CN110606985A - Preparation process of child safety light clay with antibacterial function - Google Patents
Preparation process of child safety light clay with antibacterial function Download PDFInfo
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- CN110606985A CN110606985A CN201910777637.4A CN201910777637A CN110606985A CN 110606985 A CN110606985 A CN 110606985A CN 201910777637 A CN201910777637 A CN 201910777637A CN 110606985 A CN110606985 A CN 110606985A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/36—Sulfur-, selenium-, or tellurium-containing compounds
- C08K5/45—Heterocyclic compounds having sulfur in the ring
- C08K5/46—Heterocyclic compounds having sulfur in the ring with oxygen or nitrogen in the ring
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L101/00—Compositions of unspecified macromolecular compounds
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Abstract
The invention provides a preparation process of child safety light clay with an antibacterial function, and relates to the technical field of light clay preparation. The preparation process of the child safety light clay with the antibacterial function comprises the steps of firstly putting water into a container, adding activated carbon into the water, stirring the water, then filtering the water, stirring the filtered water, adding glue, rubber powder and isothiazolinone while stirring to obtain a first product, heating and stirring the first product, adding glutaraldehyde and glycerol to obtain a second product, heating and stirring the second product, and simultaneously adding incense powder and pigment to obtain a third product. According to the preparation process of the child safety light clay with the antibacterial function, ampicillin and an anti-repellent agent are used for replacing Brobopol, so that the light clay is safer, stimulation to skin, eyes and mucous membranes of children is avoided, the phenomenon of allergy is avoided, and the produced light clay is safer.
Description
Technical Field
The invention relates to the technical field of light clay preparation, in particular to a preparation process of child safety light clay with an antibacterial function.
Background
The light clay is one of paper clay, called ultra-light clay for short, is easier and more comfortable to knead and more suitable for modeling, is a novel environment-friendly, nontoxic and naturally air-dried hand modeling material, is prepared by mainly foaming a high polymer material foaming powder, and then physically mixing the foaming powder with materials such as polihexanol, a crosslinking agent, glycerol, pigment and the like according to a certain proportion, and has the characteristics of ultra-light, ultra-flexibility, ultra-cleanness and non-stickiness.
In the process of preparing light clay, for example, the invention patent with patent number CN108440983A "an ultra-light clay and its preparation method", bronopol, also known as bronopol, is used in preparation, is white to light yellow, yellow brown crystalline powder at normal temperature, odorless and tasteless, is easily soluble in water, ethanol, propylene glycol, is insoluble in chloroform, acetone, benzene, etc., can be slowly decomposed in alkaline aqueous solution, has corrosion effect on some metals, such as aluminum, is toxic to bronopol, has irritation effect on eyes, skin and mucosa, and is colorless transparent oily liquid with irritation smell, which is soluble in hot water, has strong irritation effect on eyes, skin and mucosa, and can be used for preparing antiseptic and bactericide, bronopol can be used for children's eyes, skin and mucosa when used, Skin and mucosa cause irritation, which results in unsafe use for children.
Disclosure of Invention
The invention aims to provide a preparation process of child safety light clay with an antibacterial function, which uses ampicillin and an anti-repellent agent to replace Broboer, so that the light clay is safer, does not irritate the skin, eyes and mucous membranes of children, does not generate allergy, and is safer.
In order to achieve the purpose, the invention is realized by the following technical scheme: a preparation process of children safety light clay with an antibacterial function comprises the following steps: 70% of glue, 5% of glycerol, 3% of glue powder, 2% of glutaraldehyde, 0.8% of isothiazolinone, 2% of incense powder, 3% of pigment, 10% of water, 0.3-0.8% of ampicillin and 3-6% of antibacterial agent.
The method mainly comprises the following steps:
s1, putting water into a container, adding activated carbon into the water, stirring the water, and then filtering the water;
s2, stirring the water obtained in the step S1, and adding glue, rubber powder and isothiazolinone while stirring to obtain a first product;
s3, heating and stirring the first product obtained in the step S2, and simultaneously adding glutaraldehyde and glycerol to obtain a second product;
s4, heating and stirring the second product obtained in the S3, and simultaneously adding the incense powder and the pigment to obtain a third product;
s5, cooling the third product obtained in the step S4, stirring, and adding ampicillin and an antibacterial agent while stirring to obtain a final product;
s6, vacuum packaging the final product obtained in the S5.
Further, the preparation process of the light clay with antibacterial function for children according to claim 1 is characterized by comprising the following steps: according to the operation procedure in S2, the stirring speed is 350r/min, the stirring time is 7min, and the mixture is stirred into paste.
Further, the preparation process of the light clay with antibacterial function for children according to claim 1 is characterized by comprising the following steps: according to the operation procedure in S3, the temperature is raised to 50 ℃, the stirring speed is 350r/min, the stirring time is 8min, and the mixture is stirred into paste.
Further, the preparation process of the light clay with antibacterial function for children according to claim 1 is characterized by comprising the following steps: according to the operation procedure in S4, the temperature is raised to 70 ℃, the stirring speed is 300r/min, the stirring time is 5min, and the mixture is stirred into paste.
Further, the preparation process of the light clay with antibacterial function for children according to claim 1 is characterized by comprising the following steps: according to the operation steps in S5, stirring speed is 400/min, stirring time is 45min, and air drying is carried out to obtain the final product.
Further, the preparation process of the light clay with antibacterial function for children according to claim 1 is characterized by comprising the following steps: vacuum packaging was performed using the disintegratable packing bag according to the procedure in S6.
Further, the preparation process of the light clay with antibacterial function for children according to claim 1 is characterized by comprising the following steps: according to the operation step in S5, the cooling employs stationary cooling.
The invention provides a preparation process of child-safe light clay with an antibacterial function. The method has the following beneficial effects:
1. according to the preparation process of the child safety light clay with the antibacterial function, ampicillin and an anti-repellent agent are used for replacing Brobopol, so that the light clay is safer, stimulation to skin, eyes and mucous membranes of children is avoided, the phenomenon of allergy is avoided, and the produced light clay is safer.
2. The preparation process of the child safety light clay with the antibacterial function uses ampicillin and an anti-repellent agent to replace Brobopol, so that the antibacterial and bactericidal effects are better.
3. The preparation process of the child safety light clay with the antibacterial function uses the decomposable packaging bag for vacuum packaging, and does not pollute the environment.
Detailed Description
The invention provides a technical scheme that: a preparation process of children safety light clay with an antibacterial function comprises the following specific embodiments:
example 1
Preparing materials: 70% of glue, 5% of glycerol, 3% of rubber powder, 2% of glutaraldehyde, 0.8% of isothiazolinone, 2% of incense powder, 3% of pigment, 10% of water, 0.3% of ampicillin and 3% of antibacterial agent.
The method mainly comprises the following steps:
s1, putting water into a container, adding activated carbon into the water, stirring the water, and then filtering the water;
s2, stirring the water obtained in the step S1, adding glue, glue powder and isothiazolinone while stirring to obtain a first product, wherein the stirring speed is 350r/min, the stirring time is 7min, and the first product is stirred into paste;
s3, heating and stirring the first product obtained in the step S2, adding glutaraldehyde and glycerol to obtain a second product, heating to 50 ℃, stirring at the speed of 350r/min for 8min, and stirring into paste;
s4, heating and stirring the second product obtained in the step S3, adding the incense powder and the pigment to obtain a third product, heating to 70 ℃, stirring at the speed of 300r/min for 5min, and stirring into paste;
s5, cooling the third product obtained in the step S4, stirring, adding ampicillin and an antibacterial agent while stirring, standing and cooling to normal temperature, stirring at a speed of 400/min for 45min, air-drying to obtain a solid to obtain a final product, and cooling by standing and cooling;
s6, vacuum packaging the final product obtained in the S5, and vacuum packaging by using a decomposable packaging bag.
Example 2
Preparing materials: 70% of glue, 5% of glycerol, 3% of rubber powder, 2% of glutaraldehyde, 0.8% of isothiazolinone, 2% of incense powder, 3% of pigment, 10% of water, 0.6% of ampicillin and 5% of antibacterial agent.
The method mainly comprises the following steps:
s1, putting water into a container, adding activated carbon into the water, stirring the water, and then filtering the water;
s2, stirring the water obtained in the step S1, adding glue, glue powder and isothiazolinone while stirring to obtain a first product, wherein the stirring speed is 350r/min, the stirring time is 7min, and the first product is stirred into paste;
s3, heating and stirring the first product obtained in the step S2, adding glutaraldehyde and glycerol to obtain a second product, heating to 50 ℃, stirring at the speed of 350r/min for 8min, and stirring into paste;
s4, heating and stirring the second product obtained in the step S3, adding the incense powder and the pigment to obtain a third product, heating to 70 ℃, stirring at the speed of 300r/min for 5min, and stirring into paste;
s5, cooling the third product obtained in the step S4, stirring, adding ampicillin and an antibacterial agent while stirring, standing and cooling to normal temperature, stirring at a speed of 400/min for 45min, air-drying to obtain a solid to obtain a final product, and cooling by standing and cooling;
s6, vacuum packaging the final product obtained in the S5, and vacuum packaging by using a decomposable packaging bag.
Example 3
Preparing materials: 70% of glue, 5% of glycerol, 3% of rubber powder, 2% of glutaraldehyde, 0.8% of isothiazolinone, 2% of incense powder, 3% of pigment, 10% of water, 0.8% of ampicillin and 6% of antibacterial agent.
The method mainly comprises the following steps:
s1, putting water into a container, adding activated carbon into the water, stirring the water, and then filtering the water;
s2, stirring the water obtained in the step S1, adding glue, glue powder and isothiazolinone while stirring to obtain a first product, wherein the stirring speed is 350r/min, the stirring time is 7min, and the first product is stirred into paste;
s3, heating and stirring the first product obtained in the step S2, adding glutaraldehyde and glycerol to obtain a second product, heating to 50 ℃, stirring at the speed of 350r/min for 8min, and stirring into paste;
s4, heating and stirring the second product obtained in the step S3, adding the incense powder and the pigment to obtain a third product, heating to 70 ℃, stirring at the speed of 300r/min for 5min, and stirring into paste;
s5, cooling the third product obtained in the step S4, stirring, adding ampicillin and an antibacterial agent while stirring, standing and cooling to normal temperature, stirring at a speed of 400/min for 45min, air-drying to obtain a solid to obtain a final product, and cooling by standing and cooling;
s6, vacuum packaging the final product obtained in the S5, and vacuum packaging by using a decomposable packaging bag.
Samples of each example were taken for assay analysis and compared to the prior art to yield the following data:
| peculiar smell | Antibacterial effect | Sterilizing effect | Degree of safety | |
| Example 1 | Is free of | In general | In general | Security |
| Example 2 | Is free of | Is excellent in | Is excellent in | Security |
| Example 3 | Is free of | Good effect | Good effect | Security |
| Technical index of comparative example | Slight peculiar smell | Good effect | Good effect | Irritate skin and eyes, and some children may even generate allergy |
According to the table data, in the embodiment 2, parameters obtained by the preparation process of the child-safe light clay with the antibacterial function are odorless, good in antibacterial effect, good in sterilization effect and very safe.
The invention provides a preparation process of child safety light clay with an antibacterial function, which comprises the following steps: 70% of glue, 5% of glycerol, 3% of glue powder, 2% of glutaraldehyde, 0.8% of isothiazolinone, 2% of incense powder, 3% of pigment, 10% of water, 0.6% of ampicillin and 5% of antibacterial agent, firstly putting water into a container, adding activated carbon into the water, stirring the water, then filtering the water, removing impurities in the water, stirring the water obtained in S1, adding the glue powder, the isothiazolinone and the glue powder while stirring to obtain a first product, stirring at the speed of 350r/min for 7min to obtain paste, heating and stirring the first product obtained in S2 to obtain a second product, simultaneously adding the glutaraldehyde and the glycerol to obtain the second product, heating to the temperature of 50 ℃, stirring at the speed of 350r/min for 8min, stirring to obtain the paste, heating to prevent the second product from solidifying, heating and stirring the second product obtained in S3, adding incense powder and pigment at the same time to obtain a third product, heating to 70 ℃, stirring at the speed of 300r/min for 5min, stirring into paste to enable the incense powder and the pigment to be better fused in the second product, cooling the third product obtained in S4, stirring, adding ampicillin and an antibacterial agent while stirring, standing and cooling to normal temperature to prevent the effect of ampicillin and the antibacterial agent from losing effectiveness, stirring at the speed of 400/min, stirring for 45min, air-drying to obtain a solid, cooling, standing and cooling, vacuum-packaging the final product, vacuum-packaging by using a decomposable packaging bag, and no pollution to the environment.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various changes and modifications can be made without departing from the inventive concept of the present invention, and these changes and modifications are all within the scope of the present invention.
Claims (7)
1. A preparation process of children safety light clay with an antibacterial function is characterized by comprising the following steps: the preparation method comprises the following steps: 70% of glue, 5% of glycerol, 3% of glue powder, 2% of glutaraldehyde, 0.8% of isothiazolinone, 2% of incense powder, 3% of pigment, 10% of water, 0.3-0.8% of ampicillin and 3-6% of antibacterial agent;
the method mainly comprises the following steps:
s1, putting water into a container, adding activated carbon into the water, stirring the water, and then filtering the water;
s2, stirring the water obtained in the step S1, and adding glue, rubber powder and isothiazolinone while stirring to obtain a first product;
s3, heating and stirring the first product obtained in the step S2, and simultaneously adding glutaraldehyde and glycerol to obtain a second product;
s4, heating and stirring the second product obtained in the S3, and simultaneously adding the incense powder and the pigment to obtain a third product;
s5, cooling the third product obtained in the step S4, stirring, and adding ampicillin and an antibacterial agent while stirring to obtain a final product;
s6, vacuum packaging the final product obtained in the S5.
2. The preparation process of the light clay with antibacterial function for children according to claim 1, wherein the process comprises the following steps: according to the operation procedure in S2, the stirring speed is 350r/min, the stirring time is 7min, and the mixture is stirred into paste.
3. The preparation process of the light clay with antibacterial function for children according to claim 1, wherein the process comprises the following steps: according to the operation procedure in S3, the temperature is raised to 50 ℃, the stirring speed is 350r/min, the stirring time is 8min, and the mixture is stirred into paste.
4. The preparation process of the light clay with antibacterial function for children according to claim 1, wherein the process comprises the following steps: according to the operation procedure in S4, the temperature is raised to 70 ℃, the stirring speed is 300r/min, the stirring time is 5min, and the mixture is stirred into paste.
5. The preparation process of the light clay with antibacterial function for children according to claim 1, wherein the process comprises the following steps: according to the operation steps in S5, stirring speed is 400/min, stirring time is 45min, and air drying is carried out to obtain the final product.
6. The preparation process of the light clay with antibacterial function for children according to claim 1, wherein the process comprises the following steps: vacuum packaging was performed using the disintegratable packing bag according to the procedure in S6.
7. The preparation process of the light clay with antibacterial function for children according to claim 1, wherein the process comprises the following steps: according to the operation step in S5, the cooling employs stationary cooling.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910777637.4A CN110606985A (en) | 2019-08-22 | 2019-08-22 | Preparation process of child safety light clay with antibacterial function |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910777637.4A CN110606985A (en) | 2019-08-22 | 2019-08-22 | Preparation process of child safety light clay with antibacterial function |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101070232A (en) * | 2006-05-09 | 2007-11-14 | 北京京师奕阳教育科技有限公司 | Light clay composition and preparing method |
| KR20180034748A (en) * | 2016-09-26 | 2018-04-05 | 경북대학교 산학협력단 | Manufacturing method for polyvinylalcohol film containing antibiotics, mixed with inorganic particles |
| CN108102266A (en) * | 2017-12-21 | 2018-06-01 | 深圳市学巧教育文化传播有限公司 | A kind of ultralight clay and preparation method thereof |
| CN108440983A (en) * | 2018-01-24 | 2018-08-24 | 佛山市长飞文具有限公司 | A kind of toy ultralight clay and preparation method thereof |
-
2019
- 2019-08-22 CN CN201910777637.4A patent/CN110606985A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101070232A (en) * | 2006-05-09 | 2007-11-14 | 北京京师奕阳教育科技有限公司 | Light clay composition and preparing method |
| KR20180034748A (en) * | 2016-09-26 | 2018-04-05 | 경북대학교 산학협력단 | Manufacturing method for polyvinylalcohol film containing antibiotics, mixed with inorganic particles |
| CN108102266A (en) * | 2017-12-21 | 2018-06-01 | 深圳市学巧教育文化传播有限公司 | A kind of ultralight clay and preparation method thereof |
| CN108440983A (en) * | 2018-01-24 | 2018-08-24 | 佛山市长飞文具有限公司 | A kind of toy ultralight clay and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| YINING XIA ET AL: "Novel Active Surface Prepared by Embedded Functionalized Clays in an Acrylate Coating", 《APPL. MATER. INTERFACES》 * |
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Effective date of registration: 20210623 Address after: 276000 1202-160, No. 100, Lingong Road, comprehensive bonded zone, Linyi City, Shandong Province Applicant after: Bo Shi AI Toys Co.,Ltd. Address before: 276035 No.66 Wenhua Road, baishabu Town, Lanshan District, Linyi City, Shandong Province Applicant before: LINYI BOSHIAI STATIONERY Co.,Ltd. |
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Application publication date: 20191224 |
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