CN110387324A - It is a kind of to produce Pfansteihl device and method using Rhizopus oryzae - Google Patents

It is a kind of to produce Pfansteihl device and method using Rhizopus oryzae Download PDF

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Publication number
CN110387324A
CN110387324A CN201910707237.6A CN201910707237A CN110387324A CN 110387324 A CN110387324 A CN 110387324A CN 201910707237 A CN201910707237 A CN 201910707237A CN 110387324 A CN110387324 A CN 110387324A
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oil
shell
arm
pipe
bracket
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梁瑛
范宁
范毓纯
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Xuzhou Green Source Intelligent Technology Co Ltd
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Xuzhou Green Source Intelligent Technology Co Ltd
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    • C12M33/00Means for introduction, transport, positioning, extraction, harvesting, peeling or sampling of biological material in or from the apparatus
    • C12M33/04Means for introduction, transport, positioning, extraction, harvesting, peeling or sampling of biological material in or from the apparatus by injection or suction, e.g. using pipettes, syringes, needles
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    • C12P7/40Preparation of oxygen-containing organic compounds containing a carboxyl group including Peroxycarboxylic acids
    • C12P7/56Lactic acid

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Abstract

Pfansteihl device and method is produced using Rhizopus oryzae the invention discloses a kind of, wherein the catalysis system includes: slag tap control valve, lower part connecting flange, hot mixing room, catalysis shell, vaporization concentration sensor, vaporizing chamber, top connecting flange, catalysis reaction-filling object, net-fault column plate, promotor spray ring, heat build-up bucket;The lower part connecting flange is located at entire catalysis system lower part, and upper part is equipped with vaporizing chamber and top connecting flange, and vaporizing chamber is penetrated through with top connecting flange, is fixedly connected with catalysis shell;The upper and lower ends of catalysis shell are fixedly connected with top connecting flange, lower part connecting flange respectively, and middle and lower part connecting flange is located at catalysis lower part of the housing.Of the present invention a kind of using Rhizopus oryzae production Pfansteihl device and method, for the device using automatically controlling, simple to operate, work efficiency is high, specifically there is stronger stability.

Description

It is a kind of to produce Pfansteihl device and method using Rhizopus oryzae
Technical field
The invention belongs to biopharmaceutical technologies, and in particular to a kind of to utilize Rhizopus oryzae production Pfansteihl device and side Method.
Background technique
Pfansteihl is a kind of important organic acid, is widely used in food service industry, materials industry.It is as a kind of green Colour chemistry product, can be with degradation materials such as synthesizing polylactic acid, ethyl lactates, thus are concerned in Material Field.Currently, L- is newborn Sour generally to be synthesized using bioanalysis, the strain of production is mostly microbial strains of Rhizopus sp.Wherein, Rhizopus oryzae is authenticated as U.S. FDA Keep the safety in production bacterial strain, have growth rapidly, strong environmental adaptability, secretion organic acid and the advantages such as protein-energy is strong, to have The outstanding production strain of machine acid.Currently, related bioanalysis produces Pfansteihl equipment, inefficiency, output capacity be low, the degree of automation Difference, product is unstable, the wasting of resources is big.Therefore, it is necessary to develop dedicated Pfansteihl production equipment.
Summary of the invention
In order to solve the above-mentioned technical problem, Pfansteihl device is produced using Rhizopus oryzae the present invention relates to a kind of, comprising: molten Solve slot 1, delivery pump 2, preparing pool 3, destilling tower front pump 4, destilling tower 5, trickle bed reactor 6, sediment discharge pipe 7, sampling Exhaust pipe 8, high-position discharge pipe 9, gas-liquid separator 10, electric cabinet 11, inoculation sampling return pipe 12, main fermentation case 13, bracket 14, Regulating wheel 15;Dissolving tank 1 positioned at side is connected to by delivery pump 2 with the main fermentation case 13 for being located at upper left quarter, main fermentation case 13 Top is controllable opening enclosed structure;13 lower part of main fermentation case is equipped with preparing pool 3, top side is equipped with inoculation sampling return pipe 12, it is connected to the two pipeline, wherein inoculation sampling return pipe 12 flows back into dissolving tank 1 for being inoculated with, sampling, and by discharge water In;Portion is equipped with electric cabinet 11 on the support 14;14 side of bracket is equipped with destilling tower 5, the destilling tower 5 places vertically, bottom with External steam connection, 5 hollow structure of destilling tower, shell are made of high molecular material, and the destilling tower 5 is defeated by destilling tower Enter pump 4 to be connected to main fermentation case 13, destilling tower 5 is connected to the gas-liquid separator 10 on top;The trickle bed reactor 6 uses gas Simultaneously stream mode is connected to gas-liquid separator 10, destilling tower 5 liquid respectively;6 lower part of trickle bed reactor be equipped with sediment discharge pipe 7, Top is equipped with high-position discharge pipe 9, waist is equipped with sampling exhaust pipe 8, and trickle bed reactor 6 is connected to three;The regulating wheel 15 Positioned at 5 bottom of destilling tower, quantity is four;The delivery pump 2, destilling tower front pump 4 and 11 polygon control survey of electric cabinet link.
Further, the destilling tower 5 includes: slag notch 5-1, and slag tap control valve 5-2, distills tower shell 5-3, catalysis system Unite 5-4, outlet tube 5-5, escape pipe 5-6, inlet 5-7, steam pipe 5-8;Both slag notch 5-1 are equipped in 5 lower part of destilling tower Pass through control valve 5-2 perforation of slagging tap;Catalysis system 5-4 is equipped with inside the top control valve 5-2 of slagging tap, distillation tower shell 5-3;In The distillation side tower shell 5-3 is equipped with steam pipe 5-8, the other side is equipped with outlet tube 5-5, waist is equipped with inlet 5-7, top is equipped with Escape pipe 5-6 distills the perforation of tower shell 5-3 and four.
Further, the catalysis system 5-4 includes: the control valve 5-2 that slags tap, lower part connecting flange 5-4-2, hot mixing room 5-4-3 is catalyzed shell 5-4-4, vaporizes concentration sensor 5-4-5, vaporizing chamber 5-4-6, top connecting flange 5-4-7, and catalysis is anti- Answer filler 5-4-8, net-fault column plate 5-4-9, promotor spray ring 5-4-10, heat build-up bucket 5-4-11;The lower part connecting flange 5- 4-2 is located at the lower part entire catalysis system 5-4, and upper part is equipped with vaporizing chamber 5-4-6 and top connecting flange 5-4-7, and vaporizing chamber 5-4-6 is penetrated through with top connecting flange 5-4-7, is fixedly connected with catalysis shell 5-4-4;It is catalyzed the upper and lower ends of shell 5-4-4 It is fixedly connected respectively with top connecting flange 5-4-7, lower part connecting flange 5-4-2, middle and lower part connecting flange 5-4-2, which is located at, to be urged Change the lower part shell 5-4-4;The hot mixing room 5-4-3 is located inside catalysis shell 5-4-4, the top control valve 5-2 of slagging tap, and heat is mixed Closing room 5-4-3 is cylindrical hollow configuration up and down, and hot steam is sufficiently mixed herein with mixed liquor;Hot mixing room 5-4-3 The other end by lower part connecting flange 5-4-2 and slag tap control valve 5-2 perforation connect, wherein under the control valve 5-2 that slags tap is located at The lower part of portion connecting flange 5-4-2;The heat build-up bucket 5-4-11 is located at the top of hot mixing room 5-4-3, the two perforation connection, gathers The 5-4-11 loudspeaker moulding of heat bucket, up and down and under it is small big, surface is equipped with a large amount of through-holes, and waist is equipped with deflector, utilizes The solution that hot steam and net-fault column plate 5-4-9 are splashed down in horn mouth moulding carries out sufficient heat exchange;The catalysis reaction-filling object 5-4-8, net-fault column plate 5-4-9, promotor spray ring 5-4-10 are located at the top heat build-up bucket 5-4-11, wherein catalysis reaction-filling object 5- The quantity of 4-8 is 3 groups, is equidistantly distributed between adjacent catalyst reaction-filling object 5-4-8;The net-fault surface column plate 5-4-9 is equipped with big Measuring through-hole, quantity is 20, is equally spaced inside catalysis shell 5-4-4;Promotor spray ring 5-4-10 to catalysis shell 5-4-4 Promotor is added in interior injection;The promotor spray ring 5-4-10, catalysis reaction-filling object 5-4-8, net-fault column plate 5-4-9 are to promote It is chemically reacted into mixed liquor;The vaporization concentration sensor 5-4-5 is located at catalysis shell 5-4-4 waist, and vaporization concentration passes Sensor 5-4-5 is connect with 11 polygon control survey of electric cabinet.
Further, the trickle bed reactor 6 includes: shower washing device 6-1, catalyst adding tube 6-2, and mixing is stirred Mix device 6-3, stirring motor 6-4, automatic rinser 6-5, ripple generator 6-6;Shower washing device 6-1 positioned at side, One end is connected to external fresh water pump, and the other end generates 5 spray heads being horizontally directed to;It is equipped with and urges in the side shower washing device 6-1 Agent adding tube 6-2, catalyst adding tube 6-2 circular ring shape, hollow structure, vertical arrangement are equipped with a large amount of through-holes on its surface;In The catalyst side adding tube 6-2 is equipped with mixing agitator 6-3, the mixing agitator 6-3 and the stirring motor 6-4 on the right side of it and drives Dynamic connection, stirring motor 6-4 waterproofing design;It is equipped with automatic rinser 6-5 in 6 interior side of trickle bed reactor, and it is automatically controlled The connection of 11 wireless control of case;The ripple generator 6-6 is located inside trickle bed reactor 6, the side mixing agitator 6-3.
Further, the mixing agitator 6-3 includes: mixing inlet 6-3-1, and magnetism removes metal device 6-3-2, side door Impeller 6-3-4, antioxidant filler 6-3-5 is mixed in 6-3-3, mixes liquid outlet 6-3-6;Positioned at being mixed into for side The liquid mouth 6-3-1 and mixing liquid outlet 6-3-6 for being located at the other side is penetrated through;It is equipped with and is mixed on the inside of mixing liquid outlet 6-3-6 Impeller 6-3-4, the fixed certain amount blade in surface, by motor driven, promotes solution mutually immiscible;In mixing agitator 6- 3 interior sides are equipped with magnetism and remove metal device 6-3-2, and waterproof construction, bottom chuck are moved horizontally with lever arm;It is equipped on its opposite Side door 6-3-3, magnetism go metal device 6-3-2 lever arm to unload absorbate in side door 6-3-3;In the bottom mixing agitator 6-3 Side is equipped with antioxidant filler 6-3-5.
Further, it includes: fixed station 6-3-2-1, horizontal extension arm 6-3-2-2 that the magnetism, which removes metal device 6-3-2, greatly Arm shaft 6-3-2-3, vertical telescopic arm 6-3-2-4, automatically controlled magnetic salient point 6-3-2-5, automatically controlled magnetic ring 6-3-2-6, absorptive table 6-3-2-7, horizontal rotating shaft 6-3-2-8;Fixed station 6-3-2-1 positioned at side is fixed on base surface, with horizontal layout The 6-3-2-2 connection of horizontal extension arm, horizontal extension arm 6-3-2-2 retractable structure;Large arm shaft 6-3-2- is equipped in its end 3, horizontal extension arm 6-3-2-2 are hinged by large arm shaft 6-3-2-3 and vertical telescopic arm 6-3-2-4;Vertical telescopic arm 6-3- 2-4 retractable structure, and be rotatablely connected by horizontal rotating shaft 6-3-2-8 and the absorptive table 6-3-2-7 of lower part;In absorptive table 6-3- The lower surface 2-7 is equipped with multiple automatically controlled magnetic salient point 6-3-2-5, equidistant layout;It is surrounded by absorptive table 6-3-2-7 multiple automatically controlled Magnetic ring 6-3-2-6, equidistant layout, automatically controlled magnetic salient point 6-3-2-5, automatically controlled magnetic ring 6-3-2-6 are connect with electric cabinet 11;Magnetic Property goes metal device 6-3-2 waterproofing design.
Further, the automatic rinser 6-5 includes: cleaning shell 6-5-1, battery motor depository dish 6-5-2, signal Transceiver 6-5-3, creep adsorbent equipment 6-5-4, washer 6-5-5, seeks spot instrument 6-5-6;Automatic rinser 6-5 itself is Waterproof construction;Battery motor depository dish 6-5-2 is equipped at the center the cleaning shell 6-5-1, pull quick fixation structure, inside is equipped with Battery, driving motor, vacuum pump, the battery motor side depository dish 6-5-2 are equipped with signal transceiver 6-5-3;It is described to creep Adsorbent equipment 6-5-4 is located at cleaning shell 6-5-1 apex angle, and 4 adsorbent equipment 6-5-4 that creep collectively constitute movement mechanism;It is described Washer 6-5-5 is located at cleaning shell 6-5-1 central lower, and the lower surface washer 6-5-5 is equipped with and seeks spot instrument 6-5-6;Institute It states battery motor depository dish 6-5-2, signal transceiver 6-5-3 and seeks spot instrument 6-5-6 and connect with 11 wireless control of electric cabinet.
Further, the adsorbent equipment 6-5-4 that creeps includes: horizontal swinging arm 6-5-4-1, extending arm 6-5-4-2, stretching, extension Hydraulic press 6-5-4-3, vertical moving arm 6-5-4-4, vertical hydraulic press 6-5-4-5, positioning disk 6-5-4-6, suction tray 6-5-4- 7, fixed column 6-5-4-8, suction tray spring 6-5-4-9;The end the horizontal swinging arm 6-5-4-1 is equipped with extending arm 6-5-4-2, institute It states extending arm 6-5-4-2 and horizontal swinging arm 6-5-4-1 to be rotatablely connected, and is swung up and down using horizontal swinging arm 6-5-4-1 as rotation axis, It is equipped with stretching, extension hydraulic press 6-5-4-3 between the two, the stretching, extension hydraulic press 6-5-4-3 is connect with 11 wireless control of electric cabinet;Institute It states vertical moving arm 6-5-4-4 and is located at the end extending arm 6-5-4-2, vertical moving arm 6-5-4-4 and extending arm 6-5-4-2 are rotated Connection is equipped with vertical hydraulic press 6-5-4-5, the vertical hydraulic press between vertical moving arm 6-5-4-4 and extending arm 6-5-4-2 6-5-4-5 is connect with 11 wireless control of electric cabinet;The positioning disk 6-5-4-6 is located at the lower surface vertical moving arm 6-5-4-4, fixed It is equipped with suction tray 6-5-4-7 below the disk 6-5-4-6 of position, passes through fixation between the suction tray 6-5-4-7 and positioning disk 6-5-4-6 Column 6-5-4-8 is fixedly connected, and tracheae is equipped with inside fixed column 6-5-4-8, and tracheae one end is connected to vacuum pump, the other end and absorption Disk 6-5-4-7 connection;The one end suction tray spring 6-5-4-9 connection positioning disk 6-5-4-6, the other end and suction tray 6-5-4- 7 connections.
Further, the washer 6-5-5 includes: cleaning driving machine 6-5-5-1, fan 6-5-5-2, transmission gear 6- 5-5-3, rotating disk 6-5-5-4, keep a public place clean brush head 6-5-5-5, water pipeline 6-5-5-6;The cleaning driving machine 6-5-5-1 and electricity The connection of 11 wireless control of case is controlled, cleaning driving machine 6-5-5-1 output end is equipped with fan 6-5-5-2, dries up surface after cleaning; The transmission gear 6-5-5-3 is located at below fan 6-5-5-2, transmission gear 6-5-5-3 and cleaning driving machine 6-5-5-1 output Main shaft engagement connection;The rotating disk 6-5-5-4 is located at the lower surface transmission gear 6-5-5-3, and rotating disk 6-5-5-4 quantity is 3 Group, the lower surface rotating disk 6-5-5-4 are equipped with the brush head 6-5-5-5 that keeps a public place clean;The water pipeline 6-5-5-6 is located at transmission gear 6-5- The upper surface 5-3, water pipeline 6-5-5-6 are mutually communicated with rotating disk 6-5-5-4.
Further, the bracket 14 includes: carriage drive machine 14-1, transmission case 14-2, support gear 14-3, branch frame rail Road 14-4, bracket shell 14-5, weight body 14-6, supporter 14-7;The bracket shell 14-5 is located at the top of 14 pedestal of bracket, and two Person is independent;The bracket shell 14-5 be hollow structure, bracket track 14-4 be set to bracket shell 14-5 inside, and with 14 pedestal of bracket Vertically and it is fixedly connected;The supporter 14-7 is arranged in the side transmission case 14-2, the two connection;It is set inside transmission case 14-2 There is support gear 14-3, engages connection with the surface bracket track 14-4 rack gear;The supporter 14-7 passes through support gear 14- 3 realize and sliding on bracket track 14-4 with engaging for bracket track 14-4;The weight body 14-6 is located at supporter 14- 7 outsides, the two are fixed, and the end weight body 14-6 is stretched out outside bracket shell 14-5, and waist is fixedly connected with bracket shell 14-5;Institute It stating carriage drive machine 14-1 and is located at the lower end transmission case 14-2 side, carriage drive machine 14-1 and support gear 14-3 are sequentially connected, Carriage drive machine 14-1 is connected by conducting wire with the control of electric cabinet 11, and carriage drive machine 14-1 driving arm gear 14-3 is rotated simultaneously Transmission case 14-2, bracket shell 14-5, weight body 14-6, supporter 14-7 is driven to rise or fall along bracket track 14-4.
Further, the regulating wheel 15 includes: regulating wheel U plate 15-1, grease-box 15-2, movable pulley shaft 15-3, Movable pulley 15-4, atomizer 15-5, wheel track 15-6;The regulating wheel U plate 15-1 is that concave structure, steel plate make, two sides The design of side wall inverted trapezoidal;The movable pulley shaft 15-3 is connected between the side wall of the two sides regulating wheel U plate 15-1, movable pulley shaft 15-3 and external motor are sequentially connected, and movable pulley shaft 15-3 is equipped with movable pulley 15-4;The movable pulley 15-4 and movable pulley Shaft 15-3 rotation connection, the external motor of movable pulley 15-4 are connect with 11 polygon control survey of electric cabinet;Described wheel track 15-6 Connection is rolled in the lower part movable pulley 15-4, the two;The grease-box 15-2 is fixedly connected on the side regulating wheel U plate 15-1 side wall Outside, atomizer 15-5 are fixedly connected on the inside of regulating wheel U plate 15-1 upper wall, grease-box 15-2 by its internal oil guide pipe and Atomizer 15-5 connection.
Further, the grease-box 15-2 includes: profit oil pump 15-2-1, distributor box 15-2-2, Rose Box 15-2-3, Oil fuel tube 15-2-4, radiator 15-2-5, fixed plate 15-2-6, abutment sleeve 15-2-7, oil fuel tube export 15-2-8;The bottom of positioned at The profit oil pump 15-2-1 in portion is connected to the distributor box 15-2-2 on top, and distributor box 15-2-2 rectangular box, both ends short axle are half Circle inside sets two groups of agitator arms, diameter difference, big agitator arm diameter 30cm, small agitator arm diameter 9cm, the two Horizontal Tile layout does not stir in the same direction, stretches out two branch pipes upwards at distributor box 15-2-2 two semicircular endpoint, passes through valve and filtering Case 15-2-3 connection, two pipe diameter differences, extra heavy pipe diameter 8cm, capillary diameter 2cm are arranged in big agitator arm, small stir It mixes impeller on one side, enters Rose Box 15-2-3 to control different viscosity lubricating oil;Rose Box 15-2-3 is located at distributor box 15-2- 2 tops, the two penetrate through, and set filter screen, mud chamber, net impurity remover in Rose Box 15-2-3;Radiator 15-2-5 was located at The top filter box 15-2-3, radiator 15-2-5 red copper material are made of the superposition of multiple groups copper sheet and there are gaps between copper sheet;Radiator The outer surface 15-2-5 winds oil fuel tube 15-2-4, the winding section pressure resistance red copper material, the one end oil fuel tube 15-2-4 and Rose Box 15- 2-3 perforation, the other end pass through abutment sleeve 15-2-7 and are connected to oil fuel tube outlet 15-2-8;Mono- end cap of fixed plate 15-2-6 It connects in the outer surface abutment sleeve 15-2-7, the other end is connect with fixation wall.
Further, the atomizer 15-5 includes: main by-pass tube 15-5-1, cover shell 15-5-2, inclination angle injector body 15-5-3, oil spout mouth for adjusting 15-5-4;The cover shell 15-5-2 is the inverted round table knot of hollow, upper closed bottom opening Structure, the surface cover shell 15-5-2 is equipped with main by-pass tube 15-5-1, wherein cover shell is inserted into the bottom end main by-pass tube 15-5-1 In 15-5-2, the oil guide pipe on the top main by-pass tube 15-5-1 and top penetrates through connection;The inclination angle injector body 15-5-3 is located at cover Inside face-piece body 15-5-2, the quantity of inclination angle injector body 15-5-3 is 4~8, and adjacent inclination angle injector body 15-5-3 is with main branch Pipe 15-5-1 is that center axis is angularly distributed, and each inclination angle injector body 15-5-3 is penetrated through by oil distributing pipe and main by-pass tube 15-5-1 Connection;The oil spout mouth for adjusting 15-5-4 is fixedly connected on the lower part cover shell 15-5-2, controllable adjustment folding structure, control spray Amount of jet and angle.
Further, the inclination angle injector body 15-5-3 includes: oil inlet 15-5-3-1, tangential oil outlet 15-5-3-2, Oil spout shell 15-5-3-3, staggeredly spoiler 15-5-3-4, housing actuator 15-5-3-5, shell Reinforced Hoop 15-5-3-6;In It is equipped with oil inlet 15-5-3-1 at the top of oil spout shell 15-5-3-3, is equipped in oil spout shell 15-5-3-3 side wall a large amount of tangential fuel-displaced Mouth 15-5-3-2, lubricating oil are tangentially sprayed along the surface oil spout shell 15-5-3-3;It is equipped in oil spout shell 15-5-3-3 inner wall Largely interlock spoiler 15-5-3-4, is staggeredly fixed on inner wall surface, staggeredly spoiler 15-5-3-4 thin plate stainless steel structure, long Degree is the 4/5 of oil spout shell 15-5-3-3 length, highly 1/10 for oil spout shell 15-5-3-3 radius;Oil spout shell 15-5- Shell Reinforced Hoop 15-5-3-6, housing actuator 15-5-3-5 are equipped with outside 3-3;Wherein 2 housing actuator 15-5-3-5 or more Group, and oil spout shell 15-5-3-3 is driven to rotate simultaneously.
Further, the housing actuator 15-5-3-5 includes: shell flange 15-5-3-5-1, one 15-5-3-5- of axis 2, circumference rack gear 15-5-3-5-3, connecting plate 15-5-3-5-4, horizontal location wheel 15-5-3-5-5, circumference driving wheel 15-5-3- 5-6, two 15-5-3-5-7 of axis;It is externally surrounded by circumference rack gear 15-5-3-5-3 in oil spout shell 15-5-3-3, the two passes through company Fishplate bar 15-5-3-5-4 is fixedly connected;One group of horizontal location wheel 15-5-3-5-5 is respectively set above or below circumference rack gear 15-5-3-5-3, To prevent circumference driving wheel 15-5-3-5-6 sideslip, horizontal location wheel 15-5-3-5-5 is rotated around one 15-5-3-5-2 of axis;In water The two sides flat locating wheel 15-5-3-5-5 respectively set one group of circumference driving wheel 15-5-3-5-6, and the two is fixedly connected;Two 15-5-3-5- of axis 7 driving circumference driving wheel 15-5-3-5-6 rotations, circumference driving wheel 15-5-3-5-6 gear structure and circumference rack gear 15-5-3-5- 3 engaged transmissions;The shell flange 15-5-3-5-1 realizes oil spout shell 15-5-3-3 or more docking.
Further, the circumference rack gear 15-5-3-5-3 includes: circumference flank of tooth 15-5-3-5-3-1, fan-shaped teeth 15- 5-3-5-3-2, oiling machine 15-5-3-5-3-3, bottom transverse slat 15-5-3-5-3-4, damping spring 15-5-3-5-3-5, blower 15-5-3-5-3-6;The circumference flank of tooth 15-5-3-5-3-1 is 2 groups, and arranged opposite passes through bottom transverse slat 15-5-3-5-3-4 Connection;Being equally spaced on the surface circumference flank of tooth 15-5-3-5-3-1 has fan-shaped teeth 15-5-3-5-3-2;In bottom transverse slat 15-5- 3-5-3-4 is equipped with oiling machine 15-5-3-5-3-3, for gear engagement lubrication;The damping spring 15-5-3-5-3-5 is fixed On the bottom surface transverse slat 15-5-3-5-3-4, top is equipped with clump weight;The one end the blower 15-5-3-5-3-6 and damping bullet Spring 15-5-3-5-3-5 is threadedly coupled and passes through clump weight, damping spring 15-5-3-5-3-5, bottom transverse slat 15-5-3-5-3-4 Outside is extended to, other end outlet is directed at fan-shaped teeth 15-5-3-5-3-2, and blower 15-5-3-5-3-6 is with damping spring 15-5- 3-5-3-5 shakes and freely swings.
Further, the oiling machine 15-5-3-5-3-3 includes: protective cover 15-5-3-5-3-3-1, oil storage bag 15-5- 3-5-3-3-2 stirs separator 15-5-3-5-3-3-3, filters rotary table case 15-5-3-5-3-3-4, settling tank 15-5-3-5-3- 3-5, overflow pipe 15-5-3-5-3-3-6, oil water separator 15-5-3-5-3-3-7, settle and separate case 15-5-3-5-3-3-8 are returned Collection tube 15-5-3-5-3-3-9 separates water pipe 15-5-3-5-3-3-10, precipitates property management 15-5-3-5-3-3-11, metal sediment Pipe 15-5-3-5-3-3-12, oil input channel 15-5-3-5-3-3-13, screw thread flowline 15-5-3-5-3-3-14;Positioned at lower part Oil input channel 15-5-3-5-3-3-13, external oil with top stirring separator 15-5-3-5-3-3-3 thence into being connected to, stir Mixing has 2 groups of agitator arms, horizontal layout, does not stir at low speed in the same direction in separator 15-5-3-5-3-3-3, wherein left side paddle It takes turns top and is equipped with channel and oil storage bag 15-5-3-5-3-3-2 perforation, the periphery oil storage bag 15-5-3-5-3-3-2 is equipped with protective cover 15-5-3-5-3-3-1, upper part are equipped with screw thread flowline 15-5-3-5-3-3-14, the two perforation;In stirring separator 15-5- Agitator arm lower part is equipped with filtering rotary table case 15-5-3-5-3-3-4 on the left of 3-5-3-3-3, and the two is penetrated through by conduit, filtering circle Filter screen is equipped with inside platform case 15-5-3-5-3-3-4;The settling tank 15-5-3-5-3-3-5 is located at filtering rotary table case 15-5- The lower part 3-5-3-3-4, the two perforation connection, settling tank 15-5-3-5-3-3-5 lower right side are equipped with metal sediment pipe 15-5-3- 5-3-3-12, left upper portion are equipped with overflow pipe 15-5-3-5-3-3-6, and overflow pipe 15-5-3-5-3-3-6 oil inlet is always positioned at Solution surface in settling tank 15-5-3-5-3-3-5;Oil water separator 15-5-3-5-3-3-7 positioned at lower part passes through overflow pipe 15-5-3-5-3-3-6 and settling tank 15-5-3-5-3-3-5 is penetrated through, and in its left part, closing, right part are equipped with precipitating property management 15- 5-3-5-3-3-11, oil water separator 15-5-3-5-3-3-7 are horizontally inserted into inside settle and separate case 15-5-3-5-3-3-8, In in settle and separate case 15-5-3-5-3-3-8 inserting paragraph, realize controllable rotating and its surface be equipped with a large amount of small through hole;It is standing The top separator box 15-5-3-5-3-3-8 is equipped with recycling oil pipe 15-5-3-5-3-3-9, lower part is equipped with separation water pipe 15-5-3-5- 3-3-10。
Further, the stirring separator 15-5-3-5-3-3-3 includes: damping spring 15-5-3-5-3-3-3-1, is stirred One 15-5-3-5-3-3-3-2 of wheel is mixed, quant 15-5-3-5-3-3-3-3, two 15-5-3-5-3-3-3-4 of stirring wheel are assisted;It is stirring It mixes and is equipped with stirring wheel 15-5-3-5-3-3-3-2, two 15-5-3-5-3-3-3- of stirring wheel inside separator 15-5-3-5-3-3-3 4, the two horizontal layout is non-to be stirred in the same direction, and wherein two axle center 15-5-3-5-3-3-3-4 lower part of stirring wheel is equipped with oil input channel 15-5-3-5-3-3-13, one axle center 15-5-3-5-3-3-3-2 top of stirring wheel is equipped with edible vegetable oil outlet, lower part goes out equipped with waste oil Mouthful;It is equipped with damping spring 15-5-3-5-3-3-3-1 in separator 15-5-3-5-3-3-3 enclosure interior one end, the other end is equipped with Quant 15-5-3-5-3-3-3-3 is assisted, wherein the root damping spring 15-5-3-5-3-3-3-1 is fixed on shell, upper part certainly By swinging;The lower part quant 15-5-3-5-3-3-3-3 is assisted to be equipped with a cylinder, cylinder one end and top blade are rotatablely connected, are another One end is fixed on separator 15-5-3-5-3-3-3 enclosure interior.
It is disclosed by the invention a kind of using Rhizopus oryzae production Pfansteihl device and method, the advantage is that: the device is adopted Easy to operate with automatic control, efficient work is steady, integrated reaction unit resistance to overload shock and reduces equipment investment, Processing equipment is compact, has effectively saved cost.
Detailed description of the invention
Fig. 1 is that one of present invention utilizes Rhizopus oryzae production Pfansteihl device figure.
Fig. 2 is 5 figure of destilling tower in the present invention.
Fig. 3 is that catalysis system 5-4 schemes in the present invention.
Fig. 4 is 6 figure of trickle bed reactor in the present invention.
Fig. 5 is that mixing agitator 6-3 schemes in the present invention.
Fig. 6 is that magnetism goes metal device 6-3-2 to scheme in the present invention.
Fig. 7 is that automatic rinser 6-5 schemes in the present invention.
Fig. 8 is adsorbent equipment 6-5-4 figure of creeping in the present invention.
Fig. 9 is that washer 6-5-5 schemes in the present invention.
Figure 10 is 14 figure of bracket in the present invention.
Figure 11 is 15 figure of regulating wheel in the present invention.
Figure 12 is that grease-box 15-2 schemes in the present invention.
Figure 13 is that atomizer 15-5 schemes in the present invention.
Figure 14 is heretofore described inclination angle injector body 15-5-3 figure.
Figure 15 is that housing actuator 15-5-3-5 schemes in the present invention.
Figure 16 is that circumference rack gear 15-5-3-5-3 schemes in the present invention.
Figure 17 is that oiling machine 15-5-3-5-3-3 schemes in the present invention.
Figure 18 is that separator 15-5-3-5-3-3-3 figure is stirred in the present invention.
Specific embodiment
A kind of Rhizopus oryzae production Pfansteihl device and side is utilized to provided by the invention with reference to the accompanying drawings and examples Method is further described.
Embodiment
As shown in Figure 1, being that one of present invention utilizes Rhizopus oryzae production Pfansteihl device figure.As seen from the figure, it wraps It includes: dissolving tank 1, delivery pump 2, preparing pool 3, destilling tower front pump 4, destilling tower 5, trickle bed reactor 6, sediment discharge pipe 7, Sample exhaust pipe 8, high-position discharge pipe 9, gas-liquid separator 10, electric cabinet 11, inoculation sampling return pipe 12, main fermentation case 13, branch Frame 14, regulating wheel 15;Dissolving tank 1 positioned at side is connected to by delivery pump 2 with the main fermentation case 13 for being located at upper left quarter, main fermentation It is controllable opening enclosed structure at the top of case 13;13 lower part of main fermentation case is equipped with preparing pool 3, top side is equipped with inoculation sampling reflux Pipe 12 is connected to the two pipeline, wherein inoculation sampling return pipe 12 flows back into dissolution for being inoculated with, sampling, and by discharge water In slot 1;Portion is equipped with electric cabinet 11 on the support 14;14 side of bracket is equipped with destilling tower 5, the placement, bottom vertically of destilling tower 5 It is connected to external steam, 5 hollow structure of destilling tower, shell is made of high molecular material, and the destilling tower 5 passes through destilling tower Front pump 4 is connected to main fermentation case 13, and destilling tower 5 is connected to the gas-liquid separator 10 on top;The trickle bed reactor 6 uses Gas and liquid flowing mode is connected to gas-liquid separator 10, destilling tower 5 respectively;6 lower part of trickle bed reactor is equipped with sediment discharge pipe 7, top is equipped with high-position discharge pipe 9, waist is equipped with sampling exhaust pipe 8, and trickle bed reactor 6 is connected to three;The regulating wheel 15 are located at 5 bottom of destilling tower, and quantity is four;The delivery pump 2, destilling tower front pump 4 and 11 polygon control survey chain of electric cabinet It connects.
As shown in Fig. 2, being 5 figure of destilling tower in the present invention.As seen from the figure, comprising: slag notch 5-1, slag tap control valve 5- 2, distill tower shell 5-3, catalysis system 5-4, outlet tube 5-5, escape pipe 5-6, inlet 5-7, steam pipe 5-8;In destilling tower 5 Lower part is equipped with both slag notch 5-1 and passes through control valve 5-2 perforation of slagging tap;On the top control valve 5-2 of slagging tap, distillation tower shell 5-3 Inside is equipped with catalysis system 5-4;Steam pipe 5-8, the other side are equipped with equipped with outlet tube 5-5, waist in the distillation side tower shell 5-3 It is equipped with escape pipe 5-6 equipped with inlet 5-7, top, distills the perforation of tower shell 5-3 and four.
As shown in figure 3, being that catalysis system 5-4 schemes in the present invention.As seen from the figure, comprising: slag tap control valve 5-2, lower part Connecting flange 5-4-2, hot mixing room 5-4-3 are catalyzed shell 5-4-4, vaporize concentration sensor 5-4-5, vaporizing chamber 5-4-6, on Portion connecting flange 5-4-7 is catalyzed reaction-filling object 5-4-8, net-fault column plate 5-4-9, promotor spray ring 5-4-10, heat build-up bucket 5-4- 11;The lower part connecting flange 5-4-2 is located at the lower part entire catalysis system 5-4, and upper part is equipped with vaporizing chamber 5-4-6 and top connects Acting flange 5-4-7, and vaporizing chamber 5-4-6 is penetrated through with top connecting flange 5-4-7, is fixedly connected with catalysis shell 5-4-4;Catalysis The upper and lower ends of shell 5-4-4 are fixedly connected with top connecting flange 5-4-7, lower part connecting flange 5-4-2 respectively, middle and lower part Connecting flange 5-4-2 is located at the catalysis lower part shell 5-4-4;The hot mixing room 5-4-3 is located inside catalysis shell 5-4-4, goes out The top slag control valve 5-2, hot mixing room 5-4-3 are cylindrical hollow configuration up and down, and hot steam is filled herein with mixed liquor Divide mixing;The other end of hot mixing room 5-4-3 is connected by lower part connecting flange 5-4-2 and control valve 5-2 perforation of slagging tap, wherein The control valve 5-2 that slags tap is located at the lower part of lower part connecting flange 5-4-2;The heat build-up bucket 5-4-11 is located at hot mixing room 5-4-3's Top, both perforation connection, the moulding of heat build-up bucket 5-4-11 loudspeaker, up and down and under it is small big, surface is equipped with a large amount of through-holes, Waist is equipped with deflector, carries out sufficiently heat using the solution that hot steam and net-fault column plate 5-4-9 are splashed down in horn mouth moulding and hands over It changes;The catalysis reaction-filling object 5-4-8, net-fault column plate 5-4-9, promotor spray ring 5-4-10 are located on heat build-up bucket 5-4-11 Portion equidistantly distributes between adjacent catalyst reaction-filling object 5-4-8 wherein the quantity of catalysis reaction-filling object 5-4-8 is 3 groups; The net-fault surface column plate 5-4-9 is equipped with a large amount of through-holes, quantity is 20, is equally spaced inside catalysis shell 5-4-4;Promotor spray Promotor is added in ring 5-4-10 injection into catalysis shell 5-4-4;The promotor spray ring 5-4-10, catalysis reaction-filling object 5- 4-8, net-fault column plate 5-4-9 are that mixed liquor is promoted to be chemically reacted;The vaporization concentration sensor 5-4-5 is located at catalysis shell Body 5-4-4 waist, vaporization concentration sensor 5-4-5 are connect with 11 polygon control survey of electric cabinet.
As shown in figure 4, being 6 figure of trickle bed reactor in the present invention.As seen from the figure, comprising: shower washing device 6-1, Catalyst adding tube 6-2, mixing agitator 6-3, stirring motor 6-4, automatic rinser 6-5, ripple generator 6-6;Positioned at one The shower washing device 6-1 of side, one end are connected to external fresh water pump, and the other end generates 5 spray heads being horizontally directed to;It is cleaning The side spray equipment 6-1 is equipped with catalyst adding tube 6-2, catalyst adding tube 6-2 circular ring shape, hollow structure, vertical arrangement, In Its surface is equipped with a large amount of through-holes;The catalyst side adding tube 6-2 be equipped with mixing agitator 6-3, the mixing agitator 6-3 with Stirring motor 6-4 on the right side of it is drivingly connected, stirring motor 6-4 waterproofing design;It is equipped with certainly in 6 interior side of trickle bed reactor Dynamic cleaning machine 6-5, connect with 11 wireless control of electric cabinet;The ripple generator 6-6 is located inside trickle bed reactor 6, The side mixing agitator 6-3.
As shown in figure 5, being that mixing agitator 6-3 schemes in the present invention.As seen from the figure, comprising: mixing inlet 6-3-1, Magnetism removes metal device 6-3-2, side door 6-3-3, and impeller 6-3-4, antioxidant filler 6-3-5 is mixed, and mixes liquid outlet 6-3-6;Mixing inlet 6-3-1 positioned at side is penetrated through with the mixing liquid outlet 6-3-6 for being located at the other side;In mixing liquid outlet It is equipped on the inside of 6-3-6 and impeller 6-3-4 is mixed, the fixed certain amount blade in surface by motor driven, promotes solution phase It is immiscible;Magnetism is equipped in mixing agitator 6-3 interior side and removes metal device 6-3-2, and waterproof construction, bottom chuck are with lever arm It moves horizontally;It is equipped with side door 6-3-3 on its opposite, magnetism goes metal device 6-3-2 lever arm to be adsorbed in side door 6-3-3 unloading Object;Antioxidant filler 6-3-5 is equipped in mixing agitator 6-3 bottom side.
As shown in fig. 6, being that magnetism goes metal device 6-3-2 to scheme in the present invention.As seen from the figure, comprising: fixed station 6-3-2- 1, horizontal extension arm 6-3-2-2, large arm shaft 6-3-2-3, vertical telescopic arm 6-3-2-4, automatically controlled magnetic salient point 6-3-2-5, electricity Control magnetic ring 6-3-2-6, absorptive table 6-3-2-7, horizontal rotating shaft 6-3-2-8;Fixed station 6-3-2-1 positioned at side is fixed on base It on plinth face, is connect with the horizontal extension arm 6-3-2-2 of horizontal layout, horizontal extension arm 6-3-2-2 retractable structure;At its end Portion is equipped with large arm shaft 6-3-2-3, and horizontal extension arm 6-3-2-2 passes through large arm shaft 6-3-2-3 and vertical telescopic arm 6-3-2-4 Hingedly;Vertical telescopic arm 6-3-2-4 retractable structure, and turned by horizontal rotating shaft 6-3-2-8 and the absorptive table 6-3-2-7 of lower part Dynamic connection;Multiple automatically controlled magnetic salient point 6-3-2-5, equidistant layout are equipped in the lower surface absorptive table 6-3-2-7;In absorptive table 6-3- 2-7 is surrounded by multiple automatically controlled magnetic ring 6-3-2-6, equidistant layout, automatically controlled magnetic salient point 6-3-2-5, automatically controlled magnetic ring 6-3- 2-6 is connect with electric cabinet 11;Magnetism goes metal device 6-3-2 waterproofing design.
As shown in fig. 7, being that automatic rinser 6-5 schemes in the present invention.As seen from the figure, the automatic rinser 6-5 includes: Shell 6-5-1 is cleaned, battery motor depository dish 6-5-2, signal transceiver 6-5-3, creep adsorbent equipment 6-5-4, washer 6- 5-5 seeks spot instrument 6-5-6;Automatic rinser 6-5 itself is waterproof construction;Electricity is equipped at the center the cleaning shell 6-5-1 Pond motor depository dish 6-5-2, pull quick fixation structure, inside are equipped with battery, driving motor, vacuum pump, the battery motor storage The side box 6-5-2 is equipped with signal transceiver 6-5-3;The adsorbent equipment 6-5-4 that creeps, which is located at, cleans shell 6-5-1 apex angle, and 4 The adsorbent equipment 6-5-4 that creeps collectively constitutes movement mechanism;The washer 6-5-5 is located at cleaning shell 6-5-1 central lower, clearly Wash the lower surface device 6-5-5 be equipped with seek spot instrument 6-5-6;The battery motor depository dish 6-5-2, signal transceiver 6-5-3 and Spot instrument 6-5-6 is sought to connect with 11 wireless control of electric cabinet.
As shown in figure 8, being adsorbent equipment 6-5-4 figure of creeping in the present invention.As seen from the figure, the adsorbent equipment 6- that creeps 5-4 includes: horizontal swinging arm 6-5-4-1, extending arm 6-5-4-2, stretches hydraulic press 6-5-4-3, vertical moving arm 6-5-4-4, is hung down To hydraulic press 6-5-4-5, positioning disk 6-5-4-6, suction tray 6-5-4-7, fixed column 6-5-4-8, suction tray spring 6-5-4-9; The end the horizontal swinging arm 6-5-4-1 turns equipped with extending arm 6-5-4-2, the extending arm 6-5-4-2 and horizontal swinging arm 6-5-4-1 Dynamic connection, and swung up and down using horizontal swinging arm 6-5-4-1 as rotation axis, it is equipped with stretching, extension hydraulic press 6-5-4-3 between the two, it is described Stretching, extension hydraulic press 6-5-4-3 is connect with 11 wireless control of electric cabinet;The vertical moving arm 6-5-4-4 is located at extending arm 6-5-4- 2 ends, vertical moving arm 6-5-4-4 and extending arm 6-5-4-2 are rotatablely connected, vertical moving arm 6-5-4-4 and extending arm 6-5- Vertical hydraulic press 6-5-4-5 is equipped between 4-2, the vertical hydraulic press 6-5-4-5 is connect with 11 wireless control of electric cabinet;It is described Positioning disk 6-5-4-6 is located at the lower surface vertical moving arm 6-5-4-4, is equipped with suction tray 6-5-4-7 below positioning disk 6-5-4-6, It is fixedly connected between the suction tray 6-5-4-7 and positioning disk 6-5-4-6 by fixed column 6-5-4-8, in fixed column 6-5-4-8 Portion is equipped with tracheae, and tracheae one end is connected to vacuum pump, and the other end is connected to suction tray 6-5-4-7;The suction tray spring 6-5- The one end 4-9 connects positioning disk 6-5-4-6, the other end and suction tray 6-5-4-7 connection.
As shown in figure 9, being that washer 6-5-5 schemes in the present invention.As seen from the figure, the washer 6-5-5 includes: cleaning Driving machine 6-5-5-1, fan 6-5-5-2, transmission gear 6-5-5-3, rotating disk 6-5-5-4, keep a public place clean brush head 6-5-5-5, clear water Pipeline 6-5-5-6;The cleaning driving machine 6-5-5-1 is connect with 11 wireless control of electric cabinet, cleaning driving machine 6-5-5-1 output End is equipped with fan 6-5-5-2, dries up surface after cleaning;The transmission gear 6-5-5-3 is located at below fan 6-5-5-2, Transmission gear 6-5-5-3 engages connection with cleaning driving machine 6-5-5-1 output main shaft;The rotating disk 6-5-5-4 is located at transmission The lower surface gear 6-5-5-3, rotating disk 6-5-5-4 quantity are 3 groups, and the lower surface rotating disk 6-5-5-4 is equipped with the brush head 6-5- that keeps a public place clean 5-5;The water pipeline 6-5-5-6 is located at the upper surface transmission gear 6-5-5-3, water pipeline 6-5-5-6 and rotating disk 6-5- 5-4 is mutually communicated.
It as shown in Figure 10, is 14 figure of bracket in the present invention.As seen from the figure, the bracket 14 includes: carriage drive machine 14- 1, transmission case 14-2, support gear 14-3, bracket track 14-4, bracket shell 14-5, weight body 14-6, supporter 14-7;It is described Bracket shell 14-5 is located at the top of 14 pedestal of bracket, and the two is independent;The bracket shell 14-5 is hollow structure, bracket track 14-4 Inside bracket shell 14-5, and it is vertical with 14 pedestal of bracket and be fixedly connected;The supporter 14-7 is arranged in transmission case 14- 2 sides, the two connection;It is equipped with support gear 14-3 inside transmission case 14-2, is engaged with the surface bracket track 14-4 rack gear Connection;The supporter 14-7 is realized and on bracket track 14-4 by support gear 14-3 with engaging for bracket track 14-4 Sliding;The weight body 14-6 is located on the outside of supporter 14-7, and the two is fixed, and bracket shell 14-5 is stretched out in the end weight body 14-6 Outside, waist are fixedly connected with bracket shell 14-5;The carriage drive machine 14-1 is located at the lower end transmission case 14-2 side, bracket Driving machine 14-1 and support gear 14-3 is sequentially connected, and carriage drive machine 14-1 is connected by conducting wire with the control of electric cabinet 11, props up Frame driving machine 14-1 driving arm gear 14-3 rotates and drives transmission case 14-2, bracket shell 14-5, weight body 14-6, supporter 14-7 rises or falls along bracket track 14-4.
It as shown in figure 11, is 15 figure of regulating wheel in the present invention.As seen from the figure, the regulating wheel 15 includes: regulating wheel U plate 15-1, grease-box 15-2, movable pulley shaft 15-3, movable pulley 15-4, atomizer 15-5, wheel track 15-6;The regulating wheel U Plate 15-1 is that concave structure, steel plate production, two sides side wall inverted trapezoidal design;The movable pulley shaft 15-3 is connected to regulating wheel Between the side wall of the two sides U plate 15-1, movable pulley shaft 15-3 and external motor are sequentially connected, and movable pulley shaft 15-3 is equipped with movement Take turns 15-4;The movable pulley 15-4 and movable pulley shaft 15-3 is rotatablely connected, the external motor and electric cabinet 11 of movable pulley 15-4 Polygon control survey connection;The wheel track 15-6 is located at the lower part movable pulley 15-4, the two rolls connection;The grease-box 15-2 is solid Surely it being connected to outside the side wall of the side regulating wheel U plate 15-1, atomizer 15-5 is fixedly connected on the inside of regulating wheel U plate 15-1 upper wall, Grease-box 15-2 is connect by its internal oil guide pipe with atomizer 15-5.
It as shown in figure 12, is that grease-box 15-2 schemes in the present invention.As seen from the figure, comprising: profit oil pump 15-2-1, distribution Case 15-2-2, Rose Box 15-2-3, oil fuel tube 15-2-4, radiator 15-2-5, fixed plate 15-2-6, abutment sleeve 15-2-7, Oil fuel tube exports 15-2-8;Profit oil pump 15-2-1 positioned at bottom is connected to the distributor box 15-2-2 on top, distributor box 15-2-2 Rectangular box, both ends short axle are semicircle, and it is different inside to set two groups of agitator arms, diameter, big agitator arm diameter 30cm, Small agitator arm diameter 9cm, the two horizontal Tile layout do not stir in the same direction, stretch upwards at distributor box 15-2-2 two semicircular endpoint Two branch pipe out is connected to by valve with Rose Box 15-2-3, two pipe diameter differences, extra heavy pipe diameter 8cm, capillary diameter 2cm, point It is not arranged in big agitator arm, small agitator arm on one side, enters Rose Box 15-2-3 to control different viscosity lubricating oil;Filtering Case 15-2-3 is located at the top distributor box 15-2-2, the two perforation, and it is clear that filter screen, mud chamber, net impurity are set in Rose Box 15-2-3 Except device;Radiator 15-2-5 is located at the top Rose Box 15-2-3, and radiator 15-2-5 red copper material is made of the superposition of multiple groups copper sheet And there are gaps between copper sheet;The outer surface radiator 15-2-5 winds oil fuel tube 15-2-4, the winding section pressure resistance red copper material, oiling The one end pipe 15-2-4 and Rose Box 15-2-3 are penetrated through, and the other end passes through abutment sleeve 15-2-7 and oil fuel tube outlet 15-2-8 connects It is logical;The one end the fixed plate 15-2-6 is socketed in the outer surface abutment sleeve 15-2-7, and the other end is connect with fixation wall.
It as shown in figure 13, is that atomizer 15-5 schemes in the present invention.As seen from the figure, comprising: main by-pass tube 15-5-1, cover Shell 15-5-2, inclination angle injector body 15-5-3, oil spout mouth for adjusting 15-5-4;The cover shell 15-5-2 is hollow, upper closing The inverted round table structure of bottom opening, the surface cover shell 15-5-2 is equipped with main by-pass tube 15-5-1, wherein main by-pass tube 15- The bottom end 5-1 is inserted into cover shell 15-5-2, and the oil guide pipe on the top main by-pass tube 15-5-1 and top penetrates through connection;The inclination angle Injector body 15-5-3 is located inside cover shell 15-5-2, and the quantity of inclination angle injector body 15-5-3 is 4~8, adjacent inclination angle spray Oil body 15-5-3 is angularly distributed using main by-pass tube 15-5-1 as center axis, each inclination angle injector body 15-5-3 by oil distributing pipe with Main by-pass tube 15-5-1 perforation connection;The oil spout mouth for adjusting 15-5-4 is fixedly connected on the lower part cover shell 15-5-2, controllable Folding structure is adjusted, injection flow and angle are controlled.
It as shown in figure 14, is that injector body 15-5-3 in inclination angle schemes in the present invention.As seen from the figure, comprising: oil inlet 15-5-3- 1, tangential oil outlet 15-5-3-2, oil spout shell 15-5-3-3, staggeredly spoiler 15-5-3-4, housing actuator 15-5-3-5, Shell Reinforced Hoop 15-5-3-6;Oil inlet 15-5-3-1 is equipped at the top of oil spout shell 15-5-3-3, in oil spout shell 15-5-3- 3 side walls are equipped with a large amount of tangential oil outlet 15-5-3-2, and lubricating oil is tangentially sprayed along the surface oil spout shell 15-5-3-3;In oil spout Shell 15-5-3-3 inner wall is equipped with largely staggeredly spoiler 15-5-3-4, is staggeredly fixed on inner wall surface, staggeredly spoiler 15-5- 3-4 thin plate stainless steel structure, length are the 4/5 of oil spout shell 15-5-3-3 length, are highly oil spout shell 15-5-3-3 radius 1/10;Shell Reinforced Hoop 15-5-3-6, housing actuator 15-5-3-5 are equipped with outside oil spout shell 15-5-3-3;Wherein shell 2 groups of driver 15-5-3-5 or more, and oil spout shell 15-5-3-3 is driven to rotate simultaneously.
It as shown in figure 15, is that housing actuator 15-5-3-5 schemes in the present invention.As seen from the figure, comprising: shell flange 15- 5-3-5-1, one 15-5-3-5-2 of axis, circumference rack gear 15-5-3-5-3, connecting plate 15-5-3-5-4, horizontal location wheel 15-5-3- 5-5, circumference driving wheel 15-5-3-5-6, two 15-5-3-5-7 of axis;Circumference rack gear is externally surrounded by oil spout shell 15-5-3-3 15-5-3-5-3, the two are fixedly connected by connecting plate 15-5-3-5-4;One group is respectively set above or below circumference rack gear 15-5-3-5-3 Horizontal location wheel 15-5-3-5-5, to prevent circumference driving wheel 15-5-3-5-6 sideslip, horizontal location wheel 15-5-3-5-5 is around axis One 15-5-3-5-2 rotation;One group of circumference driving wheel 15-5-3-5-6, the two are respectively set in the two sides horizontal location wheel 15-5-3-5-5 It is fixedly connected;Two 15-5-3-5-7 of axis drives circumference driving wheel 15-5-3-5-6 rotation, circumference driving wheel 15-5-3-5-6 gear Structure and circumference rack gear 15-5-3-5-3 engaged transmission;The shell flange 15-5-3-5-1 is realized on oil spout shell 15-5-3-3 Lower docking.
It as shown in figure 16, is that circumference rack gear 15-5-3-5-3 schemes in the present invention.As seen from the figure, comprising: circumference flank of tooth 15- 5-3-5-3-1, fan-shaped teeth 15-5-3-5-3-2, oiling machine 15-5-3-5-3-3, bottom transverse slat 15-5-3-5-3-4, damping bullet Spring 15-5-3-5-3-5, blower 15-5-3-5-3-6;The circumference flank of tooth 15-5-3-5-3-1 is 2 groups, and arranged opposite passes through Bottom transverse slat 15-5-3-5-3-4 connection;Being equally spaced on the surface circumference flank of tooth 15-5-3-5-3-1 has fan-shaped teeth 15-5-3- 5-3-2;It is equipped with oiling machine 15-5-3-5-3-3, on the transverse slat 15-5-3-5-3-4 of bottom for gear engagement lubrication;It is described to subtract Shake spring 15-5-3-5-3-5 is fixed on the bottom surface transverse slat 15-5-3-5-3-4, and top is equipped with clump weight;The blower 15- The one end 5-3-5-3-6 be threadedly coupled and pass through with damping spring 15-5-3-5-3-5 clump weight, damping spring 15-5-3-5-3-5, Bottom transverse slat 15-5-3-5-3-4 extends to outside, and other end outlet is directed at fan-shaped teeth 15-5-3-5-3-2, blower 15-5-3- 5-3-6 shakes with damping spring 15-5-3-5-3-5 and is freely swung.
It as shown in figure 17, is that oiling machine 15-5-3-5-3-3 schemes in the present invention.As seen from the figure, comprising: protective cover 15-5- 3-5-3-3-1, oil storage bag 15-5-3-5-3-3-2 stir separator 15-5-3-5-3-3-3, filter rotary table case 15-5-3-5-3- 3-4, settling tank 15-5-3-5-3-3-5, overflow pipe 15-5-3-5-3-3-6, oil water separator 15-5-3-5-3-3-7 stand and divide From case 15-5-3-5-3-3-8, oil pipe 15-5-3-5-3-3-9 is recycled, separates water pipe 15-5-3-5-3-3-10, precipitates property management 15- 5-3-5-3-3-11, metal sediment pipe 15-5-3-5-3-3-12, oil input channel 15-5-3-5-3-3-13, screw thread flowline 15-5- 3-5-3-3-14;Oil input channel 15-5-3-5-3-3-13 positioned at lower part, external oil is thence into top stirring separator 15-5-3-5-3-3-3 connection, stir separator 15-5-3-5-3-3-3 in have 2 groups of agitator arms, horizontal layout, in the same direction it is low Speed stirring, wherein left side agitator arm top is equipped with channel and oil storage bag 15-5-3-5-3-3-2 is penetrated through, oil storage bag 15-5-3-5- The periphery 3-3-2 is equipped with protective cover 15-5-3-5-3-3-1, upper part is equipped with screw thread flowline 15-5-3-5-3-3-14, and the two is passed through It is logical;Agitator arm lower part, which is equipped with, on the left of stirring separator 15-5-3-5-3-3-3 filters rotary table case 15-5-3-5-3-3-4, and two Person is penetrated through by conduit, is equipped with filter screen inside filtering rotary table case 15-5-3-5-3-3-4;The settling tank 15-5-3-5-3-3- 5 are located at the filtering lower part rotary table case 15-5-3-5-3-3-4, the two perforation connection, and settling tank 15-5-3-5-3-3-5 lower right side is set There are metal sediment pipe 15-5-3-5-3-3-12, left upper portion to be equipped with overflow pipe 15-5-3-5-3-3-6, overflow pipe 15-5-3-5- 3-3-6 oil inlet is always positioned at solution surface in settling tank 15-5-3-5-3-3-5;Oil water separator 15-5-3- positioned at lower part 5-3-3-7 is penetrated through by overflow pipe 15-5-3-5-3-3-6 and settling tank 15-5-3-5-3-3-5, closing, right end in its left part Portion is equipped with precipitating property management 15-5-3-5-3-3-11, oil water separator 15-5-3-5-3-3-7 and is horizontally inserted into settle and separate case 15-5- Inside 3-5-3-3-8, wherein realizing controllable rotating in settle and separate case 15-5-3-5-3-3-8 inserting paragraph and its surface being equipped with A large amount of small through hole;It is equipped on the settle and separate top case 15-5-3-5-3-3-8 and recycles oil pipe 15-5-3-5-3-3-9, lower part is equipped with Separate water pipe 15-5-3-5-3-3-10.
It as shown in figure 18, is that separator 15-5-3-5-3-3-3 figure is stirred in the present invention.As seen from the figure, comprising: damping Spring 15-5-3-5-3-3-3-1, one 15-5-3-5-3-3-3-2 of stirring wheel assist quant 15-5-3-5-3-3-3-3, stirring wheel Two 15-5-3-5-3-3-3-4;Stirring separator 15-5-3-5-3-3-3 inside be equipped with stirring wheel 15-5-3-5-3-3-3-2, Two 15-5-3-5-3-3-3-4 of stirring wheel, the two horizontal layout is non-to be stirred in the same direction, wherein two 15-5-3-5-3- of stirring wheel The axle center 3-3-4 lower part is equipped with oil input channel 15-5-3-5-3-3-13, and one axle center 15-5-3-5-3-3-3-2 top of stirring wheel is equipped with clear Oil export, lower part are exported equipped with waste oil;Damping spring 15-5-3- is equipped in separator 15-5-3-5-3-3-3 enclosure interior one end 5-3-3-3-1, the other end are equipped with auxiliary quant 15-5-3-5-3-3-3-3, wherein the root damping spring 15-5-3-5-3-3-3-1 It is fixed on shell, upper part freely swings;Assist the lower part quant 15-5-3-5-3-3-3-3 be equipped with a cylinder, cylinder one end with The rotation connection of top blade, the other end are fixed on separator 15-5-3-5-3-3-3 enclosure interior.

Claims (10)

1. a kind of produce Pfansteihl device using Rhizopus oryzae, comprising: dissolving tank (1), delivery pump (2), preparing pool (3), distillation Tower front pump (4), destilling tower (5), trickle bed reactor (6), sediment discharge pipe (7) sample exhaust pipe (8), high-position discharge It manages (9), gas-liquid separator (10), electric cabinet (11), inoculation sampling return pipe (12), main fermentation case (13), bracket (14) is adjusted It takes turns (15);It is characterized in that, the dissolving tank (1) for being located at side passes through delivery pump (2) and the main fermentation case (13) for being located at upper left quarter Connection, main fermentation case (13) top are controllable opening enclosed structure;Main fermentation case (13) lower part is equipped with preparing pool (3), top one Side is equipped with inoculation sampling return pipe (12), is connected to the two pipeline, wherein inoculation sampling return pipe (12) is for being inoculated with, taking Sample, and discharge water is flowed back into dissolving tank (1);Electric cabinet (11) are equipped on bracket (14) top;Bracket (14) side is equipped with Destilling tower (5), the destilling tower (5) is placed vertically, bottom is connected to external steam, and destilling tower (5) hollow structure, shell is adopted It is made of high molecular material, the destilling tower (5) is connected to by destilling tower front pump (4) with main fermentation case (13), destilling tower (5) It is connected to the gas-liquid separator (10) on top;The trickle bed reactor (6) using gas and liquid flowing mode respectively with gas-liquid separation Device (10), destilling tower (5) connection;Trickle bed reactor (6) lower part is equipped with sediment discharge pipe (7), top is equipped with high-position discharge (9), waist are managed equipped with sampling exhaust pipe (8), trickle bed reactor (6) is connected to three;The regulating wheel (15) is located at distillation Tower (5) bottom, quantity are four;The delivery pump (2), destilling tower front pump (4) and electric cabinet (11) polygon control survey link;
The destilling tower (5) is equipped with catalysis system (5-4);It is internal in the top control valve of slagging tap (5-2), distillation tower shell (5-3) Equipped with catalysis system (5-4);
The catalysis system (5-4) includes: slag tap control valve (5-2), lower part connecting flange (5-4-2), hot mixing room (5-4- 3) it, is catalyzed shell (5-4-4), is vaporized concentration sensor (5-4-5), vaporizing chamber (5-4-6), top connecting flange (5-4-7) is urged Change reaction-filling object (5-4-8), net-fault column plate (5-4-9), promotor spray ring (5-4-10), heat build-up bucket (5-4-11);Under described Portion's connecting flange (5-4-2) is located at the lower part entire catalysis system (5-4), and upper part is equipped with vaporizing chamber (5-4-6) and connects with top Flange (5-4-7), and vaporizing chamber (5-4-6) and top connecting flange (5-4-7) perforation and catalysis shell (5-4-4) are fixed and are connected It connects;The upper and lower ends for being catalyzed shell (5-4-4) are fixed with top connecting flange (5-4-7), lower part connecting flange (5-4-2) respectively Connection, middle and lower part connecting flange (5-4-2) are located at catalysis lower part shell (5-4-4);The hot mixing room (5-4-3), which is located at, urges Change the inside shell (5-4-4), the top control valve of slagging tap (5-2), hot mixing room (5-4-3) is cylindrical, hollow knot up and down Structure, hot steam are sufficiently mixed herein with mixed liquor;The other end of hot mixing room (5-4-3) passes through lower part connecting flange (5-4-2) It penetrates through and connects with control valve of slagging tap (5-2), wherein control valve of slagging tap (5-2) is located at the lower part of lower part connecting flange (5-4-2);Institute It states heat build-up bucket (5-4-11) and is located at the top of hot mixing room (5-4-3), the two perforation connection, heat build-up bucket (5-4-11) loudspeaker are made Type, up and down and under it is small big, surface is equipped with a large amount of through-holes, and waist is equipped with deflector, is steamed heat using horn mouth moulding The solution that vapour and net-fault column plate (5-4-9) splash down carries out sufficient heat exchange;The catalysis reaction-filling object (5-4-8), net-fault tower Plate (5-4-9), promotor spray ring (5-4-10) are located at the top heat build-up bucket (5-4-11), wherein catalysis reaction-filling object (5-4-8) Quantity be 3 groups, equidistantly distribute between adjacent catalyst reaction-filling object (5-4-8);The net-fault column plate surface (5-4-9) is equipped with big Measuring through-hole, quantity is 20, is equally spaced internal in catalysis shell (5-4-4);Promotor spray ring (5-4-10) Xiang Cuihua shell Promotor is added in injection in (5-4-4);The promotor spray ring (5-4-10), catalysis reaction-filling object (5-4-8), net-fault column plate (5-4-9) is all that mixed liquor is promoted to be chemically reacted;The vaporization concentration sensor (5-4-5) is located at catalysis shell (5-4- 4) waist, vaporization concentration sensor (5-4-5) are connect with electric cabinet (11) polygon control survey.
2. a kind of utilization Rhizopus oryzae according to claim 1 produces Pfansteihl device, which is characterized in that the destilling tower It (5) include: slag notch (5-1), control valve of slagging tap (5-2) distills tower shell (5-3), catalysis system (5-4), outlet tube (5- 5), escape pipe (5-6), inlet (5-7), steam pipe (5-8);Both slag notch (5-1) is equipped in destilling tower (5) lower part to pass through Slag tap control valve (5-2) perforation;Catalysis system (5- is equipped with inside the top control valve of slagging tap (5-2), distillation tower shell (5-3) 4);Steam pipe (5-8), the other side, which are equipped with, in the distillation tower shell side (5-3) is equipped with inlet equipped with outlet tube (5-5), waist (5-7), top are equipped with escape pipe (5-6), distillation tower shell (5-3) and four perforations;
The trickle bed reactor (6) includes: shower washing device (6-1), catalyst adding tube (6-2), mixing agitator (6- 3), stirring motor (6-4), automatic rinser (6-5), ripple generator (6-6);Shower washing device (6-1) positioned at side, One end is connected to external fresh water pump, and the other end generates 5 spray heads being horizontally directed to;It is set in the side shower washing device (6-1) Have catalyst adding tube (6-2), catalyst adding tube (6-2) circular ring shape, hollow structure, vertical arrangement, is equipped on its surface big Measure through-hole;It is equipped with mixing agitator (6-3) in the catalyst adding tube side (6-2), the mixing agitator (6-3) and its right side Stirring motor (6-4) be drivingly connected, stirring motor (6-4) waterproofing design;It is equipped with certainly in trickle bed reactor (6) interior side Dynamic cleaning machine (6-5), connect with electric cabinet (11) wireless control;The ripple generator (6-6) is located at trickle bed reactor (6) internal, side mixing agitator (6-3);
The mixing agitator (6-3) includes: mixing inlet (6-3-1), and magnetism removes metal device (6-3-2), side door (6-3- 3) impeller (6-3-4), is mixed, antioxidant filler (6-3-5) mixes liquid outlet (6-3-6);Mixing positioned at side Inlet (6-3-1) is penetrated through with the mixing liquid outlet (6-3-6) for being located at the other side;It is equipped on the inside of mixing liquid outlet (6-3-6) It is mixed impeller (6-3-4), the fixed certain amount blade in surface by motor driven, promotes solution mutually immiscible;Mixed It closes blender (6-3) interior side to go metal device (6-3-2) equipped with magnetism, waterproof construction, bottom chuck are moved with lever arm level It is dynamic;It is equipped with side door (6-3-3) on its opposite, magnetism goes metal device (6-3-2) lever arm to be adsorbed in side door (6-3-3) unloading Object;Antioxidant filler (6-3-5) is equipped in mixing agitator (6-3) bottom side;
It includes: fixed station (6-3-2-1), horizontal extension arm (6-3-2-2), large arm shaft that the magnetism, which removes metal device (6-3-2), (6-3-2-3), vertical telescopic arm (6-3-2-4), automatically controlled magnetic salient point (6-3-2-5), automatically controlled magnetic ring (6-3-2-6), absorption Platform (6-3-2-7), horizontal rotating shaft (6-3-2-8);Fixed station (6-3-2-1) positioned at side is fixed on base surface, with water The horizontal extension arm (6-3-2-2) of plain cloth office connects, horizontal extension arm (6-3-2-2) retractable structure;It is equipped in its end big Arm shaft (6-3-2-3), horizontal extension arm (6-3-2-2) pass through large arm shaft (6-3-2-3) and vertical telescopic arm (6-3-2-4) Hingedly;Vertical telescopic arm (6-3-2-4) retractable structure, and pass through the absorptive table (6-3- of horizontal rotating shaft (6-3-2-8) and lower part 2-7) it is rotatablely connected;Multiple automatically controlled magnetic salient points (6-3-2-5), equidistant layout are equipped in the absorptive table lower surface (6-3-2-7);In Absorptive table (6-3-2-7) is surrounded by multiple automatically controlled magnetic rings (6-3-2-6), equidistant layout, automatically controlled magnetic salient point (6-3-2- 5), automatically controlled magnetic ring (6-3-2-6) connect with electric cabinet (11);Magnetism goes metal device (6-3-2) waterproofing design.
3. a kind of utilization Rhizopus oryzae according to claim 2 produces Pfansteihl device, which is characterized in that described automatic clear Washing machine (6-5) includes: cleaning shell (6-5-1), battery motor depository dish (6-5-2), signal transceiver (6-5-3), suction of creeping Adsorption device (6-5-4), washer (6-5-5) seek spot instrument (6-5-6);Automatic rinser (6-5) itself is waterproof construction; At cleaning shell (6-5-1) center be equipped with battery motor depository dish (6-5-2), pull quick fixation structure, inside be equipped with battery, Driving motor, vacuum pump, the battery motor depository dish side (6-5-2) are equipped with signal transceiver (6-5-3);The suction of creeping Adsorption device (6-5-4) is located at cleaning shell (6-5-1) apex angle, and 4 adsorbent equipments of creeping (6-5-4) collectively constitute movement mechanism; The washer (6-5-5) is located at cleaning shell (6-5-1) central lower, and the washer lower surface (6-5-5) is equipped with and seeks spot Instrument (6-5-6);The battery motor depository dish (6-5-2), signal transceiver (6-5-3) and seek spot instrument (6-5-6) and electricity Control the connection of case (11) wireless control.
4. a kind of utilization Rhizopus oryzae according to claim 3 produces Pfansteihl device, which is characterized in that the suction of creeping Adsorption device (6-5-4) includes: horizontal swinging arm (6-5-4-1), and extending arm (6-5-4-2) stretches hydraulic press (6-5-4-3), vertical Moving arm (6-5-4-4), vertical hydraulic press (6-5-4-5), positioning disk (6-5-4-6), suction tray (6-5-4-7), fixed column (6- 5-4-8), suction tray spring (6-5-4-9);The horizontal swinging arm end (6-5-4-1) is equipped with extending arm (6-5-4-2), described Extending arm (6-5-4-2) and horizontal swinging arm (6-5-4-1) are rotatablely connected, and are rotation axis or more with horizontal swinging arm (6-5-4-1) It swings, is equipped with stretching, extension hydraulic press (6-5-4-3) between the two, the stretching, extension hydraulic press (6-5-4-3) and electric cabinet (11) are wireless Control connection;The vertical moving arm (6-5-4-4) is located at the end extending arm (6-5-4-2), vertical moving arm (6-5-4-4) with Extending arm (6-5-4-2) rotation connection is equipped with vertical hydraulic between vertical moving arm (6-5-4-4) and extending arm (6-5-4-2) Machine (6-5-4-5), the vertical hydraulic press (6-5-4-5) connect with electric cabinet (11) wireless control;Positioning disk (the 6-5-4- 6) it is located at the lower surface vertical moving arm (6-5-4-4), is equipped with suction tray (6-5-4-7) below positioning disk (6-5-4-6), the suction It is fixedly connected between attached disk (6-5-4-7) and positioning disk (6-5-4-6) by fixed column (6-5-4-8), fixed column (6-5-4-8) Inside is equipped with tracheae, and tracheae one end is connected to vacuum pump, and the other end is connected to suction tray (6-5-4-7);The suction tray spring The one end (6-5-4-9) connects positioning disk (6-5-4-6), the other end and suction tray (6-5-4-7) and connects.
5. a kind of utilization Rhizopus oryzae according to claim 4 produces Pfansteihl device, which is characterized in that the washer (6-5-5) includes: cleaning driving machine (6-5-5-1), fan (6-5-5-2), transmission gear (6-5-5-3), rotating disk (6-5-5- 4), keep a public place clean brush head (6-5-5-5), water pipeline (6-5-5-6);The cleaning driving machine (6-5-5-1) and electric cabinet (11) nothing Line traffic control connection, cleaning driving machine (6-5-5-1) output end are equipped with fan (6-5-5-2), dry up surface after cleaning;It is described Transmission gear (6-5-5-3) is located at below fan (6-5-5-2), transmission gear (6-5-5-3) and cleaning driving machine (6-5-5-1) Export main shaft engagement connection;The rotating disk (6-5-5-4) is located at the lower surface transmission gear (6-5-5-3), rotating disk (6-5-5- 4) quantity is 3 groups, and the rotating disk lower surface (6-5-5-4), which is equipped with, keeps a public place clean brush head (6-5-5-5);The water pipeline (6-5-5-6) Positioned at the upper surface transmission gear (6-5-5-3), water pipeline (6-5-5-6) is mutually communicated with rotating disk (6-5-5-4).
6. a kind of utilization Rhizopus oryzae according to claim 5 produces Pfansteihl device, which is characterized in that the bracket It (14) include: carriage drive machine (14-1), transmission case (14-2), support gear (14-3), bracket track (14-4), bracket shell (14-5), weight body (14-6), supporter (14-7);The bracket shell (14-5) is located at the top of bracket (14) pedestal, the two It is independent;The bracket shell (14-5) is hollow structure, and bracket track (14-4) is set to the inside bracket shell (14-5), and and bracket (14) pedestal is vertical and is fixedly connected;The supporter (14-7) is arranged in the side transmission case (14-2), the two connection;It is being driven It is equipped with support gear (14-3) inside case (14-2), engages connection with the surface bracket track (14-4) rack gear;The supporter (14-7) engages the sliding realized and on bracket track (14-4) by support gear (14-3) and bracket track (14-4); The weight body (14-6) is located on the outside of supporter (14-7), and the two is fixed, and bracket shell (14- is stretched out in the weight body end (14-6) 5) external, waist is fixedly connected with bracket shell (14-5);The carriage drive machine (14-1) is located at the lower end transmission case (14-2) Side, carriage drive machine (14-1) and support gear (14-3) are sequentially connected, carriage drive machine (14-1) by conducting wire with it is automatically controlled Case (11) control is connected, and carriage drive machine (14-1) driving arm gear (14-3) rotates and drives transmission case (14-2), bracket Shell (14-5), weight body (14-6), supporter (14-7) rise or fall along bracket track (14-4).
7. a kind of utilization Rhizopus oryzae according to claim 6 produces Pfansteihl device, which is characterized in that the regulating wheel It (15) include: regulating wheel U plate (15-1), grease-box (15-2), movable pulley shaft (15-3), movable pulley (15-4), atomizer (15-5), wheel track (15-6);The regulating wheel U plate (15-1) is that concave structure, steel plate production, two sides side wall inverted trapezoidal are set Meter;The movable pulley shaft (15-3) is connected between the side wall of the two sides regulating wheel U plate (15-1), movable pulley shaft (15-3) and outer The connection of portion's motor drive, movable pulley shaft (15-3) are equipped with movable pulley (15-4);The movable pulley (15-4) and mobile rotation Axis (15-3) rotation connection, the external motor of movable pulley (15-4) are connect with electric cabinet (11) polygon control survey;The wheel track (15-6) is located at the lower part movable pulley (15-4), the two rolls connection;The grease-box (15-2) is fixedly connected on regulating wheel U plate Outside the side wall of the side (15-1), atomizer (15-5) is fixedly connected on the inside of regulating wheel U plate (15-1) upper wall, grease-box (15- 2) it is connect by its internal oil guide pipe with atomizer (15-5).
8. a kind of utilization Rhizopus oryzae according to claim 7 produces Pfansteihl device, which is characterized in that the lubricating oil Case (15-2) includes: profit oil pump (15-2-1), distributor box (15-2-2), Rose Box (15-2-3), oil fuel tube (15-2-4), heat dissipation Device (15-2-5), fixed plate (15-2-6), abutment sleeve (15-2-7), oil fuel tube export (15-2-8);Profit oil positioned at bottom Pump (15-2-1) is connected to the distributor box (15-2-2) on top, and distributor box (15-2-2) rectangular box, both ends short axle are semicircle Shape inside sets two groups of agitator arms, diameter difference, big agitator arm diameter 30cm, small agitator arm diameter 9cm, the two water Flat side-by-side configuration does not stir in the same direction, stretches out two branch pipes upwards at distributor box (15-2-2) two semicircular endpoint, passes through valve and filtering Case (15-2-3) connection, two pipe diameter differences, extra heavy pipe diameter 8cm, capillary diameter 2cm are arranged in big agitator arm, small Agitator arm on one side, enters Rose Box (15-2-3) to control different viscosity lubricating oil;Rose Box (15-2-3) is located at distribution The top case (15-2-2), the two perforation, Rose Box (15-2-3) is interior to set filter screen, mud chamber, net impurity remover;Radiator (15-2-5) is located at the top Rose Box (15-2-3), radiator (15-2-5) red copper material, is made of the superposition of multiple groups copper sheet and copper There are gaps between plate;The radiator outer surface (15-2-5) winds oil fuel tube (15-2-4), the winding section pressure resistance red copper material, oiling It manages the one end (15-2-4) and Rose Box (15-2-3) is penetrated through, the other end passes through abutment sleeve (15-2-7) and oil fuel tube exports (15- 2-8) it is connected to;Described fixed plate (15-2-6) one end is socketed in the outer surface abutment sleeve (15-2-7), and the other end and fixation wall connect It connects.
9. a kind of utilization Rhizopus oryzae according to claim 8 produces Pfansteihl device, which is characterized in that the atomizer (15-5) includes: main by-pass tube (15-5-1), cover shell (15-5-2), inclination angle injector body (15-5-3), oil spout mouth for adjusting (15-5-4);The cover shell (15-5-2) is the inverted round table structure of hollow, upper closed bottom opening, cover shell It is equipped with main by-pass tube (15-5-1) right above (15-5-2), wherein cover shell (15-5- is inserted into the main by-pass tube bottom end (15-5-1) 2) in, the oil guide pipe on the main by-pass tube top (15-5-1) and top penetrates through connection;The inclination angle injector body (15-5-3) is located at cover Face-piece body (15-5-2) is internal, and the quantity of inclination angle injector body (15-5-3) is 4~8, adjacent inclination angle injector body (15-5-3) with Main by-pass tube (15-5-1) is that center axis is angularly distributed, and each inclination angle injector body (15-5-3) passes through oil distributing pipe and main by-pass tube (15-5-1) perforation connection;The oil spout mouth for adjusting (15-5-4) is fixedly connected on the lower part cover shell (15-5-2), can control Folding structure is saved, injection flow and angle are controlled;
The inclination angle injector body (15-5-3) includes: oil inlet (15-5-3-1), tangential oil outlet (15-5-3-2), oil spout shell (15-5-3-3), staggeredly spoiler (15-5-3-4), housing actuator (15-5-3-5), shell Reinforced Hoop (15-5-3-6);In It is equipped with oil inlet (15-5-3-1) at the top of oil spout shell (15-5-3-3), is equipped in oil spout shell (15-5-3-3) side wall and largely cuts To oil outlet (15-5-3-2), lubricating oil is tangentially sprayed along the surface oil spout shell (15-5-3-3);In oil spout shell (15-5- 3-3) inner wall is equipped with largely staggeredly spoiler (15-5-3-4), is staggeredly fixed on inner wall surface, staggeredly spoiler (15-5-3-4) Thin plate stainless steel structure, length are the 4/5 of oil spout shell (15-5-3-3) length, are highly oil spout shell (15-5-3-3) radius 1/10;Shell Reinforced Hoop (15-5-3-6), housing actuator (15-5-3-5) are equipped with outside oil spout shell (15-5-3-3);Its 2 groups up and down of middle housing actuator (15-5-3-5), and oil spout shell (15-5-3-3) is driven to rotate simultaneously;
The housing actuator (15-5-3-5) includes: shell flange (15-5-3-5-1), axis one (15-5-3-5-2), circumferential teeth Item (15-5-3-5-3), connecting plate (15-5-3-5-4), horizontal location wheel (15-5-3-5-5), circumference driving wheel (15-5-3-5- 6), axis two (15-5-3-5-7);It is externally surrounded by circumference rack gear (15-5-3-5-3) in oil spout shell (15-5-3-3), the two is logical Connecting plate (15-5-3-5-4) is crossed to be fixedly connected;One group of horizontal location wheel (15- is respectively set up and down in circumference rack gear (15-5-3-5-3) 5-3-5-5), to prevent circumference driving wheel (15-5-3-5-6) sideslip, horizontal location wheel (15-5-3-5-5) is around one (15-5- of axis 3-5-2) rotate;One group of circumference driving wheel (15-5-3-5-6) is respectively set in the two sides horizontal location wheel (15-5-3-5-5), the two is solid Fixed connection;Axis two (15-5-3-5-7) drives circumference driving wheel (15-5-3-5-6) rotation, circumference driving wheel (15-5-3-5-6) Gear structure and circumference rack gear (15-5-3-5-3) engaged transmission;The shell flange (15-5-3-5-1) realizes oil spout shell (15-5-3-3) is docked up and down.
10. a kind of utilization Rhizopus oryzae according to claim 9 produces Pfansteihl device, which is characterized in that the circumference Rack gear (15-5-3-5-3) includes: the circumference flank of tooth (15-5-3-5-3-1), fan-shaped teeth (15-5-3-5-3-2), oiling machine (15- 5-3-5-3-3), bottom transverse slat (15-5-3-5-3-4), damping spring (15-5-3-5-3-5), blower (15-5-3-5-3- 6);The circumference flank of tooth (15-5-3-5-3-1) is 2 groups, and arranged opposite is connected by bottom transverse slat (15-5-3-5-3-4);In The surface the circumference flank of tooth (15-5-3-5-3-1) is equally spaced and has fan-shaped teeth (15-5-3-5-3-2);In bottom transverse slat (15-5-3- It 5-3-4) is equipped with oiling machine (15-5-3-5-3-3), for gear engagement lubrication;The damping spring (15-5-3-5-3-5) It is fixed on the surface bottom transverse slat (15-5-3-5-3-4), top is equipped with clump weight;Described blower (15-5-3-5-3-6) one end It is threadedly coupled with damping spring (15-5-3-5-3-5) and passes through clump weight, damping spring (15-5-3-5-3-5), bottom transverse slat (15-5-3-5-3-4) extends to outside, and other end outlet is directed at fan-shaped teeth (15-5-3-5-3-2), blower (15-5-3-5- It 3-6) shakes and freely swings with damping spring (15-5-3-5-3-5);
The oiling machine (15-5-3-5-3-3) includes: protective cover (15-5-3-5-3-3-1), oil storage bag (15-5-3-5-3-3- 2) separator (15-5-3-5-3-3-3), is stirred, is filtered rotary table case (15-5-3-5-3-3-4), settling tank (15-5-3-5-3-3- 5), overflow pipe (15-5-3-5-3-3-6), oil water separator (15-5-3-5-3-3-7), settle and separate case (15-5-3-5-3-3- 8) oil pipe (15-5-3-5-3-3-9), is recycled, is separated water pipe (15-5-3-5-3-3-10), property management (15-5-3-5-3-3- is precipitated 11), metal sediment pipe (15-5-3-5-3-3-12), oil input channel (15-5-3-5-3-3-13), screw thread flowline (15-5-3-5- 3-3-14);Oil input channel (15-5-3-5-3-3-13) positioned at lower part, external oil is thence into top stirring separator (15-5-3-5-3-3-3) connection, stirring separator (15-5-3-5-3-3-3) is interior 2 groups of agitator arms, horizontal layout, differences To stirring at low speed, wherein left side agitator arm top is equipped with channel and oil storage bag (15-5-3-5-3-3-2) is penetrated through, oil storage bag The periphery (15-5-3-5-3-3-2) is equipped with protective cover (15-5-3-5-3-3-1), upper part is equipped with screw thread flowline (15-5-3-5- 3-3-14), the two penetrates through;Agitator arm lower part is equipped with filtering rotary table case on the left of stirring separator (15-5-3-5-3-3-3) (15-5-3-5-3-3-4), the two are penetrated through by conduit, and filter screen is equipped with inside filtering rotary table case (15-5-3-5-3-3-4);Institute It states settling tank (15-5-3-5-3-3-5) and is located at filtering lower part rotary table case (15-5-3-5-3-3-4), the two perforation connection, precipitating Case (15-5-3-5-3-3-5) lower right side is equipped with metal sediment pipe (15-5-3-5-3-3-12), left upper portion is equipped with overflow pipe (15-5-3-5-3-3-6), overflow pipe (15-5-3-5-3-3-6) oil inlet are always positioned in settling tank (15-5-3-5-3-3-5) Solution surface;Oil water separator (15-5-3-5-3-3-7) positioned at lower part passes through overflow pipe (15-5-3-5-3-3-6) and precipitating Case (15-5-3-5-3-3-5) perforation, in its left part, closing, right part are equipped with precipitating property management (15-5-3-5-3-3-11), oil Separator (15-5-3-5-3-3-7) is horizontally inserted into settle and separate case (15-5-3-5-3-3-8) inside, wherein in settle and separate Case (15-5-3-5-3-3-8) inserting paragraph, realizes controllable rotating and its surface is equipped with a large amount of small through hole;In settle and separate case (15- 5-3-5-3-3-8) top is equipped with recycling oil pipe (15-5-3-5-3-3-9), lower part is equipped with separation water pipe (15-5-3-5-3-3- 10);
The stirring separator (15-5-3-5-3-3-3) includes: damping spring (15-5-3-5-3-3-3-1), stirring wheel one (15-5-3-5-3-3-3-2) is assisted quant (15-5-3-5-3-3-3-3), stirring wheel two (15-5-3-5-3-3-3-4);It is stirring It mixes and is equipped with stirring wheel (15-5-3-5-3-3-3-2), two (15-5-3-5-3- of stirring wheel inside separator (15-5-3-5-3-3-3) 3-3-4), the two horizontal layout, non-to be stirred in the same direction, wherein the axle center lower part stirring wheel two (15-5-3-5-3-3-3-4) is equipped with Oil input channel (15-5-3-5-3-3-13), the axle center top stirring wheel one (15-5-3-5-3-3-3-2) is equipped with edible vegetable oil outlet, lower part is set There is waste oil outlet;Damping spring (15-5-3-5-3-3-3- is equipped in separator (15-5-3-5-3-3-3) enclosure interior one end 1), the other end is equipped with auxiliary quant (15-5-3-5-3-3-3-3), and wherein the root damping spring (15-5-3-5-3-3-3-1) is solid It is scheduled on shell, upper part freely swings;Assist the quant lower part (15-5-3-5-3-3-3-3) be equipped with a cylinder, cylinder one end with The rotation connection of top blade, the other end are fixed on separator (15-5-3-5-3-3-3) enclosure interior;
A kind of to produce Pfansteihl device using Rhizopus oryzae, the production method of the device is:
Step 1: a kind of using in Rhizopus oryzae production Pfansteihl device;Plurality of raw materials boiling ripe material, mashing exist in proportion Dissolving tank (1) stirring is miscible, enters main fermentation case (13) by delivery pump (2) and carries out fermentation process, in the process, by connecing Kind sampling return pipe (12) accesses strain, adjusts main fermentation case (13) temperature, pH value, oxygen dissolving value, speed of agitator, meanwhile, allotment A variety of auxiliary materials are made mixed liquor and squeeze into main fermentation case (13) progress optimizing fermentation, the spillage solution of generation by pond (3) It is flowed back into dissolving tank (1) by inoculation sampling return pipe (12), is mixed as pretreated water with raw material;Fermentation liquid passes through distillation Tower front pump (4) enters destilling tower (5), and wherein gas phase is segregated into trickle bed reactor (6) by gas-liquid separator (10), other Solution is directly entered trickle bed reactor (6), carries out biochemical reaction under the effect of the catalyst, and products obtained therefrom is from high-position discharge pipe (9) it flows out, generates exhaust gas by sampling exhaust pipe (8) discharge, sediment is discharged from sediment discharge pipe (7) after processing;It reacted Cheng Zhong, operator carry out real-time monitoring to reaction process by sampling exhaust pipe (8);
Step 2: in destilling tower (5) course of work, heating steam enters from steam pipe (5-8) and each layer column plate dispensing branch Destilling tower (5) is internal, and mixed solution enters destilling tower (5) from inlet (5-7) and flows through each layer column plate before handling, and is in catalysis It unites under (5-4) effect, a part is flowed out from escape pipe (5-6) in a gaseous form, and another part is in liquid form from outlet tube (5- 5) sediment for flowing out, while generating is discharged from slag notch (5-1);Wherein slag tap control valve (5-2) control sediment discharge mistake Journey;
Step 3: in catalysis system (5-4) course of work, hot steam has bottom entrance, and the mixed liquor that top flows into splashes down respectively Onto multistage net-fault column plate (5-4-9), with hot steam carry out heat exchange, wherein hot mixing room (5-4-3) hot steam with mix Liquid is sufficiently mixed herein, promotes reaction;In heat build-up bucket (5-4-11), it utilizes loudspeaker moulding, a large amount of through-holes in surface, waist water conservancy diversion Plate, the solution that hot steam and net-fault column plate (5-4-9) are splashed down carry out sufficient heat exchange;Promotor spray ring (5-4-10), catalysis Reaction-filling object (5-4-8), net-fault column plate (5-4-9) further promote the chemical reaction of mixed liquor;Hot mixing room (5-4-3) benefit With its cylindrical hollow structure up and down, further hot steam is promoted to be sufficiently mixed with mixed liquor;Gas after vaporization is from upper Portion enters in next process, and sediment is discharged from control valve of slagging tap (5-2);
Step 4: in trickle bed reactor (6) work, use gas and liquid flowing mode, gas and liquid from trickle bed reactor (6) side enters in the same direction, and the catalyst of catalyst adding tube (6-2) outflow, which slowly enters to mix with gas, solution, to react, Stirring motor (6-4) drives mixing agitator (6-3) to mix slowly the lower promotion reaction of effect and carries out, and sediment is discharged from bottom, Product is discharged from top;When needing to clean inside trickle bed reactor (6) after material emptying, by automatic rinser (6-5) and clearly Washing and spraying device (6-1) synergy, shared cleaning;
Step 5: in mixing agitator (6-3) course of work, it is mixed that mixed solution passes through mixing inlet (6-3-1) entrance respectively It closes blender (6-3), goes metal device (6-3-2) to remove metal fillings by magnetism, antioxidant filler (6-3-5) injects antioxygen Agent prevents oxidation deterioration, and in the case where impeller (6-3-4) effect is mixed, solution passes through mixing liquid outlet (6-3-6) discharge;
Step 6: going in metal device (6-3-2) course of work in magnetism, and foreign current is conveyed to electricity in the case where electric cabinet (11) control Magnetic salient point (6-3-2-5), automatically controlled magnetic ring (6-3-2-6) are controlled, magnetic attraction is generated, container bottom and circumferential metal bits are carried out Absorption, meanwhile, electric cabinet (11) controlled level telescopic arm (6-3-2-2), vertical telescopic arm (6-3-2-4) stretching, extension or contraction, with And control large arm shaft (6-3-2-3), horizontal rotating shaft (6-3-2-8) rotation, it will entirely hold the metal fillings in its internal each corner It is adsorbed, the metal fillings of absorption is unloaded from side door (6-3-3);
Step 7: in automatic rinser (6-5) cleaning process, the spot of spot instrument (6-5-6) real-time detection tank body wall surface is sought Situation detects that wall surface passes through signal transceiver there are spot instrument (6-5-6) when spot, is sought when seeking spot instrument (6-5-6) (6-5-3) is transmitted signals to electric cabinet (11), and electric cabinet (11) controls adsorbent equipment (6-5-4) walking of creeping and arrives spot, It runs washer (6-5-5), spot is cleaned;
Step 8: in adsorbent equipment of creeping (6-5-4) work, horizontal swinging arm (6-5-4-1) promotes suction tray (6-5-4-7) left It moves right, extending arm (6-5-4-2) promotes its back-and-forth motion, and vertical moving arm (6-5-4-4) promotes it to move up and down;Vacuum pump Pumping promotes suction tray (6-5-4-7) to be tightly adsorbed on wall surface;Electric cabinet (11) open stretching, extension hydraulic press (6-5-4-3) and Vertical hydraulic press (6-5-4-5) passes through stretching, extension hydraulic press (6-5-4-3) and the stretching motion control of vertical hydraulic press (6-5-4-5) System is creeped, and adsorbent equipment (6-5-4) is continuous to be moved;
Step 9: in washer (6-5-5) work, electric cabinet (11) opens cleaning driving machine (6-5-5-1), drives driving cog It takes turns (6-5-5-3) and carries out gear power transmission, transmission gear (6-5-5-3) drives rotating disk (6-5-5-4) and the brush head (6- that keeps a public place clean It 5-5-5) is rotated, realizes and wall surface is cleared up;After cleaning driving machine (6-5-5-1) by output main shaft band Dynamic fan (6-5-5-2) carries out high speed rotary motion, dries up clean surface moisture;
Step 10: in bracket (14) operation process, powering on and start electric cabinet (11), and electric cabinet (11) controls bracket and drives Motivation (14-1) is operated, and drives support gear (14-3) rotation by transmission case (14-2), and then promote support gear Engaged transmission occurs for (14-3) and bracket track (14-4), since weight body (14-6) and bracket shell (14-5) is fixed, bracket shell (14-5) is separated with bracket (14) pedestal, bracket track (14-4) is fixed with bracket (14) pedestal, therefore in transmission process, only There are carriage drive machine (14-1), support gear (14-3), transmission case (14-2), bracket shell (14-5), weight body (14-6), support Body (14-7) moves up and down, and then realizes that bracket shell (14-5) drives bracket (14) top plate to move up and down;
Step 11: in regulating wheel (15) course of work, movable pulley shaft (15-3) is operated under the driving of external motor, And movable pulley (15-4) is driven to roll on the wheel track top (15-6), and then guarantee that destilling tower (5) carry out position adjustment;It is same with this When, grease-box (15-2) is that movable pulley (15-4) injects lubricating oil by atomizer (15-5);
Step 12: in grease-box (15-2) course of work, lubricating oil is injected into arrive distributor box (15- for profit oil pump (15-2-1) 2-2);When needing high viscosity lubricants, start distributor box (15-2-2) small agitator arm, is controlled by tubule and valve, into Enter Rose Box (15-2-3);When needing low viscosity lubricant, start distributor box (15-2-2) big agitator arm, by extra heavy pipe and Valve control, into Rose Box (15-2-3), under filter screen inside it, mud chamber, the effect of net impurity remover, edible vegetable oil into Enter oil fuel tube (15-2-4), while radiator (15-2-5) cools down to edible vegetable oil, passes through abutment sleeve (15-2-7), go out from oil fuel tube Mouth (15-2-8) flows into next procedure;
Step 13: in atomizer (15-5) course of work, lubricating oil enters in main by-pass tube (15-5-1) from oil guide pipe;With Afterwards, the lubricating oil in main by-pass tube (15-5-1) is diverted into inclination angle injector body (15-5-3) from oil distributing pipe, and from inclination angle oil spout The nozzle opening on the surface body (15-5-3) flows out, and is object rotary shaft oil injecting lubricating;
Step 14: in inclination angle injector body (15-5-3) course of work, upper and lower 2 groups of housing actuators (15-5-3-5) drive oil spout Shell (15-5-3-3) rotation, due to be internally provided with it is multiple staggeredly spoiler (15-5-3-4), when lubricating oil is from oil inlet When (15-5-3-1) enters, staggeredly spoiler (15-5-3-4) promotes the lubricating oil in oil spout shell (15-5-3-3) to rotate, and It is tangentially sprayed from tangential oil outlet (15-5-3-2), is conducive to uniformly spray;
Step 15: in housing actuator (15-5-3-5) course of work, external motor is driven by axis two (15-5-3-5-7) Circumference driving wheel (15-5-3-5-6) rotation, and then pass through circumference rack gear (15-5-3-5-3) driving oil spout shell (15-5-3-3) Rotation;
Step 16: in circumference rack gear (15-5-3-5-3) course of work, oiling machine (15-5-3-5-3-3) is gear engagement note Oil lubrication;Meanwhile the vibration generated in gear walking process is by damping spring (15-5-3-5-3-5), clump weight, blower (15-5-3-5-3-6) is absorbed, since blower (15-5-3-5-3-6) only connects with damping spring (15-5-3-5-3-5) screw thread It connects, and both ends penetrate through, the vibration generated in gear walking process promotes damping spring (15-5-3-5-3-5) to drive blower (15-5-3-5-3-6) is swung left and right, for the blowing cooling of its periphery sector teeth (15-5-3-5-3-2);
Step 17: in oiling machine (15-5-3-5-3-3) course of work, external lubrication oil passes through oil input channel (15-5-3-5-3- 3-13) enter stirring separator (15-5-3-5-3-3-3) stirring, stirring separator (15-5-3-5-3-3-3) after separation will be excellent Matter oil is conveyed to screw thread flowline (15-5-3-5-3-3-14) ejection by oil storage bag (15-5-3-5-3-3-2), to move work Part provides lubrication;The waste product oil isolated enters filtering rotary table case (15-5-3-5- from stirring separator (15-5-3-5-3-3-3) It 3-3-4) is filtered, enters back into settling tank (15-5-3-5-3-3-5), wherein metal fillings sediment is from metal sediment pipe (15- 5-3-5-3-3-12) it is discharged;Overflow pipe (15-5-3-5-3-3-6) collects settling tank (15-5-3-5-3-3-5) inner surface solution, And it is delivered to oil water separator (15-5-3-5-3-3-7), enter settle and separate case (15-5- by a large amount of small through hole of its pipe surface 3-5-3-3-8), the rotation of oil water separator (15-5-3-5-3-3-7) booting at this time promotes water-oil separating, divides after static in standing From forming water-oil separating layer in case (15-5-3-5-3-3-8), oil recovery from recycling oil pipe (15-5-3-5-3-3-9) outlet, point From water from separation water pipe (15-5-3-5-3-3-10) outlet, sediment from precipitating property management (15-5-3-5-3-3-11) outlet;
Step 18: in stirring separator (15-5-3-5-3-3-3) course of work, external lubrication oil passes through oil input channel (15-5- 3-5-3-3-13) enter stirring separator (15-5-3-5-3-3-3), in stirring wheel one (15-5-3-5-3-3-3-2), stirring wheel Along stirring separator (15-5-3-5-3-3-3) enclosure interior outer ring stream under the non-stirring in the same direction of two (15-5-3-5-3-3-3-4) It is dynamic, it is excellent due to the damping action for being damped spring (15-5-3-5-3-3-3-1), assisting quant (15-5-3-5-3-3-3-3) Matter oil is exported from top edible vegetable oil to flow out, and waste oil is exported from lower part waste oil to flow out;
Strain selects Rhizopus arrhizus Rhizopus arrizhus, Rhizopus oryzae Rhizopus oryzae, Rhizopus niveus, rhizopus chinensis One or more of Mixed Microbes are inoculated in first class seed pot culture, obtain first order seed;Obtained single colonie is seeded to liquid Shaken cultivation in body culture medium, obtains secondary seed;Secondary seed is inoculated into shaken cultivation in fermentation liquid, obtains three-level kind Activation fermenting microbe is made in son;Plurality of raw materials is cornstarch, potato starch, corn mash, tapioca, wheat shallow lake Powder, sweet potato starch, two kinds of sorghum starch or bean starch or these starch mixture;Cellulase hydrolysis is added simultaneously Liquid, diammonium hydrogen phosphate, corn pulp, potassium chloride, bitter salt, dipotassium hydrogen phosphate, green vitriol, water, are mixed into Slurry;Auxiliary material be fish meal, peptone, yeast extract, sodium chloride, bean cake powder, diammonium hydrogen phosphate, ferrous sulfate, sodium citrate, Potassium dihydrogen phosphate, zinc sulfate, magnesium sulfate, calcium chloride.
CN201910707237.6A 2019-08-01 2019-08-01 It is a kind of to produce Pfansteihl device and method using Rhizopus oryzae Withdrawn CN110387324A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112973161A (en) * 2019-12-12 2021-06-18 江苏民生特种设备集团有限公司 Internal packing device of distillation tower
CN114486372A (en) * 2021-12-30 2022-05-13 江苏集萃未来城市应用技术研究所有限公司 Online sampling device for mucilage production and use method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112973161A (en) * 2019-12-12 2021-06-18 江苏民生特种设备集团有限公司 Internal packing device of distillation tower
CN114486372A (en) * 2021-12-30 2022-05-13 江苏集萃未来城市应用技术研究所有限公司 Online sampling device for mucilage production and use method

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Application publication date: 20191029