CN114486372A - Online sampling device for mucilage production and use method - Google Patents
Online sampling device for mucilage production and use method Download PDFInfo
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- CN114486372A CN114486372A CN202111657675.XA CN202111657675A CN114486372A CN 114486372 A CN114486372 A CN 114486372A CN 202111657675 A CN202111657675 A CN 202111657675A CN 114486372 A CN114486372 A CN 114486372A
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- sampling
- mucilage
- pipeline
- cavity
- pipe
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- 238000005070 sampling Methods 0.000 title claims abstract description 116
- 239000000853 adhesive Substances 0.000 title claims abstract description 49
- 229920000715 Mucilage Polymers 0.000 title claims abstract description 47
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 24
- 238000000034 method Methods 0.000 title claims abstract description 14
- 230000002572 peristaltic effect Effects 0.000 claims abstract description 24
- 238000007599 discharging Methods 0.000 claims abstract description 22
- 238000005192 partition Methods 0.000 claims abstract description 8
- 239000000084 colloidal system Substances 0.000 claims abstract description 7
- 239000002893 slag Substances 0.000 claims description 23
- 239000004568 cement Substances 0.000 claims description 7
- 239000011148 porous material Substances 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 5
- 238000007789 sealing Methods 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims description 2
- 239000002184 metal Substances 0.000 claims description 2
- 230000001070 adhesive effect Effects 0.000 description 2
- 238000001723 curing Methods 0.000 description 2
- 238000003848 UV Light-Curing Methods 0.000 description 1
- 238000012824 chemical production Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 238000002407 reforming Methods 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000002834 transmittance Methods 0.000 description 1
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Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
- G01N1/14—Suction devices, e.g. pumps; Ejector devices
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- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
An online sampling device and a using method for mucilage production are disclosed, wherein 1) a production line is reformed: a sampling hole is formed in the side wall of a main discharging pipeline of a mucilage production line, a feeding hole of a valve is directly connected to the sampling hole, a discharging hole of the valve is connected with a peristaltic pump, and a discharging hole of the peristaltic pump is connected with a sampling pipeline; 2) at the time of sampling: opening a valve and starting a peristaltic pump, discharging part of the solidified colloid in the sampling pipe out of the pipe by using the pressure of a main discharging pipe and the pressure of the peristaltic pump, and collecting; then, collecting and sampling normal mucilage; the sampling device is a sampling tank, the hollow interior of the sampling tank is divided into two independent cavities by a partition plate, the upper part of the partition plate is provided with a communication hole, and the two cavities are communicated through the communication hole; 3) and after sampling is finished, closing the peristaltic pump and the valve, and at the moment, leaving the mucilage in the sampling pipeline to naturally solidify and plug the sampling pipeline. The device and the method are used for online sampling, so that the influence on the quality of the produced product is avoided.
Description
Technical Field
The invention belongs to the technical field of chemical production, and particularly relates to an online sampling device for cement paste production and a using method.
Background
The mucilage is a practical common material for bonding, sealing and the like. In the case of encapsulating circuits or integrated circuits, the curing of the paste used is either by UV curing or moisture in air. In the production process of the mucilage, sampling detection is carried out by installing a branched sampling tube on a production pipeline and installing a valve on the sampling tube. During sampling, the mucilage left in the sampling pipe is solidified and the sampling pipe is blocked if the position of the valve is close to the main pipeline; if the valve is positioned close to the sampling pipe opening, part of the previous batch of samples remains in the sampling pipe, and the accuracy of the samples is influenced.
Disclosure of Invention
In order to solve the technical problems, the invention provides an online sampling device for mucilage production and a using method, 1) a production line is modified: a sampling hole is formed in the side wall of a main discharging pipeline of the mucilage production line, and a flange plate is welded on the side wall and is aligned with the sampling hole; a feed port of a valve is directly connected to the flange plate, a discharge port of the valve is connected with a peristaltic pump, and a discharge port of the peristaltic pump is connected with a sampling pipeline; the sampling pipeline is hard;
2) at the time of sampling: opening a valve and starting a peristaltic pump, discharging part of the solidified colloid in the sampling pipe out of the pipe by using the pressure of a main discharging pipe and the pressure of the peristaltic pump, and collecting; then, collecting and sampling normal mucilage;
the sampling device is a sampling tank, and the sampling tank structurally comprises a closed hard shell;
the hollow part in the sampling tank is divided into two independent cavities by a partition plate, one cavity is a slag receiving cavity, and the other cavity is a sample reserving cavity; the top of the slag receiving cavity is provided with a feed inlet and an exhaust outlet, and the bottom of the slag receiving cavity is provided with a slag cleaning port capable of being opened and closed; the bottom of the sample reserving cavity is provided with a switchable discharge hole; the upper part of the clapboard is provided with a communicating hole, and the slag receiving cavity is communicated with the sample reserving cavity through the communicating hole;
during sampling, a feed port of the sampling tank is connected with the sampling pipe, and an exhaust port is opened; part of the solidified colloid enters the slag receiving cavity from the feed inlet; after the slag receiving cavity is filled with the normal mucilage and reaches the height of the intercommunicating pore, the mucilage which subsequently enters the feed inlet flows into the sample reserving cavity from the intercommunicating pore; when extracting the mucilage sample, opening a discharge hole and an exhaust port of the sample reserving cavity, and discharging the mucilage from the sample reserving cavity;
3) and after sampling is finished, closing the peristaltic pump and the valve, and at the moment, reserving the mucilage in the sampling pipeline, naturally curing the mucilage and plugging the sampling pipeline.
The principle of the scheme is that the valve is close to the main discharging pipe by opening the hole of the main discharging pipe close to the main discharging pipe. Because the flange inner hole is bigger, the degree of depth is shallower, can not produce the stock.
The sampling pipeline is long, the previous mucilage sample is remained in the sampling pipeline, and the mucilage sample is solidified at the position of the pipe orifice. The solidified part plugs the pipeline, so that air is prevented from entering the pipeline and then entering the main pipeline through a small gap of the valve.
Because of the presence of the solidified portion, the solidified portion is extruded by means of a peristaltic pump when the pressure of the main pipe is not sufficient to press out the solidified portion at the time of sampling.
In the sampling tank, through its specific structure, make the solidification part that flows out earlier and the mucilage remaining part when taking a sample the time before get into and connect the sediment chamber to by the sample pressure of this time sampling at the bottom of the chamber, newly sample flows into from the intercommunicating pore and reserves the appearance chamber. Because the age of the mucilage is higher, the mucilage in the sampling tank is more stable, and the mucilage in the two cavities can not be mixed unless the sampling tank is turned on one side.
The mucilage left in the sampling pipeline after sampling is naturally cured, and the plugging effect is achieved.
The device and the method are used for online sampling, so that the influence on the quality of the produced product is avoided. Meanwhile, the accuracy of the sampled sample is high.
Drawings
FIG. 1 is a schematic diagram of the present solution;
FIG. 2 is a schematic view of the structure of a sampling hole portion;
FIG. 3 is a schematic view of the construction of a sampling tank;
in the figure: the device comprises a main discharge pipeline 1, a sampling hole 2, a flange 3, a valve 4, a peristaltic pump 5, a sampling pipeline 6, a sampling tank 7, an air pump 8, a slag receiving cavity 9, a sample reserving cavity 10, a feed inlet 11, an exhaust port 12, a slag removing port 14, a discharge port 15, a partition plate 16, a communicating hole 17 and an extension pipe 18.
Detailed Description
The invention is further described with reference to the following detailed description and accompanying drawings.
Referring to fig. 1, in the online sampling device for cement production and the use method of the present example,
1) the production line is reformed: a sampling hole 2 is formed in the side wall of a main discharging pipeline 1 of a mucilage production line, and a flange plate 3 is welded on the side wall and aligned with the sampling hole; a feed port of a valve 4 is directly connected to the flange plate, a discharge port of the valve 4 is connected with a peristaltic pump 5, and a discharge port of the peristaltic pump is connected with a sampling pipeline 6; the sampling pipeline is hard; as shown in fig. 2.
2) At the time of sampling: opening a valve and starting a peristaltic pump, discharging part of the solidified colloid in the sampling pipe out of the pipe by using the pressure of a main discharging pipe and the pressure of the peristaltic pump, and collecting; then, a sample of the normal cement was taken.
As shown in fig. 3, the sampling device is a sampling tank 7, and the structure of the sampling tank comprises a closed hard shell;
the hollow inside of the sampling tank is divided into two independent cavities by a partition plate 16, one cavity is a slag receiving cavity 9, and the other cavity is a sample reserving cavity 10; the top of the slag receiving cavity is provided with a feed inlet 11 and an exhaust port 12, and the bottom of the slag receiving cavity is provided with a slag removing port 14 which can be opened and closed; the bottom of the sample reserving cavity is provided with a switchable discharge hole 15; the upper part of the clapboard is provided with a communicating hole 17, and the slag receiving cavity is communicated with the sample reserving cavity through the communicating hole;
during sampling, connecting a feed inlet of a sampling tank with a sampling pipeline, and opening an exhaust port; part of the solidified colloid enters the slag receiving cavity from the feeding hole; after the slag receiving cavity is filled with the normal mucilage and reaches the height of the intercommunicating pore, the mucilage which subsequently enters the feed inlet flows into the sample reserving cavity from the intercommunicating pore; when extracting the mucilage sample, opening a discharge hole and an exhaust port of the sample reserving cavity, and discharging the mucilage from the sample reserving cavity;
3) and after sampling is finished, closing the peristaltic pump and the valve, and at the moment, leaving the mucilage in the sampling pipeline and plugging the sampling pipeline by the mucilage after the mucilage is naturally cured.
In the present embodiment;
the hollow shape of the interior of the sampling tank is a cuboid shape, and the height of the cuboid is far greater than the width and the length of the cuboid; the height direction of the partition board is the same as that of the cuboid.
The feed inlet 11 and the exhaust port 12 of the sampling tank 7 are both connected with upward extension pipes 18, and the extension pipes 18 are detachably connected with sealing covers;
when sampling, the inside cavity of sample jar is filled completely to the adhesive cement to there is the adhesive cement in the extension pipe, has avoided the influence of outside air to the sample.
An air pump 8 is connected to an exhaust port of the sampling tank.
The sampling pipeline is made of TPX materials, and two ends of the sampling pipeline are respectively connected with a flange plate used for connecting a discharge hole of the peristaltic pump and a metal external thread used for connecting a feed hole of the sampling tank; the open end of the extension pipe is connected with an internal thread nut interface used for connecting a sampling pipeline.
When reforming transform the production line, open a plurality of thief holes on the main discharging pipeline lateral wall of mucilage glue production line, the thief hole is arranged along the length direction of main discharging pipeline.
In this example, the sampling tube is made of stainless steel, except that the sampling tube is made of TPX. The TPX material has high light transmittance, and the hardness of the TPX material can be selected according to the grade.
Claims (6)
1. An online sampling device for cement production and a using method are characterized in that:
1) the production line is reformed: a sampling hole is formed in the side wall of a main discharging pipeline of the mucilage production line, and a flange plate is welded on the side wall and is aligned with the sampling hole; a feed port of a valve is directly connected to the flange plate, a discharge port of the valve is connected with a peristaltic pump, and a discharge port of the peristaltic pump is connected with a sampling pipeline; the sampling pipeline is hard;
2) at the time of sampling: opening a valve and starting a peristaltic pump, discharging part of the solidified colloid in the sampling pipe out of the pipe by using the pressure of a main discharging pipe and the pressure of the peristaltic pump, and collecting; then, collecting and sampling normal mucilage;
the sampling device is a sampling tank, and the sampling tank structurally comprises a closed hard shell;
the hollow part in the sampling tank is divided into two independent cavities by a partition plate, one cavity is a slag receiving cavity, and the other cavity is a sample reserving cavity; the top of the slag receiving cavity is provided with a feed inlet and an exhaust outlet, and the bottom of the slag receiving cavity is provided with a slag cleaning port capable of being opened and closed; the bottom of the sample reserving cavity is provided with a switchable discharge hole; the upper part of the clapboard is provided with a communicating hole, and the slag receiving cavity is communicated with the sample reserving cavity through the communicating hole;
during sampling, connecting a feed inlet of a sampling tank with a sampling pipeline, and opening an exhaust port; part of the solidified colloid enters the slag receiving cavity from the feeding hole; after the slag receiving cavity is filled with the normal mucilage and reaches the height of the intercommunicating pore, the mucilage which subsequently enters the feed inlet flows into the sample reserving cavity from the intercommunicating pore; when extracting the mucilage sample, opening a discharge hole and an exhaust port of the sample reserving cavity, and discharging the mucilage from the sample reserving cavity;
3) and after sampling is finished, closing the peristaltic pump and the valve, and at the moment, leaving the mucilage in the sampling pipeline to naturally solidify and plug the sampling pipeline.
2. The online sampling device and the use method for the production of the mucilage as recited in claim 1, wherein the hollow shape inside the sampling tank is a cuboid shape, and the height of the cuboid is far greater than the width and the length of the cuboid; the height direction of the partition board is the same as that of the cuboid.
3. The online sampling device and the use method for the production of the mucilage as recited in claim 1 are characterized in that a feed inlet and an exhaust port of the sampling tank are both connected with upward extension pipes, and the extension pipes are detachably connected with sealing covers;
when sampling, the inside cavity of sample jar is filled completely to the mucilage to there is the mucilage in the extension pipe.
4. The on-line sampling device and the use method for the production of the mucilage as recited in claim 1 are characterized in that an air suction pump is connected to an air outlet of a sampling tank.
5. The online sampling device and the use method for mucilage production as recited in claim 3, wherein the sampling pipe is made of TPX material, and both ends of the sampling pipe are respectively connected with a flange plate for connecting a discharge port of a peristaltic pump and a metal external thread for connecting a feed port of a sampling tank; the open end of the extension pipe is connected with an internal thread nut interface used for connecting a sampling pipeline.
6. The apparatus and method of claim 1, wherein the sidewall of the main discharge pipe of the cement production line is provided with a plurality of sampling holes arranged along the length of the main discharge pipe.
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CN202111657675.XA CN114486372A (en) | 2021-12-30 | 2021-12-30 | Online sampling device for mucilage production and use method |
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CN202111657675.XA CN114486372A (en) | 2021-12-30 | 2021-12-30 | Online sampling device for mucilage production and use method |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN117023155A (en) * | 2023-10-08 | 2023-11-10 | 常州常衡德宇粉体集成系统有限公司 | Powder positive pressure conveying system and conveying method |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN117023155B (en) * | 2023-10-08 | 2023-12-12 | 常州常衡德宇粉体集成系统有限公司 | Powder positive pressure conveying system and conveying method |
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