CN110652459A - Emulsion production method - Google Patents

Emulsion production method Download PDF

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Publication number
CN110652459A
CN110652459A CN201910973875.2A CN201910973875A CN110652459A CN 110652459 A CN110652459 A CN 110652459A CN 201910973875 A CN201910973875 A CN 201910973875A CN 110652459 A CN110652459 A CN 110652459A
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CN
China
Prior art keywords
emulsion
connecting rod
stirring
storage barrel
material receiving
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Withdrawn
Application number
CN201910973875.2A
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Chinese (zh)
Inventor
曹建华
曹亦徐
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Hainan Zangxinge Fragrance Industry Co Ltd
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Hainan Zangxinge Fragrance Industry Co Ltd
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Priority to CN201910973875.2A priority Critical patent/CN110652459A/en
Publication of CN110652459A publication Critical patent/CN110652459A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04Dispersions; Emulsions
    • A61K8/06Emulsions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/362Polycarboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/733Alginic acid; Salts thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A61K8/988Honey; Royal jelly, Propolis
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 

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  • Animal Behavior & Ethology (AREA)
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  • Mycology (AREA)
  • Microbiology (AREA)
  • Botany (AREA)
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  • Engineering & Computer Science (AREA)
  • Dispersion Chemistry (AREA)
  • Zoology (AREA)
  • Dermatology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mixers With Rotating Receptacles And Mixers With Vibration Mechanisms (AREA)

Abstract

The invention discloses an emulsion production method, which comprises the following steps: a. weighing jojoba oil 0.5-4.0g, olive oil 0.5-4.0g, glyceryl monostearate 2.0-10g, span 800.3-3g, and vitamin E0.1-3.0g, heating to 70-85 deg.C, completely melting, stirring, and mixing to obtain oil phase; b. weighing 1-10g of poloxamer, 2.0-20g of glycerol, 0.6-5g of propylene glycol, 14.0-50.0g of distilled water, 0.3-3g of honey, 0.1-4.0g of urea, 0.3-3ml of 1% sodium hyaluronate, 0.1-0.5mg of disodium ethylenediamine tetraacetate and 0.02-1.0g of L-serine, heating to 70-85 ℃, completely melting the materials, and uniformly stirring to obtain a water phase; c. pouring the water phase into the oil phase at 70-85 ℃, stirring for 5-15 minutes after adding to form uniform emulsion, cooling to room temperature, adding 1-10ml of lily extract, 1-10ml of prunus mume extract, 2-15ml of coconut juice, 1-10ml of waxgourd seed extract, 1-10ml of corn stigma extract, 0.05-2ml of essence, 6-25g of sodium alginate solution, 0.1-2g of sorbic acid and 10-30g of carbomer 941 solution, and uniformly stirring to obtain the nourishing and moisturizing emulsion; d. and (4) putting the prepared emulsion into a filling machine, and filling the emulsion.

Description

Emulsion production method
Technical Field
The invention belongs to the technical field of cosmetic production, and particularly relates to a method for producing emulsion.
Background
The filling machine is widely applied to the automatic production of daily cosmetics, in the production of cosmetics, the filling machine injects quantitative products into a cosmetic container to efficiently and stably finish the bottling production of the cosmetics, and meanwhile, the filling machine can be added with liquid, emulsion and paste, and can be used for products in various states.
Its inner wall usually can be stained with after the filling operation of liquid filling machine and remain, especially after the filling emulsion, its inner wall adheres to and has more to remain, need do comparatively careful clearance to liquid filling machine inside in order to be ready for next use, and the clearance process is comparatively inconvenient, if the clearance does not go clean the emulsion that remains in the liquid filling machine after long-time placing easy rotten influence emulsion filling quality.
Disclosure of Invention
The invention provides a method for producing emulsion to overcome the defects of the prior art.
In order to achieve the purpose, the invention adopts the following technical scheme: a method of producing an emulsion comprising:
a. weighing jojoba oil 0.5-4.0g, olive oil 0.5-4.0g, glyceryl monostearate 2.0-10g, span 800.3-3g, and vitamin E0.1-3.0g, heating to 70-85 deg.C, completely melting, stirring, and mixing to obtain oil phase;
b. weighing 1-10g of poloxamer, 2.0-20g of glycerol, 0.6-5g of propylene glycol, 14.0-50.0g of distilled water, 0.3-3g of honey, 0.1-4.0g of urea, 0.3-3ml of 1% sodium hyaluronate, 0.1-0.5mg of disodium ethylenediamine tetraacetate and 0.02-1.0g of L-serine, heating to 70-85 ℃, completely melting the materials, and uniformly stirring to obtain a water phase;
c. pouring the water phase into the oil phase at 70-85 ℃, stirring for 5-15 minutes after adding to form uniform emulsion, cooling to room temperature, adding 1-10ml of lily extract, 1-10ml of prunus mume extract, 2-15ml of coconut juice, 1-10ml of waxgourd seed extract, 1-10ml of corn stigma extract, 0.05-2ml of essence, 6-25g of sodium alginate solution, 0.1-2g of sorbic acid and 10-30g of carbomer 941 solution, and uniformly stirring to obtain the nourishing and moisturizing emulsion;
d. putting the prepared emulsion into a filling machine, and filling the emulsion;
the filling machine in the step d comprises a storage barrel, a first cover plate arranged at the top of the storage barrel and a discharge pipe arranged at the bottom of the storage barrel, wherein the discharge pipe is communicated with a discharge port of the storage barrel, a stirring device is arranged in the storage barrel, the bottom of the storage barrel is of a conical structure, a third connecting rod is arranged on the inner wall of the storage barrel, a first mounting plate is arranged on the third connecting rod, a driving motor is arranged on the first mounting plate, the stirring device comprises a stirring shaft arranged on an output shaft of the driving motor and a stirring blade arranged on the stirring shaft, a first movable cavity is arranged on the stirring blade, a scraping plate is arranged in the first movable cavity, and a first push rod for driving the scraping plate to move along the inner wall of the first movable cavity is arranged on the first cover plate; after the emulsion is prepared, pouring the emulsion into a storage barrel, placing an emulsion bottle below a discharge pipe, and injecting the emulsion into the emulsion bottle through the discharge pipe; the driving motor drives the stirring blade to rotate, and the stirring blade stirs the emulsion to enable the emulsion to be in a motion state, so that the emulsion is discharged from the discharge pipe.
After the filling operation is finished, the first push rod is pressed down to enable the scraper to extend out of the first movable cavity, the scraper is in contact with the inner wall of the storage barrel, the driving motor drives the stirring shaft to rotate, the stirring shaft drives the scraper to rotate, emulsion on the inner wall of the storage barrel is scraped under the action of the scraper, so that the inner wall of the storage barrel is cleaned, the emulsion on the inner wall of the storage barrel is scraped, the emulsion is prevented from remaining on the inner wall of the storage barrel to affect the quality of the emulsion, and the cleaning difficulty of the storage barrel is reduced; under the action of the stirring device, the emulsion in the storage barrel is stirred, so that the emulsion is in a continuous motion state, the emulsion is prevented from precipitating after standing, and the uniform mixing of the emulsion is ensured, thereby improving the quality of the emulsion; the emulsion in the storage barrel flows towards the discharge pipe better under the arrangement of the conical structure at the bottom of the storage barrel, so that the residue of the emulsion in the storage barrel is reduced, and the waste of the emulsion is reduced; when the stirring blade stirs the emulsion, the scraper is positioned in the first movable cavity and is not contacted with the inner wall of the storage barrel, so that the phenomenon that the scraper is contacted with the inner wall of the storage barrel for a long time to block the rotation of the stirring blade is avoided, and a driving motor is protected; with scraper blade direct bonding on agitating unit, to agitating unit make full use of, need not to do the clearance to the storage vat inner wall with other clearance pieces in addition, reduce the storage vat clearance degree of difficulty, make the clearance of storage vat more convenient.
The preparation method of the seaweed mud solution comprises the following steps: weighing 5-15g of sodium alginate, adding 100 ml of distilled water, standing and stirring to fully swell the sodium alginate into uniform and transparent liquid.
The preparation method of the carbomer solution comprises the following steps: weighing 9412-15g carbomer, adding 1000ml distilled water 100-
The essence is one of juicy peach essence, cucumber essence, rose essence, sweet osmanthus essence and pineapple essence.
The lily extracting solution is prepared by the following method: weighing an appropriate amount of lily, heating to 90-100 ℃, decocting and extracting for 3 times, adding 8-15 times of water for the first time, extracting for 0.5-1.5h, adding 6-12 times of water for the second time, extracting for 0.5-1.5h, adding 4-10 times of water for the third time, extracting for 0.5-1.5h, filtering with three layers of gauze each time, combining filtrates, heating and concentrating to 3-6 times of the weight of lily in terms of ml/g, and filtering with three layers of gauze.
The bottom of the first movable cavity is provided with a first movable groove, the bottom of the scraper blade is provided with a first connecting plate, the first connecting plate penetrates through the first movable groove, the bottom of the first connecting plate is provided with a bearing plate, the bottom of the stirring blade is provided with a first material receiving box, and the bearing plate is provided with a first chute matched with the first material receiving box; the stirring blade is provided with a mounting frame, the first material receiving box is arranged on the mounting frame, the first material receiving box is provided with a second cover plate, the second cover plate is detachably connected to the bearing plate, the top of the second cover plate is provided with a second chute matched with the first chute, and the first material receiving box is provided with a first chute matched with the second cover plate; when the storage barrel is cleaned, the first push rod is pressed down to enable the scraper to extend out of the first movable cavity, the scraper drives the second cover plate to move, the second cover plate is moved away from the top of the first material receiving box to enable the first material receiving box to be in an open state, the driving motor drives the stirring shaft to rotate, the scraper is in contact with the inner wall of the storage barrel to scrape emulsion on the inner wall of the storage barrel, the scraped emulsion flows onto the receiving plate along the side wall of the scraper, the emulsion flows downwards along the first chute and the second chute to enable the emulsion to flow into the first material receiving box, and the emulsion on the inner wall of the storage barrel is collected in the first material receiving box; after the emulsion on the inner wall of the storage barrel is scraped by the scraper, the emulsion is collected through the first material receiving box, and the emulsion attached to the inner wall of the storage barrel is recycled, so that the waste of the emulsion is reduced; the emulsion in the first material receiving box is protected under the action of the second cover plate, the emulsion in the first material receiving box is prevented from shaking out of the first material receiving box when the stirring rod rotates, and the emulsion is stably collected in the first material receiving box; the position of the second cover plate is controlled through the movement of the scraper, so that the first material receiving box is directly in an open state when the scraper is in contact with the inner wall of the storage barrel, and the emulsion is collected in the first material receiving box to be recycled; the chute is arranged to guide the emulsion, and the emulsion in the storage barrel is collected in the first material receiving box, so that the emulsion on the inner wall of the storage barrel is prevented from dropping to the bottom of the storage barrel again to cause inconvenience in cleaning; after emulsion in the first material receiving box is filled, the first material receiving box is detached from the mounting frame, so that the emulsion in the first material receiving box can be directly collected, and the emulsion recovery difficulty is reduced.
A sealing block is arranged in the discharge pipe, a linear opening is formed in the sealing block, a second movable cavity matched with the sealing block is arranged on the inner wall of the discharge pipe, and a first opening is formed in the side wall of the second movable cavity; a second mounting plate is arranged on the side wall of the discharge pipe, an air cylinder is arranged on the second mounting plate, a piston rod of the air cylinder is arranged in the first opening in a penetrating mode, a first connecting rod and a second connecting rod are arranged in a second movable cavity, the first connecting rod and the second connecting rod are respectively in two groups, the first connecting rod is hinged to the inner wall of the second movable cavity, one end of the second connecting rod is hinged to the first connecting rod, the other end of the second connecting rod is hinged to a third connecting rod, the two groups of the first connecting rods and the two groups of the second connecting rods are matched with each other to form a diamond structure, and the third connecting rod is arranged on the piston rod of the; when the emulsion bottle moves to the position below the discharge pipe, the air cylinder pushes the piston rod to move forwards, so that the piston rod pushes the third connecting rod to move, the first connecting rod and the second connecting rod rotate around the connecting point, the second connecting rod moves towards the middle of the second movable cavity, the second connecting rod extrudes the sealing block to deform the sealing block, the linear opening is opened after the sealing block is deformed, so that emulsion is discharged from the discharge pipe, and the emulsion is injected into the emulsion bottle; when the sealing block is not deformed, the discharge pipe is in a closed state, so that emulsion is prevented from flowing out of the discharge pipe, and emulsion waste is prevented; the on-off of the liquid outlet pipe is controlled under the action of the air cylinder, so that emulsion is prevented from hanging on the sealing block, and the controllability of the liquid outlet pipe is improved; by utilizing the self property of the sealing block, the liquid outlet pipe is sealed when the sealing block is not stressed, so that the liquid outlet pipe is in a normally closed state, and the working stability of the filling machine is improved.
The invention has the following advantages: strike off the emulsion on the storage vat inner wall under the scraper blade effect to do the clearance to the storage vat inner wall, strike off the emulsion of storage vat inner wall, prevent that the emulsion from remaining on the storage vat inner wall to emulsion quality production influence, reduce the storage vat clearance degree of difficulty.
Drawings
Fig. 1 is a schematic structural diagram of a filling machine of the present invention.
Fig. 2 is a first cross-sectional view of the filling machine of the present invention.
Fig. 3 is an enlarged view of a portion a in fig. 2.
Fig. 4 is an enlarged view of fig. 2 at B.
Fig. 5 is an enlarged view of fig. 2 at C.
Fig. 6 is an enlarged view of fig. 2 at D.
Fig. 7 is a second schematic cross-sectional view of the filling machine of the present invention.
Fig. 8 is an enlarged view of fig. 7 at E.
Fig. 9 is an enlarged view of fig. 7 at F.
Fig. 10 is a third schematic cross-sectional view of the filling machine of the present invention.
Fig. 11 is an enlarged view at G in fig. 10.
Fig. 12 is an enlarged view of fig. 10 at H.
Fig. 13 is a fourth schematic cross-sectional view of the filling machine of the present invention.
Fig. 14 is an enlarged view at I in fig. 13.
Fig. 15 is a schematic cross-sectional view of the filling machine of the present invention.
Fig. 16 is an enlarged view at J in fig. 15.
Detailed Description
Example 1:
a method of producing an emulsion comprising: a. weighing 0.5g of jojoba oil, 0.5g of olive oil, 2.0g of glyceryl monostearate, 800.3g of span and 0.1g of vitamin, heating to 70 ℃, completely melting, and uniformly stirring and mixing to obtain an oil phase; b. weighing 1g of poloxamer, 2.0g of glycerol, 0.6g of propylene glycol, 14.0g of distilled water, 0.3-3g of honey, 0.1g of urea, 0.3ml of 1% sodium hyaluronate, 0.1mg of disodium ethylenediamine tetraacetic acid and 0.02g of L-serine, heating to 70 ℃, completely melting the L-serine, and uniformly stirring and mixing to obtain a water phase; c. pouring the water phase into the oil phase at 70 ℃, stirring for 5 minutes after adding the water phase to form uniform emulsion, cooling to room temperature, adding 1ml of lily extract, 1ml of prunus mume extract, 2ml of coconut juice, 1ml of waxgourd seed extract, 1ml of corn stigma extract, 0.05ml of essence, 6g of sodium alginate solution, 0.1g of sorbic acid and 10g of carbomer 941 solution, and uniformly stirring to obtain finished emulsion; d. putting the prepared emulsion into a filling machine, and filling the emulsion; the lily extracting solution is prepared by the following method: weighing a proper amount of lily, putting the lily into a treatment barrel, heating to 90 ℃, decocting and extracting for 3 times, adding 8 times of water for the first time to extract for 0.5h, adding 6 times of water for the second time to extract for 0.5h, adding 4 times of water for the third time to extract for 0.5h, filtering with three layers of gauze each time, combining filtrates, heating and concentrating to 3 times of the weight of the lily in terms of ml/g, and filtering with three layers of gauze to obtain the lily tea beverage; the red plum extract is prepared by the following method: weighing a certain amount of prunus mume, heating to 90 ℃, decocting and extracting for 3 times, adding 30 times of water for the first time, extracting for 0.5h, adding 25 times of water for the second time, extracting for 0.5h, adding 20 times of water for the third time, extracting for 0.5h, filtering with three layers of gauze each time, combining filtrates, heating and concentrating to 3 times of the weight of prunus mume in terms of ml/g, and filtering with three layers of gauze to obtain the product; weighing semen Benincasae, heating to 90 deg.C, decocting for 3 times, extracting with 8 times of water for 0.5 hr, 6 times of water for 0.5 hr, and 6 times of water for 0.5 hr, extracting with 0.5 hr, filtering with three layers of gauze, mixing filtrates, heating and concentrating to 3 times of semen Benincasae weight in ml/g, and filtering with three layers of gauze; the corn stigma extracting solution is prepared by the following method: weighing a certain amount of corn stigma, heating to 90 ℃, decocting and extracting for 3 times, wherein the first time is 0.5h with 8 times of water, the second time is 0.5h with 6 times of water, the third time is 0.5h with 6 times of water, filtering with three layers of gauze each time, combining filtrates, heating and concentrating to 3 times of the weight of the corn stigma in ml/g, and filtering with three layers of gauze to obtain the corn stigma extract; the essence is juicy peach essence; the preparation method of the seaweed mud solution comprises the following steps: weighing 5-15g of sodium alginate, adding 100 ml of distilled water, standing and stirring to fully swell the sodium alginate into uniform transparent liquid; the preparation method of the carbomer solution comprises the following steps: weighing 9412-15g of carbomer, adding 1000ml of distilled water, standing and stirring to fully swell the carbomer into uniform transparent liquid.
As shown in fig. 1 to 16, the filling machine in step d includes a storage tank 1, a first cover plate 2 disposed on the top of the storage tank 1, and a discharge pipe 11 disposed on the bottom of the storage tank 1, the discharge pipe 11 is communicated with the discharge hole of the storage barrel 1, a stirring device is arranged in the storage barrel 1, the bottom of the storage barrel 1 is of a conical structure, the inner wall of the storage barrel 1 is provided with a third connecting rod 121, the third connecting rod 121 is provided with a first mounting plate 12, the first mounting plate 12 is provided with a driving motor 13, the stirring device comprises a stirring shaft 3 arranged on an output shaft of the driving motor 13 and a stirring blade 31 arranged on the stirring shaft 3, a first movable cavity is arranged on the stirring blade 31, a scraping plate 32 is arranged in the first movable cavity, the first cover plate 2 is provided with a first push rod 21 for driving the scraper 32 to move along the inner wall of the first movable cavity; after the emulsion is prepared, pouring the emulsion into the storage barrel 1, placing an emulsion bottle below the discharge pipe 11, and injecting the emulsion into the emulsion bottle through the discharge pipe 11; the driving motor 13 drives the stirring blade 31 to rotate, and the stirring blade 31 stirs the emulsion to enable the emulsion to be in a moving state so as to discharge the emulsion from the discharge pipe 11.
After the filling operation is finished, the first push rod is pressed down to enable the scraper to extend out of the first movable cavity, the scraper is in contact with the inner wall of the storage barrel, the driving motor drives the stirring shaft to rotate, the stirring shaft drives the scraper to rotate, emulsion on the inner wall of the storage barrel is scraped under the action of the scraper, so that the inner wall of the storage barrel is cleaned, the emulsion on the inner wall of the storage barrel is scraped, the emulsion is prevented from remaining on the inner wall of the storage barrel to affect the quality of the emulsion, and the cleaning difficulty of the storage barrel is reduced; under the action of the stirring device, the emulsion in the storage barrel is stirred, so that the emulsion is in a continuous motion state, the emulsion is prevented from precipitating after standing, and the uniform mixing of the emulsion is ensured, thereby improving the quality of the emulsion; the emulsion in the storage barrel flows towards the discharge pipe better under the arrangement of the conical structure at the bottom of the storage barrel, so that the residue of the emulsion in the storage barrel is reduced, and the waste of the emulsion is reduced; when the stirring blade stirs the emulsion, the scraper is positioned in the first movable cavity and is not contacted with the inner wall of the storage barrel, so that the phenomenon that the scraper is contacted with the inner wall of the storage barrel for a long time to block the rotation of the stirring blade is avoided, and a driving motor is protected; with scraper blade direct bonding on agitating unit, to agitating unit make full use of, need not to do the clearance to the storage vat inner wall with other clearance pieces in addition, reduce the storage vat clearance degree of difficulty, make the clearance of storage vat more convenient.
The output shaft of the driving motor is provided with an installation block 14, the installation block is provided with an installation groove, the stirring shaft is inserted into the installation groove, the inner wall of the installation groove is provided with a first limit groove, the stirring shaft is provided with a third movable cavity, the side wall of the bottom of the third movable cavity is provided with a second opening, a first limit block 36 matched with the first limit groove is arranged in the second opening in a penetrating manner, and when the first push rod moves downwards, the first limit block enters the third movable cavity, so that the first limit block is separated from the first limit groove, and the stirring shaft is conveniently detached from the installation block; still be equipped with the second spacing groove on the mounting groove inner wall, (mixing) shaft bottom be equipped with second spacing groove matched with third stopper 33, under the mutually supporting of third stopper and second spacing groove, play the effect of stalling to the (mixing) shaft to drive the (mixing) shaft rotation under the driving motor effect.
The third movable cavity is communicated with the first movable cavity, a connecting block 35 is arranged in the third movable cavity, a fourth movable cavity is arranged on the connecting block, compressed air is filled in the fourth movable cavity, a branch is arranged on the side wall of the connecting block, the fourth movable cavity extends to the branch, a second push rod 353 is arranged in the fourth movable cavity in the branch, and a first limiting plate is arranged at one end of the second push rod 353 to prevent the second push rod from falling out of the fourth movable cavity; a third push rod 351 penetrates through the top of the third movable cavity, a support spring 352 is arranged at the bottom of the third push rod, and the support spring is connected with the bottom of the fourth movable cavity; the top of the third movable cavity is provided with a first through cavity matched with the first push rod, and when the first cover plate covers the storage barrel, the bottom of the first push rod is directly contacted with the third push rod; a connecting spring 321 is arranged on the side wall of the scraper plate, and one end of the connecting spring is fixedly connected to the inner wall of the first movable cavity; after emulsion in the storage barrel is filled, the first push rod is pushed to move downwards, the first push rod pushes the third push rod to move towards the third movable cavity, air in the third movable cavity is pressed into the connecting block branch under the action of the third push rod, so that air flow pushes the second push rod to move outwards, the second push rod pushes the scraper to move towards the outer side of the first movable cavity, the scraper is made to contact with the inner wall of the storage barrel, the emulsion on the inner wall of the storage barrel is scraped, and the cleaning effect on the storage barrel is improved; after the storage vat clearance was accomplished, first push rod of up pulling, the third push rod up motion under the supporting spring effect, the scraper blade is under the connecting spring effect down toward the inside motion of first activity chamber, accomplishes the reseing of scraper blade.
A fourth push rod 354 is arranged at the bottom of the connecting block, a fourth connecting rod 361 is hinged to one end of the first limiting block, the fourth push rod is hinged to the fourth connecting rod, a return spring 355 is further arranged at the bottom of the connecting block, and the return spring is sleeved on the outer side of the fourth push rod; the bottom of the first limiting block is of an arc-shaped structure, when the stirring shaft is installed, the stirring shaft is directly inserted into the installation groove, and the first limiting block enters the third movable cavity under the action of the arc surface, so that the first limiting block is prevented from blocking the installation of the stirring shaft; after the emulsion on the inner wall of the storage barrel is scraped by the scraper, the first push rod is continuously pressed downwards to enable the first push rod to continuously push the third push rod to move downwards, the third push rod cannot move downwards and then enables the whole connecting block to move downwards, the connecting block pushes the fourth push rod to move downwards, the fourth push rod drives the fourth connecting rod to move, the first limiting block is pulled into the third movable cavity, the first limiting block is separated from the first limiting groove, so that the stirring shaft can be directly taken out of the mounting block, and the difficulty in assembling and disassembling the stirring shaft is reduced; when first apron lid was on the storage vat, its bottom contacted with the (mixing) shaft top, played the fixed action to the (mixing) shaft, promoted the stability of (mixing) shaft work.
A second through cavity is formed in the first cover plate, the first push rod penetrates through the second through cavity, three movable grooves are formed in the inner wall of the second through cavity, openings are formed in the bottoms of the two movable grooves located above the second through cavity, a second limiting block matched with the openings is arranged on the first push rod, when the storage barrel is cleaned, the first push rod is rotated, the second limiting block is aligned with the openings in the topmost movable groove, the first push rod is pushed downwards, the second limiting block is moved into the movable groove in the middle, and therefore the first push rod pushes the third push rod to move downwards to push the scraper out of the first movable cavity; when the stirring shaft is detached from the mounting block, the first push rod is rotated to align the second limiting block with the opening on the middle movable groove, the first push rod is pushed downwards to enable the second limiting block to move into the bottommost movable groove, so that the first push rod pushes the connecting block to move downwards to enable the first limiting block to enter the third movable cavity; under the mutually supporting of second stopper and activity groove, play limiting displacement to first push rod, what make the scraper blade last stretches out from first activity intracavity to do the clearance to the storage vat inner wall under the scraper blade effect.
A first movable groove is formed in the bottom of the first movable cavity, a first connecting plate is arranged at the bottom of the scraping plate 32 and penetrates through the first movable groove, a bearing plate is arranged at the bottom of the first connecting plate, a first material receiving box 34 is arranged at the bottom of the stirring blade 31, and a first inclined groove matched with the first material receiving box 34 is formed in the bearing plate; the stirring blade 31 is provided with a mounting frame 311, the first material receiving box 34 is arranged on the mounting frame 311, the first material receiving box 34 is provided with a second cover plate 341, the second cover plate 341 is detachably connected to the receiving plate, the top of the second cover plate 341 is provided with a second chute matched with the first chute, and the first material receiving box 34 is provided with a first chute matched with the second cover plate 341; when the storage vat 1 is cleaned, the first push rod 21 is pressed down to enable the scraper 32 to extend out of the first movable cavity, the scraper 32 drives the second cover plate 341 to move, the second cover plate 341 is moved away from the top of the first material receiving box 34 to enable the first material receiving box 34 to be in an open state, the driving motor 13 drives the stirring shaft 3 to rotate, the scraper 32 is in contact with the inner wall of the storage vat 1 to scrape emulsion on the inner wall of the storage vat 1, the scraped emulsion flows onto the receiving plate along the side wall of the scraper 32, the emulsion flows downwards along the first chute and the second chute to enable the emulsion to flow into the first material receiving box 34, and the emulsion on the inner wall of the storage vat 1 is collected in the first material receiving box 34; the position of the second cover plate is controlled through the movement of the scraper, so that the first material receiving box is directly in an open state when the scraper is in contact with the inner wall of the storage barrel, and the emulsion is collected in the first material receiving box to be recycled; the chute is arranged to guide the emulsion, and the emulsion in the storage barrel is collected in the first material receiving box, so that the emulsion on the inner wall of the storage barrel is prevented from dropping to the bottom of the storage barrel again to cause inconvenience in cleaning; after emulsion in the first material receiving box is filled, the first material receiving box is detached from the mounting frame, so that the emulsion in the first material receiving box can be directly collected, and the emulsion recovery difficulty is reduced.
A first connecting groove is formed in the side wall of the first material receiving box, a third through cavity is formed in the mounting frame, a second connecting plate 312 matched with the first connecting groove is arranged in the third through cavity in a penetrating mode, a second limiting plate 3121 is arranged at one end of the second connecting plate, a first connecting frame 313 is arranged on the mounting frame, a third limiting plate 314 is arranged in the first connecting frame in a penetrating mode, a third limiting groove matched with the third limiting plate is formed in the second connecting plate, a fourth limiting plate 3141 is arranged at the top of the third limiting plate, a fourth limiting block is further arranged on the third limiting plate, and a second movable groove matched with the fourth limiting block is formed in the first connecting frame; under the action of the fourth limiting block, the third limiting plate is prevented from excessively descending to influence the matching effect of the third limiting plate and the second connecting plate; when the first material receiving box is installed, the second connecting plate is pulled out of the third through cavity, the first material receiving box is pushed into the installation frame, the first connecting groove moves to one side of the third through cavity, the second connecting plate is pushed into the first connecting groove, the second connecting plate is embedded into the first connecting groove, and the first material receiving box is fixed under the mutual matching of the second connecting plate and the first connecting groove; the third limiting plate is pushed downwards, the third limiting plate is inserted into the third limiting groove, the second connecting plate is fixed under the action of the third limiting plate, the matching effect of the second connecting plate and the first connecting groove is improved, and therefore the mounting effect of the first material receiving box and the mounting frame is improved.
Be equipped with first slider on the second apron lateral wall, accept be equipped with on the board with first slider matched with second spread groove, when packing into the installation piece with first material receiving box, make first slider and second spread groove align, pack into the second spread groove with first slider, accomplish the second apron and accept being connected of board, make the scraper blade drive and accept the board and drive the second apron and together remove when removing, realize the simultaneous movement of second apron and scraper blade, the second apron is opened when making the scraper blade lie in the contact of storage vat inner wall, the second apron is closed when the scraper blade is in first activity intracavity, emulsion enters into first material receiving box when avoiding filling with the emulsion in the storage vat, reduce the waste of emulsion.
A sealing block 113 is arranged in the discharge pipe 11, the sealing block is made of rubber, a linear opening is formed in the sealing block 113, and the linear opening can be formed by cutting the sealing block by a blade; a second movable cavity matched with the sealing block 113 is arranged on the inner wall of the discharge pipe 11, and a first opening is formed in the side wall of the second movable cavity; a second mounting plate 111 is arranged on the side wall of the discharge pipe 11, an air cylinder 4 is arranged on the second mounting plate 111, a piston rod of the air cylinder 4 is arranged in the first opening in a penetrating manner, a first connecting rod and a second connecting rod 114 are arranged in the second movable cavity, the first connecting rod and the second connecting rod 114 are respectively divided into two groups, the first connecting rod is hinged to the inner wall of the second movable cavity, one end of the second connecting rod 114 is hinged to the first connecting rod, the other end of the second connecting rod is hinged to a third connecting rod 45, the two groups of the first connecting rods and the two groups of the second connecting rods 114 are matched with each other to form a diamond structure, and the third connecting rod 45 is arranged on the piston rod of the; after the emulsion bottle moves to the lower part of the discharge pipe 11, the air cylinder 4 pushes the piston rod to move forwards, so that the piston rod pushes the third connecting rod 45 to move, the first connecting rod and the second connecting rod 114 rotate around the connecting point, the second connecting rod 114 moves towards the middle part of the second movable cavity, the second connecting rod 114 extrudes the sealing block 113 to enable the sealing block 114 to deform, the linear opening is opened after the sealing block 114 deforms, so that emulsion is discharged from the discharge pipe 11, and the emulsion is injected into the emulsion bottle; when the sealing block is not deformed, the discharge pipe is in a closed state, so that emulsion is prevented from flowing out of the discharge pipe, and emulsion waste is prevented; the on-off of the liquid outlet pipe is controlled under the action of the air cylinder, so that emulsion is prevented from hanging on the sealing block, and the controllability of the liquid outlet pipe is improved; by utilizing the self property of the sealing block, the liquid outlet pipe is sealed when the sealing block is not stressed, so that the liquid outlet pipe is in a normally closed state, and the working stability of the filling machine is improved.
A second connecting frame 41 is arranged on a piston rod of the air cylinder, a third connecting plate 42 is arranged at the bottom of the second connecting frame, a material receiving plate 43 is arranged at the bottom of the third connecting plate, a guide rod 112 is arranged on the side wall of the discharge pipe, a through hole matched with the guide rod is arranged on the second connecting frame, a second material receiving box 44 is arranged at the bottom of the material receiving plate, a second sliding block is arranged at the top of the second material receiving box, and a second sliding groove matched with the second sliding block is arranged at the bottom of the material receiving plate; a third opening is formed in the third connecting plate, a third chute is formed in the material receiving plate, and the third opening is formed in the bottom end of the third chute; when the emulsion bottle moves to the position below the discharge pipe, the air cylinder pushes the piston rod to move forwards, the piston rod pushes the second connecting rod to extrude the sealing block, and meanwhile, the piston rod drives the second connecting frame to move forwards, so that the material receiving plate is moved away from the position below the discharge pipe, and the emulsion can be directly injected into the emulsion bottle; after emulsion filling is accomplished, the cylinder drive piston rod moves back, connects the flitch to remove to the discharging pipe below again, and the emulsion that remains on the sealed piece drips under the action of gravity on connecing the flitch, and the emulsion that drops on connecing the flitch enters into third opening department along the third chute, collects the emulsion in the second connects the material box, prevents that the emulsion from directly dripping to cause the waste of emulsion and the inconvenience of clearance on the conveyer belt, reduces emulsion manufacturing cost.
After the emulsion is filled into the storage barrel, the first cover plate is covered, the driving motor drives the stirring shaft to rotate, so that the stirring shaft drives the stirring blades to rotate, the stirring blades play a stirring role on the emulsion, the emulsion is prevented from being precipitated, and the quality effect of the emulsion is improved; when the emulsion bottle moves to the position below the discharge pipe, the air cylinder pushes the piston rod to extend out, the sealing block deforms under the action of pressure, the discharge pipe is in an open state, the material receiving plate is moved away from the position below the discharge pipe, and emulsion is directly injected into the emulsion bottle; after emulsion in the storage vat is filled, the first push rod is pushed downwards, the first push rod is made to push the third push rod to move downwards, the scraper blade extends out of the first movable cavity, the scraper blade is made to contact with the inner wall of the storage vat, emulsion on the inner wall of the storage vat is scraped, the scraped emulsion flows downwards along the scraper blade, the emulsion flows into the first material receiving box, the emulsion is collected through the first material receiving box, the emulsion adhered to the inner wall of the storage vat is recycled, waste of the emulsion is reduced, and the production cost of the emulsion is reduced.
Example 2:
a method of producing an emulsion comprising: a. weighing 4.0g of jojoba oil, 4.0g of olive oil, 10g of glyceryl monostearate, 803g of span and 3.0g of vitamin E, heating to 85 ℃, completely melting, and uniformly stirring and mixing to obtain an oil phase; b. weighing 10g of poloxamer, 20g of glycerol, 5g of propylene glycol, 50.0g of distilled water, 3g of honey, 4.0g of urea, 3 g/ml of 1% sodium hyaluronate, 3ml, 0.5mg of disodium ethylene diamine tetraacetate and 1.0g of L-serine, heating to 85 ℃, completely melting the materials, and uniformly stirring and mixing to obtain a water phase; c. pouring the water phase into the oil phase at 85 ℃, stirring for 15 minutes after adding the water phase to form uniform emulsion, cooling to room temperature, adding 10ml of lily extract, 10ml of prunus mume extract, 15ml of coconut juice, 10ml of waxgourd seed extract, 10ml of corn stigma extract, 2ml of essence, 25g of sodium alginate solution, 2g of sorbic acid and 30g of carbomer 941 solution, and uniformly stirring to obtain finished emulsion; d. putting the prepared emulsion into a filling machine, and filling the emulsion; the lily extracting solution is prepared by the following method: weighing a proper amount of lily, placing the lily into a treatment barrel, heating to 100 ℃, decocting and extracting for 3 times, adding 15 times of water for the first time to extract for 1.5 hours, adding 12 times of water for the second time to extract for 1.5 hours, adding 10 times of water for the third time to extract for 1.5 hours, filtering with three layers of gauze each time, combining filtrates, heating and concentrating by ml/g to 6 times of the weight of the lily, and filtering with three layers of gauze to obtain the lily tea beverage; the red plum extract is prepared by the following method: weighing a certain amount of red chocolate, heating to 100 ℃, decocting and extracting for 3 times, adding 50 times of water for the first time, extracting for 1.5h, adding 40 times of water for the second time, extracting for 1.5h, adding 30 times of water for the third time, extracting for 1.5h, filtering with three layers of gauze each time, combining filtrates, heating and concentrating to 3-6 times of the weight of the red chocolate in terms of ml/g, and filtering with three layers of gauze to obtain the product; weighing semen Benincasae, heating to 100 deg.C, decocting for 3 times, extracting with 15 times of water for 1.5 hr, 12 times of water for 1.5 hr, 10 times of water for 1.5 hr, filtering with three layers of gauze, mixing filtrates, heating and concentrating to 6 times of semen Benincasae weight in ml/g, and filtering with three layers of gauze; the corn stigma extracting solution is prepared by the following method: weighing a certain amount of corn stigma, heating to 100 ℃, decocting and extracting for 3 times, extracting for 1.5h with 15 times of water for the first time, extracting for 1.5h with 10 times of water for the second time, extracting for 1.5h with 10 times of water for the third time, filtering with three layers of gauze each time, combining filtrates, heating and concentrating to 6 times of the weight of the corn stigma in ml/g, and filtering with three layers of gauze to obtain the corn stigma extract; the essence is cucumber essence; the essence is juicy peach essence; the preparation method of the seaweed mud solution comprises the following steps: weighing 5-15g of sodium alginate, adding 100 ml of distilled water, standing and stirring to fully swell the sodium alginate into uniform transparent liquid; the preparation method of the carbomer solution comprises the following steps: weighing 9412-15g of carbomer, adding 1000ml of distilled water and 100-; the structure of the filling machine is the same as that of the filling machine in embodiment 1.

Claims (7)

1. A method for producing an emulsion, comprising: the method comprises the following steps:
a. weighing jojoba oil 0.5-4.0g, olive oil 0.5-4.0g, glyceryl monostearate 2.0-10g, span 800.3-3g, and vitamin E0.1-3.0g, heating to 70-85 deg.C, completely melting, stirring, and mixing to obtain oil phase;
b. weighing 1-10g of poloxamer, 2.0-20g of glycerol, 0.6-5g of propylene glycol, 14.0-50.0g of distilled water, 0.3-3g of honey, 0.1-4.0g of urea, 0.3-3ml of 1% sodium hyaluronate, 0.1-0.5mg of disodium ethylenediamine tetraacetate and 0.02-1.0g of L-serine, heating to 70-85 ℃, completely melting the materials, and uniformly stirring to obtain a water phase;
c. pouring the water phase into the oil phase at 70-85 ℃, stirring for 5-15 minutes after adding to form uniform emulsion, cooling to room temperature, adding 1-10ml of lily extract, 1-10ml of prunus mume extract, 2-15ml of coconut juice, 1-10ml of waxgourd seed extract, 1-10ml of corn stigma extract, 0.05-2ml of essence, 6-25g of sodium alginate solution, 0.1-2g of sorbic acid and 10-30g of carbomer 941 solution, and uniformly stirring to obtain the nourishing and moisturizing emulsion;
d. putting the prepared emulsion into a filling machine, and filling the emulsion;
the filling machine in the step d comprises a storage barrel (1), a first cover plate (2) arranged at the top of the storage barrel (1) and a discharge pipe (11) arranged at the bottom of the storage barrel (1), wherein the discharge pipe (11) is communicated with a discharge hole of the storage barrel (1), a stirring device is arranged in the storage barrel (1), the bottom of the storage barrel (1) is of a conical structure, a third connecting rod (121) is arranged on the inner wall of the storage barrel (1), a first mounting plate (12) is arranged on the third connecting rod (121), a driving motor (13) is arranged on the first mounting plate (12), the stirring device comprises a stirring shaft (3) arranged on an output shaft of the driving motor (13) and stirring blades (31) arranged on the stirring shaft (3), a first movable cavity is arranged on the stirring blades (31), and a scraping plate (32) is arranged in the first movable cavity, a first push rod (21) for driving the scraper (32) to move along the inner wall of the first movable cavity is arranged on the first cover plate (2); after the emulsion is prepared, pouring the emulsion into a storage barrel (1), placing an emulsion bottle below a discharge pipe (11), and injecting the emulsion into the emulsion bottle through the discharge pipe (11); the driving motor (13) drives the stirring blade (31) to rotate, and the stirring blade (31) stirs the emulsion to enable the emulsion to be in a motion state so as to discharge the emulsion from the discharge pipe (11).
2. A process for the production of an emulsion according to claim 1, characterized in that: the preparation method of the seaweed mud solution comprises the following steps: weighing 5-15g of sodium alginate, adding 100 ml of distilled water, standing and stirring to fully swell the sodium alginate into uniform and transparent liquid.
3. A process for the production of an emulsion according to claim 1, characterized in that: the preparation method of the carbomer solution comprises the following steps: weighing 9412-15g of carbomer, adding 1000ml of distilled water, standing and stirring to fully swell the carbomer into uniform transparent liquid.
4. A process for the production of an emulsion according to claim 1, characterized in that: the essence is one of juicy peach essence, cucumber essence, rose essence, sweet osmanthus essence and pineapple essence.
5. A process for the production of an emulsion according to claim 1, characterized in that: the lily extracting solution is prepared by the following method: weighing an appropriate amount of lily, heating to 90-100 ℃, decocting and extracting for 3 times, adding 8-15 times of water for the first time, extracting for 0.5-1.5h, adding 6-12 times of water for the second time, extracting for 0.5-1.5h, adding 4-10 times of water for the third time, extracting for 0.5-1.5h, filtering with three layers of gauze each time, combining filtrates, heating and concentrating to 3-6 times of the weight of lily in terms of ml/g, and filtering with three layers of gauze.
6. A process for the production of an emulsion according to claim 1, characterized in that: a first movable groove is formed in the bottom of the first movable cavity, a first connecting plate is arranged at the bottom of the scraping plate (32) and penetrates through the first movable groove, a bearing plate is arranged at the bottom of the first connecting plate, a first material receiving box (34) is arranged at the bottom of the stirring blade (31), and a first inclined groove matched with the first material receiving box (34) is formed in the bearing plate; the stirring blade (31) is provided with a mounting rack (311), the first material receiving box (34) is arranged on the mounting rack (311), the first material receiving box (34) is provided with a second cover plate (341), the second cover plate (341) is detachably connected to the receiving plate, the top of the second cover plate (341) is provided with a second chute matched with the first chute, and the first material receiving box (34) is provided with a first chute matched with the second cover plate (341); when the storage barrel (1) is cleaned, the first push rod (21) is pressed down to enable the scraper (32) to extend out of the first movable cavity, the scraper (32) drives the second cover plate (341) to move, the second cover plate (341) is moved away from the top of the first material receiving box (34) to enable the first material receiving box (34) to be in an open state, the driving motor (13) drives the stirring shaft (3) to rotate, the scraper (32) is in contact with the inner wall of the storage barrel (1) to scrape emulsion on the inner wall of the storage barrel (1), the scraped emulsion flows to the receiving plate along the side wall of the scraper (32), the emulsion flows downwards along the first chute and the second chute to enable the emulsion to flow into the first material receiving box (34), and the emulsion on the inner wall of the storage barrel (1) is collected in the first material receiving box (34).
7. A process for the production of an emulsion according to claim 1, characterized in that: a sealing block (113) is arranged in the discharge pipe (11), a linear opening is formed in the sealing block (113), a second movable cavity matched with the sealing block (113) is formed in the inner wall of the discharge pipe (11), and a first opening is formed in the side wall of the second movable cavity; a second mounting plate (111) is arranged on the side wall of the discharge pipe (11), an air cylinder (4) is arranged on the second mounting plate (111), a piston rod of the air cylinder (4) penetrates through the first opening, a first connecting rod and a second connecting rod (114) are arranged in the second movable cavity, the first connecting rod and the second connecting rod (114) are respectively divided into two groups, the first connecting rod is hinged to the inner wall of the second movable cavity, one end of the second connecting rod (114) is hinged to the first connecting rod, the other end of the second connecting rod (114) is hinged to a third connecting rod (45), the two groups of the first connecting rod and the two groups of the second connecting rod (114) are mutually matched to form a diamond structure, and the third connecting rod (45) is arranged on the piston rod of the air cylinder (4); after the emulsion bottle removed discharging pipe (11) below, cylinder (4) promoted the piston rod and moved forward, make the piston rod promote third connecting rod (45) and remove, head rod and second connecting rod (114) rotate around the tie point, make second connecting rod (114) move toward second activity chamber middle part, second connecting rod (114) extrusion sealing piece (113) make sealing piece (114) take place deformation, a style of calligraphy opening is opened after sealing piece (114) deformation, make the emulsion discharge in discharging pipe (11), pour into the emulsion bottle with the emulsion in.
CN201910973875.2A 2019-10-14 2019-10-14 Emulsion production method Withdrawn CN110652459A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111530899A (en) * 2020-05-29 2020-08-14 桂林益克垃环保科技有限公司 Integrated domestic garbage multifunctional treatment equipment
CN114516571A (en) * 2021-12-29 2022-05-20 南通文凯化纤有限公司 Transmission device with automatic moisturizing function for polyester stretch yarn

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111530899A (en) * 2020-05-29 2020-08-14 桂林益克垃环保科技有限公司 Integrated domestic garbage multifunctional treatment equipment
CN114516571A (en) * 2021-12-29 2022-05-20 南通文凯化纤有限公司 Transmission device with automatic moisturizing function for polyester stretch yarn

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Application publication date: 20200107