Segmented continuous heat treating furnace and material heat treatment process
Technical field
The present invention relates to a kind of segmented continuous heat treating furnace and material heat treatment process.
Background technique
Currently, the vacuum and atmosphere heat treatment furnace for non-crystalline material or nanocrystalline material product are period furnace, production
In each furnace require to undergo very long heating, heat preservation, temperature-fall period, waste a large amount of time lifting thermophase, the period
The limited production capacity of heat treatment amount of furnace list furnace is low, and time length, low efficiency, waste electric energy, and if desired producing in enormous quantities can only adopt
It is produced simultaneously with more furnaces, all brings great pressure to electric power and place demand and artificial demand.
Summary of the invention
The technical problem to be solved by the present invention is to overcome the deficiencies of existing technologies, a kind of segmented continuous heat is provided
Furnace, it can reach more period furnace production capacities, additionally it is possible to avoid causing workpiece performance discrete because of each furnace temperature absolute temperature difference
The excessive problem of property, to ensure workpiece, the especially consistency and stability of amorphous or nano crystalline substance workpiece performance.
In order to solve the above-mentioned technical problems, the present invention provides a kind of segmented continuous heat treating furnace, it include furnace body and
Conveying device;Wherein,
Preheating zone furnace chamber, heating zone furnace chamber, heat preservation zone furnace chamber and the cooling area furnace chamber set gradually is equipped in the furnace body;
The preheating zone furnace chamber, heating zone furnace chamber, heat preservation zone furnace chamber are respectively equipped with the heating device heated to corresponding furnace chamber,
The cooling area furnace chamber is equipped with the cooling device to cool down to cooling area furnace chamber;
It is additionally provided with and is suitable for individually to preheating zone furnace chamber, heating zone furnace chamber, heat preservation zone furnace chamber and cooling area furnace chamber point on the furnace body
The vacuum evacuation device that does not vacuumize and it is suitable for individually to preheating zone furnace chamber, heating zone furnace chamber, heat preservation zone furnace chamber and cooling area furnace
Chamber each lead into inert gas for inert gas installation;
The furnace body is additionally provided with the material platform import being connected with the preheating zone furnace chamber, and the furnace body is additionally provided with and is suitable for opening
Or close the import fire door of the material platform import;
The furnace body is additionally provided with the material platform outlet being connected with the cooling area furnace chamber, and the furnace body is additionally provided with and is suitable for opening
Or close the outlet fire door of the material platform outlet;
The conveying device includes accommodating the material platform of material and being connected with material platform pre- the material platform for accommodating material to be successively transported to
In hot-zone furnace chamber, heating zone furnace chamber, heat preservation zone furnace chamber and cooling area furnace chamber and make to expect platform during transport in each furnace chamber
The material platform driving device rested;
Adjacent in preheating zone furnace chamber, heating zone furnace chamber, heat preservation zone furnace chamber and cooling area furnace chamber of the furnace body is divided between the two
The access or the adjacent access between the two of opening that She You be suitable for being actuated to close adjacent between the two are in material platform driving
The isolation door gear of material platform is fed forward under the driving of device.
Further, the material platform driving device include respectively with preheating zone furnace chamber, heating zone furnace chamber, heat preservation zone furnace chamber and drop
The material platform driving assembly that warm area furnace chamber is correspondingly arranged;Wherein,
The material platform driving assembly includes:
In corresponding furnace chamber and the conveying roller group suitable for accepting the material platform, the conveying roller group rotation are connected to the furnace body
On in the roller frame that is arranged in corresponding furnace chamber;
It is connected with the conveying roller group to drive the conveying roller group to rotate to be fed forward the driving mechanism of material platform.
Further, the driving mechanism includes:
The sprocket wheel being connected respectively with the conveying roller in conveying roller group;
Connect the chain of all sprocket wheels;
It is connected with one of sprocket wheel to drive the sprocket wheel to rotate or be connected with one of conveying roller to drive the conveying roller to revolve
The driving source turned.
Further, the isolation door gear includes:
Be movably arranged in preheating zone furnace chamber, heating zone furnace chamber, heat preservation zone furnace chamber and the cooling area furnace chamber it is adjacent between the two
Isolating door;
Be connected with isolating door with drive isolating door mobile with close adjacent access between the two or open it is adjacent between the two
At least one isolation door drive of access.
Further, the isolation door drive includes:
Rack gear on isolating door side wall;
Connection is engaged with rack and rotates the gear being connected on the furnace body;
It is connected with gear to drive the gear rotary drive mechanism of the gear rotation.
Further, the gear rotary drive mechanism includes:
Chain wheel pair, the chain wheel pair include drive sprocket, driven sprocket and the connection drive sprocket and the driven sprocket
Driving chain, the driven sprocket and the gear pass through transmission transmission connection;
Rotary driving source, the rotary driving source are connected to drive the drive sprocket to rotate with the drive sprocket.
Another aspect, the present invention also provides a kind of material heat treatment process, the step of technique in include:
During the primary intermittent transport of material,
First material is placed in the furnace chamber of preheating zone, carrying out heating to preheating zone furnace chamber makes 200 ~ 400 DEG C of its temperature and to preheating
Area's furnace chamber, which first vacuumizes, to be passed through inert gas afterwards its internal pressure power is made to be maintained at 0.1 ~ 0.15MPa, and material is maintained at preheating zone furnace
Chamber is for a period of time;
After place it in temperature be 300 ~ 500 DEG C and first vacuumize be passed through afterwards inert gas make its internal pressure power be maintained at 0.1 ~
The heating zone furnace chamber of 0.15MPa is for a period of time;
Then place it in temperature be 400 ~ 600 DEG C and first vacuumize be passed through afterwards inert gas make its internal pressure power be maintained at 0.08 ~
The heat preservation zone furnace chamber of 0.15MPa is for a period of time;
It places it in first to vacuumize again and is passed through the cooling area furnace chamber that inert gas makes its internal pressure power be maintained at 0.1 ~ 0.15MPa afterwards,
Carrying out cooling to cooling area furnace chamber makes 20 ~ 200 DEG C of its temperature.
Further, the step of technique is implemented by the segmented continuous heat treating furnace.
Further, in two batch materials, previous batch materials are placed in the environment of previous furnace chamber, latter batch materials be placed in it is described
In the environment of the corresponding latter furnace chamber of the environment of previous furnace chamber;Wherein, front and back is the conveying direction of material.
Further, the material is the product made of non-crystalline material or nanocrystalline material.
After above-mentioned technical proposal, the present invention can be during the primary intermittent transport of material, by material point
Not Jing Guo corresponding conditions treated preheating zone furnace chamber, heating zone furnace chamber, heat preservation zone furnace chamber and to cooling area furnace chamber, realize to object
Preheating, heating, heat preservation and the cooling processing of material;In the present invention, beating by isolation door gear, import fire door and outlet fire door
It is open and close that material is allowed to enter preheating zone furnace chamber, heating zone furnace chamber, heat preservation zone furnace chamber under the action of conveying device
With to cooling area furnace chamber;Simultaneously can by vacuum evacuation device individually to preheating zone furnace chamber, heating zone furnace chamber, heat preservation zone furnace chamber and
Cooling area furnace chamber vacuumize respectively and by for inert gas installation individually to preheating zone furnace chamber, heating zone furnace chamber, heat preservation zone furnace
Chamber and cooling area furnace chamber each lead into inert gas;Respectively by heating device to the preheating zone furnace chamber, heating zone furnace chamber, guarantor
Warm area furnace chamber is heated and is kept the temperature, and is cooled down by cooling device to the cooling area furnace chamber, segmentation through the invention
Formula continuous heat treating furnace reaches more period furnace production capacities, additionally it is possible to avoid leading to workpiece because of each furnace temperature absolute temperature difference
Can the excessive problem of discreteness, to ensure workpiece, the especially consistency and stabilization of amorphous or nano crystalline substance workpiece performance
Property.
Detailed description of the invention
Fig. 1 is the structure chart of the segmented continuous heat treating furnace of the embodiment of the present invention;
Fig. 2 is the vertical view schematic internal view of Fig. 1.
Specific embodiment
In order that the present invention can be more clearly and readily understood, right below according to specific embodiment and in conjunction with attached drawing
The present invention is described in further detail.
As shown in Figure 1, 2, a kind of segmented continuous heat treating furnace, it includes furnace body 1 and conveying device;Wherein,
Preheating zone furnace chamber, heating zone furnace chamber 12, heat preservation zone furnace chamber 13 and the cooling area furnace chamber set gradually is equipped in the furnace body 1
14;
The preheating zone furnace chamber, heating zone furnace chamber 12, heat preservation zone furnace chamber 13 are respectively equipped with the heating heated to corresponding furnace chamber
Device, the cooling area furnace chamber 14 are equipped with the cooling device to cool down to cooling area furnace chamber 14;
It is additionally provided with and is suitable for individually to preheating zone furnace chamber, heating zone furnace chamber 12, heat preservation zone furnace chamber 13 and cooling area furnace on the furnace body 1
The vacuum evacuation device and be suitable for individually to preheating zone furnace chamber, heating zone furnace chamber 12, heat preservation zone furnace chamber 13 that chamber 14 vacuumizes respectively
With cooling area furnace chamber 14 each lead into inert gas for inert gas installation;
The furnace body 1 is additionally provided with the material platform import being connected with the preheating zone furnace chamber, and the furnace body 1 is additionally provided with and is suitable for beating
The import fire door 15 of the material platform import is closed on or off;
The furnace body 1 is additionally provided with the material platform outlet being connected with the cooling area furnace chamber 13, and the furnace body 1 is additionally provided with and is suitable for
Open or close the outlet fire door 16 of the material platform outlet;
The conveying device includes accommodating the material platform 21 of material 10 and being connected with material platform 21 will accommodate the material platform 21 of material successively
It is transported in preheating zone furnace chamber, heating zone furnace chamber 12, heat preservation zone furnace chamber 13 and cooling area furnace chamber 14 and makes to expect that platform 21 is being conveyed through
The material platform driving device rested in each furnace chamber in journey;
The adjacent the two of the furnace body 1 in preheating zone furnace chamber, heating zone furnace chamber 12, heat preservation zone furnace chamber 13 and cooling area furnace chamber 14
Between be respectively equipped with and be suitable for being actuated to the access closed adjacent between the two or open adjacent access between the two to expect
The isolation door gear of material platform 21 is fed forward under the driving of platform driving device.
In the present embodiment, heating device, cooling device and vacuum means are set to the usual device of those skilled in the art,
For heating device by the way of circulating air, cooling device can be using air-cooled or water leaching cooling device or its equivalent way, drop
Warm device can be realized by way of vacuum pumping pump+pipeline, and about its specific structure, the present embodiment does not do specific superfluous
It states;In addition, being also the usual device of those skilled in the art for inert gas installation, can be incited somebody to action by way of pump+pipeline
Inert gas is pumped into corresponding furnace chamber, and may be implemented to recycle, and about its specific structure, the present embodiment does not do specific superfluous
It states.
As shown in Figure 1, 2, the material platform driving device such as, but not limited to flowering structure, including respectively with preheating zone furnace
The material platform driving assembly that chamber, heating zone furnace chamber 12, heat preservation zone furnace chamber 13 and cooling area furnace chamber 14 are correspondingly arranged;Wherein,
The material platform driving assembly includes:
In corresponding furnace chamber and the conveying roller group suitable for accepting the material platform, the conveying roller group rotation are connected to the furnace body
In the roller frame 3 being arranged in corresponding furnace chamber on 1;
It is connected with the conveying roller group to drive the conveying roller group to rotate to be fed forward the driving mechanism of material platform 21.
It, can during transport, individually to meet it by the way that material platform driving assembly is separately provided to each furnace chamber is corresponding
The purpose of a period of time is rested in each furnace chamber.
As shown in Fig. 2, the driving mechanism is such as, but not limited to flowering structure, comprising:
The sprocket wheel 23 being connected respectively with the conveying roller 22 in conveying roller group;
Connect the chain 24 of all sprocket wheels 23;
It is connected with one of sprocket wheel 23 to drive the sprocket wheel 23 to rotate or be connected with one of conveying roller 22 to drive this defeated
The driving source 25 for sending roller 22 to rotate.
In the present embodiment, driving source 25 can be motor.
When driving source 25 acts, one of sprocket wheel 23 or in which conveying roller 22 rotate, then by sprocket wheel 23 with
The cooperation of chain 24 drives other conveying rollers 22 to rotate, thus material conveying platform 21, can by controlling the movement of driving source 25,
To control resting for material platform 21.
As shown in Figure 1, 2, the isolation door gear is such as, but not limited to flowering structure, comprising:
It is movably arranged at adjacent the two in preheating zone furnace chamber, heating zone furnace chamber 12, heat preservation zone furnace chamber 13 and cooling area furnace chamber 14
Between isolating door 41;
It is connected with isolating door 41 and closes adjacent adjacent the two of access or opening between the two to drive isolating door 41 mobile
Between access at least one isolation door drive.
As shown in Figure 1, 2, the isolation door drive is such as, but not limited to flowering structure, comprising:
Rack gear 42a on 41 side wall of isolating door;
It is engaged with rack gear 42a and connects and rotate the gear 42b being connected on the furnace body 1;
It is connected with gear 42b to drive the gear rotary drive mechanism of the gear 42b rotation.
As shown in Figure 1, the gear rotary drive mechanism is such as, but not limited to flowering structure, comprising:
Chain wheel pair, the chain wheel pair include drive sprocket 43a, driven sprocket 43b and the connection drive sprocket 43a and described
The driving chain 43c, the driven sprocket 43b and the gear 42b of driven sprocket 43b is sequentially connected by transmission;
Rotary driving source 43d, the rotary driving source 43d are connected to drive the drive sprocket 43a with the drive sprocket 43a
Rotation.
Rotary driving source 43d can be motor.
In the present embodiment, the isolation door drive on an isolating door 41 is provided with two, corresponding rack gear
42a is correspondingly arranged in the two side walls of isolating door 41.
It when rotary driving source 43d is acted, is rotated by chain wheel pair band moving gear 42b, on gear 42b rotation band carry-over bar 42
Lower movement, so that isolating door 41 be driven to move up and down, with close adjacent access between the two or open it is adjacent between the two
Access, when opening, material platform 21 can enter next furnace chamber, and when closing, corresponding furnace chamber can be heated and be vacuumized and be passed through
Inert gas.
Embodiment two
Include: in a kind of the step of material heat treatment process, technique
During the primary intermittent transport of material 10,
First material is placed in the furnace chamber of preheating zone, carrying out heating to preheating zone furnace chamber makes 200 ~ 400 DEG C of its temperature and to preheating
Area's furnace chamber, which first vacuumizes, to be passed through inert gas afterwards its internal pressure power is made to be maintained at 0.1 ~ 0.15MPa, and material is maintained at preheating zone furnace
Chamber is for a period of time;
After place it in temperature be 300 ~ 500 DEG C and first vacuumize be passed through afterwards inert gas make its internal pressure power be maintained at 0.1 ~
12 a period of time of heating zone furnace chamber of 0.15MPa;
Then place it in temperature be 400 ~ 600 DEG C and first vacuumize be passed through afterwards inert gas make its internal pressure power be maintained at 0.08 ~
13 a period of time of heat preservation zone furnace chamber of 0.15MPa;
It places it in first to vacuumize again and is passed through the cooling area furnace chamber that inert gas makes its internal pressure power be maintained at 0.1 ~ 0.15MPa afterwards
14, carrying out cooling to cooling area furnace chamber 14 makes 20 ~ 200 DEG C of its temperature.
The step of technique, is implemented by the segmented continuous heat treating furnace in embodiment one.
In two batch materials, previous batch materials 10 are placed in the environment of previous furnace chamber, latter batch materials 10 be placed in it is described before
In the environment of the corresponding latter furnace chamber of the environment of one furnace chamber;Wherein, front and back is the conveying direction of material 10.
Specifically, the segmented continuous heat treating furnace in one in conjunction with the embodiments, is specifically addressed process above.
Step 1: material is placed on material platform 21, import fire door 15 is opened, material platform 21 is pushed into preheating zone furnace chamber, is closed
Import fire door 15 is closed, while ensuring that the isolating door 41 between preheating zone furnace chamber and heating zone furnace chamber 12 is in close state, to pre-
Hot-zone furnace chamber vacuumizes until furnace chamber air pressure in preheating zone is -0.1MPa, while preheating zone cavity temperature is arranged between 200-400 DEG C
Between begin to warm up, closing vacuumizes and being passed through inert gas makes preheating zone furnace chamber internal pressure power be maintained at 0.1-0.15MPa, is setting
Determine to keep a period of time (depending on the process) under temperature and pressure.
Step 2: ensuring isolating door 41 between preheating zone furnace chamber and heating zone furnace chamber 12 and heating zone furnace chamber 12 and heat preservation
Isolating door 41 between area's furnace chamber 13 is passed through inert gas all in closed state after vacuumizing to heating zone furnace chamber 12, heating
Air pressure in area's furnace chamber 12 is suitable with preheating zone furnace chamber, and temperature in heating zone furnace chamber 12 is arranged and starts to add between 300-500 DEG C
Heat.
Step 3: directly opening isolating door 41 after the completion of the first step and second step, it will expect that platform 21 transports using conveying device
To heating zone furnace chamber 12, it is then shut off isolating door 41, the vent valve that preheating zone furnace chamber is opened after closing makes gas in the furnace chamber of preheating zone
Pressure is atmospheric pressure, opens import fire door 15, repeats the first step and carries out the preheating that feeds intake, and is kept after 12 temperature of heating zone furnace chamber is stablized
For a period of time (depending on the process).
Step 4: ensure isolating door 41 between heating zone furnace chamber 12 and heat preservation zone furnace chamber 13 and heat preservation zone furnace chamber 13 with
Isolating door 41 between cooling area furnace chamber 14 is passed through inert gas after vacuumizing to heat preservation zone furnace chamber 13 all in closed state,
Quite, setting 13 furnace temperature of heat preservation zone furnace chamber is begun to warm up between 400-600 DEG C for air pressure and heating zone furnace chamber 12.
Step 5: after the completion of third step and the 4th step, directly between unlatching heating zone furnace chamber 12 and heat preservation zone furnace chamber 13
Isolating door 41 is transported to heat preservation zone furnace chamber 13 using the material platform 21 that conveying device will heat up area's furnace chamber 12, is then shut off heating zone
Isolating door 41 between furnace chamber 12 and heat preservation zone furnace chamber 13 repeats third step after closing, 21 turns of material platform for completing preheating zone furnace chamber
Feeding intake for heating zone furnace chamber 12 and preheating zone furnace chamber is moved to, 12 temperature of heating zone furnace chamber is kept for a period of time (depending on work after stablizing
Depending on skill).
Step 6: ensure isolating door 41 between heat preservation zone furnace chamber 13 and cooling area furnace chamber 14 and outlet fire door 16 all in
Closed state, is passed through inert gas after vacuumizing to cooling area furnace chamber 14, air pressure and heat preservation zone furnace chamber 13 are suitable.
Step 7: after the completion of the 5th step and the 6th step, directly between unlatching heat preservation zone furnace chamber 13 and cooling area furnace chamber 14
The material platform 21 of heat preservation zone furnace chamber 13 is transported to cooling area furnace chamber 14 using conveying device, is then shut off heat preservation zone by isolating door 41
Isolating door 41 between furnace chamber 13 and cooling area furnace chamber 14 opens cooling device (air-cooled or water drenches cooling device) to drop after closing
Warm area furnace chamber 14 is cooled down, then repeatedly the 5th step, completes heating zone furnace chamber 12, the material platform 21 of preheating zone furnace chamber shifts respectively
To feeding intake for heat preservation zone furnace chamber 13, heating zone furnace chamber 12 and preheating zone furnace chamber.
Step 8: cooling terminates when the workpiece temperature in cooling area furnace chamber 14 is down to 20-200 DEG C, cooling area furnace is opened
14 vent valve of chamber makes furnace chamber air pressure be down to atmospheric pressure, and opening outlet fire door 16 will expect that platform 21 takes out, and completes the heat of the first batch materials
Processing.
Step 9: the 4th section of furnace temperature, which closes discharging door after restoring to room temperature, repeats the 6th step, then repeatedly the 7th step is complete
At complete third, two, the material platform of primary reformer chamber be transferred to feeding intake for the four, the three, secondary reformer chamber and preheating zone furnace chamber respectively.
The technique of the present embodiment is especially suitable for the heat treatment to the product made of non-crystalline material or nanocrystalline material.
Particular embodiments described above, pair present invention solves the technical problem that, technical scheme and beneficial effects carry out
It is further described, it should be understood that the above is only a specific embodiment of the present invention, is not limited to this
Invention, all within the spirits and principles of the present invention, any modification, equivalent substitution, improvement and etc. done should be included in this hair
Within bright protection scope.
In the description of the present invention, it is to be understood that, indicating position or the term of positional relationship are based on shown in attached drawing
Orientation or positional relationship, be merely for convenience of description of the present invention and simplification of the description, rather than the equipment of indication or suggestion meaning
Or element must have a particular orientation, be constructed and operated in a specific orientation, therefore be not considered as limiting the invention.
In the present invention unless specifically defined or limited otherwise, term " installation ", " connected ", " connection ", " fixation " etc.
Term shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or integral;It can be mechanical connect
It connects, is also possible to be electrically connected;It can be directly connected, can also can be in two elements indirectly connected through an intermediary
The interaction relationship of the connection in portion or two elements.It for the ordinary skill in the art, can be according to specific feelings
Condition understands the concrete meaning of above-mentioned term in the present invention.
In the description of the present invention, it should be noted that term " center ", "upper", "lower", "left", "right", "vertical",
The orientation or positional relationship of the instructions such as "horizontal", "inner", "outside" is to be based on the orientation or positional relationship shown in the drawings, or be somebody's turn to do
Invention product using when the orientation or positional relationship usually put, be merely for convenience of description of the present invention and simplification of the description, without
It is that the device of indication or suggestion meaning or element must have a particular orientation, be constructed and operated in a specific orientation, therefore not
It can be interpreted as limitation of the present invention.In addition, term " first ", " second ", " third " etc. are only used for distinguishing description, and cannot manage
Solution is indication or suggestion relative importance.
In addition, the terms such as term "horizontal", "vertical", " pendency " are not offered as requiring component abswolute level or pendency, and
It is that can be slightly tilted.It is not to indicate the structure if "horizontal" only refers to that its direction is more horizontal with respect to for "vertical"
It has to fully horizontally, but can be slightly tilted.
In the present invention unless specifically defined or limited otherwise, fisrt feature can be on or below second feature
Directly contacted including the first and second features, also may include the first and second features be not direct contact but by them it
Between other characterisation contact.Moreover, fisrt feature is on second feature, top and above include fisrt feature second spy
Right above sign and oblique upper, or first feature horizontal height is merely representative of higher than second feature.Fisrt feature second feature it
Under, lower section and fisrt feature included below be directly below and diagonally below the second feature, or be merely representative of first feature horizontal height
Less than second feature.