CN1106292A - Method for prodn. of Rhodiola kirilowii dry powder - Google Patents
Method for prodn. of Rhodiola kirilowii dry powder Download PDFInfo
- Publication number
- CN1106292A CN1106292A CN 94111884 CN94111884A CN1106292A CN 1106292 A CN1106292 A CN 1106292A CN 94111884 CN94111884 CN 94111884 CN 94111884 A CN94111884 A CN 94111884A CN 1106292 A CN1106292 A CN 1106292A
- Authority
- CN
- China
- Prior art keywords
- dry powder
- regel
- maxim
- production method
- rhodiola kirilowii
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The method for producing dry powder of narrow-leaf rhodiola root, which may be directly used in pharmaceutical industry and health-care food production includes preparation of raw material, reflux extraction, concentrating supernatant, drying and pulverization, and features high output, short processing period, extraction of full active components, and less equipment.
Description
What the present invention relates to is the production method of a kind of narrow leaf (big strain) Radix Rhodiolae dry powder.
Radix Rhodiolae is the extremely strong plant of a kind of vitality between the rock that is grown under plateau snow mountain height above sea level severe cold more than 3500～4000 meters, anoxia, the changeable harsh weather, contain multiple special efficacy components such as rhodioloside, butyl alcohol, lactone in the Radix Rhodiolae, not only have the nourishing excitation of Radix Ginseng but also can suppress to be overexcited, and have the tranquil function of Radix Et Caulis Acanthopanacis Senticosi concurrently, have special dual regulation; Anti-hypoxia, defying age, antifatigue effect are particularly evident.The kind of Radix Rhodiolae has tens kinds, and the tool commercial development of Rhodiola kirilowii (Regel) Maxim. is worth after deliberation, and its effective component content height (containing rhodioloside composition height) is convenient to gather, volume of production is big.The method of active ingredient is that raw material is directly soaked extraction in the Radix Rhodiolae and extract traditionally at present, time is long, active ingredient is extracted not exclusively, extracting solution, extractum can't be preserved, because of the collection of raw material only has 3～4 months the whole year, untimely processing raw material just can be gone bad, and active ingredient is lost, so traditional production method is not suitable for large-scale industrial production.
In view of above reason, the objective of the invention is in order to provide a kind of volume of production big, the time is short, and extract is easy to long preservation, extracts the production method that active ingredient can be carried out the Rhodiola kirilowii (Regel) Maxim. dry powder of large-scale industrial production completely.
Production method of the present invention is as follows:
1), get the raw materials ready: gather the Rhodiola kirilowii (Regel) Maxim. raw material 9～November annual 3～May, clean, section is equipped with edible ethanol in addition;
2), blanking: the solvent that places edible ethanol and water to make the Radix Rhodiolae raw material section of getting ready soaks;
3), reflux, extract;
4), supernatant concentration;
5), dry, powder process;
6), packing, warehouse-in.
The above-mentioned Rhodiola kirilowii (Regel) Maxim. raw material and the ratio of solvent are 1: 5, and the percentage by weight of edible ethanol and water is in the solvent: (0～95): (100～5).
Adopt dual factors to regulate extraction method in the above-mentioned reflux, extract, operation: promptly thermoregulation is from 60 ℃～boiling; Raw material and solvent are dropped in the backflow multi-functional extractor in proportion, and heating was at least 1 hour to container, when temperature rises to boiling, and constant temperature at least four hours, cooling goes out first liquid naturally; This method adopts three times, and the liquid material is filtered or get supernatant and three liquid mixing for standby use, remains a small amount of active ingredient as only adopting extracted twice, just can propose effective ingredient fully three times, temperature is not higher than 100 ℃ in the constant temperature time, helps protecting active ingredient.
Adopting the mode concentrated supernatant of reduction vaporization in the above-mentioned supernatant concentration operation is fluid extract.
Adopting thin film concentration in the above-mentioned supernatant concentration operation, is 1.1～1.25 fluid extract to proportion with supernatant concentration.
In the above-mentioned dry powder process operation, can adopt the exsiccant mode of baking, promptly adopt 60～70 ℃ of dryings of steady temperature, drying time was at least 24 hours for the first time, take out dry by the fire again more after treatment to water content less than 6%, the baking time was at least 14 hours again, beat powder and sieved.
In the above-mentioned dry powder process operation, can adopt spray-dired mode, being about to fluid extract, to adjust proportion be 1.08～1.12 to be used for carrying out spray drying again after the concentration of spray dryer, and inlet temperature is 120～180 ℃, outlet temperature is 50～90 ℃, and water content is less than 6%.
When above-mentioned dry powder process operation, the fluid extract with after concentrating places the pallet of lining cloth and the thickness of fluid extract must not surpass 0.5cm, toasting for the first time when not dried fully, lining cloth is separated with dried cream, remakes baking, can not take out as after dried fully.
Adopt the present invention to be used for the production of Rhodiola kirilowii (Regel) Maxim. dry powder, volume of production is big, and process time is short, and extract is easy to long preservation, and it is complete to propose active ingredient.Production method is simple, and equipment needed thereby is few, can be used for large-scale industrial production.The Radix Rhodiolae dry powder that adopts the method to produce can be directly used in medicine and the health care food production.As long as carry out suitable mixed processing, just can produce as health beverage, food such as " rhodiola root wine ", " Radix Rhodiolae cookiess ", good health care effect, cost is low.
Introduce embodiments of the invention below in detail:
The method that present embodiment is taked is as follows:
1), get the raw materials ready: select for use do not have corruption, the Rhodiola kirilowii (Regel) Maxim. raw material of free from admixture, no branch and leaf (must annual 3～May, gather 9～November), the rhizome diameter must not cut into slices, dry less than 2cm, in addition edible ethanol fully;
2), blanking: by the percentage by weight (0～95) of edible ethanol and water: (100～5) preparation solvent is in the backflow multi-functional extractor, and the weight ratio 1: 5 of pressing raw material and solvent is with in the raw material input backflow multi-functional extractor;
3), reflux, extract: to container heating (not direct heating), temperature rises to default definite value (design temperature must not be higher than 100 ℃ in one hour, but be not less than 80 ℃) time constant temperature 4 hours, naturally cooling then, go out first liquid, this kind method adopts three times, and the liquid material is filtered or get supernatant and three liquid mixing use;
4), concentrating of extracting solution: can adopt two kinds of methods:
A/. reduction vaporization
B/. thin film concentration: it is 1.1～1.25 fluid extract that extracting solution is concentrated into proportion;
No matter be that reduction vaporization equipment or thin film concentration equipment are known equipment.
5), the drying of extractum, can adopt following two kinds of methods:
A/. baking is dry: adopt 60～70 ℃ of steady temperatures, drying time is 24 hours for the first time, take out dry again more after treatment to water content less than 6%, multiple drying time was at least 14 hours, beat powder sieve (80 order).
B/. fluid extract is adjusted proportion and be 1.08～1.12 and carry out spray drying after being applicable to the concentration of spray dryer, inlet temperature is 120～180 ℃, and outlet temperature is 50～90 ℃, and water content is beaten powder and sieved less than 6%.
During baking, spissated fluid extract should be placed the pallet that contains lining cloth and the thickness of fluid extract to be no more than 0.5cm, when baking is dried fully for the first time, take out, lining cloth is separated with dried cream, remake baking.
6), the dry powder of preparation weighed immediately to be loaded in the aseptic thin-film bag and sealing, reinstalls in the moistureproof hard outer package.The dry powder weighing and bagging should be finished in half an hour.
Sanitary index to Radix Rhodiolae dry powder should be by medicine requirement check, and the content of rhodioloside (C14H20H7) must not be less than 1%.
Claims (8)
1, the production method of Rhodiola kirilowii (Regel) Maxim. dry powder is characterized in that described production method is as follows:
1), get the raw materials ready: gather the Rhodiola kirilowii (Regel) Maxim. raw material 9～November annual 3～May, clean, section is equipped with edible ethanol in addition;
2), blanking: the solvent that places edible ethanol and water to make the Radix Rhodiolae raw material section of getting ready soaks;
3), reflux, extract;
4), supernatant concentration;
5), dry, powder process;
6), packing, warehouse-in.
2, the production method of Rhodiola kirilowii (Regel) Maxim. dry powder as claimed in claim 1 is characterized in that the ratio of described Rhodiola kirilowii (Regel) Maxim. raw material and solvent is 1: 5, and the percentage by weight of edible ethanol and water is in the solvent: (0～95): (100～5).
3, the production method of Rhodiola kirilowii (Regel) Maxim. dry powder as claimed in claim 1, it is characterized in that adopting in the reflux, extract, operation dual factors to regulate extraction method: promptly thermoregulation is from 60 ℃～boiling; Raw material and solvent are dropped in the backflow multi-functional extractor in proportion, and heating was at least 1 hour to container, and constant temperature was at least four hours when temperature rose to boiling, naturally cooling, go out first liquid, this method adopts three times, and the liquid material is filtered or get supernatant and three liquid mixing for standby use.
4, the production method of Rhodiola kirilowii (Regel) Maxim. dry powder as claimed in claim 1 is characterized in that adopting the mode concentrated supernatant of reduction vaporization in the supernatant concentration operation is fluid extract.
5, the production method of Rhodiola kirilowii (Regel) Maxim. dry powder as claimed in claim 1 is characterized in that adopting thin film concentration in the supernatant concentration operation, is 1.1～1.25 fluid extract to proportion with supernatant concentration.
6, the production method of Rhodiola kirilowii (Regel) Maxim. dry powder as claimed in claim 1, when it is characterized in that dry powder process operation, can adopt the exsiccant mode of baking, promptly adopt 60～70 ℃ of dryings of steady temperature, drying time was at least 24 hours for the first time, take out dry by the fire again more after treatment to water content less than 6%, be at least when drying by the fire again 14 hours, beat powder and sieve.
7, the production method of Rhodiola kirilowii (Regel) Maxim. dry powder as claimed in claim 1, when it is characterized in that dry powder process operation, can adopt spray-dired mode, being about to fluid extract, to adjust proportion be 1.08～1.12 to carry out spray drying after being applicable to the concentration of spray dryer, inlet temperature is 120～180 ℃, outlet temperature is 50～90 ℃, and water content is less than 6%.
8, as the production method of claim 6 or 7 described Rhodiola kirilowii (Regel) Maxim. dry powder, when it is characterized in that described dry powder process operation, with the fluid extract after concentrating, place the pallet of lining cloth and the thickness of fluid extract must not surpass 0.5cm, when the first time, baking was not dried fully, lining cloth is separated with dried cream, remake baking.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 94111884 CN1106292A (en) | 1994-08-31 | 1994-08-31 | Method for prodn. of Rhodiola kirilowii dry powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 94111884 CN1106292A (en) | 1994-08-31 | 1994-08-31 | Method for prodn. of Rhodiola kirilowii dry powder |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1106292A true CN1106292A (en) | 1995-08-09 |
Family
ID=5035713
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 94111884 Pending CN1106292A (en) | 1994-08-31 | 1994-08-31 | Method for prodn. of Rhodiola kirilowii dry powder |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1106292A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100998409A (en) * | 2006-12-26 | 2007-07-18 | 沈阳药科大学 | Raw material for making health-care food with functions of tonifying, refreshing and lowering user's weight and its product |
-
1994
- 1994-08-31 CN CN 94111884 patent/CN1106292A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100998409A (en) * | 2006-12-26 | 2007-07-18 | 沈阳药科大学 | Raw material for making health-care food with functions of tonifying, refreshing and lowering user's weight and its product |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN100345952C (en) | Lavender essence oil extracting method | |
| Shehata et al. | Effects of bioactive component of kiwi fruit and avocado (fruit and seed) on hypercholesterolemic rats. | |
| CN111407678B (en) | Microemulsion with moisturizing, skin-brightening and anti-aging effects and preparation method thereof | |
| CN107362084A (en) | A kind of facial mask containing Chinese sumac leaf extract and preparation method thereof | |
| CN104450396B (en) | A kind of preparation method of sticky rice wine | |
| CN108157968A (en) | A kind of compound electuary of blueberry for adjusting and improving human endocrine system and preparation method thereof | |
| CN104666226B (en) | A kind of floral water containing pummelo peel extract and preparation method thereof | |
| CN102329715A (en) | Compound Rhodiola rosea wine and preparation method thereof | |
| CN105733809A (en) | Method and equipment for producing jasmine hydrolat through low temperature distillation | |
| CN101129441A (en) | Rhodiola rosea capsule and its preparing method | |
| CN1560046A (en) | Process for extracting water grind thisvine using alcohole as single organic dissolvent | |
| CN1106292A (en) | Method for prodn. of Rhodiola kirilowii dry powder | |
| Bagheri et al. | Creating incremental revenue from industrial cherry wastes | |
| Ousaaid et al. | New insights into Phytochemical Content and antioxidant activities of Moroccan Fruit vinegars | |
| CN1075710C (en) | Beehive tea and its preparation method | |
| CN107260977A (en) | A kind of brain tonic and intelligence development oral liquid and its preparation technology | |
| RU2710261C1 (en) | Method for complex treatment fresh fruits of hawthorn | |
| CN113881503A (en) | Artemisia annua essential oil and white tea essential oil with anti-inflammatory effect, and their composition | |
| CN106666004A (en) | Wild vine tea extract health-care beverage | |
| Patel et al. | A Review on Different Extraction Method of Plants: Innovation from Ancient to Modern Technology | |
| Bhuyar et al. | Maejo International Journal of Energy and Environmental Communication | |
| Singh | Maceration, Percolation and Infusion Techniques of Extraction of Medicinal and Aromatic Plants (MAPs) | |
| CN115364019B (en) | Millettia speciosa-dendrobe-noni composite enzyme, preparation method thereof and application thereof as sun-screening agent | |
| CN1219734C (en) | Method for preparing compound phenolhydrocarbon sodium | |
| BR102019026639A2 (en) | BIOACTIVE EXTRACTS FROM FERMENTED GRANADILLA SEED FLOUR (PASSIFLORA LIGULARIS) |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C06 | Publication | ||
| PB01 | Publication | ||
| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |