CN110566816A - preparation method of tar viscosity reducer for reducing viscosity of tar - Google Patents
preparation method of tar viscosity reducer for reducing viscosity of tar Download PDFInfo
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- CN110566816A CN110566816A CN201910910812.2A CN201910910812A CN110566816A CN 110566816 A CN110566816 A CN 110566816A CN 201910910812 A CN201910910812 A CN 201910910812A CN 110566816 A CN110566816 A CN 110566816A
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- tar
- viscosity
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- isopropanol
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
- F17D—PIPE-LINE SYSTEMS; PIPE-LINES
- F17D1/00—Pipe-line systems
- F17D1/08—Pipe-line systems for liquids or viscous products
- F17D1/16—Facilitating the conveyance of liquids or effecting the conveyance of viscous products by modification of their viscosity
- F17D1/17—Facilitating the conveyance of liquids or effecting the conveyance of viscous products by modification of their viscosity by mixing with another liquid, i.e. diluting
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- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Public Health (AREA)
- Water Supply & Treatment (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention discloses a preparation method of a tar viscosity reducer for reducing tar viscosity. The invention is applied to the coking industry, and the viscosity of tar can be reduced at normal temperature by adding the invention into the tar, thereby achieving the functions of convenient transportation and reducing danger. A preparation method of a tar viscosity reducer for reducing tar viscosity is characterized by comprising the following steps: the formula contains surfactant, alkaline reagent, isopropanol and deionized water.
Description
Technical Field
the invention discloses a preparation method of a tar viscosity reducer for reducing tar viscosity. The invention is applied to the coking industry, and the viscosity of tar can be reduced at normal temperature by adding the invention into the tar, thereby achieving the functions of convenient transportation and reducing danger.
Background
In the existing coking industry, there is a great inconvenience in the transportation of tar. The tar is viscous black liquid at normal temperature, has a flash point of about 80-90 ℃, and belongs to flammable liquid. The viscosity of tar decreases with the increase of temperature, but the steam and air can form explosive mixture at high temperature, and the tar is easy to burn and explode when exposed to open fire and high heat. Contact with oxidant and react violently. If high heat is encountered, the internal pressure of the container is increased, and the danger of cracking and explosion is caused.
The invention can reduce the viscosity of tar and enhance the fluidity of tar at normal temperature, and is more beneficial to the transportation of tar. In addition, the viscosity of tar is reduced at normal temperature, the consumption of steam is reduced, the fluidity of the tar is not maintained at high temperature, the energy consumption is greatly reduced, the cost is reduced, and the economic benefit of a company is increased.
According to the existing conditions, the invention discloses a preparation method of a tar viscosity reducer for reducing the viscosity of tar, aiming at reducing the viscosity of the tar, keeping the tar in a liquidity state at normal temperature, and reducing the cost in the transportation process and the danger at high temperature.
The surface active agent can reduce the viscosity, has less dosage of the surface active agent, convenient operation, no toxicity and no corrosion, and is an ideal chemical product, thereby having important application in factories and scientific research. When the concentration is the same, the non-polar component in the surfactant is large, and the surfactant has strong surface activity. That is, among the homologs, the surface activity is large when the number of carbon atoms is large. However, if the carbon chain is too long, the solubility in water is too low, and thus the carbon chain is of no practical value.
Disclosure of Invention
In view of the above problems, an object of the present invention is to provide a method for producing a viscosity reducing agent for tar, which is capable of reducing the viscosity of tar at normal temperature.
In order to achieve the purpose, the invention adopts the following technical scheme:
A preparation method of a tar viscosity reducer for reducing tar viscosity is characterized by comprising the following steps: the formula contains surfactant, alkaline reagent, isopropanol and deionized water.
The preparation method of the tar viscosity reducer for reducing the viscosity of tar is characterized by comprising the following steps: the surfactant accounts for 1.5-2% of the total weight of the invention, the alkaline agent accounts for 0.5% of the total weight of the invention, the isopropanol accounts for 5% of the total weight of the invention, and the rest is deionized water.
The preparation method of the tar viscosity reducer for reducing the viscosity of tar is characterized by comprising the following steps: the surfactant is one or a mixture of two of lauryl sodium sulfate and tetradecyl sodium sulfate, and the mixing ratio is not limited.
The preparation method of the tar viscosity reducer for reducing the viscosity of tar is characterized by comprising the following steps: the alkaline reagent is sodium hydroxide.
The preparation method of the tar viscosity reducer for reducing the viscosity of tar is characterized by comprising the following steps: the viscosity reducer is a water-soluble viscosity reducer.
The preparation method of the tar viscosity reducer for reducing the viscosity of tar comprises the following steps: adding 93% of deionized water into a reaction kettle, then adding 0.5% of sodium hydroxide into the reaction kettle, and stirring for 30 minutes; cooling to room temperature after the sodium hydroxide is completely dissolved, adding 5% isopropanol, stirring for 5-10 minutes, fully and uniformly mixing, adding 1.5% -2% of surfactant, and stirring for 30-60 minutes.
Due to the adoption of the technical scheme, the method has the following advantages:
The invention can effectively reduce the viscosity of tar, increase the fluidity of the tar without high-temperature heating in the pipeline transportation process, reduce energy consumption and reduce the danger brought by high temperature.
Embodiment 1
Selecting raw materials according to weight percentage
93 percent of deionized water
Isopropanol 5%
0.5 percent of sodium hydroxide
Sodium dodecyl sulfate 1.5%
Adding 93% of deionized water into a reaction kettle, then adding 0.5% of sodium hydroxide into the reaction kettle, and stirring for 30 minutes; cooling to room temperature after the sodium hydroxide is completely dissolved, adding 5% isopropanol, stirring for 5-10 min, mixing uniformly, adding 1.5% sodium dodecyl sulfate, and stirring for 30-60 min.
Example II
Selecting raw materials according to weight percentage
93 percent of deionized water
Isopropanol 5%
0.5 percent of sodium hydroxide
Sodium tetradecyl sulfate 1.5%
Adding 93% of deionized water into a reaction kettle, then adding 0.5% of sodium hydroxide into the reaction kettle, and stirring for 30 minutes; cooling to room temperature after the sodium hydroxide is completely dissolved, adding 5% isopropanol, stirring for 5-10 min, mixing well, adding 1.5% sodium tetradecyl sulfate, and stirring for 30-60 min.
Example three
Selecting raw materials according to weight percentage
92.5 percent of deionized water
Isopropanol 5%
0.5 percent of sodium hydroxide
Sodium dodecyl sulfate 2%
Adding 93% of deionized water into a reaction kettle, then adding 0.5% of sodium hydroxide into the reaction kettle, and stirring for 30 minutes; cooling to room temperature after the sodium hydroxide is completely dissolved, adding 5% isopropanol, stirring for 5-10 min, mixing uniformly, adding 2% sodium dodecyl sulfate, and stirring for 30-60 min.
Example four
Selecting raw materials according to weight percentage
92.5 percent of deionized water
Isopropanol 5%
0.5 percent of sodium hydroxide
Sodium tetradecyl sulfate 2%
Adding 93% of deionized water into a reaction kettle, then adding 0.5% of sodium hydroxide into the reaction kettle, and stirring for 30 minutes; cooling to room temperature after the sodium hydroxide is completely dissolved, adding 5% isopropanol, stirring for 5-10 min, mixing uniformly, adding 2% sodium tetradecyl sulfate, and stirring for 30-60 min.
Test example 1
The kinematic viscosity of the tar at 40 ℃ is measured in the test, then four parts of the tar with the same mass are respectively added into the test case with 20ppm, and are fully dissolved at 40 ℃, and the viscosity of the tar is measured:
| Case(s) | Blank space | Case one | Case two | Case three | Case four |
| Viscosity mm/s | 2.3 | 1.9 | 1.7 | 1.8 | 1.5 |
The data show that the viscosity of tar in the embodiment is lower than that of tar without the added medicament, the viscosity reduction performance of 2% of surfactant in the test is better than 1.5%, and the effect of tetradecyl sodium sulfate is better than that of dodecyl sodium sulfate.
Claims (6)
1. A preparation method of a tar viscosity reducer for reducing tar viscosity is characterized by comprising the following steps: the formula contains surfactant, alkaline reagent, isopropanol and deionized water.
2. The method of claim 1, wherein the viscosity of tar is reduced by the steps of: the surfactant accounts for 1.5-2% of the total weight of the invention, the alkaline agent accounts for 0.5% of the total weight of the invention, the isopropanol accounts for 5% of the total weight of the invention, and the rest is deionized water.
3. The process for producing a viscosity reducing agent for tar according to claim 1 or 2, wherein: the surfactant is one or a mixture of two of lauryl sodium sulfate and tetradecyl sodium sulfate, and the mixing ratio is not limited.
4. The process for producing a viscosity reducing agent for tar according to claim 1 or 2, wherein: the alkaline reagent is sodium hydroxide.
5. The process for producing a viscosity reducing agent for tar according to claim 1 or 2, wherein: the viscosity reducer is a water-soluble viscosity reducer.
6. The composition of claim 1, wherein said viscosity reducing agent for tar is prepared by a method comprising: adding 93% of deionized water into a reaction kettle, then adding 0.5% of sodium hydroxide into the reaction kettle, and stirring for 30 minutes; cooling to room temperature after the sodium hydroxide is completely dissolved, adding 5% isopropanol, stirring for 5-10 minutes, fully and uniformly mixing, adding 1.5% -2% of surfactant, and stirring for 30-60 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910910812.2A CN110566816A (en) | 2019-09-25 | 2019-09-25 | preparation method of tar viscosity reducer for reducing viscosity of tar |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910910812.2A CN110566816A (en) | 2019-09-25 | 2019-09-25 | preparation method of tar viscosity reducer for reducing viscosity of tar |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110566816A true CN110566816A (en) | 2019-12-13 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201910910812.2A Pending CN110566816A (en) | 2019-09-25 | 2019-09-25 | preparation method of tar viscosity reducer for reducing viscosity of tar |
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Citations (14)
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| US4343323A (en) * | 1979-06-08 | 1982-08-10 | Research Council Of Alberta | Pipeline transportation of heavy crude oil |
| SU1364827A1 (en) * | 1986-03-20 | 1988-01-07 | Центральная научно-исследовательская лаборатория Производственного объединения "Оренбургнефть" | Composition for transferring highly viscous water-petroleum emulsions through pipeline |
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| CN103468235A (en) * | 2013-09-26 | 2013-12-25 | 东北石油大学 | Chemical assistant for thermal recovery of thick oil and application thereof |
| CN203836475U (en) * | 2014-05-04 | 2014-09-17 | 河北九鼎冶金设备制造有限公司 | Tar conveying device with steam heating function |
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-
2019
- 2019-09-25 CN CN201910910812.2A patent/CN110566816A/en active Pending
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| SU1364827A1 (en) * | 1986-03-20 | 1988-01-07 | Центральная научно-исследовательская лаборатория Производственного объединения "Оренбургнефть" | Composition for transferring highly viscous water-petroleum emulsions through pipeline |
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| CN1195576A (en) * | 1998-01-21 | 1998-10-14 | 辽河石油勘探局勘察设计研究院 | Emulsifying viscosity-reducing agent for superthick emulsified oil combustion |
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| CN1554725A (en) * | 2002-11-29 | 2004-12-15 | 中国石油化工股份有限公司河南油田分 | Thickened oil steam production synergist and its preparing method |
| CN101024764A (en) * | 2007-01-12 | 2007-08-29 | 图们市方正化工助剂厂 | Surface activating agent for oil-field thick-oil well |
| CN101402880A (en) * | 2008-11-13 | 2009-04-08 | 辽宁石油化工大学 | Additive used for delay coking process for final residuum |
| CN101463249A (en) * | 2009-01-16 | 2009-06-24 | 北京奥尔创新石油工程技术有限公司 | Oil soluble heavy crude thinner and preparation thereof |
| CN103468235A (en) * | 2013-09-26 | 2013-12-25 | 东北石油大学 | Chemical assistant for thermal recovery of thick oil and application thereof |
| CN203836475U (en) * | 2014-05-04 | 2014-09-17 | 河北九鼎冶金设备制造有限公司 | Tar conveying device with steam heating function |
| CN104293401A (en) * | 2014-10-28 | 2015-01-21 | 山东中大药业有限公司 | Coal-water slurry blended fuel and preparation method thereof |
| CN108003909A (en) * | 2018-01-02 | 2018-05-08 | 北京三聚绿能科技有限公司 | A kind of composite demulsifying agent for wood tar dehydration |
| CN108949266A (en) * | 2018-07-20 | 2018-12-07 | 北京三聚环保新材料股份有限公司 | A kind of wood tar viscosity reduction polymerization inhibitor and its preparation method and application |
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Application publication date: 20191213 |
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