CN110558342A - Household fly bait composition and preparation method thereof - Google Patents
Household fly bait composition and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
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- A01N43/80—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,2
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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Abstract
The invention discloses a family fly bait composition and a preparation method thereof, and relates to the technical field of daily sanitary insecticide. The composition comprises 0.1 to 1 percent of systemic sanitary insecticide; 1-10% of sugar; 0.01 to 5 percent of sodium chloride; 0.01-5% of alkyl glycoside; 0.01-5% of citric acid; 0.3-60% of attractant; octyl isothiazolinone 0.1-2%; 0.01 to 5 percent of potassium chloride; 0.1 to 2 percent of gellan gum; the balance of distilled water. The invention adopts alkyl glycoside as synergist of systemic sanitary insecticide, and matches with components such as attractant, sodium chloride, citric acid, sugar and the like, so as to increase palatability of the bait to flies, attract houseflies and flea flies to continuously take food to poison flies; the alkyl glycoside in the composition can promote the migration of effective components of the pesticide, and when the housefly and the flea fly eat the composition, the alkyl glycoside can promote the systemic sanitary pesticide to enter the fly body, so that the acting time can be accelerated, the dosage of the pesticide can be reduced, and the use safety can be ensured.
Description
Technical Field
The invention relates to the technical field of daily sanitary insecticidal products, in particular to a family fly bait composition and a preparation method thereof.
Background
The flies in China mainly include flower flies, house flies (houseflies), rotten ropes, toilet flies, black flies, green flies, golden flies, city flies, flea flies and the like, and are widely distributed in rural areas. In the indoor environment of urban families in China, due to improvement of environmental sanitation, the number of varieties of bothersome flies is reduced, and houseflies and flea flies with relatively miscellaneous feeding habits are common. The houseflies belong to indoor true housing area flies, larvae are omnivorous, are widely distributed in more than 20 kinds of breeding places, are common in garbage, and adult flies enter and exit a housing and are indoor dominant fly species. Houseflies mostly live in places with rich feces, garbage and organic matters, and main foods are liquid substances including sweet juice, cow milk, sugar water, rotten fruits, liquid excrement containing protein and the like. The adult flea flies like to gather around rotten plants and sewers and have phototaxis and decay tendency, the flea flies are easier to breed than the houseflies, and the flea flies can be bred in household kitchen garbage. Flowers and plants, vegetables and kitchen garbage are planted in families, and the two flies are easily bred in sewers.
The luring poison bait is the most effective method for preventing and controlling flies, and the action principle of the luring poison bait is luring and poisoning. The research shows that the method for attracting houseflies and flea flies comprises the following steps: food smell attraction, food palatability attraction and phototaxis attraction, so that the indoor flies fly to the bait and stop falling. Factors affecting the poisoning effect include: difficulty in taking and taking, and quick action.
Most of fly killing bait sold in the market at present is in the form of granules or powder, and the fly killing bait in the form of the fly killing bait is difficult to eat and has insufficient feed intake. After being eaten, flies in the form of particles or powder have slow onset time and still fly for a certain distance to be completely knocked down. Especially, on the large-sized housefly mouthparts, even the powdery bait can be seen to be stuck on the housefly mouthparts, and the powdery bait cannot be eaten and absorbed quickly. Once the housefly and the flea fly still do not take effect quickly after eating, the housefly and the flea fly away from the house fly and fly.
Disclosure of Invention
The invention aims to solve the technical problems that fly killing bait products in the market have weak attraction to family flies, the flies are not easy to eat, the effect is slow and the like, and provides a family fly attracting composition and a preparation method thereof.
in order to solve the above problems, the present invention proposes the following technical solutions:
in a first aspect, the embodiment of the invention provides a family fly bait composition, which comprises the following components in percentage by mass:
Systemic sanitary insecticide 0.1-1%;
1-10% of sugar;
0.01 to 5 percent of sodium chloride;
0.01-5% of alkyl glycoside;
0.01-5% of citric acid;
0.3-60% of attractant;
Octyl isothiazolinone 0.1-2%;
Potassium chloride: 0.01 to 5 percent;
0.1 to 2 percent of gellan gum;
The balance of distilled water.
the technical scheme is that the systemic sanitary insecticide is dinotefuran.
The further technical scheme is that the structural formula of the alkyl glycoside is as follows:
Wherein X is 1.3 to 1.7 and R is an alkyl group of 8 to 10 carbon atoms.
The further technical scheme is that the sugar is brown sugar.
the further technical scheme is that the attractant is at least one of yeast hydrolysate, juicy peach extract or grape extract.
The technical scheme is that the domestic fly bait composition comprises, by mass, 0.1-40% of yeast hydrolysate and 0.1-10% of juicy peach extract; the content of grape extract is 0.1-10%.
The technical scheme is that the formulation of the household fly bait composition is gel bait or fluid bait. Preferably a gel.
in a second aspect, the present invention provides a method for preparing a domestic fly bait composition as described in the first aspect, including the following steps:
stirring systemic sanitary pesticide, sugar, sodium chloride, alkyl glycoside, citric acid, yeast hydrolysate, juicy peach extract, grape extract, octyl isothiazolinone and water accounting for 50% of the total water amount until the feed liquid is completely dissolved, heating to 50-60 ℃, and keeping the temperature for later use to obtain feed liquid A;
adding gellan gum into the rest water, mixing, heating to above 80 ℃, adding potassium chloride, cooling to 50-60 ℃, adding the feed liquid A, fully and uniformly stirring, filling into a container, and cooling to obtain the family fly bait composition.
compared with the prior art, the invention can achieve the following technical effects:
The invention adopts alkyl glycoside as synergist of systemic insecticide, matches with attractant, sodium chloride, citric acid, sugar and other components, increases palatability of bait to flies, attracts houseflies and flea flies to continuously take food, and kills flies by systemic insecticide; in addition, the alkyl glycoside and gellan gum are similar in structure and mutually soluble, and the alkyl glycoside and gellan gum are matched to facilitate the pesticide to diffuse and migrate to the surface of the bait to form an effective component mucoid film layer, so that flies land on the surface of the bait, and the mouth parts of the flies can easily take the pesticide, the concentration of the liquid pesticide taken is higher, the effect is quicker, the systemic hygienic pesticide is promoted to enter the bodies of the flies, and the effect taking time of the systemic hygienic pesticide can be accelerated.
Detailed Description
The technical solutions in the examples will be clearly and completely described below. It is apparent that the embodiments to be described below are only a part of the embodiments of the present invention, and not all of them. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
It will be understood that the terms "comprises" and/or "comprising," when used in this specification and the appended claims, specify the presence of stated features, integers, steps, operations, elements, and/or components, but do not preclude the presence or addition of one or more other features, integers, steps, operations, elements, components, and/or groups thereof.
it is also to be understood that the terminology used in the description of the embodiments of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the embodiments of the invention. As used in the description of embodiments of the present invention and the appended claims, the singular forms "a," "an," and "the" are intended to include the plural forms as well, unless the context clearly indicates otherwise.
The embodiment of the invention provides a family fly bait composition which comprises the following components in percentage by mass:
0.1 to 1 percent of dinotefuran;
1-10% of sugar;
0.01 to 5 percent of sodium chloride;
0.01-5% of alkyl glycoside;
0.01-5% of citric acid;
0.3-60% of attractant;
octyl isothiazolinone 0.1-2%;
potassium chloride: 0.01 to 5 percent;
0.1 to 2 percent of gellan gum;
the balance of distilled water.
in a specific embodiment, the alkyl glycoside has the following structural formula:
Wherein X is 1.3 to 1.7 and R is an alkyl group of 8 to 10 carbon atoms. The alkyl glycoside is a nonionic surfactant, has mild property, no toxicity or irritation, good compatibility with skin, no irritation to mouthparts of flies when added into the bait, and no contraindication to flies after eating the bait. The alkyl glycoside and dinotefuran are similar to each other and dissolved mutually, under the condition of gel bait or fluid bait, the gel bait and the fluid bait are migrated to the surface of the bait to form an effective component mucoid film layer, flies are stopped on the surface of the bait, a mouthpart of the flies is easy to eat, the concentration of the eaten liquid medicine is higher, and the effect is quicker. When the gel bait is used, water can be added into the gel system after the water in the gel system is evaporated and dried, and the gel bait can be repeatedly used after the water in the gel system is absorbed.
In a specific implementation, the sugar is brown sugar.
In specific implementation, the attractant is at least one of yeast hydrolysate, juicy peach extract or grape extract.
it is known that flies are sensitive to smell and taste, and substances with fishy smell, salty taste and sweet taste have certain attraction to flies. Through a large number of experimental screens, the invention screens out the components which are attractive to houseflies and flea flies: yeast hydrolysate, the smell of yeast hydrolysate, has a strong attraction for houseflies and flea flies. It is characterized by that after the wall-breaking of yeast, the protein, nucleic acid and vitamins in the yeast are extracted, and then undergone the processes of directional enzymolysis and biological enzymolysis, so that it is rich in small molecular amino acids, peptides, nucleotides and vitamins, etc. The amino acid content is more than 30%, the total protein content is more than 50%, the nucleotide content is more than 10%, the nutritional ingredients meet the nutritional requirements of flies, and the food intake of the flies is obviously improved.
Through experimental screening, the odor of the juicy peach extract and the grape extract is found to have strong attraction to houseflies. The honey peaches and grapes have high sugar content, and fresh fruits are easy to rot during natural storage, so that favorable conditions are provided for the eggs laying of the Sidae, and therefore, the odor and the taste of the extracts of the two fruits have strong attraction to the Sidae.
Therefore, the attractant used in the embodiment of the invention is at least one of yeast hydrolysate, honey peach extract or grape extract.
in one embodiment, the attractants used in embodiments of the invention are yeast hydrolysate and juicy peach extract.
In one embodiment, the attractants used in embodiments of the invention are yeast hydrolysate and grape extract.
in one embodiment, the attractant is a mixture of yeast hydrolysate, juicy peach extract and grape extract.
In specific implementation, in the household fly bait composition, the yeast hydrolysate accounts for 0.1-40% and the honey peach extract accounts for 0.1-10% by mass percentage; the content of grape extract is 0.1-10%.
The embodiment of the invention adopts the yeast hydrolysate, the juicy peach extract and the grape extract which have strong attraction to the houseflies and the flea flies, and the alkyl glycoside is used as the synergist of the dinotefuran, so that the composition has strong attraction effect on the houseflies and the flea flies.
In specific implementation, the formulation of the household fly bait composition is gel bait or fluid bait.
the technical scheme of the invention is that the bait is made into gel bait or fluid bait, which is more beneficial to the feeding of flies and the effect of the product.
the fly belongs to a licking mouth device, the main part of the fly is a kiss head which is mainly composed of a lower lip, and the kiss end is a lipped which is composed of a pseudo-trachea formed by the lower lip and is used for collecting liquid on the surface of an object; the lower lip encloses the upper lip and the tongue, which form a food passage, and the tongue also contains a saliva tube. The fly is easy to lick the surface of fluid, solid particles and powder bait are generally difficult to enable the fly to quickly absorb, absorb and kill, the solid particles can block a mouth of the fly and cannot be eaten continuously, however, the addition amount of effective components must be increased to improve the pesticide effect on the fly, the increased effective components have certain toxicity, the toxicity of the product is increased, and the health risk of the product in use is increased.
therefore, the gel or fluid bait is more beneficial to flies to eat, requires lower effective pesticide dosage and is safe to use.
in a second aspect, the present invention provides a method for preparing the above-mentioned fly bait composition, including the following steps:
stirring systemic sanitary pesticide, sugar, sodium chloride, alkyl glycoside, citric acid, yeast hydrolysate, juicy peach extract, grape extract, octyl isothiazolinone and water accounting for 50% of the total water amount until the feed liquid is completely dissolved, heating to 50-60 ℃, and keeping the temperature for later use to obtain feed liquid A;
adding gellan gum into the rest water, mixing, heating to above 80 ℃, adding potassium chloride, cooling to 50-60 ℃, adding the feed liquid A, fully and uniformly stirring, filling into a container, and cooling to obtain the family fly bait composition.
The specific embodiment is as follows:
examples 1 to 8 of the fly bait composition for house use according to the present invention were prepared according to the formulation shown in table 1.
TABLE 1 formulation proportions for examples 1-8
The preparation method of the fly bait composition for family use of the present examples 1-8 is as follows:
According to the proportion in the table 1, evenly stirring dinotefuran, brown sugar, sodium chloride, alkyl glycoside, citric acid, yeast hydrolysate, juicy peach extract, grape extract, octyl isothiazolinone and water accounting for 50 percent of the total water content until the materials are completely dissolved, heating to 50-60 ℃, and preserving heat for later use to obtain feed liquid A;
adding gellan gum into the rest water, mixing, heating to above 80 deg.C, adding potassium chloride, cooling to 50-60 deg.C, adding feed liquid A, and stirring to obtain the composition.
effects of the implementation
Experiment one
The purpose of this experiment was: the attraction of the fly bait compositions for family provided in examples 1 to 8 of the present invention to the housefly and the attraction of the fly compositions for comparative examples 1 to 2 to the housefly were observed in a laboratory environment. Comparative example 1 is a commercial block of fly killing gel bait. Comparative example 2 is a commercially available granular fly bait.
the experimental method is briefly described as follows:
Indoor simulation field fly killing effect test
the test device comprises: square room, area 10 square meters, height 2.5 meters.
the test conditions are as follows: temperature (26 ℃ C. + -. 1 ℃ C.), humidity (65% + -. 10%).
Testing insects: and (4) emerging of the adult insects for 3-4 days, wherein 200 adult insects are female and male.
The experimental method comprises the following steps: 200 flies were placed in the simulation room, in two petri dishes, diagonally, at the actual amount recommended for bait in one room. And (3) placing fly feed at the other diagonal, placing a culture dish containing a soaked cotton ball in the center of the simulation room, simulating day and night, wherein the light source is turned off at 18 o 'clock in the morning at 6 o' clock at night, the light source is turned on at the rest time, checking the number of dead test insects after 24h, and calculating the death rate.
Determination of onset speed: the center of the specimen culture dish is the center of a circle, and 0.3 m is taken as a radius to draw a circle respectively. When the number of dead test insects is checked, the total number of dead test insects in the circle is calculated, and the proportion of the dead test insects in the total number of the test insects is calculated. The drug effect taking speed of the bait agent and the competitive products is compared.
The results of the indoor simulation field fly killing effect test are shown in table 2.
table 2 simulated field test fly-luring effect of the bait compositions of examples 1-8 and comparative examples 1-2
as can be seen from Table 2, the composition provided by the embodiment of the invention can effectively improve the death speed of the houseflies, obviously shorten the struggle and fly distance of the houseflies, take effect quickly, and reduce the pollution of the flies to the surrounding environment. As can also be seen from Table 2, in example 2, the attraction to flies was slightly insufficient due to the decrease of the yeast hydrolysate, so the experimental effect was poor; also, example 7 decreased the attraction to flies due to the lack of grape extract, and thus the number of deaths from houseflies was low; therefore, by reasonably matching the yeast hydrolysate, the juicy peach extract and the grape extract, the luring force on flies can be improved in the aspects of smell, taste and the like, so that the luring and killing effect is improved.
experiment two
the purpose of this experiment was: the attraction of the household fly bait compositions of examples 1 to 8 and the fly compositions of comparative examples 1 to 2 to house flies and flea flies in the actual use environment was observed.
The experimental method is briefly described as follows:
The fly bait compositions of examples 1 to 8 were put into a commercially available trapping device, and an attraction test for the field environment was performed. Only dead houseflies and flea flies were counted.
A trapping site: three courtyards with similar environment and fly density and rain shelters are selected for residences near a certain aquaculture farm in the mountain of the crane in Jiangmen province, Guangdong province.
The trapping device comprises: the baits of examples 1 to 8 and the baits of comparative examples 1 to 2, each 50g, were placed in a commercially available trapping device, and the device was placed on the ground of a yard and continuously tested for 5 days.
Determination of onset speed: the center of the trapping device is taken as the center of a circle, and 0.3 m is taken as the radius to draw a circle respectively. When the number of dead test insects is checked, the total number of dead test insects in the circle is calculated, and the proportion of the dead test insects in the total number of the test insects is calculated. The onset of action of the bait of examples 1-8 of the invention was compared with that of comparative examples 1-2.
The results of the attraction test of the baits of examples 1 to 8 of the present invention and comparative examples 1 to 2 for house flies and flea flies in the actual use environment are shown in Table 3.
TABLE 3 fly-luring Effect of real Environment use test of examples 1-8 and comparative examples 1-2
as can be seen from Table 3, the household fly bait compositions of examples 1-8 of the present invention have better killing numbers and killing speed on houseflies than comparative examples 1-2, and have much greater attraction on flea flies than comparative examples in practical use environments.
Experiment three
The purpose of this experiment was: the water in the gel can be dehydrated and dried along with the prolonging of the standing time, the gel is shrunk, and the attractive force can be changed. When the actual use was observed, the change of the attracting force with the lapse of time.
The experimental method is briefly described as follows:
The gel-like bait composition for house flies obtained in example 3 was subjected to an attraction test in the field environment in comparison with comparative example 1. Only dead houseflies and flea flies were counted.
A trapping site: a courtyard with a canopy near an aquaculture farm of a certain mountain of the crane of Jiangmen, Guangdong province.
The trapping device comprises: 50g of each of the baits of example 3 and comparative example 1 were placed in a commercially available attracting device, the device was placed on the floor of a yard and naturally lit during the day and unlit at night, flies were attracted by the odor emitted from the bait, and the test was continued by recording the daily knockdown test insects every five days.
determination of onset speed: the center of the trapping device is taken as the center of a circle, and 0.3 m is taken as the radius to draw a circle respectively. When the number of dead test insects is checked, the total number of dead test insects in the circle is calculated, and the proportion of the dead test insects in the total number of the test insects is calculated. The drug effect taking speed of the bait agent and the competitive products is compared.
The results of the tests on the bait's attractive force as a function of time of use are shown in Table 4.
Table 4 use test of example 3 and comparative example 1 fly-luring effect
as can be seen from the results in table 4, the formulation of example 3 has a reduced attraction with comparative example 1 and a lower onset of action against house flies, but the killing number and killing speed against house flies are higher than those of comparative example 1, and the attraction of the formulation of example 3 to flea flies is much greater than that of comparative example 1.
Experiment four
The purpose of this experiment was: when the gel is used for a period of time, the gel can be dehydrated, dried, shrunk and re-supplemented with water, and the change of the bait agent attraction force is observed when the gel is repeatedly used.
The experimental method is briefly described as follows:
The sample of example 3, which had been used for 20 days in experiment three, was supplemented with purified water (commercially available reverse osmosis purified water) to make the total weight the same as before use. And sealing, and performing attraction experiments in the field environment after 24 hours until all water is absorbed by the gel. Only dead houseflies and flea flies were counted.
A trapping site: a courtyard with a canopy near an aquaculture farm of a certain mountain of the crane of Jiangmen, Guangdong province.
The trapping device comprises: 50g of the bait agent in example 3 is taken and placed in a trapping device, the device is placed on the ground of a courtyard, a natural light source is provided in the daytime, no light source is provided at night, flies are attracted by means of the smell emitted by the bait agent, continuous testing is carried out, and the insect knockdown condition on the day is recorded every five days.
Determination of onset speed: the center of the luring device is taken as the center of a circle, and 0.3 m is taken as the radius to draw a circle respectively. When the number of dead test insects is checked, the total number of dead test insects in the circle is calculated, and the proportion of the dead test insects in the total number of the test insects is calculated. The results of the bait formulation after water addition for the attraction test are shown in Table 5.
Table 5 example 3 fly-luring effect of real use test after water addition
As can be seen from Table 5, the bait can be recycled by adding water in the actual use environment for 1 time, the drug effect is not reduced basically, and the effective use time is prolonged.
In the above embodiments, the descriptions of the respective embodiments have respective emphasis, and for parts that are not described in detail in a certain embodiment, reference may be made to related descriptions of other embodiments.
While the invention has been described with reference to specific embodiments thereof, it will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention as defined by the appended claims. Therefore, the protection scope of the present invention shall be subject to the protection scope of the claims.
Claims (9)
1. The household fly bait composition is characterized by comprising the following components in percentage by mass:
systemic sanitary insecticide 0.1-1%;
1-10% of sugar;
0.01 to 5 percent of sodium chloride;
0.01-5% of alkyl glycoside;
0.01-5% of citric acid;
0.3-60% of attractant;
Octyl isothiazolinone 0.1-2%;
Potassium chloride: 0.01 to 5 percent;
0.1 to 2 percent of gellan gum;
The balance of distilled water.
2. The household fly bait composition as claimed in claim 1, wherein the systemic hygienic insecticide is dinotefuran.
3. The home fly bait composition of claim 1, wherein the alkyl glycoside has the following structural formula:
Wherein X is 1.3 to 1.7 and R is an alkyl group of 8 to 10 carbon atoms.
4. The housefly bait composition, according to claim 1, wherein the sugar is brown sugar.
5. The family fly bait composition of claim 1, wherein the attractant is at least one of yeast hydrolysate, juicy peach extract, or grape extract.
6. the housefly bait composition according to claim 5, wherein the attractant is a mixture of yeast hydrolysate, honey peach extract and grape extract.
7. The home fly bait composition according to claim 6, wherein the yeast hydrolysate is 0.1 to 40% and the honey peach extract is 0.1 to 10% by mass; the content of grape extract is 0.1-10%.
8. the home fly bait composition according to any one of claims 1 to 7, wherein the home fly bait composition is in the form of gel bait or fluid bait.
9. A method of preparing a fly bait composition for home use as claimed in any one of claims 1 to 7, comprising the steps of:
Stirring systemic sanitary pesticide, sugar, sodium chloride, alkyl glycoside, citric acid, yeast hydrolysate, juicy peach extract, grape extract, octyl isothiazolinone and water accounting for 50% of the total water amount until the feed liquid is completely dissolved, heating to 50-60 ℃, and keeping the temperature for later use to obtain feed liquid A;
Adding gellan gum into the rest water, mixing, heating to above 80 ℃, adding potassium chloride, cooling to 50-60 ℃, adding the feed liquid A, fully and uniformly stirring, filling into a container, and cooling to obtain the family fly bait composition.
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