CN110522680A - A kind of skin care item carrier and preparation method thereof - Google Patents

A kind of skin care item carrier and preparation method thereof Download PDF

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Publication number
CN110522680A
CN110522680A CN201910650183.4A CN201910650183A CN110522680A CN 110522680 A CN110522680 A CN 110522680A CN 201910650183 A CN201910650183 A CN 201910650183A CN 110522680 A CN110522680 A CN 110522680A
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CN
China
Prior art keywords
water
carrier
parts
collagen
hectorite
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910650183.4A
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Chinese (zh)
Inventor
吕晓敏
谢铁强
吕集贤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangzhou Yaxin Cosmetics Co Ltd
Original Assignee
Guangzhou Yaxin Cosmetics Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guangzhou Yaxin Cosmetics Co Ltd filed Critical Guangzhou Yaxin Cosmetics Co Ltd
Priority to CN201910650183.4A priority Critical patent/CN110522680A/en
Publication of CN110522680A publication Critical patent/CN110522680A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • A61K8/9717Rhodophycota or Rhodophyta [red algae], e.g. Porphyra
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin

Abstract

The invention discloses a kind of skin care item carriers and preparation method thereof.The carrier is made of 10 parts of Chondrus crispus extract, 1 part of collagen, 5-15 parts of hectorite.Preparation method is to be uniformly mixed dissolution of raw material, the newborn paste that it is by mass percentage 4%-10% containing total solid that mixture, which is added water and is diluted to,;Newborn paste is placed in closed container, 70-90 DEG C of heating, until static at transparent nonfluid jelly, stirring, at transparent fluid glue;Be freeze-dried into solid to get.Skin care item carrier of the invention has the advantages of uniform, to stablize, promote the stability of product, improve product efficacy.

Description

A kind of skin care item carrier and preparation method thereof
Technical field
The present invention relates to a kind of skin care item carriers and preparation method thereof.
Background technique
Chondrus crispus extract be allow in national skin care or cosmetic material catalogue using natural polymer raw material One of, for from pure natural oceanic product, main includes the polysaccharide component in seaweed, unique skin sense.With highly-water-soluble, can make Make transparent aqua product.It can promote skin metabolism, and stimulation fibrocyte manufactures more colloids, elasticin matter And mucopolysaccharide etc., promote epidermal growth, boost metabolism, prevents skin aging.Cost performance is high.Natural smell.Without spy Different bad smell, easily with other raw material fusion applications.Safe without toxic side effect.The product is free of toxin, edible.Oil is equal Wherein, then becoming emulsion not needs using emulsifier for even distribution.Increase into quality sense and viscosity.Can be used for facial mask, cream and Toner etc., as moisturizer, thickener and aqueous medium.Smooth skin sense, have after skin care item, face cleaning can be allowed to wash away it is soft and moist, Smooth skin sense.External application is safe and non-stimulating.It can be directly as gel, facial mask in face and eye, non-stimulated and sensitization.
Collagen is that have good biocompatibility, trophism, prosthetic, guarantor from the intracorporal class protein of animal Moist, compatibility, so being widely used in biomedical material, cosmetics etc..Collagen is also that cosmetic material catalogue is recorded Allow using raw material.
Hectorite be also allow in national cosmetic raw material catalogue using natural inorganic mineral raw material, have layered crystal Structure.It has excellent hydrophilic swelling and suspension thixotropy, can disperse well in water.It is usually used in skin care or cosmetics Cream, control thixotropy in type of latex type product and improve viscosity, additionally it is possible to improve the skin sense of cosmetics, and there is moisturizing, increase The white effect with reparation skin.
Currently, cosmetics such as cream is refreshing etc., be mostly by various raw materials by being suspended, mixing, the processes such as emulsification be simply mixed and At the stability (stability including physical stability and functional product) of product is poor, and technology content is not high, influences product effect With.
Summary of the invention
For overcome the deficiencies in the prior art, it is an object of that present invention to provide a kind of skin care item carrier and its preparation side Method, this carrier can be used as the cosmetics such as eye cream, face cream, the carrier of skin care product or matrix, can be fused with other compositions, dispersion Property and excellent in stability.
Support material of the invention by following mass ratio material composition, 10 parts of Chondrus crispus extract, 1 part of collagen, 5-15 parts of hectorite compositions.
Preparation method the following steps are included:
1, Chondrus crispus extract is dissolved in water, collagen is dissolved in water, and hectorite adds water dispersion agglutination;
2, above-mentioned three kinds of solution is mixed, is diluted with water to by mass percentage, total solid 4%-10%, mixed Uniformly, until forming the newborn paste of white;
3, the newborn paste of the white is placed in closed container, 70-90 DEG C of heating, until static gluey at transparent nonfluid Object, stirring, at transparent fluid glue;Be freeze-dried into solid to get.
Optimum ratio: 10 parts of Chondrus crispus extract, 1 part of collagen, 10 parts of hectorite be made.
The total solid of step (2) is preferably 10%, and (3 heating temperatures are preferably 90 DEG C to step.
In use, it is spare water can be added as needed to form fluid glue.
This carrier has the advantages of uniform, to stablize, promote the stability of product, improve product efficacy.
Specific embodiment
It elaborates combined with specific embodiments below to the present invention, but the present invention is not limited thereto.
The preparation of 1 carrier 1 of embodiment
Chondrus crispus extract is dissolved in water heating by 10 parts of Chondrus crispus extract, 1 part of collagen, 5 parts of hectorite It is substantially soluble in water, collagen is dissolved in water, and the water-dispersible agglutination of hectorite takes above-mentioned sample to be mixed respectively, water is added to make always Solid is 4%, starts to generate White Flocculus when stirring, continues to stir evenly, and white newborn paste is generated, then in closed It is heated in container in 70 DEG C, after about 5 hours, becomes mobility liquid shape, after continuing heating about 20 hours, become static state at saturating Bright nonfluid jelly, stirring, then at transparent thick colloidal fluid.It after sampling freeze-drying, adds water and stirs again, restores glue Shape.
The preparation of 2 carrier 2 of embodiment
Chondrus crispus extract is dissolved in water heating by 10 parts of Chondrus crispus extract, 1 part of collagen, 5 parts of hectorite It is substantially soluble in water, collagen is dissolved in water, and the water-dispersible agglutination of hectorite takes above-mentioned sample to be mixed respectively, water is added to make always Solid is 4%, starts to generate White Flocculus when stirring, continues to stir evenly, and white newborn paste is generated, then in closed It is heated in container in 90 DEG C, after about 3 hours, becomes mobility liquid shape, after continuing heating about 12 hours, become static state at saturating Bright nonfluid jelly, stirring, then at transparent thick colloidal fluid.It after sampling freeze-drying, adds water and stirs again, restores glue Shape.
The preparation of 3 carrier 3 of embodiment
10 parts of Chondrus crispus extract, 1 part of collagen, 15 parts of hectorite, Chondrus crispus extract is dissolved in water Heat is substantially soluble in water, and collagen is dissolved in water, and the water-dispersible agglutination of hectorite takes above-mentioned sample to be mixed respectively, water is added to make Total solid is 6%, starts to generate White Flocculus when stirring, continues to stir evenly, and white newborn paste is generated, then in close Close in container and heated in 70 DEG C, after about 5 hours, become mobility liquid shape, after continuing heating about 20 hours, become it is static at Transparent elastic solid colloidal object, stirring, then at transparent very thick colloidal fluid.After sampling freeze-drying, add water and stir again, Restore gluey.
The preparation of 4 carrier 4 of embodiment
Chondrus crispus extract is dissolved in water heating by 10 parts of Chondrus crispus extract, 1 part of collagen, 5 parts of hectorite It is substantially soluble in water, collagen is dissolved in water, and the water-dispersible agglutination of hectorite takes above-mentioned sample to be mixed respectively, water is added to make always Solid is 10%, starts to generate White Flocculus when stirring, continues to stir evenly, and white newborn paste is generated, then in closed It is heated in container in 90 DEG C, after about 3 hours, becomes mobility liquid shape, after continuing heating about 12 hours, become static state at saturating Bright elastic solid (Hookean body) shape object, stirring, then at transparent very thick colloidal fluid.It after sampling freeze-drying, adds water and stirs, restores again It is gluey.
The preparation of 5 carrier 5 of embodiment
10 parts of Chondrus crispus extract, 1 part of collagen, 10 parts of hectorite, Chondrus crispus extract is dissolved in water Heat is substantially soluble in water, and collagen is dissolved in water, and the water-dispersible agglutination of hectorite takes above-mentioned sample to be mixed respectively, water is added to make Total solid is 4%, starts to generate White Flocculus when stirring, continues to stir evenly, and white newborn paste is generated, then in close Close in container and heated in 70 DEG C, after about 5 hours, become mobility liquid shape, after continuing heating about 20 hours, become it is static at Transparent nonfluid jelly, stirring, then at transparent thick colloidal fluid.It after sampling freeze-drying, adds water and stirs again, restores glue Shape.
The preparation of 6 carrier 6 of embodiment
Chondrus crispus extract is dissolved in water heating by 10 parts of Chondrus crispus extract, 1 part of collagen, 8 parts of hectorite It is substantially soluble in water, collagen is dissolved in water, and the water-dispersible agglutination of hectorite takes above-mentioned sample to be mixed respectively, water is added to make always Solid is 8%, starts to generate White Flocculus when stirring, continues to stir evenly, and white newborn paste is generated, then in closed It is heated in container in 90 DEG C, after about 3 hours, becomes mobility liquid shape, after continuing heating about 12 hours, become static state at saturating Bright nonfluid jelly, stirring, then at transparent thick colloidal fluid.It after sampling freeze-drying, adds water and stirs again, restores glue Shape.
The preparation of 7 carrier 7 of embodiment
10 parts of Chondrus crispus extract, 1 part of collagen, 10 parts of hectorite, Chondrus crispus extract is dissolved in water Heat is substantially soluble in water, and collagen is dissolved in water, and the water-dispersible agglutination of hectorite takes above-mentioned sample to be mixed respectively, water is added to make Total solid is 10%, starts to generate White Flocculus when stirring, continues to stir evenly, and white newborn paste is generated, then in close Close in container and heated in 80 DEG C, after about 5 hours, become mobility liquid shape, after continuing heating about 20 hours, become it is static at Transparent elastic solid colloidal object, stirring, then at transparent very thick colloidal fluid.After sampling freeze-drying, add water and stir again, Restore gluey.
The preparation of 8 carrier 8 of embodiment
10 parts of Chondrus crispus extract, 1 part of collagen, 10 parts of hectorite, Chondrus crispus extract is dissolved in water Heat is substantially soluble in water, and collagen is dissolved in water, and the water-dispersible agglutination of hectorite takes above-mentioned sample to be mixed respectively, water is added to make Total solid is 10%, starts to generate White Flocculus when stirring, continues to stir evenly, and white newborn paste is generated, then in close Close in container and heated in 90 DEG C, after about 3 hours, become mobility liquid shape, after continuing heating about 12 hours, become it is static at Transparent elastic solid-like object, stirring, then at transparent very thick colloidal fluid.After sampling freeze-drying, add water and stir again, it is extensive Re-glue shape.
The preparation of 9 carrier 9 of embodiment
Chondrus crispus extract is dissolved in water heating by 10 parts of Chondrus crispus extract, 1 part of collagen, 5 parts of hectorite It is substantially soluble in water, collagen is dissolved in water, and the water-dispersible agglutination of hectorite takes above-mentioned sample to be mixed respectively, water is added to make always Solid is 5%, starts to generate White Flocculus when stirring, continues to stir evenly, and white newborn paste is generated, then in closed It is heated in container in 60 DEG C, until 48 is small into rear, it is still mobility liquid shape.Trial-production failure.
The preparation of 10 carrier 10 of embodiment
10 parts of Chondrus crispus extract, 1 part of collagen, 10 parts of hectorite, Chondrus crispus extract is dissolved in water Heat is substantially soluble in water, and collagen is dissolved in water, and the water-dispersible agglutination of hectorite takes above-mentioned sample to be mixed respectively, water is added to make Total solid is 5%, starts to generate White Flocculus when stirring, continues to stir evenly, and white newborn paste is generated, then in close It closes in container and is heated in 60 DEG C, until 48 is small into rear, it is still mobility liquid shape.Trial-production failure.
The preparation of 11 eye cream of embodiment
100 grams of eye cream ingredient amounts prepare eye cream according to the form below.Carrier 1-8 is taken to prepare to obtain eye cream 1-8 respectively; Separately the mixture of 10 parts of Chondrus crispus extract, 1 part of collagen, 5 parts of hectorite is taken directly to prepare eye cream in 3% ratio addition, Obtain eye cream 9.
The test of 12 antioxidation in vitro of embodiment
(1) to Hydroxyl Radical Scavenging: taking 3 10mL colorimetric cylinders, be separately added into 7.5mmol/L Phen solution 0.2mL, 7.5mmol/L l ferrous ammonium sulfate solution 0.2mL, pH=7.47Tris-HCl buffer solution 1.0mL, in 2, No. 3 colorimetrics Guan Zhong is separately added into 7.5mmol/L H2O21.0mL, is separately added into appropriate test sample in No. 3 colorimetric cylinders, fixed with distilled water Hold to scale, 1h is reacted in 37 DEG C of water-baths, cold water is cooling, measures absorbance at 508nm by reference of water, calculates clearance rate (P)。
In formula: A sample --- the respectively absorbance of the hydroxy radical system of addition test sample
A damage ----it is the absorbance that H2O2 system is added
A is not damaged --- and it is the absorbance that H2O2 system is not added.
(2) to ultra-oxygen anion free radical scavenging effect: taking 3 dry 10mL colorimetric cylinders, be separately added into (pH=8.3) Tris-HCl buffer solution 4.4mL, the constant temperature 20min in 25 DEG C of water-baths are separately added into appropriate test specimens in 1, No. 2 colorimetric cylinder Product are separately added into 0.2mmol/L pyrogallol solution 0.5mL in 2, No. 3 colorimetric cylinders, 3 colorimetric cylinders are mixed, in 25 DEG C of water 8mol/L HCl 3 is added in each pipe and drips, mixes by constant temperature 4min in bath after taking-up.Suction is measured at 320nm as reference using water Luminosity calculates clearance rate (P).
In formula: A0 is that test sample system absorbance is not added;A1 is test sample to be added pyrogallol solution system is not added Absorbance;A2 is the absorbance that test sample and pyrogallol solution system is added.
(3) to hydrogen peroxide scavenging effect: taking 3 10mL colorimetric cylinders, number 1,2,3.In 1, No. 2 colorimetric cylinder respectively 10mmol/L hydrogen peroxide-phosphoric acid solution (pH=7.4) 5mL is added, is separately added into appropriate test specimens in 2, No. 3 colorimetric cylinders 1, No. 3 colorimetric cylinder is diluted with water to scale by product, is mixed.Absorbance is measured at 200nm by reference of water, calculates clearance rate (P)。
In formula: A0, A1, A2 are respectively the hydrogenperoxide steam generator system that test sample is not added plus test sample and peroxidating Hydrogen solution system and test sample are added without the absorbance of hydrogenperoxide steam generator system.
As a result: in the case where carrier concn is the concentration of 0.01mg/ml, eye cream 1-8 to the clearance rate of hydroxy radical is 73.5%~93.8%, the clearance rate of No. 9 samples is 53%;Eye cream 1-8 clearance rate to superoxide anion be 41.2%~ 52.7%, the clearance rate of No. 9 samples is 32.1%;Eye cream 1-8 clearance rate to hydrogen peroxide be 97.5%-100.2%, 9 The clearance rate of number sample is 93.5%.
Embodiment 13 resists cold and heat-resistance test
Above-mentioned 9 eye cream samples are put in closed glass jar, at 40 DEG C ± 2 DEG C of temperature, place 24 hours after, take out, put to 25 DEG C of room temperature observations, No. 9 samples are obviously thinning, and 1-8 sample does not have significant change.Continue to place to three months, No. 9 samples Color obviously deepens micro- Huang, and 1-8 sample does not have significant change.Above-mentioned 9 eye cream samples are put in closed glass jar, in temperature Degree -10 DEG C ± 2 DEG C, place 10 days, No. 9 surface layers of sample have a floor water appearance, and 1-8 sample cap removing on have a little droplet Outside, there is not significant change.It hyperphoric -5 DEG C ± 2 DEG C, places 10 days, has no significant change.

Claims (4)

1. a kind of skin care item carrier, it is characterised in that: the carrier is by 10 parts of Chondrus crispus extract, 1 part of collagen, hectorite 5-15 parts are made.
2. a kind of skin care item carrier, it is characterised in that: the carrier is by 10 parts of Chondrus crispus extract, 1 part of collagen, hectorite 10 parts are made.
3. the preparation method of carrier as claimed in claim 1 or 2, it is characterised in that the following steps are included:
(1) Chondrus crispus extract is dissolved in water, collagen is dissolved in water, and hectorite adds water dispersion agglutination;
(2) above-mentioned three kinds of solution is mixed, is diluted with water to by mass percentage, total solid 4%-10%, mixing is equal It is even, until forming the newborn paste of white;
(3) the newborn paste of white is placed in closed container, 70-90 DEG C of heating, until it is static at transparent nonfluid jelly, Stirring, at transparent fluid glue;Be freeze-dried into solid to get.
4. the preparation method of carrier as claimed in claim 3, which is characterized in that the total solid is 10%, and step (3) is described Heating temperature is 90 DEG C.
CN201910650183.4A 2019-07-18 2019-07-18 A kind of skin care item carrier and preparation method thereof Pending CN110522680A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070286826A1 (en) * 2006-05-24 2007-12-13 Grune Guery L Nontoxic, non-endocrine disrupting, cytoprotective, UV-radiation resistant sunblock compositions
WO2010143196A1 (en) * 2009-04-03 2010-12-16 Cavinkare Pvt Ltd. Novel synergistic transparent / translucent hydrogel composition; method of preparing it and a sheet / film made thereform
JP2015168627A (en) * 2014-03-05 2015-09-28 株式会社希松 oil-in-water type cosmetic
US20150342854A1 (en) * 2012-12-27 2015-12-03 Hayashibara Co., Ltd. External dermal composition for anti-ageing and method for producing the same
KR20160118824A (en) * 2015-04-03 2016-10-12 박성용 Manufacturing method of Foaming clay structure and Foaming structure manufactured by the same
CN107961208A (en) * 2017-12-06 2018-04-27 广州蜜妆生物科技有限公司 A kind of small molecule modeling face is compacted spraying and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070286826A1 (en) * 2006-05-24 2007-12-13 Grune Guery L Nontoxic, non-endocrine disrupting, cytoprotective, UV-radiation resistant sunblock compositions
WO2010143196A1 (en) * 2009-04-03 2010-12-16 Cavinkare Pvt Ltd. Novel synergistic transparent / translucent hydrogel composition; method of preparing it and a sheet / film made thereform
US20150342854A1 (en) * 2012-12-27 2015-12-03 Hayashibara Co., Ltd. External dermal composition for anti-ageing and method for producing the same
JP2015168627A (en) * 2014-03-05 2015-09-28 株式会社希松 oil-in-water type cosmetic
KR20160118824A (en) * 2015-04-03 2016-10-12 박성용 Manufacturing method of Foaming clay structure and Foaming structure manufactured by the same
CN107961208A (en) * 2017-12-06 2018-04-27 广州蜜妆生物科技有限公司 A kind of small molecule modeling face is compacted spraying and preparation method thereof

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Application publication date: 20191203