CN110542629A - Pyrolysis tar atomization level evaluation test system - Google Patents

Pyrolysis tar atomization level evaluation test system Download PDF

Info

Publication number
CN110542629A
CN110542629A CN201910934117.XA CN201910934117A CN110542629A CN 110542629 A CN110542629 A CN 110542629A CN 201910934117 A CN201910934117 A CN 201910934117A CN 110542629 A CN110542629 A CN 110542629A
Authority
CN
China
Prior art keywords
pipeline
pyrolysis tar
storage tank
oil storage
atomization
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201910934117.XA
Other languages
Chinese (zh)
Other versions
CN110542629B (en
Inventor
姚宗路
贾吉秀
郝晓文
赵立欣
丛宏斌
赵亚男
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Institute of Environment and Sustainable Development in Agriculturem of CAAS
Original Assignee
Institute of Environment and Sustainable Development in Agriculturem of CAAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Institute of Environment and Sustainable Development in Agriculturem of CAAS filed Critical Institute of Environment and Sustainable Development in Agriculturem of CAAS
Priority to CN201910934117.XA priority Critical patent/CN110542629B/en
Publication of CN110542629A publication Critical patent/CN110542629A/en
Application granted granted Critical
Publication of CN110542629B publication Critical patent/CN110542629B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N11/00Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
    • G01N11/10Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material
    • G01N11/14Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material by using rotary bodies, e.g. vane
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/02Investigating particle size or size distribution

Landscapes

  • Chemical & Material Sciences (AREA)
  • Biochemistry (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Dispersion Chemistry (AREA)
  • Investigating Or Analyzing Materials Using Thermal Means (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention discloses a pyrolysis tar atomization level evaluation test system which comprises an oil storage tank, an air storage tank, an atomization chamber and an atomization effect detection device, wherein the atomization chamber is provided with an atomization nozzle, the oil storage tank is provided with a heating device, the oil storage tank is communicated with a first port of the atomization nozzle through a first pipeline, an oil pump is arranged on the first pipeline, the air storage tank is communicated with a second port of the atomization nozzle through a second pipeline, the air storage tank is connected with an air compressor through a pipeline, the second pipeline is provided with a heating chamber, the lower end of the atomization chamber is provided with a recovery funnel, and the atomization effect detection device is used for detecting the atomization granularity of substances in the atomization chamber. By the pyrolysis tar atomization level evaluation test system, the influence of pyrolysis tar temperature, pyrolysis tar pressure, air temperature, air pressure, a pyrolysis tar modifier and an atomization nozzle on pyrolysis tar atomization can be researched, and data support is provided for full combustion of pyrolysis tar.

Description

Pyrolysis tar atomization level evaluation test system
Technical Field
The invention relates to the technical field of renewable energy sources, in particular to a pyrolysis tar atomization level evaluation test system.
Background
in recent years, attention has been paid to energy and environmental problems caused by the large-scale exploitation and utilization of fossil fuels such as coal and petroleum, and the search for a new renewable clean energy source is urgent from the viewpoint of energy development and environmental protection. The biomass energy is solar energy stored in a chemical energy form, has the characteristics of wide distribution, reproducibility and no pollution, and has high-efficiency conversion and clean utilization which are widely regarded. The main utilization mode of biomass as a renewable novel energy source is thermochemical conversion, including pyrolysis, gasification, direct combustion and the like. The byproducts such as tar and the like inevitably generated in the processes not only reduce the utilization rate of biomass resources, but also pollute and damage production equipment and the surrounding environment. However, the research finds that the biomass tar is an excellent liquid fuel and chemical industrial raw material as a pyrolysis byproduct, and the research on the chemical property and the utilization of the biomass tar can achieve the double effects of pollution treatment and resource utilization.
At present, the fuel utilization of tar generally uses tar generated by pyrolysis as fuel for combustion, and uses generated high-temperature flue gas as a heat source to provide heat for front-end pyrolysis equipment. Compared with crude oil, the biomass tar has the defects of high impurity content, high water content, low combustible component content, low heat value, high flash point and the like, so that the problems of difficult tar ignition, unstable combustion of a heating furnace, low combustion efficiency, wear of a burner, coking of an air disc, scaling of a heating surface and the like are caused. The spray combustion is carried out by adopting a pyrolysis tar spraying mode, so that the problem can be better solved. In the atomization combustion process, the quality of the fuel atomization effect is the key for determining the combustion condition. The good atomization effect is the premise of realizing high-efficiency combustion, and has very important significance for energy conservation and purification. Therefore, the components and properties of the biomass tar are analyzed, the tar atomization mechanism is clarified, the spraying characteristics and method are researched, and the mixing process of spraying and air is proved, so that the combustion is reasonably organized, and the method is of great importance for improving the tar combustion efficiency.
Disclosure of Invention
The invention aims to provide a pyrolysis tar atomization level evaluation test system, which is used for solving the problems in the prior art, exploring the influence of pyrolysis tar temperature, pyrolysis tar pressure, air temperature and air pressure, a pyrolysis tar modifier and an atomization nozzle on pyrolysis tar atomization, and providing data support for full combustion of pyrolysis tar.
In order to achieve the purpose, the invention provides the following scheme:
The invention provides a pyrolysis tar atomization level evaluation test system which comprises an oil storage tank, an air storage tank, an atomization chamber and an atomization effect detection device, wherein the atomization chamber is provided with an atomization nozzle, the atomization nozzle is detachably connected with the atomization chamber, the oil storage tank is provided with a heating device, the oil storage tank is communicated with a first port of the atomization nozzle through a first pipeline, an oil pump is arranged on the first pipeline, the air storage tank is communicated with a second port of the atomization nozzle through a second pipeline, the air storage tank is connected with an air compressor through a pipeline, the second pipeline is provided with a heating chamber, the lower end of the atomization chamber is provided with a recovery funnel, and the atomization effect detection device is used for detecting the atomization granularity and the cumulative distribution condition of substances in the atomization chamber.
Preferably, a first manual pyrolysis tar valve, a second manual pyrolysis tar valve, a first Y-shaped filter and a first basket filter are arranged on the first pipeline between the oil storage tank and the oil pump, and an oil pressure gauge and a first pyrolysis tar electromagnetic valve are arranged on the first pipeline between the oil pump and the first port of the atomizer.
Preferably, the system further comprises a fourth pipeline, one end of the fourth pipeline is communicated with the first pipeline between the first manual pyrolysis tar valve and the second manual pyrolysis tar valve, the other end of the fourth pipeline is communicated with the first pipeline between the first basket filter and the oil pump, and the fourth pipeline is provided with a third manual pyrolysis tar valve, a second Y-type filter and a second basket filter.
Preferably, the device further comprises a fifth pipeline, one end of the fifth pipeline is communicated with the first pipeline between the first manual pyrolysis tar valve and the second manual pyrolysis tar valve, the other end of the fifth pipeline is communicated with the outside, and a fourth manual pyrolysis tar valve is arranged on the fifth pipeline.
Preferably, the device also comprises a third pipeline, wherein one end of the third pipeline is communicated with the oil storage tank, the other end of the third pipeline is communicated with the first pipeline, and a second pyrolysis tar electromagnetic valve is arranged on the third pipeline; the first pipeline with the third pipeline outside all wraps up heat preservation device, heat preservation device includes heating wire and asbestos heat preservation, the heating wire winding is in the first pipeline with on the third pipeline, the asbestos heat preservation parcel is in the heating wire outside.
preferably, a heating sleeve is arranged outside the oil storage tank, an end cover is arranged at the upper end of the oil storage tank, the end cover is hermetically connected with the oil storage tank, a chemical feeding port is formed in the end cover, a stirring device is arranged on the oil storage tank, the stirring device comprises a stirring shaft, a stirring paddle and a driving motor, the stirring shaft penetrates through the end cover and extends into the oil storage tank, the stirring paddle is arranged at the lower end of the stirring shaft, the driving motor is arranged at the upper end of the stirring shaft and located outside the oil storage tank, and the driving motor is used for driving the stirring paddle to rotate; the end cover is provided with a viscometer which penetrates through the end cover and is used for measuring the viscosity in the oil storage tank, and the oil storage tank is also internally provided with a thermocouple which is used for measuring the temperature of the pyrolysis tar in the oil storage tank; the oil storage tank, the end cover, the stirring shaft and the stirring paddle are all made of stainless steel.
Preferably, a first manual gas valve, a gas pressure reducing valve, a flow meter and a pressure gauge are arranged on the second pipeline between the gas storage tank and the heating chamber, and a first manual gas control valve is arranged on the second pipeline between the heating chamber and the second port of the atomizing spray head.
Preferably, the pneumatic control valve further comprises a sixth pipeline, one end of the sixth pipeline is communicated with the first pipeline, the other end of the sixth pipeline is communicated with the second pipeline, and a second pneumatic manual control valve is arranged on the sixth pipeline.
preferably, the atomizing chamber is made of transparent glass, a sliding cover is arranged at the upper end of the atomizing chamber, the sliding cover is connected with the atomizing chamber in a sliding mode through a sliding groove in the upper end of the atomizing chamber, and an air hole is formed in the middle of the sliding cover.
Preferably, atomization effect detection device includes particle size analyzer transmitter, particle size analyzer receiver and three-dimensional moving platform, three-dimensional moving platform includes horizontal structure and vertical structure, particle size analyzer transmitter with particle size analyzer receiver sets up relatively and is located same water flat line, the atomizer chamber is located particle size analyzer transmitter with between the particle size analyzer receiver, particle size analyzer transmitter with particle size analyzer receiver is located respectively horizontal structure's both ends, vertical structure lower extreme is provided with the universal wheel.
Compared with the prior art, the invention has the following technical effects:
The first pipeline for conveying the pyrolysis tar and the second pipeline for conveying the gas are two independent pipelines, the temperature of the pyrolysis tar is changed through a heating device of an oil storage tank, the pressure of the pyrolysis tar is changed through an oil pump, the temperature of the air is changed through a heating chamber, the pressure of the air is changed through an air compressor, different pyrolysis tar modifiers are added into the oil storage tank, different atomizing spray heads are replaced, the pyrolysis tar and the air with different temperature and pressure conditions are sprayed into the atomizing chamber through the different atomizing spray heads, the atomizing effect under different conditions is detected through an atomizing effect detection device, the influence of the temperature, the pressure, the air temperature, the air pressure, the pyrolysis tar modifier and the atomizing spray heads on the atomization of the pyrolysis tar can be researched, and data support is provided for the sufficient combustion of the pyrolysis tar.
Drawings
in order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings needed in the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art to obtain other drawings without creative efforts.
FIG. 1 is a schematic structural view of a pyrolysis tar atomization level evaluation test system of the present invention;
FIG. 2 is a schematic view of an atomization chamber and an atomization effect monitoring device in accordance with the present invention;
FIG. 3 is a schematic cross-sectional view of a third conduit in accordance with the present invention;
Wherein: 101-oil storage tank, 102-end cap, 103-stirring device, 104-heating jacket, 105-viscometer, 106-thermocouple; 201- -a third pipeline, 202- -a heat preservation device, 203- -a second manual valve for pyrolysis tar, 204- -a first Y-type filter, 205- -a first basket filter, 206- -an oil pump, 207- -a second electromagnetic valve for pyrolysis tar, 208- -an oil pressure gauge, 209- -a first pipeline, 210- -a fourth pipeline, 211- -a fifth pipeline, 212- -a first electromagnetic valve for pyrolysis tar, 213- -a third manual valve for pyrolysis tar, 214- -a second Y-type filter, 215- -a second basket filter, 216- -a first manual valve for pyrolysis tar, 217- -a fourth manual valve for pyrolysis tar; 301-air compressor, 302-air storage tank, 303-first manual gas valve, 304-gas pressure reducing valve, 305-flowmeter, 306-air pressure gauge, 307-heating chamber, 308-second manual gas control valve, 309-first manual gas control valve, 310-second pipeline, 311-sixth pipeline; 401-atomizer, 402-slide, 403-atomizer chamber, 404-recovery funnel; 501-particle size analyzer transmitter, 502-particle size analyzer receiver, 503-three-dimensional moving platform.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without inventive effort based on the embodiments of the present invention, are within the scope of the present invention.
The invention aims to provide a pyrolysis tar atomization level evaluation test system, which is used for solving the problems in the prior art, exploring the influence of pyrolysis tar temperature, pyrolysis tar pressure, air temperature and air pressure, a pyrolysis tar modifier and an atomization nozzle on pyrolysis tar atomization, and providing data support for full combustion of pyrolysis tar.
In order to make the aforementioned objects, features and advantages of the present invention comprehensible, embodiments accompanied with figures are described in further detail below.
As shown in fig. 1-3: this embodiment provides a pyrolysis tar atomization level evaluation test system, including oil storage tank 101, gas holder 302, atomizer 403 and atomization effect detection device, atomizer 403 is provided with atomizer 401, oil storage tank 101 is provided with heating device, oil storage tank 101 communicates through first pipeline 209 with atomizer 401's first port, be provided with oil pump 206 on the first pipeline 209, oil pump 206 provides power and control pyrolysis tar flow, carry the pyrolysis tar after will preheating to atomizer 403, gas holder 302 communicates through second pipeline 310 with atomizer 401's second port, gas holder 302 has air compressor 301 through the pipe connection, be provided with heating chamber 307 on the second pipeline 310, atomizer 403 lower extreme is provided with recovery funnel 404, atomization effect detection device is used for detecting the atomized particles degree and the cumulative distribution condition of the interior material of atomizer 403. The first pipeline 209 and the second pipeline 310 of carrier gas that this embodiment carried pyrolysis tar are two independent pipelines, the heating device through oil storage tank 101 changes the temperature of pyrolysis tar, the pressure of pyrolysis tar is changed through oil pump 206, the temperature of air is changed through heating chamber 307, the pressure of air is changed through air compressor machine 301, with different temperatures, the pyrolysis tar of pressure condition and air spout into atomizer 403 through different atomizer 401, detect the atomization effect under the different condition through atomization effect detection device, pyrolysis tar temperature can be researched, pyrolysis tar pressure, air temperature, air pressure, pyrolysis tar modifier and atomizer 401 are to the atomizing influence of pyrolysis tar, provide data support for the abundant burning of pyrolysis tar.
in this embodiment, a first pipeline 209 between the oil storage tank 101 and the oil pump 206 is provided with a first manual pyrolysis tar valve 216, a second manual pyrolysis tar valve 203, a first Y-shaped filter 204 and a first basket filter 205, the first Y-shaped filter 204 and the first basket filter 205 perform filtration cleaning, dust removal, impurity removal and decoking on pyrolysis tar in the pipeline, an oil pressure gauge 208 and a first electromagnetic pyrolysis tar valve 212 are arranged on the first pipeline 209 between the oil pump 206 and the first port of the atomizer 401, and the oil pressure gauge 208 is used for detecting the pressure of the pyrolysis tar in the pipeline.
The embodiment further comprises a fourth pipeline 210, one end of the fourth pipeline 210 is communicated with a first pipeline 209 between the first manual valve 216 for pyrolysis tar and the second manual valve 203 for pyrolysis tar, the other end of the fourth pipeline 210 is communicated with a first pipeline 209 between the first basket filter 205 and the oil pump 206, a third manual valve 213 for pyrolysis tar, a second Y-shaped filter 214 and a second basket filter 215 are arranged on the fourth pipeline 210, and the second Y-shaped filter 214 and the second basket filter 215 are used for filtering, cleaning, dedusting, impurity removing and coke removing pyrolysis tar in the pipeline. The third manual pyrolysis tar valve 213, the second Y-shaped filter 214 and the second basket filter 215 on the fourth pipeline 210 can be replaced when the second manual pyrolysis tar valve 203, the first Y-shaped filter 204 and the first basket filter 205 on the first pipeline 209 cannot be used normally, so as to ensure that the device can work normally.
The embodiment further comprises a fifth pipeline 211, one end of the fifth pipeline 211 is communicated with the first pipeline 209 between the first manual pyrolysis tar valve 216 and the second manual pyrolysis tar valve 203, the other end of the fifth pipeline 211 is communicated with the outside, and a fourth manual pyrolysis tar valve 217 is arranged on the fifth pipeline 211. The second manual pyrolysis tar valve 203 and the third manual pyrolysis tar valve 213 are closed, and the first manual pyrolysis tar valve 216 and the fourth manual pyrolysis tar valve 217 are opened, so that the pyrolysis tar in the oil tank 101 can be discharged.
The embodiment also comprises a third pipeline 201, wherein one end of the third pipeline 201 is communicated with the oil storage tank 101, the other end of the third pipeline 201 is communicated with the first pipeline 209, and a second pyrolysis tar electromagnetic valve 207 is arranged on the third pipeline 201; the heat preservation device 202 is wrapped on the outer sides of the first pipeline 209 and the third pipeline 201, the heat preservation device 202 comprises heating wires and asbestos heat preservation layers, the heating wires are wound on the first pipeline 209 and the third pipeline 201, the asbestos heat preservation layers are wrapped on the outer sides of the heating wires, and the heat preservation device 202 ensures that pyrolysis tar of the first pipeline 209 and the third pipeline 201 cannot block pipelines due to temperature reduction in the conveying process.
In this embodiment, a heating jacket 104 is disposed outside the oil storage tank 101, the heating jacket 104 is sleeved outside the oil storage tank 101 and detachably connected to the oil storage tank 101, an end cover 102 is disposed at the upper end of the oil storage tank 101, the end cover 102 is hermetically connected to the oil storage tank 101, a chemical feeding port is disposed on the end cover 102, the chemical feeding port is used for feeding a modifying agent into the oil storage tank 101, a stirring device 103 is disposed on the oil storage tank 101, the stirring device 103 includes a stirring shaft, a stirring paddle and a driving motor, the stirring shaft penetrates through the end cover 102 and extends into the oil storage tank 101, the stirring paddle is disposed at the lower end of the stirring shaft, the driving motor is disposed at the upper end of the stirring shaft and is located outside the oil storage tank 101, the driving motor is used for driving the stirring paddle to rotate, the stirring paddle can cause the pyrolysis tar and the modifying agent to be uniformly mixed, and can also enhance the, the homogeneous liquid state of the pyrolysis tar can be kept by matching with the stirring paddle; the end cover 102 is provided with a viscometer 105, the viscometer 105 penetrates through the end cover 102 and is used for measuring the viscosity in the oil storage tank 101, the viscometer 105 adopts a digital rotational viscometer and can carry out continuous measurement, and a liquid crystal screen directly displays data such as the viscosity, the rotating speed and the like; a thermocouple 106 is also arranged in the oil storage tank 101, and the thermocouple 106 is used for measuring the temperature of the pyrolysis tar in the oil storage tank 101; the oil storage tank 101, the end cover 102, the stirring shaft and the stirring paddle are all made of stainless steel, and the oil storage tank has the characteristics of corrosion resistance and easiness in cleaning.
In this embodiment, a first manual gas valve 303, a gas pressure reducing valve 304, a flow meter 305 and a pressure gauge 306 are arranged on a second pipeline 310 between the gas storage tank 302 and the heating chamber 307, a first manual gas control valve 309 is arranged on the second pipeline 310 between the heating chamber 307 and the second port of the atomizer 401, the gas pressure reducing valve 304 is used for reducing the pressure of air, the flow meter 305 is used for measuring the flow rate of gas in the second pipeline 310, and the pressure gauge 306 is used for measuring the pressure of gas in the second pipeline 310. The structure on the second line 310 ensures that a precisely metered amount of gas is accurately delivered to the nebulizing chamber 403. The heating chamber 307 heats the filtered air to prevent the condensation of the pyrolysis tar after the cold air is mixed with the pyrolysis tar. An air filter is also disposed on the second pipeline 310 for filtering air.
The embodiment further comprises a sixth pipeline 311, one end of the sixth pipeline 311 is communicated with the first pipeline 209, the other end of the sixth pipeline 311 is communicated with the second pipeline 310, and the sixth pipeline 311 is provided with a second pneumatic manual control valve 308. In this embodiment, each pipeline is stainless steel pipeline, can prevent to corrode and easy the washing.
In this embodiment, the atomizing chamber 403 is made of transparent glass, which is convenient for observation, the upper end of the atomizing chamber 403 is provided with the sliding cover 402, the sliding cover 402 is slidably connected with the atomizing chamber 403 through the sliding groove at the upper end of the atomizing chamber 403, the middle part of the sliding cover 402 is provided with the air hole, the air hole can balance the pressure in the atomizing chamber 403, the container is arranged below the atomizer, and the pyrolysis tar is collected into the container through the recovery funnel 404 below the atomizing chamber 403.
In this embodiment, the atomization effect detection apparatus includes a particle size analyzer and a three-dimensional moving platform 503, the particle size analyzer is in the prior art, the particle size analyzer includes a particle size analyzer transmitter 501 and a particle size analyzer receiver 502, and the particle size analyzer is connected to a computer and can generate a particle size distribution diagram on a computer interface. The three-dimensional moving platform 503 of this embodiment can make the atomization effect detection device move in a three-dimensional space, and can measure the particle size distribution of the atomization section in the whole process. Three-dimensional moving platform 503 includes horizontal structure and vertical structure, and particle size analyzer transmitter 501 and particle size analyzer receiver 502 set up relatively and are located same water flat line, and atomizer chamber 403 is located between particle size analyzer transmitter 501 and particle size analyzer receiver 502, and particle size analyzer transmitter 501 and particle size analyzer receiver 502 are located horizontal structure's both ends respectively, and the vertical structure lower extreme is provided with the universal wheel, can change atomization effect detection device's position through the universal wheel. In this embodiment, the horizontal structure and the vertical structure are both retractable structures, the horizontal structure can be adjusted according to the size of the atomizing chamber 403, the vertical structure can be adjusted according to the height of the atomizing chamber 403 and the height of the atomizing nozzle 401,
in this embodiment, atomizer 401 is detachable construction, can change different atomizer 401 according to the needs of difference, obtains different atomization effect, can change pressure atomizing nozzle or air atomizing nozzle as required, wherein pressure atomizing nozzle oil pressure 1.2 ~ 2.0MPa, atomizing angle 45 ~ 60, air atomizing nozzle oil pressure 0.05 ~ 0.1MPa, atmospheric pressure >0.5 MPa.
When the pyrolytic tar atomization level evaluation test system is used, pyrolytic tar and related modifying agents are added into an oil storage tank 101 with good sealing performance for preheating, the temperature of the pyrolytic tar is controlled to be about 100 ℃ by a heating sleeve 104, a mixture is uniformly stirred by a stirring device 103, and the viscosity of the pyrolytic tar is measured by a viscometer 105; then, a first manual pyrolysis tar valve 216 and a second manual pyrolysis tar valve 203 are opened, pyrolysis tar flows into the first pipeline 209 from the oil storage tank 101, is filtered and cleaned through the first Y-shaped filter 204 and the first basket filter 205, and a certain amount of pyrolysis tar is conveyed to the tail end of the pipeline through the oil pump 206; meanwhile, a first gas manual valve 303 of a second pipeline 310 is opened, air is conveyed into an air filter for filtering by an air storage tank 302 under the action of an air compressor 301, then the flow rate of the air is controlled by a flowmeter 305, the gas pressure is controlled by a gas pressure gauge 306 and a gas pressure reducing valve 304, and the air is heated by a heating chamber 307, so that the air with certain pressure, flow rate and temperature and the liquid pyrolysis tar conveyed by the first pipeline 209 are injected into an atomizing chamber 403 through an atomizing nozzle 401; the particle size analyzer analyzes the atomization condition in the atomization chamber 403 through the three-dimensional mobile platform 503 in different directions and angles through the glass chamber wall of the atomization chamber 403, and uploads data information to a computer terminal, and finally, researchers obtain evaluation results through data analysis; the atomized pyrolysis tar flows into the oil drum through the recovery hopper 404 for recovery.
Compared with the prior art, the embodiment has the following advantages:
1. The method can evaluate the atomization level of the pyrolysis tar, explore the influence of parameters such as pyrolysis tar temperature, atomization pressure, air temperature, pyrolysis tar modifier (such as blending with diesel oil, gasoline and ethanol or cyclic blending modification) and atomizer on the atomization of the pyrolysis tar, is suitable for analyzing the atomization level of the biomass pyrolysis tar under different conditions, is beneficial to optimizing atomization process parameters, and provides data support for the sufficient combustion of the pyrolysis tar;
2. The pyrolysis tar atomization level evaluation test system can realize temperature regulation (0-100 ℃), oil pressure regulation (0.2-1.0 MPa) and air pressure regulation (0.2-0.8 MPa);
3. The atomization effect monitoring device in the embodiment can realize multi-azimuth and multi-angle atomization particle detection, so that the atomization effect detection is more reliable;
4. The embodiment utilizes pyrolysis tar to preheat to 100 ℃ in the oil storage tank 101 at the higher performance that the mobility is better of temperature in the certain limit, sets up heat preservation device 202 at pyrolysis tar conveying line simultaneously to guarantee that pyrolysis tar can not block up the pipeline in transportation process, and the required pyrolysis tar volume of transport that can be accurate.
The principle and the implementation mode of the present invention are explained by applying specific examples in the present specification, and the above descriptions of the examples are only used to help understanding the method and the core idea of the present invention; meanwhile, for a person skilled in the art, according to the idea of the present invention, the specific embodiments and the application range may be changed. In view of the above, the present disclosure should not be construed as limiting the invention.

Claims (10)

1. The utility model provides a pyrolysis tar atomization level appraises test system which characterized in that: including oil storage tank, gas holder, atomizer chamber and atomization effect detection device, the atomizer chamber is provided with atomizer, atomizer with the connection can be dismantled to the atomizer chamber, the oil storage tank is provided with heating device, the oil storage tank with atomizer's first port is through first pipeline intercommunication, be provided with the oil pump on the first pipeline, the gas holder with atomizer's second port is through second pipeline intercommunication, the gas holder has the air compressor machine through the pipe connection, be provided with the heating chamber on the second pipeline, the atomizer chamber lower extreme is provided with retrieves the funnel, atomization effect detection device is used for detecting the atomizing granularity and the accumulation distribution condition of material in the atomizer chamber.
2. The pyrolysis tar atomization level evaluation test system of claim 1, wherein: the oil-gas separation device is characterized in that a first pipeline between the oil storage tank and the oil pump is provided with a first manual pyrolysis tar valve, a second manual pyrolysis tar valve, a first Y-shaped filter and a first basket type filter, and an oil pressure gauge and a first pyrolysis tar electromagnetic valve are arranged on the first pipeline between the oil pump and the first port of the atomizing spray head.
3. The pyrolysis tar atomization level evaluation test system of claim 2, wherein: the oil pump is characterized by further comprising a fourth pipeline, one end of the fourth pipeline is communicated with the first pipeline between the first manual pyrolysis tar valve and the second manual pyrolysis tar valve, the other end of the fourth pipeline is communicated with the first pipeline between the first basket type filter and the oil pump, and the fourth pipeline is provided with a third manual pyrolysis tar valve, a second Y-type filter and a second basket type filter.
4. The pyrolysis tar atomization level evaluation test system of claim 2, wherein: the device is characterized by further comprising a fifth pipeline, wherein one end of the fifth pipeline is communicated with the first pipeline between the first manual pyrolysis tar valve and the second manual pyrolysis tar valve, the other end of the fifth pipeline is communicated with the outside, and a fourth manual pyrolysis tar valve is arranged on the fifth pipeline.
5. The pyrolysis tar atomization level evaluation test system of claim 1, wherein: the device also comprises a third pipeline, wherein one end of the third pipeline is communicated with the oil storage tank, the other end of the third pipeline is communicated with the first pipeline, and a second pyrolysis tar electromagnetic valve is arranged on the third pipeline; the first pipeline with the third pipeline outside all wraps up heat preservation device, heat preservation device includes heating wire and asbestos heat preservation, the heating wire winding is in the first pipeline with on the third pipeline, the asbestos heat preservation parcel is in the heating wire outside.
6. The pyrolysis tar atomization level evaluation test system of claim 1, wherein: the heating device comprises an oil storage tank, and is characterized in that a heating sleeve is arranged outside the oil storage tank, an end cover is arranged at the upper end of the oil storage tank, the end cover is hermetically connected with the oil storage tank, a chemical feeding port is formed in the end cover, a stirring device is arranged on the oil storage tank, the stirring device comprises a stirring shaft, a stirring paddle and a driving motor, the stirring shaft penetrates through the end cover and extends into the oil storage tank, the stirring paddle is arranged at the lower end of the stirring shaft, the driving motor is arranged at the upper end of the stirring shaft and is positioned outside the oil storage tank, and the driving motor is used for driving the stirring paddle; the end cover is provided with a viscometer which penetrates through the end cover and is used for measuring the viscosity in the oil storage tank, and the oil storage tank is also internally provided with a thermocouple which is used for measuring the temperature of the pyrolysis tar in the oil storage tank; the oil storage tank, the end cover, the stirring shaft and the stirring paddle are all made of stainless steel.
7. the pyrolysis tar atomization level evaluation test system of claim 1, wherein: a first manual gas valve, a gas pressure reducing valve, a flow meter and a barometer are arranged on the second pipeline between the gas storage tank and the heating chamber, and a first manual gas control valve is arranged on the second pipeline between the heating chamber and the second port of the atomizing spray head.
8. The pyrolysis tar atomization level evaluation test system of claim 1, wherein: the pneumatic control valve further comprises a sixth pipeline, one end of the sixth pipeline is communicated with the first pipeline, the other end of the sixth pipeline is communicated with the second pipeline, and a second pneumatic manual control valve is arranged on the sixth pipeline.
9. the pyrolysis tar atomization level evaluation test system of claim 1, wherein: the atomizer chamber is made of transparent glass, a sliding cover is arranged at the upper end of the atomizer chamber, the sliding cover passes through a sliding groove at the upper end of the atomizer chamber and is in sliding connection with the atomizer chamber, and an air hole is formed in the middle of the sliding cover.
10. The pyrolysis tar atomization level evaluation test system of claim 1, wherein: atomization effect detection device includes particle size analyzer transmitter, particle size analyzer receiver and three-dimensional moving platform, three-dimensional moving platform includes horizontal structure and vertical structure, particle size analyzer transmitter with the particle size analyzer receiver sets up relatively and is located same water flat line, the atomizer chamber is located particle size analyzer transmitter with between the particle size analyzer receiver, particle size analyzer transmitter with the particle size analyzer receiver is located respectively horizontal structure's both ends, vertical structure lower extreme is provided with the universal wheel.
CN201910934117.XA 2019-09-29 2019-09-29 Pyrolysis tar atomization level evaluation test system Active CN110542629B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910934117.XA CN110542629B (en) 2019-09-29 2019-09-29 Pyrolysis tar atomization level evaluation test system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910934117.XA CN110542629B (en) 2019-09-29 2019-09-29 Pyrolysis tar atomization level evaluation test system

Publications (2)

Publication Number Publication Date
CN110542629A true CN110542629A (en) 2019-12-06
CN110542629B CN110542629B (en) 2024-02-13

Family

ID=68715014

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910934117.XA Active CN110542629B (en) 2019-09-29 2019-09-29 Pyrolysis tar atomization level evaluation test system

Country Status (1)

Country Link
CN (1) CN110542629B (en)

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20100097484A (en) * 2009-02-26 2010-09-03 최이교 Combustion device for mixed fuel ana water
CN205402707U (en) * 2016-03-10 2016-07-27 南阳市亚龙筑路机械制造有限公司 Medium bubble atomizing heavy oil burner
CN107620957A (en) * 2017-08-30 2018-01-23 昆明理工大学 A kind of industrial furnace high-efficient atomizing combustion system and its method based on high viscosity biomass fuel
CN108397773A (en) * 2018-03-02 2018-08-14 农业部规划设计研究院 A kind of mixed combustion equipment of biomass pyrolytic oil gas
CN109835938A (en) * 2019-03-20 2019-06-04 金川集团股份有限公司 A kind of device and its application method for copper nitrate solution spray pyrolysis
CN110057570A (en) * 2019-05-27 2019-07-26 中船动力研究院有限公司 A kind of experimental rig and test method for the test of urea pulverability
CN210604285U (en) * 2019-09-29 2020-05-22 中国农业科学院农业环境与可持续发展研究所 Pyrolysis tar atomization level evaluation test system

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20100097484A (en) * 2009-02-26 2010-09-03 최이교 Combustion device for mixed fuel ana water
CN205402707U (en) * 2016-03-10 2016-07-27 南阳市亚龙筑路机械制造有限公司 Medium bubble atomizing heavy oil burner
CN107620957A (en) * 2017-08-30 2018-01-23 昆明理工大学 A kind of industrial furnace high-efficient atomizing combustion system and its method based on high viscosity biomass fuel
CN108397773A (en) * 2018-03-02 2018-08-14 农业部规划设计研究院 A kind of mixed combustion equipment of biomass pyrolytic oil gas
CN109835938A (en) * 2019-03-20 2019-06-04 金川集团股份有限公司 A kind of device and its application method for copper nitrate solution spray pyrolysis
CN110057570A (en) * 2019-05-27 2019-07-26 中船动力研究院有限公司 A kind of experimental rig and test method for the test of urea pulverability
CN210604285U (en) * 2019-09-29 2020-05-22 中国农业科学院农业环境与可持续发展研究所 Pyrolysis tar atomization level evaluation test system

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
兰珊;赵立欣;姚宗路;丛宏斌;郭占斌;: "外加热式生物质连续热解设备燃气净化系统的研究", 现代化工, no. 05 *

Also Published As

Publication number Publication date
CN110542629B (en) 2024-02-13

Similar Documents

Publication Publication Date Title
CN202256220U (en) Evaluation device for researching thermal coking and scale deposition of heavy hydrocarbon oil
CN210604285U (en) Pyrolysis tar atomization level evaluation test system
WO2021129022A1 (en) Biomass-based long-chain alcohol ether oxygen-containing additive, preparation method therefor and application thereof
CN211201912U (en) Device for evaluating wellbore sand production and prevention during hydrate exploitation by CO2/N2 displacement method
CN1601265A (en) Analyzer for analyzing moisture in ground conductance
CN106468645B (en) Heavy oil coking tendency evaluation device and heavy oil coking tendency evaluation method
CN110542629A (en) Pyrolysis tar atomization level evaluation test system
CN110542630B (en) Pyrolysis tar atomization level evaluation test method
CN103131453B (en) Pyrolytic evaluation device for carbon-containing substances
CN104498099A (en) Gasifier burner and application method thereof, and gasifier containing gasifier burner
CN219016163U (en) Online measuring device for water content of crude oil of oil well
CN202119691U (en) Samper for detecting oil content and dust content in coke oven gas
CN205353083U (en) Experimental device for super thick crude oil oxygenated fuel deposit
CN200952994Y (en) Apparatus for measuring high temperature and high-pressure oil-coal-slurry viscosity
CN209636597U (en) A kind of highway engineering asphalt mortar, bituminous mortar mixing plant
CN206935053U (en) A kind of oil liquefied gas desulfurizing tower
CN207571084U (en) Laboratory prepares the experimental provision of isooctane
CN216837832U (en) Naphtha raw materials desulfurization acid dip pickle
CN108872526A (en) A kind of rapid detection method of coal stability
CN107805521B (en) Method and device for evaluating direct coal liquefaction reaction characteristics
CN204314178U (en) A kind of dynamic stability test device of Cemented filling coal water mixture
CN104910947B (en) A kind of continuous feed, the safety and environmental protection oil refining apparatus of the waste and old organic cracking regeneration of deslagging and technique
CN203174038U (en) Evaluation device for pyrolysis of carbon-containing matter
CN106244254B (en) Biomass boiler fuel oil production technology and device
CN209076644U (en) A kind of equipment preventing catalysis feed nozzle internal surface of sleeve pipe coking

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant