CN110478126B - Nano-silver antibacterial adhesive bandage with fragrance - Google Patents
Nano-silver antibacterial adhesive bandage with fragrance Download PDFInfo
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- CN110478126B CN110478126B CN201910608713.9A CN201910608713A CN110478126B CN 110478126 B CN110478126 B CN 110478126B CN 201910608713 A CN201910608713 A CN 201910608713A CN 110478126 B CN110478126 B CN 110478126B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F13/00—Bandages or dressings; Absorbent pads
- A61F13/00051—Accessories for dressings
- A61F13/00063—Accessories for dressings comprising medicaments or additives, e.g. odor control, PH control, debriding, antimicrobic
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F13/00—Bandages or dressings; Absorbent pads
- A61F13/02—Adhesive plasters or dressings
- A61F13/0203—Adhesive plasters or dressings having a fluid handling member
- A61F13/0206—Adhesive plasters or dressings having a fluid handling member the fluid handling member being absorbent fibrous layer, e.g. woven or nonwoven absorbent pad, island dressings
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/18—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing inorganic materials
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
- A61L15/46—Deodorants or malodour counteractants, e.g. to inhibit the formation of ammonia or bacteria
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/04—Making microcapsules or microballoons by physical processes, e.g. drying, spraying
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F13/00—Bandages or dressings; Absorbent pads
- A61F2013/00361—Plasters
- A61F2013/00544—Plasters form or structure
- A61F2013/00604—Multilayer
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F13/00—Bandages or dressings; Absorbent pads
- A61F2013/00361—Plasters
- A61F2013/00902—Plasters containing means
- A61F2013/00906—Plasters containing means for transcutaneous or transdermal drugs application
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F13/00—Bandages or dressings; Absorbent pads
- A61F2013/00361—Plasters
- A61F2013/00902—Plasters containing means
- A61F2013/0091—Plasters containing means with disinfecting or anaesthetics means, e.g. anti-mycrobic
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F13/00—Bandages or dressings; Absorbent pads
- A61F2013/00361—Plasters
- A61F2013/00902—Plasters containing means
- A61F2013/00914—Plasters containing means with deodorising or perfuming means
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/10—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing inorganic materials
- A61L2300/102—Metals or metal compounds, e.g. salts such as bicarbonates, carbonates, oxides, zeolites, silicates
- A61L2300/104—Silver, e.g. silver sulfadiazine
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/40—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices characterised by a specific therapeutic activity or mode of action
- A61L2300/404—Biocides, antimicrobial agents, antiseptic agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/60—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices characterised by a special physical form
- A61L2300/62—Encapsulated active agents, e.g. emulsified droplets
- A61L2300/622—Microcapsules
Abstract
A nano-silver antibacterial bandage with fragrance comprises: base material, water absorbing layer, microcapsule layer, medicine layer, and release paper; one side surface of the base material is coated with viscose, a water absorbing layer, a microcapsule layer and a medicine layer are sequentially compounded in the middle of the side surface coated with the viscose, and anti-sticking paper covers the medicine layer; the microcapsule takes natural high molecular chitosan and gelatin as capsule walls and essence oil and nano silver as capsule cores; the invention provides a wound plaster with aromatic odor, which is characterized in that the common wound plaster is supplemented with aromatherapy in terms of the functions, and after smelling the aromatic odor, a wounded person can calm and calm the nerves, relax the nervous mood, keep good mood and be beneficial to the healing of the wounded person; the essence essential oil and the nano-silver are coated in the microcapsule technology, so that the flavor of the essence essential oil is ensured, and the loss of the nano-silver is prevented; the microcapsule technology is adopted to enable the fragrance nano silver to be released continuously, so that the effects of long-term fragrance retention and continuous antibiosis are achieved.
Description
(I) technical field
The invention belongs to the field of medical instruments, and particularly relates to a nano-silver antibacterial adhesive bandage with aromatic smell.
(II) background of the invention
The wound plaster, also called as a hemostatic plaster, is a common surgical medicine in daily life and also a necessary help for emergency treatment of trauma for every family. Is mainly used for treating small wounds and has the effects of quickly stopping bleeding, protecting wound surfaces and preventing infection. However, these functions are not ideal, for example, the existing wound dressings have no pleasant smell, some have even peculiar smell, and thus have adverse effects on the wounded.
In recent years, attention has been paid to the medical effects of aromatic plant essential oils such as forest bath, aromatherapy, and phytoncide. With the intensive research on the fragrance, people find that the fragrance has the effects of relaxing nervous mood, relieving stress, stimulating people and the like. For example, vanilla, clove, lavender, peppermint, turpentine, etc. have sedative effect, whereas chamomile and lavender have bactericidal effect.
In addition, the common adhesive bandage only consists of an adhesive tape, a water absorption layer and an isolation layer, functional components are not contained in the product structure, so that the common adhesive bandage has no sterilization effect, although a plurality of nano-silver antibacterial adhesive bandages exist at present, nano-silver is easy to lose, Chinese patent CN200920117403.9 designs a nano-silver antibacterial adhesive bandage, the method is to coat or permeate nano-silver or a nano-silver compound containing silver ions on a middle base layer, a medical net film is covered on the upper surface of the nano-silver antibacterial adhesive bandage, the medical net film serves as a barrier to prevent the nano-silver from losing, but only coating and permeating cannot enable the nano-silver to be firmly combined with the middle base layer, and even if one layer of the medical net film is covered, the nano-silver particles cannot be guaranteed not to lose.
Disclosure of the invention
Aiming at the problems in the prior art, the invention designs the adhesive bandage with pleasant aromatic smell and long-term antibacterial property, and adopts the microcapsule technology, thereby maintaining the stability and lasting fragrance of the essence and ensuring that the nano silver particles are not lost.
The technical scheme of the invention is as follows:
a nano-silver antibacterial bandage with fragrance comprises: base material, water absorbing layer, microcapsule layer, medicine layer, and release paper;
one side surface of the base material is coated with viscose, a water absorbing layer, a microcapsule layer and a medicine layer are sequentially compounded in the middle of the side surface coated with the viscose, and anti-sticking paper covers the medicine layer;
furthermore, the base material is also provided with a plurality of air holes which are regularly arranged, and the air holes are arranged at the middle position of the base material which is compounded with the water absorption layer, the microcapsule layer and the medicine layer;
furthermore, the anti-sticking paper is divided into two pieces which are respectively arranged at the two ends of the base material and are overlapped and covered with the medicine layer.
In the present invention,
the water absorption layer, the microcapsule layer and the medicine layer can be bonded and compounded on the base material through the medical pressure-sensitive adhesive;
the water absorption layer is made of non-woven fabric;
the medicine component of the medicine layer is antibacterial and anti-inflammatory medicine;
the microcapsule takes natural high molecular chitosan and gelatin as capsule walls and essence oil and nano silver as capsule cores;
the preparation method of the microcapsule comprises the following steps:
(1) taking essence essential oil, adding dry nano silver powder and emulsifier sodium dodecyl sulfate, and stirring at the speed of 8000-10000 r/min for 15-45 min to form uniform emulsion;
the mass usage of the nano silver powder is 0.1-1% of the mass of the essence essential oil;
the mass usage amount of the emulsifier is 1-2% of the total mass of the system;
the essence essential oil such as rose essence, jasmine essence, lemon essence, lavender essence or sweet orange essence;
(2) preparing a chitosan acetic acid aqueous solution and a gelatin aqueous solution, adding the emulsion obtained in the step (1) and an emulsifier Span-80 into the chitosan acetic acid aqueous solution for emulsification for 20-40 min, then respectively dropwise adding the gelatin aqueous solution and glutaraldehyde, stirring and curing at 60 ℃ for 2-4 h, carrying out suction filtration, washing a filter cake with deionized water, and carrying out freeze drying to obtain microcapsules;
in the chitosan acetic acid aqueous solution, the mass fraction of chitosan is 1-2%, and the volume fraction of acetic acid is 1-3%;
in the gelatin aqueous solution, the mass fraction of gelatin is 1-3%;
the volume ratio of the emulsion obtained in the step (1), the chitosan acetic acid aqueous solution and the gelatin aqueous solution is 1-2: 1: 0.5 to 1;
the volume consumption of the emulsifier Span-80 is 1-5% of the total volume of the chitosan acetic acid aqueous solution and the gelatin aqueous solution;
the volume consumption of the glutaraldehyde is 5-10% of the total volume of the chitosan acetic acid aqueous solution and the gelatin aqueous solution.
(IV) description of the drawings
FIG. 1 is a schematic structural view of a cross-section of a wound covering of the present invention;
FIG. 2 is a schematic view of the structure of a substrate;
in the figure: 1. a substrate; 2. a water-absorbing layer; 3. a microcapsule layer; 4. a drug layer; 5. release paper; 6. and (4) air holes.
(V) detailed description of the preferred embodiments
The present invention will be described in further detail with reference to the accompanying drawings, but the scope of the present invention is not limited thereto.
Example 1
As shown in fig. 1, the fragrant nano-silver antibacterial bandage shown in fig. 2 comprises a base material 1 coated with viscose, a plurality of air holes 6 regularly arranged are arranged in the middle of the base material 1, a water absorbing layer 2 formed by artificial cotton fiber is tightly attached to the middle of the base material, a microcapsule layer 3 coated with essence essential oil and nano-silver is arranged above the water absorbing layer 2, a medicine layer 4 is arranged above the microcapsule layer 3, anti-sticking paper 5 covers the base material 1 and the medicine layer 4, the anti-sticking paper 5 is overlapped by two pieces, and the anti-sticking paper is torn down from the middle to two sides during use.
The microcapsule is prepared by a complex coacervation method by using natural polymer chitosan and gelatin as capsule walls and essence essential oil and nano silver as capsule cores, and the preparation method of the microcapsule comprises the following steps:
(1) taking 20g of essence essential oil, adding 0.04g of dry nano silver powder and 0.2g of emulsifier sodium dodecyl sulfate, stirring and emulsifying at the speed of 10000r/min for 30min to form uniform emulsion;
(2) preparing a 1.5 mass percent chitosan acetic acid aqueous solution and a 2 mass percent gelatin aqueous solution, adding 10mL of the emulsion obtained in the step (1) and 1mL of Span-80 into 10mL of the chitosan acetic acid aqueous solution for emulsification for 30min, then respectively dropwise adding 10mL of the gelatin aqueous solution and 2mL of glutaraldehyde, stirring and curing for 2h at 60 ℃, carrying out suction filtration, washing a filter cake with deionized water, and carrying out freeze drying to obtain the microcapsule.
The above-mentioned embodiments are provided for further understanding of the present invention, and are not intended to limit the present invention, and any modifications and changes made to the present invention are included in the protection scope of the present invention without departing from the spirit of the present invention.
Claims (4)
1. A nano-silver antibacterial bandage with fragrance is characterized in that the bandage comprises: base material, water absorbing layer, microcapsule layer, medicine layer, and release paper;
one side surface of the base material is coated with viscose, a water absorbing layer, a microcapsule layer and a medicine layer are sequentially compounded in the middle of the side surface coated with the viscose, and anti-sticking paper covers the medicine layer;
the microcapsule takes natural high molecular chitosan and gelatin as capsule walls and essence oil and nano silver as capsule cores;
the preparation method of the microcapsule comprises the following steps:
(1) taking essence essential oil, adding dry nano silver powder and emulsifier sodium dodecyl sulfate, and stirring at the speed of 8000-10000 r/min for 15-45 min to form uniform emulsion;
the mass usage of the nano silver powder is 0.1-1% of the mass of the essence essential oil;
the mass usage amount of the emulsifier is 1-2% of the total mass of the system;
(2) preparing a chitosan acetic acid aqueous solution and a gelatin aqueous solution, adding the emulsion obtained in the step (1) and an emulsifier Span-80 into the chitosan acetic acid aqueous solution for emulsification for 20-40 min, then respectively dropwise adding the gelatin aqueous solution and glutaraldehyde, stirring and curing at 60 ℃ for 2-4 h, carrying out suction filtration, washing a filter cake with deionized water, and carrying out freeze drying to obtain microcapsules;
in the chitosan acetic acid aqueous solution, the mass fraction of chitosan is 1-2%, and the volume fraction of acetic acid is 1-3%;
in the gelatin aqueous solution, the mass fraction of gelatin is 1-3%;
the volume ratio of the emulsion obtained in the step (1), the chitosan acetic acid aqueous solution and the gelatin aqueous solution is 1-2: 1: 0.5 to 1;
the volume consumption of the emulsifier Span-80 is 1-5% of the total volume of the chitosan acetic acid aqueous solution and the gelatin aqueous solution;
the volume consumption of the glutaraldehyde is 5-10% of the total volume of the chitosan acetic acid aqueous solution and the gelatin aqueous solution.
2. The antiseptic bandage with fragrance and nano silver of claim 1 wherein the base material further comprises a plurality of regularly arranged air holes, wherein the air holes are formed in the middle of the base material where the water absorbing layer, the microcapsule layer and the drug layer are combined.
3. The scented nanosilver antimicrobial wound covering of claim 1, wherein the release paper is provided in two pieces, one at each end of the base material, and the drug layer is overlapped.
4. The nanosilver antibacterial wound covering with aroma of claim 1, wherein the essence essential oil is rose essence, jasmine essence, lemon essence, lavender essence or sweet orange essence.
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CN201910608713.9A CN110478126B (en) | 2019-07-08 | 2019-07-08 | Nano-silver antibacterial adhesive bandage with fragrance |
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CN110478126B true CN110478126B (en) | 2021-10-15 |
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CN112089529B (en) * | 2020-08-24 | 2022-01-25 | 浙江珍琦护理用品有限公司 | Paper diaper capable of keeping skin clean and healthy |
CN116099030A (en) * | 2022-11-15 | 2023-05-12 | 青岛海诺生物工程有限公司 | Chitosan breathable adhesive bandage and preparation method thereof |
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