115006287A (en) * 2022-05-27 2022-09-06 惠州市蓝桥实业有限公司 Explosive salt and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2013087105A (en) * 2011-10-21 2013-05-13 Goshu Yakuhin Kk Bubble-generating bath agent
CN106102693A (en) * 2014-03-10 2016-11-09 乌瑞斯化妆品有限公司 Effervescence combination
CN107970135A (en) * 2017-12-12 2018-05-01 惠州兆骐礼品有限公司 A kind of appearance is in the explosion salt of quality as metal
CN108294965A (en) * 2017-12-21 2018-07-20 惠州兆骐礼品有限公司 A kind of mounting flower explosion salt
CN108852867A (en) * 2018-07-25 2018-11-23 惠州兆婷化妆品有限公司 One kind is swum the salt and preparation method thereof that explodes

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2013087105A (en) * 2011-10-21 2013-05-13 Goshu Yakuhin Kk Bubble-generating bath agent
CN106102693A (en) * 2014-03-10 2016-11-09 乌瑞斯化妆品有限公司 Effervescence combination
CN107970135A (en) * 2017-12-12 2018-05-01 惠州兆骐礼品有限公司 A kind of appearance is in the explosion salt of quality as metal
CN108294965A (en) * 2017-12-21 2018-07-20 惠州兆骐礼品有限公司 A kind of mounting flower explosion salt
CN108852867A (en) * 2018-07-25 2018-11-23 惠州兆婷化妆品有限公司 One kind is swum the salt and preparation method thereof that explodes

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115006287A (en) * 2022-05-27 2022-09-06 惠州市蓝桥实业有限公司 Explosive salt and preparation method thereof

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Application publication date: 20200117