CN210474035U - Distiller - Google Patents
Distiller Download PDFInfo
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- CN210474035U CN210474035U CN201921437624.4U CN201921437624U CN210474035U CN 210474035 U CN210474035 U CN 210474035U CN 201921437624 U CN201921437624 U CN 201921437624U CN 210474035 U CN210474035 U CN 210474035U
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- distillation
- pipe
- collector
- distiller
- communicating
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Abstract
The utility model discloses a distiller, including distillation tube, collector and communicating pipe, the distillation tube is made by quartz material, and during the distillation tube arranged in accuse temperature electric jacket, the distillation tube is equipped with the distillation chamber, and distillation chamber bottom is equipped with the inlet of intercommunication distillation chamber, the collector is equipped with collects the chamber, collects the chamber bottom and is equipped with the fraction collection mouth that the chamber was collected in the intercommunication, the collector is located the distillation tube below, the distillation tube passes through communicating pipe intercommunication collector, the upper end of communicating pipe extends to distillation chamber top, the lower extreme of communicating pipe extends to the collector bottom, the gas vent of putting outward is seted up at the top of collector. Compared with a common open distiller, the distiller has the advantages of simple operation, simplicity in operation, realization of integrated distillation, reduction of working strength and operation risk of operators, wide application range, manual or automatic cleaning and convenience in cleaning.
Description
Technical Field
The utility model relates to an experimental apparatus field, in particular to distiller.
Background
As shown in fig. 1, a common distillation apparatus is assembled by a plurality of glass components, such as an alcohol burner 1 ', a flask 2', a condenser 3 ', a receiving bottle 4', etc., and the connection, installation and operation of each glass component are complicated, the volume is large, and the requirement for airtightness is high.
The distillation process adopts the mode such as alcohol burner or electric heater heating flask, forms steam and gets into the condenser pipe after the liquid boils in the flask, makes the steam cooling become liquid after cold water flows through the condenser pipe, flows into the erlenmeyer flask and collects, carries out follow-up detection or processing again.
After the use, the device is required to be detached for cleaning so as to be used continuously, and the operation is complicated. Particular attention is paid to observing the liquid level of the distillation flask to avoid dry burning, otherwise the flask is cracked to cause danger, the problem of vessel breakage often occurs even in normal operation, and the distillation operation is dangerous work in a laboratory.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a distillatory can integrate, reduce operating personnel's working strength and operational risk, and simple structure, the range of application is wide.
In order to achieve the above object, the technical solution of the present invention is as follows:
a distiller comprises a distillation tube, a collector and a communicating tube, wherein the distillation tube is made of quartz material and is arranged in a temperature control electric heating jacket;
the distillation pipe is provided with a distillation cavity, the bottom of the distillation cavity is provided with a liquid inlet communicated with the distillation cavity, the collector is provided with a collection cavity, and the bottom of the collection cavity is provided with a fraction collection port communicated with the collection cavity;
the collector is located distillation tube below, the distillation tube passes through communicating pipe intercommunication collector, the upper end of communicating pipe extends to distillation chamber top, the lower extreme of communicating pipe extends to the collector bottom, the gas vent of putting outward is seted up at the top of collector.
Preferably, the distiller is further provided with a first electric pump assembly and a second electric pump assembly or a rubber pipe, wherein the first electric pump assembly or the rubber pipe is arranged at the liquid inlet position to control liquid to flow in and out, and the second electric pump assembly or the rubber pipe is arranged at the fraction collecting port position to control liquid to flow in and out.
Preferably, the first electric pump assembly and the second electric pump assembly are respectively provided with an electric multi-way valve, the electric multi-way valve of the first electric pump assembly is used for switching the circulation of the distillate bottle, the cleaning liquid bottle and the waste liquid bottle with the liquid inlet, and the electric multi-way valve of the second electric pump assembly is used for switching the circulation of the distillate bottle, the cleaning liquid bottle and the waste liquid bottle with the distillate collecting port.
Preferably, the communicating pipe is formed in a split mode and comprises a communicating upper pipe and a communicating lower pipe, the upper end of the communicating upper pipe extends to the top of the distillation cavity, and the lower end of the communicating upper pipe protrudes out of the lower portion of the distillation pipe; the upper end of the communicating lower pipe protrudes out of the collector, and the lower end of the communicating lower pipe extends to the bottom of the collector, so that the lower end of the communicating upper pipe can be detachably connected with the upper end of the communicating lower pipe.
Preferably, the lower end of the upper communicating pipe and the upper end of the lower communicating pipe are connected through a sealing connector.
Preferably, the sealing connecting piece can adopt an anticorrosion heat-insulation rubber sleeve, and the anticorrosion heat-insulation rubber sleeve is coated at the joint of the lower end of the communicated upper pipe and the upper end of the communicated lower pipe.
Preferably, the bottom of the distillation tube is paved with anti-boiling glass beads.
Preferably, the bottom of the collector is paved with condensation glass beads.
Preferably, the collector may be made of a quartz material.
Preferably, the retort is provided with a suspension loop to suspend the retort.
After the scheme is adopted, the utility model discloses a gain effect does:
1) the integrated distillation is simple to operate and has no operation risk: the distiller is installed in accuse temperature electric jacket, and the automatic control temperature, then add liquid through the inlet, get into communicating pipe through communicating pipe top behind the liquid gasification, steam always flows to and condenses in the collector of communicating pipe bottom, and the collector is with the air-cooled mode condensation, need not extra radiator unit, the gas vent is used for balanced external pressure to accomplish the distillation, after the distillation finishes, follow fraction collection mouth discharge fraction and carry out analysis or follow-up operation. Compare in current open distiller, the utility model discloses it is simpler and easy to move, falls to the minimum with safe risk.
2) The cleaning is convenient: distilled water or other cleaning liquid is added into the distillation tube through the liquid inlet to fully immerse the distillation cavity, waste liquid is discharged after the distillation cavity is immersed, and the process can be repeated to clean the distillation cavity and the communicating tube. And the collecting cavity is the same, distilled water or other cleaning solution is added into the collector through the fraction collecting port to fully immerse the collecting cavity, waste liquid is discharged after the collecting cavity is immersed, the cleaning can be repeated, and the next step of distillation operation can be carried out after the cleaning is finished. The cleaning can avoid cross contamination, and due to the special structure of the distillation tube and the collector, the cleaning is difficult to be convenient and the cross contamination is avoided.
3) The structure is exquisite, and the range of application is wide: the distillation column can be used as an analytical instrument component and a conventional distiller, saves a plurality of assembly costs, and has no leakage problem.
Drawings
FIG. 1 is a schematic view showing a structure of a general distillation apparatus;
fig. 2 is a schematic structural diagram of the present invention.
Description of reference numerals:
Detailed Description
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings needed to be used in the description of the embodiments or the prior art will be briefly introduced below, it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the drawings without inventive labor, please refer to fig. 2.
The utility model provides a distiller, includes distillation tube 1, collector 2 and communicating pipe 3, distillation tube 1 is equipped with distillation chamber 11, and distillation chamber 11 bottom is equipped with the inlet 12 of intercommunication distillation chamber, collector 2 is equipped with collects chamber 21, collects chamber 21 bottom and is equipped with the fraction collection mouth 22 that the chamber was collected in the intercommunication.
The collector 2 is positioned below the distillation tube 1, so that the distillation tube 1 and the collector 2 are distributed up and down, and a hanging ring is arranged at the top of the distiller to hang the distiller for the convenience of operation of a user.
The distillation tube 1 and the collector 2 are both made of quartz material, and the communicating tube 3 can also be made of quartz material because the communicating tube 3 is formed on the distillation tube 1 and the collector 2. The quartz material can work for a long time in a high-temperature environment as high as 1100 ℃, and can resist a quenching and shock heating environment, so that the distiller has the advantages of compact structure, corrosion resistance, high and low temperature difference resistance, and dry burning without explosion risk. During the temperature control electric jacket was arranged in to distillation tube 1, the automatic control temperature, then added liquid through inlet 12, got into communicating pipe 3 top behind the liquid gasification, steam always flowed to and condenses in collector 2 communicating pipe 3 bottom, and collector 2 need not extra radiator unit with the air-cooled mode condensation, accomplishes the distillation, after the distillation finishes, carries out analysis or follow-up operation from fraction collection port 22 discharge fraction. Compare in ordinary open distiller, as long as adopt the utility model discloses just can realize the integration distillation, easy operation, it is simpler and easy to move, reduces operating personnel's working strength and operational risk.
The utility model can realize the cleaning function which comprises an automatic mode and a manual mode, in order to realize the cleaning function, the distiller is provided with a first electric pump component 4, a second electric pump component 5 or a rubber tube (not shown in the figure), the first electric pump component 4 or the rubber tube is arranged at the position of the liquid inlet 12 to control the liquid to flow in and out, the second electric pump component 5 or the rubber tube is arranged at the position of the fraction collecting port 22 to control the liquid to flow in and out, the automatic cleaning and the manual cleaning are as follows,
automatic cleaning: distilled water or other cleaning solution is added into the distillation pipe 1 through the liquid inlet 12 by using the first electric pump assembly 4 to fully immerse the distillation cavity 11, after the distillation cavity 11 is immersed, the first electric pump assembly 4 reversely rotates to discharge waste liquid, and the process can be repeated to clean the distillation cavity 11 and the communicating pipe 3. The collecting cavity 21 is similar, distilled water or other cleaning solution is added into the collector 2 through the fraction collecting port 22 by using the second electric pump assembly 5 to fully immerse the collecting cavity 21, after the collecting cavity 21 is immersed, the second electric pump assembly 5 reversely rotates to discharge waste liquid, cleaning can be carried out repeatedly, and next distillation operation can be carried out after cleaning is finished. The automatic cleaning energy consumption is low, and the application range is wide.
And (3) manual cleaning: the rubber tube is manually used to be respectively connected with the liquid inlet 12 and the fraction collecting port 22, the rubber tube is closed to stop injecting liquid into the distillation cavity 11 or the collecting cavity 21, and the rubber tube is opened to inject or discharge the liquid when in use, so that the parts do not need to be disassembled, and the operation is convenient and safe; the opening and closing of the rubber tube can be controlled by a tube clamp.
The cleaning can avoid cross contamination, and due to the special structure of the distillation tube 1 and the collector 2, the cleaning is not convenient, and the cross contamination is avoided. In addition, the subassembly of ordinary distiller is in large quantity, and it is big to wash the water quantity, the utility model discloses simple structure can save the water resource greatly.
The liquid inlet 12 is typically manually exchanged for communication with a distillate bottle, a cleaning solution bottle, and a waste solution bottle, and similarly, the distillate collection port 22 is manually exchanged for communication with a distillate bottle, a cleaning solution bottle, and a waste solution bottle, in order to further optimize the first electric pump assembly 4 and the second electric pump assembly 5 of the present embodiment, an electric multi-way valve (not shown in the figure) is respectively designed on the first electric pump assembly 4 and the second electric pump assembly 5, the electric multi-way valve of the first electric pump assembly 4 is used for switching the flow of the distillate bottle, the cleaning solution bottle and the waste solution bottle to the liquid inlet, the electric multi-way valve of the second electric pump assembly 5 is used for switching the flow of the distillate bottle, the cleaning solution bottle and the waste solution bottle to the distillate collecting port, therefore, different liquid transmission is realized by switching different flow paths through the electric multi-way valve and positive and negative rotation of the electric pump. For example, the operation of a distillation tube, an electric multi-way valve is turned to a distillate bottle, and distillate is pumped in; after distillation is finished, the electric multi-way valve is transferred to a cleaning liquid bottle, cleaning liquid is pumped in, the electric multi-way valve is transferred to a waste liquid bottle, and the first electric pump assembly reversely pumps waste liquid; similarly, when fractions need to be collected, an electric multi-way valve at the fraction collecting port is switched to a fraction bottle, and the fractions are pumped out; then the electric multi-way valve is transferred to a cleaning liquid bottle, cleaning liquid is pumped in, the electric multi-way valve is transferred to a waste liquid bottle, and the second electric pump assembly reversely pumps waste liquid; this design helps further realizing automatic washing and automatic distillation, need not artificial operation, makes the utility model discloses develop toward automation, intelligent direction more.
As the optimization scheme of the utility model, the communicating pipe 3 is formed in a split way and comprises a communicating upper pipe 31 and a communicating lower pipe 32, the upper end 311 of the communicating upper pipe extends to the top of the distillation cavity 11, and the lower end 312 of the communicating upper pipe protrudes out of the lower part of the distillation pipe 1; the upper end 321 of the communicating lower pipe protrudes above the collector 2, and the lower end 322 of the communicating lower pipe extends to the bottom of the collector 2, so that the lower end 312 of the communicating upper pipe is detachably connected with the upper end 321 of the communicating lower pipe, and the distiller is convenient to detach and store; further, the lower extreme 312 of intercommunication upper tube and the upper end 321 of intercommunication low tube are connected through a sealing connection piece 33, guarantee the gas tightness and prevent revealing, sealing connection piece 33 can adopt anticorrosive thermal-insulated gum cover, and anticorrosive thermal-insulated gum cover cladding is in the junction of the lower extreme 312 of intercommunication upper tube and the upper end 321 of intercommunication low tube, and anticorrosive thermal-insulated gum cover plays corrosion-resistant, thermal-insulated effect.
In one embodiment, the bottom of the distillation tube 1 is paved with anti-boiling glass beads 6, and the anti-boiling glass beads 6 can effectively prevent the distilled water from bumping, so that the unvaporized distillate is prevented from boiling to enter the upper end 311 of the communicating upper tube. Condensation glass beads 7 are paved at the bottom of the collector 2, and the condensation glass beads 7 are large in surface area, so that steam in the collector can be effectively condensed.
The basic principles and main features of the invention and the advantages of the invention have been shown and described above. It will be understood by those skilled in the art that the present invention is not limited to the above embodiments, and that the foregoing embodiments and descriptions are provided only to illustrate the principles of the present invention without departing from the spirit and scope of the present invention. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (10)
1. A distiller, characterized by: the distillation tube is made of quartz materials and is arranged in a temperature control electric heating jacket;
the distillation pipe is provided with a distillation cavity, the bottom of the distillation cavity is provided with a liquid inlet communicated with the distillation cavity, the collector is provided with a collection cavity, and the bottom of the collection cavity is provided with a fraction collection port communicated with the collection cavity;
the collector is located distillation tube below, the distillation tube passes through communicating pipe intercommunication collector, the upper end of communicating pipe extends to distillation chamber top, the lower extreme of communicating pipe extends to the collector bottom, the gas vent of putting outward is seted up at the top of collector.
2. A distiller as defined in claim 1, wherein: the distiller is also provided with a first electric pump assembly and a second electric pump assembly or a rubber pipe, wherein the first electric pump assembly or the rubber pipe is arranged at the position of the liquid inlet to control liquid to enter and exit, and the second electric pump assembly or the rubber pipe is arranged at the position of the fraction collecting port to control liquid to enter and exit.
3. A distiller as defined in claim 2, wherein: the first electric pump assembly and the second electric pump assembly are respectively provided with an electric multi-way valve, the electric multi-way valve of the first electric pump assembly is used for switching the circulation of the distillate bottle, the cleaning liquid bottle, the waste liquid bottle and the liquid inlet, and the electric multi-way valve of the second electric pump assembly is used for switching the circulation of the distillate bottle, the cleaning liquid bottle, the waste liquid bottle and the distillate collecting port.
4. A distiller as defined in claim 1, wherein: the communicating pipe is formed in a split mode and comprises a communicating upper pipe and a communicating lower pipe, the upper end of the communicating upper pipe extends to the top of the distillation cavity, and the lower end of the communicating upper pipe protrudes out of the lower portion of the distillation pipe; the upper end of the communicating lower pipe protrudes out of the collector, and the lower end of the communicating lower pipe extends to the bottom of the collector, so that the lower end of the communicating upper pipe can be detachably connected with the upper end of the communicating lower pipe.
5. A distiller as defined in claim 4, wherein: the lower end of the communicating upper pipe is connected with the upper end of the communicating lower pipe through a sealing connecting piece.
6. A distiller as defined in claim 5, wherein: the sealing connecting piece can adopt an anticorrosion heat-insulation rubber sleeve, and the anticorrosion heat-insulation rubber sleeve is coated at the joint of the lower end of the communicated upper pipe and the upper end of the communicated lower pipe.
7. A distiller as defined in claim 1, wherein: and anti-boiling glass beads are paved at the bottom of the distillation tube.
8. A distiller as defined in claim 1, wherein: and condensed glass beads are paved at the bottom of the collector.
9. A distiller as defined in claim 1, wherein: the collector may be made of quartz material.
10. A distiller as defined in claim 1, wherein: the distiller is provided with a suspension loop to suspend the distiller.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201921437624.4U CN210474035U (en) | 2019-08-30 | 2019-08-30 | Distiller |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201921437624.4U CN210474035U (en) | 2019-08-30 | 2019-08-30 | Distiller |
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| Publication Number | Publication Date |
|---|---|
| CN210474035U true CN210474035U (en) | 2020-05-08 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201921437624.4U Active CN210474035U (en) | 2019-08-30 | 2019-08-30 | Distiller |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110394205A (en) * | 2019-08-30 | 2019-11-01 | 西安拜森仪器有限公司 | A kind of distiller |
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2019
- 2019-08-30 CN CN201921437624.4U patent/CN210474035U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110394205A (en) * | 2019-08-30 | 2019-11-01 | 西安拜森仪器有限公司 | A kind of distiller |
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