CN110394205A - A kind of distiller - Google Patents
A kind of distiller Download PDFInfo
- Publication number
- CN110394205A CN110394205A CN201910817541.6A CN201910817541A CN110394205A CN 110394205 A CN110394205 A CN 110394205A CN 201910817541 A CN201910817541 A CN 201910817541A CN 110394205 A CN110394205 A CN 110394205A
- Authority
- CN
- China
- Prior art keywords
- distillation
- collector
- chamber
- distiller
- communicating pipe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000004821 distillation Methods 0.000 claims abstract description 79
- 239000000463 material Substances 0.000 claims abstract description 8
- 239000010453 quartz Substances 0.000 claims abstract description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000005485 electric heating Methods 0.000 claims abstract description 5
- 239000007788 liquid Substances 0.000 claims description 34
- 238000004140 cleaning Methods 0.000 claims description 30
- 239000002699 waste material Substances 0.000 claims description 16
- 239000011521 glass Substances 0.000 claims description 8
- 238000009835 boiling Methods 0.000 claims description 7
- 238000009833 condensation Methods 0.000 claims description 6
- 239000011324 bead Substances 0.000 claims description 5
- 238000000465 moulding Methods 0.000 claims description 3
- 239000003292 glue Substances 0.000 claims 1
- 230000003670 easy-to-clean Effects 0.000 abstract description 4
- 239000000243 solution Substances 0.000 description 13
- 238000000034 method Methods 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 238000012864 cross contamination Methods 0.000 description 4
- 239000012153 distilled water Substances 0.000 description 4
- 238000004080 punching Methods 0.000 description 4
- 229920006395 saturated elastomer Polymers 0.000 description 4
- 238000002386 leaching Methods 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 2
- 238000009841 combustion method Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 230000017525 heat dissipation Effects 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 1
- 230000009172 bursting Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002309 gasification Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000012913 prioritisation Methods 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L3/00—Containers or dishes for laboratory use, e.g. laboratory glassware; Droppers
- B01L3/16—Retorts
Landscapes
- Health & Medical Sciences (AREA)
- Clinical Laboratory Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The present invention discloses a kind of distiller, including distillation cascade, collector and communicating pipe, the distillation cascade is made of quartz material, and distillation cascade is placed in control-temperature electric heating set, the distillation cascade is equipped with distillation chamber, distill the inlet that bottom of chamber portion is equipped with connection distillation chamber, the collector is equipped with collecting chamber, collecting chamber bottom is equipped with the fraction collection mouth of connection collecting chamber, the collector is located at below the distillation cascade, the distillation cascade is connected to collector by communicating pipe, the upper end of the communicating pipe extends to distillation top of chamber, the lower end of the communicating pipe extends to collector bottom, the exhaust outlet put outside is opened up at the top of the collector.This case is easy to operate compared to common open distiller, behaves simpler, realizes integrated distillation, reduces the working strength and operational risk of operator, have a wide range of application, and can manually or automatically clean, easy to clean.
Description
Technical field
The present invention relates to experimental instrument field, in particular to a kind of distiller.
Background technique
As shown in Figure 1, common distillation apparatus is assembled using multiple glass components, such as alcolhol burner 1 ', flask 2 ', condensation
The connection of device 3 ', receiving bottle 4 ' etc., each glass assembly is installed and complicated operation, and volume is big and to air-tightness requirement
Height, because whole system be it is open, energy consumption is high, needs when operation carefully to avoid scalding.
Distillation procedure process heats flask using modes such as alcolhol burner or electric heaters, is formed and is steamed after liquid boiling in flask
Vapour enters condenser pipe, and steam is made to be cooled to liquid after cold water flows through condenser pipe, flows into conical flask and is collected, then carries out
Subsequent detection or processing.
It can just be continued to use using finishing to need to dismantle device and cleaned, it is relatively complicated.It is especially noted that observation is steamed
It evaporates flask liquid level and forbids dry combustion method, flask can otherwise burst and causes danger, vessel often occur in normal operation
Splintering problem, distillation procedure are work more dangerous in laboratory.
Summary of the invention
The purpose of the present invention is to provide it is a kind of can integrated distillation distiller, reduce operator working strength and
Operational risk, and structure is simple, has a wide range of application.
In order to achieve the above objectives, technical scheme is as follows:
A kind of distiller, including distillation cascade, collector and communicating pipe, the distillation cascade are made of quartz material, and distill
Pipe is placed in control-temperature electric heating set；
The distillation cascade is equipped with distillation chamber, and distillation bottom of chamber portion is equipped with the inlet of connection distillation chamber, and the collector is equipped with
Collecting chamber, collecting chamber bottom are equipped with the fraction collection mouth of connection collecting chamber；
The collector is located at below the distillation cascade, and the distillation cascade is connected to collector, the connection by communicating pipe
The upper end of pipe extends to distillation top of chamber, and the lower end of the communicating pipe extends to collector bottom, opens at the top of the collector
If the exhaust outlet put outside.
Preferably, which is additionally provided with the first electric pump component, the second electric pump component or sebific duct, the first electric pump component
Or sebific duct is set to inlet position to control liquid disengaging, the second electric pump component or sebific duct be set to fraction collection mouth position with
Control liquid disengaging.
Preferably, the first electric pump component and the second electric pump component are respectively additionally provided with electric multi-way valve, the first electric pump component
Electric multi-way valve be used to switch the circulation of distillate bottle, cleaning solution bottle, waste liquid bottle and inlet, the second electric pump component
Electric multi-way valve be used to switch the circulation of fraction bottle, cleaning solution bottle, waste liquid bottle and fraction collection mouth.
Preferably, the communicating pipe is seperated molding, including connection upper tube and is connected to down tube, the upper end for being connected to upper tube
Distillation top of chamber is extended to, the lower end for being connected to upper tube externally protrudes out in below distillation cascade；The upper end of the connection down tube externally protrudes out in collection
Above device, the lower end for being connected to down tube extends to collector bottom, so that the lower end of connection upper tube is detachably connected connection down tube
Upper end.
Preferably, the lower end of the connection upper tube is connected with the upper end for being connected to down tube by a sealed connecting component.
Preferably, anticorrosive heat insulating gum cover can be used in the sealed connecting component, and anticorrosive heat insulating gum cover is coated on connection upper tube
The junction of lower end and the upper end for being connected to down tube.
Preferably, the distillation bottom of the tube is laid with anti-boiling bead.
Preferably, the collector bottom is laid with anti-condensation glass pearl.
Preferably, the collector can be made of quartz material.
Preferably, the distiller is equipped with link to hang distiller.
After adopting the above scheme, gain effect of the invention are as follows:
1) integrated distillation, easy to operate, without operational risk: distiller is mounted in control-temperature electric heating set, automatically controls temperature
Then liquid is added by inlet in degree, and by communicating pipe top into communicating pipe after liquid gasification, steam flows to always connection
It is condensed in the collector of bottom of the tube, collector is condensed with air cooling way, is not necessarily to extra heat dissipation component, and the exhaust outlet is used for
External pressure is balanced, to complete to distill, after distillation, carries out analysis or subsequent operation from fraction collection mouth discharge fraction.
Compared to existing open distiller, the present invention is behaved more simply, and security risk is minimized.
2) easy to clean: distilled water being added to distillation cascade by inlet or other cleaning solutions are saturated with distillation chamber, distills chamber
Waste liquid is discharged after punching leaching, repeats the process and carries out cleaning distillation chamber and communicating pipe.Collecting chamber similarly, by fraction collection mouth to
Distilled water is added in collector or other cleaning solutions are saturated with collecting chamber, and waste liquid is discharged after punching leaching collecting chamber, repeats cleaning, has cleaned
Next step distillation procedure can be carried out by finishing.Cleaning is avoided that cross contamination in this way, has benefited from the special knot of distillation cascade and collector
Otherwise structure is difficult to easy to clean, while no cross contamination.
3) delicate structure has a wide range of application: can be used as analysis Instrument part and conventional distil-lation device uses, save multiple components
Cost, no leakage problem.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of common distillation apparatus；
Fig. 2 is structural schematic diagram of the invention.
Description of symbols:
Distillation cascade 1, distillation chamber 11, inlet 12, collector 2, collecting chamber 21, collection port 22, exhaust outlet 23, communicating pipe 3,
It is connected to upper tube 31, is connected to upper tube upper end 311, is connected to upper tube lower end 312, is connected to down tube 32, down tube upper end 321 is connected to, under connection
Pipe lower end 322, sealed connecting component 33, the first electric pump component 4, the second electric pump component 5, anti-boiling bead 6, anti-condensation glass pearl 7.
Specific embodiment
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below
There is attached drawing needed in technical description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this
Some embodiments of invention without any creative labor, may be used also for those of ordinary skill in the art
To obtain other drawings based on these drawings, Fig. 2 is please referred to.
A kind of distiller, including distillation cascade 1, collector 2 and communicating pipe 3, the distillation cascade 1 are equipped with distillation chamber 11, distillation
11 bottom of chamber is equipped with the inlet 12 of connection distillation chamber, and the collector 2 is equipped with collecting chamber 21, and 21 bottom of collecting chamber is equipped with connection
The fraction collection mouth 22 of collecting chamber.
The collector 2 is located at 1 lower section of distillation cascade, makes distillation cascade 1 and collector 2 in distribution up and down, for convenience
The top of user's operation, the distiller is equipped with link, for hanging up the distiller.
The distillation cascade 1 extends to distillation chamber 11 and pushes up by being connected to collector 2, the upper end of the communicating pipe 3 communicating pipe 3
Portion, the lower end of the communicating pipe 3 extend to 2 bottom of collector, and the top of the collector 2 opens up the exhaust outlet 23 put outside, row
Port 23 is a hollow pipeline for balancing external pressure, communicating pipe 3.
The distillation cascade 1 and collector 2 are all made of quartz material, since communicating pipe 3 takes shape in distillation cascade 1 and collector
2, therefore quartz material can also be used in communicating pipe 3 is made.Quartz material can the long-term work under up to 1100 degree of hot environment, energy
Be resistant to suddenly cold and hot environment, make the distiller have compact-sized, corrosion-resistant, tolerable high-low temperature difference, can dry combustion method without bursting wind
The advantage of danger.Distillation cascade 1 is placed in control-temperature electric heating set, and then liquid, liquid gas is added by inlet 12 in A.T.C
Enter the top of communicating pipe 3 after change, steam flows to always to be condensed in the collector 2 of 3 bottom of communicating pipe, and collector 2 is with air-cooled
Mode condenses, and is not necessarily to extra heat dissipation component, completes distillation, after distillation, fraction is discharged from fraction collection mouth 22 and is analyzed
Or subsequent operation.It is easy to operate as long as can be achieved with integrated distillation using the present invention compared to common open distiller,
It behaves more simply, reduces the working strength and operational risk of operator.
The cleaning function including automatically and manually two ways, in order to realize the function, the distiller can be achieved in the present invention
Equipped with the first electric pump component 4, the second electric pump component 5 or sebific duct (not shown), the first electric pump component 4 or sebific duct are set to
For 12 position of inlet to control liquid disengaging, the second electric pump component 5 or sebific duct are set to 22 position of fraction collection mouth to control
Liquid disengaging, automation cleaning and Manual-cleaning are as follows,
Automation cleaning: distilled water or other cleanings are added to distillation cascade 1 using the first electric pump component 4 by inlet 12
Liquid is saturated with distillation chamber 11, and after the distillation punching leaching of chamber 11, the first electric pump component 4 reversion discharge waste liquid repeats the process and cleaned
Distill chamber 11 and communicating pipe 3.Collecting chamber 21 similarly, by fraction collection mouth 22 is added using the second electric pump component 5 to collector 2
Distilled water or other cleaning solutions are saturated with collecting chamber 21, and after collecting chamber 21 is soaked in punching, the second electric pump component 5 reversion discharge waste liquid can be weighed
Multiple cleaning, cleaning, which finishes, can carry out next step distillation procedure.Automation cleaning energy consumption is lower, has a wide range of application.
Manual-cleaning: being separately connected inlet 12, fraction collection mouth 22 using sebific duct manually, closes sebific duct to stop to steaming
It evaporates chamber 11 or collecting chamber 21 and injects liquid, sebific duct opens injection or discharge liquid when use, without dismantling component, operation side
Just, safety；Pipe clamp can be used to control in the switch of sebific duct.
Cleaning is avoided that cross contamination in this way, has benefited from the special construction of distillation cascade 1 and collector 2, is otherwise difficult to
Not only easy to clean, but also guarantee no cross contamination simultaneously.In addition, the component count of common distiller is more, cleaning water consumption is big, this hair
Bright structure is simple, can greatly save water resource.
Circulation of the inlet 12 generally between distillate bottle, cleaning solution bottle, waste liquid bottle needs artificial carry out more
It changes, similarly, fraction collection mouth 22 and fraction bottle, cleaning solution bottle, the circulation between waste liquid bottle are also required to artificially carry out
Replacement, in order to advanced optimize the first electric pump component 4 and the second electric pump component 5 described in the present embodiment, therefore in first electric pump
Respectively design has electric multi-way valve (not shown), the electric multi-way valve of the first electric pump component 4 for component 4 and the second electric pump component 5
It is electronic more at the second electric pump component 5 for switching the circulation of distillate bottle, cleaning solution bottle, waste liquid bottle and inlet
Port valve is used to switch the circulation of fraction bottle, cleaning solution bottle, waste liquid bottle and fraction collection mouth, to pass through electric multi-way valve
Switch different flow paths and different liquids transmission is realized in electric pump positive and negative rotation.Such as the operation of distillation cascade, electric multi-way valve go to distillation
Liquid bottle, is pumped into distillate；Distillation terminates, and electric multi-way valve goes to cleaning solution bottle, is pumped into cleaning solution, and electric multi-way valve turns again
To waste liquid bottle, the first electric pump component reversion extraction waste liquid；With should fraction need to collect when, it is electronic more at fraction collection mouth
Port valve goes to fraction bottle, pumps out fraction；Electric multi-way valve goes to cleaning solution bottle later, is pumped into cleaning solution, electric multi-way valve
Return again to waste liquid bottle, the second electric pump component reversion extraction waste liquid；The design helps to further realize automation cleaning and oneself
Dynamicization distillation, is not necessarily to manual operation, makes the present invention more toward automation, intelligent direction development.
As prioritization scheme of the invention, the communicating pipe 3 is seperated molding, including connection upper tube 31 be connected to down tube
32, the upper end 311 of the connection upper tube extends to 11 top of distillation chamber, and the lower end 312 for being connected to upper tube externally protrudes out under distillation cascade 1
Side；The upper end 321 of the connection down tube externally protrudes out in 2 top of collector, and the lower end 322 for being connected to down tube extends to 2 bottom of collector,
So that the lower end 312 of connection upper tube is detachably connected the upper end 321 of connection down tube, convenient for distiller disassembly storage；Further,
The lower end 312 of the connection upper tube and be connected to the upper end 321 of down tube by a sealed connecting component 33 connection, come guarantee air-tightness with
It prevents from revealing, anticorrosive heat insulating gum cover can be used in the sealed connecting component 33, and anticorrosive heat insulating gum cover is coated on the lower end of connection upper tube
312 play corrosion-resistant, heat-insulated effect with the junction for the upper end 321 for being connected to down tube, anticorrosive heat insulating gum cover.
In one embodiment, 1 bottom of distillation cascade is laid with anti-boiling bead 6, and anti-boiling bead 6 can effectively prevent distillation
Water bumping avoids unvaporized distillate from boiling and enters the upper end 311 of connection upper tube.2 bottom of collector is laid with condensation glass
Glass pearl 7,7 surface area of anti-condensation glass pearl is big, so that the steam in collector is condensed out.
Basic principles and main features and advantages of the present invention of the invention have been shown and described above.The skill of the industry
Art personnel it should be appreciated that the present invention is not limited to the above embodiments, the above embodiments and description only describe
The principle of the present invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these
Changes and improvements all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and
Its equivalent thereof.
Claims (10)
1. a kind of distiller, it is characterised in that: including distillation cascade, collector and communicating pipe, the distillation cascade is by quartz material system
At, and distillation cascade is placed in control-temperature electric heating set；
The distillation cascade is equipped with distillation chamber, and distillation bottom of chamber portion is equipped with the inlet of connection distillation chamber, and the collector, which is equipped with, to be collected
Chamber, collecting chamber bottom are equipped with the fraction collection mouth of connection collecting chamber；
The collector is located at below the distillation cascade, and the distillation cascade is connected to collector by communicating pipe, the communicating pipe
Upper end extends to distillation top of chamber, and the lower end of the communicating pipe extends to collector bottom, opens up at the top of the collector outer
The exhaust outlet put.
2. a kind of distiller according to claim 1, it is characterised in that: the distiller is additionally provided with the first electric pump component,
Two electric pump components or sebific duct, the first electric pump component or sebific duct are set to inlet position and are passed in and out with controlling liquid, and described second
Electric pump component or sebific duct are set to fraction collection mouth position to control liquid disengaging.
3. a kind of distiller according to claim 2, it is characterised in that: the first electric pump component and the second electric pump component
It is respectively additionally provided with electric multi-way valve, the electric multi-way valve of the first electric pump component is for switching distillate bottle, cleaning solution bottle, waste liquid
The circulation of bottle and inlet, the electric multi-way valve of the second electric pump component is for switching fraction bottle, cleaning solution bottle, waste liquid bottle
The circulation of son and fraction collection mouth.
4. a kind of distiller according to claim 1, it is characterised in that: the communicating pipe is seperated molding, including connection
Upper tube extends to distillation top of chamber with down tube, the upper end of the connection upper tube is connected to, and the lower end for being connected to upper tube externally protrudes out in distillation cascade
Lower section；The upper end of the connection down tube externally protrudes out in above collector, and the lower end for being connected to down tube extends to collector bottom, so that even
The lower end of logical upper tube is detachably connected the upper end of connection down tube.
5. a kind of distiller according to claim 4, it is characterised in that: it is described connection upper tube lower end be connected to down
The upper end of pipe is connected by a sealed connecting component.
6. a kind of distiller according to claim 5, it is characterised in that: anticorrosive heat insulating glue can be used in the sealed connecting component
Set, anticorrosive heat insulating gum cover are coated on lower end and the junction for the upper end for being connected to down tube of connection upper tube.
7. a kind of distiller according to claim 1, it is characterised in that: the distillation bottom of the tube is laid with anti-boiling bead.
8. a kind of distiller according to claim 1, it is characterised in that: the collector bottom is laid with anti-condensation glass pearl.
9. a kind of distiller according to claim 1, it is characterised in that: the collector can be made of quartz material.
10. a kind of distiller according to claim 1, it is characterised in that: the distiller is equipped with link to hang distillation
Device.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910817541.6A CN110394205A (en) | 2019-08-30 | 2019-08-30 | A kind of distiller |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910817541.6A CN110394205A (en) | 2019-08-30 | 2019-08-30 | A kind of distiller |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110394205A true CN110394205A (en) | 2019-11-01 |
Family
ID=68329601
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910817541.6A Withdrawn CN110394205A (en) | 2019-08-30 | 2019-08-30 | A kind of distiller |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110394205A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB743750A (en) * | 1952-08-06 | 1956-01-25 | Eastman Kodak Co | High vacuum fractional distillation apparatus |
| CN102661769A (en) * | 2012-05-07 | 2012-09-12 | 广州市怡文环境科技股份有限公司 | Distilling and condensing device and distilling and condensing method |
| CN104784956A (en) * | 2015-03-06 | 2015-07-22 | 兰州空间技术物理研究所 | Ultrahigh vacuum molecular distillation equipment |
| CN207300686U (en) * | 2017-10-30 | 2018-05-01 | 山东省环境监测中心站 | Determine nitrogen microdistillation device |
| US20180161693A1 (en) * | 2017-08-03 | 2018-06-14 | Elliot Kremerman | Integrated Distillation Chamber and Discharge Unit with Integrated Key |
| CN210474035U (en) * | 2019-08-30 | 2020-05-08 | 西安拜森仪器有限公司 | Distiller |
-
2019
- 2019-08-30 CN CN201910817541.6A patent/CN110394205A/en not_active Withdrawn
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB743750A (en) * | 1952-08-06 | 1956-01-25 | Eastman Kodak Co | High vacuum fractional distillation apparatus |
| CN102661769A (en) * | 2012-05-07 | 2012-09-12 | 广州市怡文环境科技股份有限公司 | Distilling and condensing device and distilling and condensing method |
| CN104784956A (en) * | 2015-03-06 | 2015-07-22 | 兰州空间技术物理研究所 | Ultrahigh vacuum molecular distillation equipment |
| US20180161693A1 (en) * | 2017-08-03 | 2018-06-14 | Elliot Kremerman | Integrated Distillation Chamber and Discharge Unit with Integrated Key |
| CN207300686U (en) * | 2017-10-30 | 2018-05-01 | 山东省环境监测中心站 | Determine nitrogen microdistillation device |
| CN210474035U (en) * | 2019-08-30 | 2020-05-08 | 西安拜森仪器有限公司 | Distiller |
Non-Patent Citations (1)
| Title |
|---|
| 王志祥;林文;于颖;: "分子蒸馏设备的现状及其展望", 化工进展, no. 03, pages 15 - 18 * |
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| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20191101 |
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| WW01 | Invention patent application withdrawn after publication |