CN110632335A - Full-automatic system for batch determination of pH value - Google Patents
Full-automatic system for batch determination of pH value Download PDFInfo
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- CN110632335A CN110632335A CN201910967990.9A CN201910967990A CN110632335A CN 110632335 A CN110632335 A CN 110632335A CN 201910967990 A CN201910967990 A CN 201910967990A CN 110632335 A CN110632335 A CN 110632335A
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N35/00—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
- G01N35/02—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor using a plurality of sample containers moved by a conveyor system past one or more treatment or analysis stations
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N35/00—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
- G01N35/02—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor using a plurality of sample containers moved by a conveyor system past one or more treatment or analysis stations
- G01N35/04—Details of the conveyor system
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N35/00—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
- G01N35/02—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor using a plurality of sample containers moved by a conveyor system past one or more treatment or analysis stations
- G01N35/04—Details of the conveyor system
- G01N2035/0401—Sample carriers, cuvettes or reaction vessels
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Automatic Analysis And Handling Materials Therefor (AREA)
Abstract
The invention discloses a full-automatic system for batch measurement of pH values, which comprises a sample tray, a calibration cup, a cleaning tank, an electrode protection tank, a sample tank, a mechanical arm, an automatic liquid adding and stirring device and an electrode probe. The invention has the advantages that the full-automatic completion of liquid adding, stirring, measuring and data output is realized by placing the weighed sample on the sample tray, and meanwhile, the time of workers is effectively saved, the cost is reduced and the working efficiency is improved by adopting the low-price disposable sample cup.
Description
Technical Field
The invention belongs to the technical field of PH measurement, and relates to a full-automatic system for measuring pH values in batches.
Background
At present, the step of measuring the pH in an analytical chemistry laboratory is to weigh a sample, place the sample in a sample cup, manually add the leaching liquor, manually stir or vibrate for 1-5min at 180r/min by an oscillator, stand for 5-120min, and then measure by a pH meter, but all the steps are manual single measurement, and after the measurement is completed, a sample box needs to be cleaned, which wastes time and labor, and particularly when the samples are measured in batches, the time of workers cannot be effectively saved, and the work efficiency is reduced. And the process of manually sampling and then carrying out chemical analysis and measurement of the pH value in a laboratory is complicated, the measurement period is long, the change of the pH value in the water body cannot be accurately and timely found, and errors can also occur when the number of measurement points is increased.
Disclosure of Invention
The invention aims to provide a full-automatic system for batch measurement of pH value, which has the advantages that the full-automatic completion of liquid adding, stirring, measurement and data output is realized by placing a weighed sample on a sample tray, and meanwhile, the time of workers is effectively saved, the cost is reduced and the working efficiency is improved by adopting a low-price disposable sample cup.
The technical scheme adopted by the invention is carried out according to the following steps:
1) the device comprises a sample tray, a calibration cup, a cleaning tank, an electrode protection tank and a sample tank, wherein the cleaning tank is provided with a washing inlet and a diversion outlet and is provided with a waste liquid cylinder; the size of the sample disk is 40 × 60cm, and each position is provided with a fixed number; the sample cup is 50ml in size and is a disposable polypropylene plastic cup;
2. the arrangement of the mechanical arm: the sample tray is connected with the sample tray, and a transmission line is arranged in the sample tray, so that the moving distance, the descending distance and the moving position of the mechanical arm can be controlled; the hole site and the clamping groove are arranged, and the electrode, the liquid adding device and the stirring device can be placed and fixed;
3. automatic liquid feeding, agitating unit and electrode probe's setting: the liquid adding and stirring device is a hollow metal tube with the length of 10cm, the external diameter of 0.2cm, the hollow diameter of 0.15cm, the bottom end is connected with a stirring sheet, the stirring sheet is in a compass shape, the length of 1cm and the width of 0.2cm, the liquid adding amount can be controlled to be 1-50ml, the stirring time can be controlled to be 1-60min, the rotating speed of a rotor can be controlled to be 1-300r/min, the descending height can be controlled, and the device is externally connected with a data line and a liquid adding tube; the descending height of the test electrode, the test time can be controlled, and the data wire is arranged to transmit the data to the output terminal; the liquid adding stirring device and the electrode device can respectively descend, and act in a row at the same time.
4. The control system comprises a control unit, a plurality of PH measuring circuits and an analog-to-digital conversion unit, wherein the control unit is respectively connected with the PH measuring circuits through the analog-to-digital conversion unit, and each PH measuring circuit is respectively connected with a PH measuring terminal and a temperature measuring terminal. The control unit sends out signals, and the PH measuring terminal and the temperature measuring terminal upload measured analog values to the terminal after being converted by the analog-to-digital conversion unit, so that the measuring results can be observed in real time.
Further, the sample well 6 × 10 is 60 holes.
Furthermore, the size of the sample cup is 3.5cm at the lower aperture, 5cm at the upper aperture and 5cm at the height.
Detailed Description
The present invention will be described in detail with reference to the following embodiments.
The invention relates to a full-automatic system for batch measurement of pH values, which comprises:
1. the device comprises a sample tray, a calibration cup, a cleaning tank, an electrode protection tank and a sample tank with a hole position of 6 x 10 ═ 60, wherein the cleaning tank is provided with a washing inlet and a diversion outlet and is provided with a waste liquid cylinder; the size of the sample plate is 40 x 60cm, and each position has a fixed number, such as calibration 1 to calibration 6, and sample 1 to sample 60; the sample cup is 50ml (the size is 3.5cm of lower aperture, 5cm of upper aperture and 5cm of height), and is a disposable polypropylene plastic cup (the cost is lower, and the cost is about 30 yuan for 1000 cups);
2. the arrangement of the mechanical arm: the sample tray is connected with the sample tray, and a transmission line is arranged in the sample tray, so that the moving distance, the descending distance and the moving position of the mechanical arm can be controlled; the hole site and the clamping groove are arranged, and the electrode, the liquid adding device and the stirring device can be placed and fixed;
3. automatic liquid feeding, agitating unit and electrode probe's setting: the liquid adding and stirring device is a hollow metal tube with the length of 10cm, the external diameter of 0.2cm, the hollow diameter of 0.15cm, the bottom end is connected with a stirring sheet, the stirring sheet is in a compass shape, the length of 1cm and the width of 0.2cm, the liquid adding amount can be controlled to be 1-50ml, the stirring time can be controlled to be 1-60min, the rotating speed of a rotor can be controlled to be 1-300r/min, the descending height can be controlled, and the device is externally connected with a data line and a liquid adding tube; the descending height of the test electrode, the test time can be controlled, and the data wire is arranged to transmit the data to the output terminal; the liquid adding stirring device and the electrode device can respectively descend, and only one row of the liquid adding stirring device and the electrode device act simultaneously.
4. The control system comprises a control unit, a plurality of PH measuring circuits and an analog-to-digital conversion unit, wherein the control unit is respectively connected with the PH measuring circuits through the analog-to-digital conversion unit, and each PH measuring circuit is respectively connected with a PH measuring terminal and a temperature measuring terminal. The control unit sends out signals, and the PH measuring terminal and the temperature measuring terminal upload measured analog values to the terminal after being converted by the analog-to-digital conversion unit, so that the measuring results can be observed in real time.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not intended to limit the present invention in any way, and all simple modifications, equivalent variations and modifications made to the above embodiments according to the technical spirit of the present invention are within the scope of the present invention.
Claims (3)
1. A full-automatic system for batch measurement of pH value is characterized by comprising the following steps:
1) the device comprises a sample tray, a calibration cup, a cleaning tank, an electrode protection tank and a sample tank, wherein the cleaning tank is provided with a washing inlet and a diversion outlet and is provided with a waste liquid cylinder; the size of the sample disk is 40 × 60cm, and each position is provided with a fixed number; the sample cup is 50ml in size and is a disposable polypropylene plastic cup;
2) the arrangement of the mechanical arm: the sample tray is connected with the sample tray, and a transmission line is arranged in the sample tray, so that the moving distance, the descending distance and the moving position of the mechanical arm can be controlled; the hole site and the clamping groove are arranged, and the electrode, the liquid adding device and the stirring device can be placed and fixed;
3) automatic liquid feeding, agitating unit and electrode probe's setting: the liquid adding and stirring device is a hollow metal tube with the length of 10cm, the external diameter of 0.2cm, the hollow diameter of 0.15cm, the bottom end is connected with a stirring sheet, the stirring sheet is in a compass shape, the length of 1cm and the width of 0.2cm, the liquid adding amount can be controlled to be 1-50ml, the stirring time can be controlled to be 1-60min, the rotating speed of a rotor can be controlled to be 1-300r/min, the descending height can be controlled, and the device is externally connected with a data line and a liquid adding tube; the descending height of the test electrode, the test time can be controlled, and the data wire is arranged to transmit the data to the output terminal; the liquid adding stirring device and the electrode device can respectively descend, and a row of liquid adding stirring devices and the electrode device act simultaneously;
4) the control system comprises a control unit, a plurality of PH measuring circuits and an analog-to-digital conversion unit, wherein the control unit is respectively connected with the plurality of PH measuring circuits through the analog-to-digital conversion unit, and each PH measuring circuit is respectively connected with a PH measuring terminal and a temperature measuring terminal; the control unit sends out signals, and the PH measuring terminal and the temperature measuring terminal upload measured analog values to the terminal after being converted by the analog-to-digital conversion unit, so that the measuring results can be observed in real time.
2. A fully automated system for batch pH determination according to claim 1, wherein: the sample well 6 x 10 is 60 holes.
3. A fully automated system for batch pH determination according to claim 1, wherein: the sizes of the sample cup are 3.5cm of lower caliber, 5cm of upper caliber and 5cm of height.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910967990.9A CN110632335A (en) | 2019-10-12 | 2019-10-12 | Full-automatic system for batch determination of pH value |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910967990.9A CN110632335A (en) | 2019-10-12 | 2019-10-12 | Full-automatic system for batch determination of pH value |
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| CN110632335A true CN110632335A (en) | 2019-12-31 |
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| CN201910967990.9A Pending CN110632335A (en) | 2019-10-12 | 2019-10-12 | Full-automatic system for batch determination of pH value |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113933368A (en) * | 2021-09-30 | 2022-01-14 | 深圳市中金岭南有色金属股份有限公司凡口铅锌矿 | Ore pulp pH value detection system |
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| CN202453323U (en) * | 2012-02-24 | 2012-09-26 | 深圳市特种设备安全检验研究院 | Device for continuously analyzing pH (potential of hydrogen) value, phenolphthalein alkalinity, total alkalinity and chlorine ion concentration |
| CN206027745U (en) * | 2016-07-19 | 2017-03-22 | 周学军 | Sample preparation test tube is used in oncology laboratory |
| CN206601362U (en) * | 2017-03-28 | 2017-10-31 | 中国纺织信息中心 | A kind of mechanical arm sample introduction equipment determined for pH value of fabrics |
| CN108362546A (en) * | 2018-04-27 | 2018-08-03 | 上海厦泰生物科技有限公司 | A kind of full-automatic stirring sampling device with collision prevention function |
| CN208026671U (en) * | 2018-01-05 | 2018-10-30 | 中国科学院、水利部成都山地灾害与环境研究所 | Automate Soil K+adsorption instrument |
| CN109856220A (en) * | 2019-03-07 | 2019-06-07 | 中南大学 | A kind of pH value on-line measuring device and its control and calibration pre-judging method |
| CN208984486U (en) * | 2018-08-30 | 2019-06-14 | 吉林省农业科学院 | Sample container |
| CN109900746A (en) * | 2019-03-27 | 2019-06-18 | 深圳呼客仪器有限公司 | A kind of full-automatic P in soil H analyzer and method |
| CN109916962A (en) * | 2019-04-16 | 2019-06-21 | 吉林大学 | A kind of Portable meat moisture content detection device and its detection method |
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2019
- 2019-10-12 CN CN201910967990.9A patent/CN110632335A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202453323U (en) * | 2012-02-24 | 2012-09-26 | 深圳市特种设备安全检验研究院 | Device for continuously analyzing pH (potential of hydrogen) value, phenolphthalein alkalinity, total alkalinity and chlorine ion concentration |
| CN206027745U (en) * | 2016-07-19 | 2017-03-22 | 周学军 | Sample preparation test tube is used in oncology laboratory |
| CN206601362U (en) * | 2017-03-28 | 2017-10-31 | 中国纺织信息中心 | A kind of mechanical arm sample introduction equipment determined for pH value of fabrics |
| CN208026671U (en) * | 2018-01-05 | 2018-10-30 | 中国科学院、水利部成都山地灾害与环境研究所 | Automate Soil K+adsorption instrument |
| CN108362546A (en) * | 2018-04-27 | 2018-08-03 | 上海厦泰生物科技有限公司 | A kind of full-automatic stirring sampling device with collision prevention function |
| CN208984486U (en) * | 2018-08-30 | 2019-06-14 | 吉林省农业科学院 | Sample container |
| CN109856220A (en) * | 2019-03-07 | 2019-06-07 | 中南大学 | A kind of pH value on-line measuring device and its control and calibration pre-judging method |
| CN109900746A (en) * | 2019-03-27 | 2019-06-18 | 深圳呼客仪器有限公司 | A kind of full-automatic P in soil H analyzer and method |
| CN109916962A (en) * | 2019-04-16 | 2019-06-21 | 吉林大学 | A kind of Portable meat moisture content detection device and its detection method |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113933368A (en) * | 2021-09-30 | 2022-01-14 | 深圳市中金岭南有色金属股份有限公司凡口铅锌矿 | Ore pulp pH value detection system |
| CN113933368B (en) * | 2021-09-30 | 2023-12-26 | 深圳市中金岭南有色金属股份有限公司凡口铅锌矿 | Pulp pH value detecting system |
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