CN110455835A - A kind of Soft X-ray microimaging detector - Google Patents

A kind of Soft X-ray microimaging detector Download PDF

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Publication number
CN110455835A
CN110455835A CN201910771982.7A CN201910771982A CN110455835A CN 110455835 A CN110455835 A CN 110455835A CN 201910771982 A CN201910771982 A CN 201910771982A CN 110455835 A CN110455835 A CN 110455835A
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China
Prior art keywords
soft
cavity
ray
opening
detector according
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CN201910771982.7A
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Chinese (zh)
Inventor
郑睿
肖鹏
谢庆国
钟胜
王卫东
唐江
褚倩
白翔
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Suzhou Ruipening Technology Co Ltd
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Suzhou Ruipening Technology Co Ltd
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Priority to CN201910771982.7A priority Critical patent/CN110455835A/en
Publication of CN110455835A publication Critical patent/CN110455835A/en
Priority to PCT/CN2020/108479 priority patent/WO2021031936A1/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N23/00Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
    • G01N23/02Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material
    • G01N23/04Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material and forming images of the material

Abstract

The invention discloses a kind of Soft X-ray microimaging detectors, including cavity, fluorescence conversion screen and electrooptical device, cavity includes the first opening and the second opening, inside cavity is provided with will reflex to the reflection device of the second opening from the light of the first opening incidence, and light is open between the direction propagated to the reflection device direction propagated and self-reflection device to the second opening from first has the first angle;Fluorescence conversion screen is set to the first opening;Electrooptical device is set to the second opening, and electrooptical device, fluorescence conversion screen and cavity form confined space.The invention avoids grenz rays to be directly radiated on electrooptical device, improves Effect on Detecting, extends the service life of electrooptical device, has the advantages of simple structure and easy realization.

Description

A kind of Soft X-ray microimaging detector
Technical field
The present invention relates to micro-imaging technique fields, relate more specifically to a kind of Soft X-ray microimaging detector.
Background technique
Traditional optical microscopy imaging technology is imaged using visible light (wave-length coverage 390nm~700nm), due to by To the limitation of diffraction limit, resolution ratio is extremely difficult to 200nm or less.Electron Microscope images technology is imaged using electronics, Although resolution ratio improve, since the penetration capacity of electronics is weak, can not penetrating cell to cell interior carry out three-dimensional imaging;Together When, whens Electron Microscope images, needs to be sliced biological sample, be dehydrated etc. processing, this undoubtedly destroys the interior of sample Portion's structural information, it is impossible to which complete water-containing cell is imaged.
X-ray has very high penetrating power, many substances opaque to visible light can be penetrated, in general, wavelength is less than The title Super-hard X-ray of 0.1 Ethylmercurichlorendimide, title hard X ray of the wavelength within the scope of 0.1~10 Ethylmercurichlorendimide, wavelength is in 10~100 Ethylmercurichlorendimide ranges Interior title grenz ray.In recent years, grenz ray is gradually applied in micro-imaging technique.Compared to optical microscopy imaging and electricity Sub- microscope imaging technology, Soft X-ray microimaging technology have its unique advantage.
Grenz ray of the Soft X-ray microimaging technology using wavelength much smaller than visible wavelength is imaged, theoretic Limiting resolution can reach 1.2nm;Meanwhile in the section of certain wavelength of soft X-ray, for example, wavelength 2.3nm~4.4nm, energy Measure 284eV~534eV, the high an order of magnitude of absorptance water of protein, lipid and other carbon containing, nitrogen compounds to photon, In Water environment is transparent relative to biological sample in the wave band, can provide clearly cell image by nature contrast.Therefore, soft X is penetrated Line micro-imaging technique sample used, which is typically without, to be carried out dehydrating, can without the state for being in high vacuum when observation Preferably show the nature of organism, and the bio-imaging information of quantitative.Further pass through tomographic imaging and three-dimensional Reconfiguration technique, Soft X-ray microimaging technology can also obtain the three-dimensional fine structure of cell interior.
Soft X-ray microimaging equipment uses soft x-ray detector to obtain the structure data for projection of sample, therefore, soft X Ray detector is the key factor for influencing equipment imaging effect.Soft x-ray detector can be divided into indirect detection type and directly Detecting, wherein grenz ray is converted into visible light using fluorescent screen, scintillation crystal etc. by indirect detection type, then by with flashing The electrooptical device of crystal coupling is detected, and indirect detection type has high dynamic range, wide energy coverage area, CCD core The advantages that piece service life is long;Direct detection type then utilizes depletion layer interaction in the photon and detector chip of grenz ray to generate Electron hole pair realize detection, direct detection type have many advantages, such as spatial resolution height, high sensitivity.For example, common is straight The quantum efficiency of the Soft X-Ray Region of detecting is connect up to 80% or more, Pixel Dimensions at 15 microns or less.
There are still problems for traditional soft x-ray detector, for example, traditional grenz ray imaging device uses laser Plasma is as light source, and not only Soft X-Ray Region radiation efficiency is low, but also along with from visible light to X-ray broadband range Interior electromagnetic interference, these visible lights, ultraviolet light and X-ray are difficult to be purged using conventional light path design, can be right Imaging makes a big impact;Simultaneously because the intensity of light source of Soft X-ray microimaging instrument is weaker, traditional ccd detector is logical Time exposure is crossed to obtain imaging picture, is a kind of week that the duration is very short using the grenz ray that laser plasma generates The pulse of phase property, within this section of time for exposure, effective duration proportion very little of grenz ray causes a large amount of noise Accumulation, reduces imaging signal to noise ratio.Secondly, traditional soft x-ray detector is detected using direct detection type CCD, CCD core Piece is exposed outside, is easy to be contaminated by dust, splash etc., damage;Therefore, it is necessary to optional equipment filter discs, and filter disc is generally by several The metallic film of hundred nanometer thickness is constituted, using metal mesh as support, it is easy to damage.Again, traditional grenz ray, which is imaged, visits The X-ray that survey device not can avoid higher-energy directly radiates on CCD chip, can not only generate noise jamming, make for a long time With can also damage chip.In addition, equipment also needs the optical devices such as optional equipment aperture, cone, use it is sufficiently complex, Light leakage phenomena generation is not can avoid.
Summary of the invention
The object of the present invention is to provide a kind of Soft X-ray microimaging detectors, to solve the problems, such as above-mentioned at least one.
Soft X-ray microimaging detector provided by the invention, which includes cavity, glimmering Light conversion screen and electrooptical device, cavity include the first opening and the second opening, and the inside cavity is provided with will be from institute The light for stating the incidence of the first opening reflexes to the reflection device of second opening, and the light is open from described first to described The direction and there is the first angle from the reflection device between the direction of the second opening propagation that reflection device is propagated;Institute It states fluorescence conversion screen and is set to first opening;The electrooptical device is set to second opening, the light Power conversion device, the fluorescence conversion screen and the cavity form confined space.
According to one embodiment of present invention, the cavity includes interconnected the first cavity and the second cavity, described First opening is located on first cavity, and second opening is located on second cavity.
According to one embodiment of present invention, is formed between first cavity and the extending direction of second cavity Two angles, second angle are identical as the size of first angle.
According to one embodiment of present invention, the range of first angle is between 30 ° -270 °.
According to one embodiment of present invention, the fluorescence conversion screen is scintillation material, and the scintillation material includes silicic acid Yttrium lutetium, sodium iodide, cesium iodide, bismuth germanium oxide, cesium iodide, ceramic scintillator or plastic scintillant.
According to one embodiment of present invention, the direction of propagation of the plane where the fluorescence conversion screen and the light is hung down Directly, the thickness of the fluorescence conversion screen is between 10 μm -100 μm.
According to one embodiment of present invention, filter disc is provided on the surface of the fluorescence conversion screen.
According to one embodiment of present invention, less than 1%, the soft X of the filter disc is penetrated the visible light transmittance of the filter disc Line transmitance is not less than 60%.
According to one embodiment of present invention, the thickness of the filter disc is between 60nm-500nm.
According to one embodiment of present invention, the filter disc is aluminium, titanium, copper, iron, gold or nickel.
According to one embodiment of present invention, it is anti-not less than 98% to be provided with light reflectivity for the surface of the reflection device Penetrate film.
According to one embodiment of present invention, the electrooptical device is silicon photo multiplier device.
According to one embodiment of present invention, the first condenser lens is additionally provided in the cavity, described first focuses thoroughly Mirror is between the reflection device and the electrooptical device.
According to one embodiment of present invention, focus lens group is provided in the cavity, the focus lens group includes It is set between the reflection device and the electrooptical device and the first condenser lens being parallel to each other and second focuses thoroughly Mirror.
According to one embodiment of present invention, first opening is provided with adjusting aperture, inside the adjusting aperture Hollow and have loophole, the loophole is oppositely arranged with the fluorescence conversion screen.
According to one embodiment of present invention, second opening is provided with cooling-part, and the cooling-part is to institute State the transmitting of electrooptical device heat.
Soft X-ray microimaging detector provided by the invention, by by light path design at the deflection with certain angle It avoids grenz ray to be directly radiated on electrooptical device, improve Effect on Detecting while extending electrooptical device Service life, it is also an option that different optical path lengths is to meet the imaging demands of different spatial resolutions.The present invention is further By the way that filter disc is arranged in fluorescence conversion screen, the conversion quality of grenz ray can be improved, while guaranteeing that filter disc is less likely to be damaged, It avoids generating light leakage phenomena.In addition, the configuration of the present invention is simple, it is easy to accomplish, save the cost.
Detailed description of the invention
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below There is attached drawing needed in technical description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this The some embodiments recorded in invention, for those of ordinary skill in the art, in the premise of not making the creative labor property Under, it is also possible to obtain other drawings based on these drawings.
Fig. 1 is the diagrammatic cross-section of Soft X-ray microimaging detector according to an embodiment of the invention;
Fig. 2 is the diagrammatic cross-section of Soft X-ray microimaging detector in accordance with another embodiment of the present invention;
Fig. 3 is the diagrammatic cross-section of the Soft X-ray microimaging detector of another embodiment according to the present invention;
Fig. 4 is the diagrammatic cross-section of Soft X-ray microimaging detector in accordance with another embodiment of the present invention;
Fig. 5 is the diagrammatic cross-section of the Soft X-ray microimaging detector of another embodiment according to the present invention;
Fig. 6 is the diagrammatic cross-section of Soft X-ray microimaging detector in accordance with another embodiment of the present invention.
Specific embodiment
Below in conjunction with specific embodiment, the present invention will be further described.It should be understood that following embodiment is merely to illustrate this The range of invention and is not intended to limit the present invention.
It should be noted that it can directly set when component/part is referred to as on " setting exists " another component/part It sets on another component/part or there may also be component/parts placed in the middle.When component/part is referred to as " connection/connection Connect " to another component/part, it, which can be, is directly connected to/is attached to another component/part or may be simultaneously present residence Middle component/part.Term as used herein " connection/connection " may include electrical and/or mechanical-physical connection/connection.This Term "comprises/comprising" used in text refers to feature, step or the presence of component/part, but is not precluded one or more Other feature, step or the presence of component/part or addition.Term as used herein "and/or" includes one or more phases Close any and all combinations of listed item.
Unless otherwise defined, all technical and scientific terms used herein and the technical field for belonging to the application The normally understood meaning of technical staff is identical.Term used herein is intended merely to the purpose of description specific embodiment, and It is not intended to limitation the application.
In addition, term " first ", " second " etc. are used for description purposes only pair similar with distinguishing in the description of the present application As between the two and sequencing being not present, indication or suggestion relative importance can not be interpreted as.In addition, the application's In description, unless otherwise indicated, the meaning of " plurality " is two or more.
Fig. 1 is the diagrammatic cross-section of Soft X-ray microimaging detector according to an embodiment of the invention, can by Fig. 1 Know, Soft X-ray microimaging detector provided by the invention include at least cavity 10, fluorescence conversion screen 20, reflection device 30 with And electrooptical device 40, wherein cavity 10 includes the first cavity 11 and the second cavity between extending direction at an angle 12, the first cavity 11 and the second cavity 12 are interconnected and end is respectively arranged with opening, and the opening of the first cavity 11 is set It is equipped with fluorescence conversion screen 20, the opening of the second cavity 12 is provided with electrooptical device 40, and reflection device 30 is set to cavity 10 inside and the junction for being located at the first cavity 11 and the second cavity 12, the position of reflection device 30 is adjustable so that from the The light of one cavity, 11 opening incidence, which can be reflected by reflection device 30 and pass through the second cavity 12, is mapped to electrooptical device On 40.
More specifically, cavity 10 can be using the material production that can shield grenz ray, such as lead, the thickness of cavity 10 It can be selected according to related radiation protection standard, the first cavity 11 and the second cavity 12 of cavity 10 are preferably manufactured to cylindrical shape, It will be appreciated by those skilled in the art that cavity 10 can also be made as other shapes, such as rectangular section tube or variable cross-section Pipe etc., details are not described herein.
Fluorescence conversion screen 20 is preferably using the material that grenz ray can be converted to visible light, such as scintillation crystal, packet Include LYSO, NaI, BGO, CsI etc.;The propagation of the extending direction or light of plane and the first cavity 11 where fluorescence conversion screen 20 Direction is vertical, and the shape of fluorescence conversion screen 20 is preferably matched with the shape of the cross section of the first cavity 11, so as to pass through Fluorescence conversion screen 20 is fixed on the opening of the first cavity 11 by conventional sealing technology;The thickness of fluorescence conversion screen 20 is preferably Between 10 μm -100 μm, more preferably between 20 μm -50 μm, so that fluorescence conversion screen 20 will can effectively enter The grenz ray penetrated is converted to visible light.
Further, Soft X-ray microimaging detector provided by the invention can also include filter disc 21, and filter disc 21 is arranged In in fluorescence conversion screen 20, filter disc 21 is preferably plated on by fluorescence conversion screen using coating process (such as technique for vacuum coating etc.) On 20 outer surfaces;The preferably use of filter disc 21 can filter out visible light and material, such as aluminium, nickel etc. through grenz ray;Filter The thickness of piece 21 is preferably ranges between 60nm-500nm, more preferably 100nm, so that filter disc 21 can effectively be gone Except the visible component in incident light, through the grenz ray of the overwhelming majority.Those skilled in the art should be noted that selection Filter disc 21 grenz ray transmitance should be made not less than 60%, it is seen that light transmission rate is lower than 1%, the measurement of specific transmitance For technical means commonly used by such a person skilled in the art, details are not described herein.Plated film is carried out using on the surface of fluorescence conversion screen 20 Filter disc 21 is made, fluorescence conversion screen 20 can be effectively utilized as support protection, so that filter disc 21 is less likely to be damaged, mention significantly High service life, while adopting coating film treatment and being also possible that the completely covering fluorescence conversion screen 20 of filter disc 21, it is existing to avoid light leakage The generation of elephant.
Reflection device 30 preferably uses reflecting mirror, and reflective film can be set in the surface of reflection device 30, for example is arranged The high-reflecting film of assembly of thin films material, the thickness of reflective film and period can be set according to the peak wavelength of fluorescence conversion screen 20 Meter, it is therefore an objective to so that visible reflectance is maintained at 98% or more, guarantee the propagation efficiency of visible light.Reflection device 30 can change The direction of propagation on darkening road, so that a part of grenz ray through fluorescence conversion screen 20 will not be irradiated to electrooptical device 40 On, avoid noise jamming and chip damage.
Electrooptical device 40 receives fluorescence conversion screen 20 and converts and pass through the visible light that reflection device 30 reflects, simultaneously These visible lights are converted into electric signal, electric signal is further transmitted by the electronic system connecting with electrooptical device 40 It is handled to computer, specific signal processing belongs to technical means commonly used by such a person skilled in the art, and details are not described herein. Electrooptical device 40 preferably uses silicon photo multiplier device (SiPM), the number that SiPM can be independently read out using each channel Change design technology, while meeting highly sensitive, single pixel size is at 30 microns hereinafter, performance is splendid.Those skilled in the art Member is it should be noted that the refreshing frequency of electrooptical device 40 should be with the plasma light pulse for generating grenz ray Frequency matching, the i.e. refreshing frequency of electrooptical device 40 are matched not less than the frequency of plasma light pulse, preferably the two frequency Rate is identical to realize optimal detection efficient.
In the embodiment in figure 1, Soft X-ray microimaging detector provided by the invention can also include that the first focusing is saturating Mirror 50, the first condenser lens 50 are installed in cavity 10 and between 30 remaining light power conversion device 40 of reflection device, at this point, glimmering The distance between light conversion screen 20 and reflection device 30 be L, between reflection device 30 and the center of the first condenser lens 50 away from From for H, the distance between the center of the first condenser lens 50 and electrooptical device 40 are S, can be made by adjusting L, H and S Visible light focuses on electrooptical device 40, is conducive to the signal changing effect for improving electrooptical device 40.
It is worth noting that, after cavity 10, fluorescence conversion screen 20 and electrooptical device 40 are installed, cavity 10 Inside be it is closed lighttight, this, which is conducive to improve transmitting of the visible light converted of fluorescence conversion screen 20 cavity 10 inside, imitates Rate.
Fig. 2 is the diagrammatic cross-section according to the Soft X-ray microimaging detector of another embodiment of the present invention, Fig. 2's Embodiment is compared with the embodiment of Fig. 1, and same or similar component is indicated by increasing by 100 appended drawing reference, herein Only description and the different part of a upper embodiment.In the embodiment of fig. 2, the grenz ray caused by the soft X_ray source When being incident on fluorescence conversion screen 120 across filter disc 121, a part of grenz ray is converted to visible light by fluorescence conversion screen 120, can The light-exposed folding angles α reflected after reflection device 130 that is incident on along the first cavity 111 is 60 degree, those skilled in the art Member according to different paths it should be noted that need and observation needs, and (i.e. light is from the first chamber by the folding angles α of optical path Body 111 is mapped to the total angle reflected after reflection device 130) it is preferably ranges between 30 ° -270 °.Those skilled in the art It should be noted that the essence of cavity 100 is so that the optical path of visible light changes, so that electrooptical device is no longer at In the incident direction of grenz ray, so that noise jamming and chip be avoided to damage, the quality of signal conversion, therefore, cavity are improved The shape of 100 concrete shape or the first cavity and the second cavity should not become limitation of the invention, and details are not described herein.
Fig. 3 is the diagrammatic cross-section according to the Soft X-ray microimaging detector of another embodiment of the present invention, Fig. 3's Embodiment is compared with the embodiment of Fig. 1, and same or similar component is indicated by increasing by 200 appended drawing reference, herein Only description and the different part of Fig. 1 embodiment.In the fig. 3 embodiment, Soft X-ray microimaging detector can also wrap It includes and adjusts aperture 260, adjust the opening that aperture 260 is set to the first cavity 211, the inside for adjusting aperture 260 is hollow knot Structure and there is loophole 261, the diameter of loophole 261 is less than the diameter for adjusting 260 interior hollow section of aperture, while light transmission 261 face filter disc 221 of hole and fluorescence conversion screen 220, the diameter of loophole 261, which can according to need, selects different sizes.Soft X After the grenz ray that ray source generates passes through sample, stray light therein can be effectively removed by adjusting aperture 260, so that by Effective grenz ray of sample enters directive filter disc 221 by loophole 261, prevents the interference of refracted light.
Fig. 4 is the diagrammatic cross-section according to the Soft X-ray microimaging detector of another embodiment of the present invention, Fig. 4's Embodiment is compared with the embodiment of Fig. 1, and same or similar component is indicated by increasing by 300 appended drawing reference, herein Only description and the different part of Fig. 1 embodiment.In the fig. 4 embodiment, Soft X-ray microimaging detector can also wrap Cooling-part 370 is included, cooling-part 370 is set to the opening of the second cavity 312, cooling-part 370 and electrooptical device 340 can carry out heat transmitting to cool down to electrooptical device 340.Cooling-part 370 should have the system at least down to -60 DEG C Cold energy power is to guarantee the thermal noise for having enough abilities to reduce electrooptical device 340.
Fig. 5 is the diagrammatic cross-section according to the Soft X-ray microimaging detector of another embodiment of the present invention, Fig. 5's Embodiment is compared with the embodiment of Fig. 4, and same or similar component is indicated by increasing by 100 appended drawing reference, herein Only description and the different part of Fig. 4 embodiment.In the 5 embodiment of figure 5, the first condenser lens 450 and electrooptical device In addition second condenser lens 451 is provided between 440, the first condenser lens 450 constitutes poly- with the second condenser lens 451 Focus lens group, at this point, the distance between fluorescence conversion screen 420 and reflection device 430 are L, reflection device 430 and condenser lens The distance between 450 center is H, and the distance between the center of condenser lens 450 and the second condenser lens 451 are M, and second is poly- The distance between focus lens 451 and electrooptical device 440 are N, and the size by adjusting L, H and M, N can make visible light more It focuses on well on electrooptical device 440, is conducive to the signal changing effect for improving electrooptical device 440.
Fig. 6 is the diagrammatic cross-section according to the Soft X-ray microimaging detector of another embodiment of the present invention, Fig. 6's Embodiment is compared with the embodiment of Fig. 2, and same or similar component is indicated by increasing by 400 appended drawing reference, herein Only description and the different part of Fig. 2 embodiment.In the embodiment in fig 6, cavity 510 includes the first cavity interconnected 511 and second cavity 512, the first cavity 511 and the second cavity 512 is interconnected and end is respectively arranged with opening, wherein The first opening of end setting of first cavity 511, the second opening of end setting of the second cavity 512, the first cavity 511 The center line of extending direction l by a dotted line1It indicates, the center line of the extending direction of the second cavity 512 l by a dotted line3It indicates, instead Emitter part 530 is set to the junction of the first cavity 511 and the second cavity 512, and reflection device 530 will be from the incidence of the first opening Light reflex to the second opening, at this point, light from first be open to reflection device propagate direction and l1It is overlapped, light is by reflection The l by a dotted line of the direction of propagation afterwards2It indicates, by the incident direction l of light1With reflection direction l2Between angle be known as the first angle α, by the extending direction l of the first cavity 5111With the extending direction l of the second cavity 5123Between angle be known as the second angle β, can With discovery, in the embodiment in fig 6, the first angle α can be different from the size of the second angle β.It is opened in order to facilitate observation, second The plane where electrooptical device 540 and condenser lens 550 at mouthful is generally in a horizontal direction.
The present invention is placed in by sample when in use, and fluorescence conversion screen is placed towards sample, the soft X that soft X_ray source generates After ray passes through sample, it may be adjusted the loophole on aperture and be incident on fluorescence conversion screen, fluorescence conversion screen is by grenz ray Be converted to visible light, it is seen that light further passes through the reflection directive electrooptical device of reflection device, light in closed cavity Power conversion device will be seen that light is converted to electric signal and exports and be further processed.The present invention is filtered by being arranged in fluorescence conversion screen Piece, can be improved the conversion quality of grenz ray, while guarantee that filter disc is less likely to be damaged, and avoid generating light leakage phenomena;The present invention is logical It crosses and light path design is avoided into grenz ray at the deflection with certain angle is directly radiated on electrooptical device, improve Effect on Detecting extends the service life of electrooptical device simultaneously, can also adjust the length of optical path to meet different spaces point The imaging demand of resolution;In addition, electrooptical device uses SiPM, be conducive to carry out electric signal totally digitilized sampling processing, The frequency of plasma light pulse can not only be preferably matched, has more saved cost while guaranteeing Effect on Detecting.
Above-described, only presently preferred embodiments of the present invention, the range being not intended to limit the invention, of the invention is upper Stating embodiment can also make a variety of changes.Made by i.e. all claims applied according to the present invention and description Simply, equivalent changes and modifications fall within the claims of the invention patent.The not detailed description of the present invention is Routine techniques content.

Claims (16)

1. a kind of Soft X-ray microimaging detector, which is characterized in that the Soft X-ray microimaging detector includes:
Cavity, the cavity include the first opening and the second opening, and the inside cavity is provided with will be from first opening Incident light reflexes to the reflection device of second opening, and the light is open from described first and propagates to the reflection device Direction and from the reflection device to it is described second opening propagate direction between have the first angle;
Fluorescence conversion screen, the fluorescence conversion screen are set to first opening;And
Electrooptical device, the electrooptical device are set to second opening, the electrooptical device, described glimmering Light conversion screen and the cavity form confined space.
2. Soft X-ray microimaging detector according to claim 1, which is characterized in that the cavity includes mutually interconnecting Logical the first cavity and the second cavity, first opening are located on first cavity, and second opening is located at described the On two cavitys.
3. Soft X-ray microimaging detector according to claim 2, which is characterized in that first cavity with it is described The second angle is formed between the extending direction of second cavity, second angle is identical as the size of first angle.
4. Soft X-ray microimaging detector according to claim 1, which is characterized in that the range of first angle Between 30 ° -270 °.
5. Soft X-ray microimaging detector according to claim 1, which is characterized in that the fluorescence conversion screen is to dodge Bright material, the scintillation material includes yttrium luetcium silicate, sodium iodide, cesium iodide, bismuth germanium oxide, cesium iodide, ceramic scintillator or modeling Expect scintillator.
6. Soft X-ray microimaging detector according to claim 1, which is characterized in where the fluorescence conversion screen Plane it is vertical with the direction of propagation of the light, the thickness of the fluorescence conversion screen is between 10 μm -100 μm.
7. Soft X-ray microimaging detector according to claim 1, which is characterized in that the table of the fluorescence conversion screen Filter disc is provided on face.
8. Soft X-ray microimaging detector according to claim 7, which is characterized in that the visible light of the filter disc is saturating Rate is crossed less than 1%, the grenz ray transmitance of the filter disc is not less than 60%.
9. Soft X-ray microimaging detector according to claim 7, which is characterized in that the thickness of the filter disc between Between 60nm-500nm.
10. Soft X-ray microimaging detector according to claim 7, which is characterized in that the filter disc be aluminium, titanium, Copper, iron, gold or nickel.
11. according to claim 1 or Soft X-ray microimaging detector described in 7, which is characterized in that the reflection device Surface be provided with light reflectivity be not less than 98% reflective film.
12. Soft X-ray microimaging detector according to claim 1, which is characterized in that the electrooptical device is Silicon photo multiplier device.
13. Soft X-ray microimaging detector according to claim 1, which is characterized in that be additionally provided in the cavity First condenser lens, first condenser lens is between the reflection device and the electrooptical device.
14. Soft X-ray microimaging detector according to claim 1, which is characterized in that be provided in the cavity poly- Focus lens group, the focus lens group include being set between the reflection device and the electrooptical device and being parallel to each other The first condenser lens and the second condenser lens.
15. Soft X-ray microimaging detector according to claim 1, which is characterized in that the first opening setting There is an adjusting aperture, the adjusting aperture inner hollow and there is loophole, the loophole is opposite with the fluorescence conversion screen to be set It sets.
16. Soft X-ray microimaging detector according to claim 1, which is characterized in that the second opening setting There is cooling-part, the cooling-part is transmitted to the electrooptical device heat.
CN201910771982.7A 2019-08-21 2019-08-21 A kind of Soft X-ray microimaging detector Pending CN110455835A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2021031936A1 (en) * 2019-08-21 2021-02-25 苏州瑞派宁科技有限公司 Soft x-ray microscopic imaging detector

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