CN110368351A - A kind of pearl essence liquid and the preparation method and application thereof - Google Patents
A kind of pearl essence liquid and the preparation method and application thereof Download PDFInfo
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- CN110368351A CN110368351A CN201910664591.5A CN201910664591A CN110368351A CN 110368351 A CN110368351 A CN 110368351A CN 201910664591 A CN201910664591 A CN 201910664591A CN 110368351 A CN110368351 A CN 110368351A
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- pearl
- preparation
- essence liquid
- mixed liquor
- pearl essence
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/413—Nanosized, i.e. having sizes below 100 nm
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Zoology (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to cosmetic technical field, a kind of pearl essence liquid and the preparation method and application thereof is specifically disclosed.The preparation method of the pearl essence liquid includes: to obtain mixed liquor after being sufficiently mixed pearl powder and pure water, the mixed liquor is ultrasonically treated, active oxygen species are introduced into the mixed liquor after ultrasonic treatment under fast stirring later to be reacted, and are stood after reaction and are collected upper suspension.The present invention organically combines the efficient depolymerisation of ultrasonic extracting process and active oxygen species, after strong cavitation effect and stirring action that pearl powder suspension is generated through ultrasound first, it is sufficiently merged with pure water, on this basis, using the efficient depolymerisation of active oxygen species, pearl is promoted effectively to decompose, and discharges itself benefit materials Yu Shuizhong, on the basis of utmostly retaining pearl beneficiating ingredient, it is translated into the small-molecule substance being easily absorbed by the human body.
Description
Technical field
The present invention relates to cosmetic technical fields, specifically, being related to a kind of pearl essence liquid and preparation method thereof and answering
With.
Background technique
Pearl is a kind of natural rare traditional Chinese medicine, contains 18 kinds of amino acid, 30 various trace elements, taurine and rich
Rich vitamin, peptides etc..The Pharmacopoeia of the People's Republic of China and " dictionary of medicinal plant " indicate: pearl have calm the nerves arresting convulsion,
Shade removing, solution taking poison and growing muscle due and other effects.In addition, modern research shows that pearl improve the immunity of the human body, delay senescence, nti-freckle beauty
It is white etc. that all there is unique effect.
Facial mask is one kind of skin care item, by being covered on face, improves facial temperature, expands facial pores, promote face
While sweat gland secretion and metabolism, contained nutrient in facial mask is set to penetrate into skin cuticula, depth nourishes skin.
In existing pearl facial mask, pearl is added directly into face pack prescription in the form of a powder mostly, however, due to treasure
Pearl is insoluble in water, and a large amount of beneficiating ingredients contained therein are difficult to effectively be absorbed by human body, causes facial mask using effect poor.Part is specially
Hydrolyzate is made in pearl by benefit, is added in facial mask by way of hydrolyzate, although improving facial mask to a certain extent
Using effect, but hydrolysis liquid preparing process used by it is mostly acidolysis or enzymatic isolation method, is inevitably drawn during the preparation process
The additive unfavorable to human body is entered, while the loss of pearl beneficiating ingredient can be caused to a certain extent.
Summary of the invention
In order to solve the problems in the existing technology, the object of the present invention is to provide a kind of pearl essence liquid and its preparations
Method and application.
In order to achieve the object of the present invention, technical scheme is as follows:
In a first aspect, the present invention provides a kind of preparation method of pearl essence liquid, the preparation method includes: by pearl powder
Mixed liquor is obtained after being sufficiently mixed with pure water, the mixed liquor is ultrasonically treated, later under fast stirring to ultrasound
Active oxygen species are introduced in treated mixed liquor to be reacted, and are stood after reaction and are collected upper suspension to get pearl cyanines
Magnificent liquid.
Further, the preparation method includes: to obtain mixed liquor after being sufficiently mixed pearl powder and pure water, 20~
30~60min is ultrasonically treated to the mixed liquor under the ultrasonic power of 80W, later under fast stirring to mixed after ultrasonic treatment
Close liquid in introduce active oxygen species react 10~60min, after the reaction was completed stand 20~60min, collect upper suspension to get
Pearl essence liquid.
Further, in the preparation method, under rapid stirring through ozone generator into mixed liquor
Introduce 0.3~1.0mg/L of active oxygen species.
Preferably, the pearl powder is pearl powder of the partial size less than 20 microns (crossing 600 meshes), further preferred partial size
Less than the pearl powder of 15 microns (crossing 800 meshes).
Preferably, the mass ratio of the pearl powder and pure water is 1:100~1:50 in the mixed liquor.
Second aspect, the present invention provide the pearl essence liquid being prepared by aforementioned preparation process.
The third aspect, the present invention provide application of the pearl essence liquid in terms of preparing skin care item or cosmetics.
Fourth aspect, the present invention provide the skin care item or cosmetics for containing the pearl essence liquid.
The skin care item or cosmetics include but is not limited to toner, essence liquid, lotion, face cream, facial mask, eye mask, sun-proof
Frost etc..
In a specific embodiment of the invention, with facial mask exemplary illustration as one preferred.The facial mask is by facial mask
Paper and facial mask base fluid composition, the facial mask base fluid contain pearl essence liquid of the present invention.
More specifically, the facial mask base fluid is composed of the following raw materials in parts by mass: 3~5 parts of butanediol, Sodium Hyaluronate
3~8 parts, 0.5~3 part of dimethyl silicone polymer hydrocarbon, 0.5~1 part of EDETATE SODIUM, 5~8 parts of dipotassium glycyrrhizinate, dehydroactic acid 0.5
~5 parts, it is 500~1000 parts of pearl essence liquid described.
Preferably, the facial mask base fluid is composed of the following raw materials in parts by mass: 3 parts of butanediol, 5 parts of Sodium Hyaluronate,
1 part of dimethyl silicone polymer hydrocarbon, 1 part of EDETATE SODIUM, 5 parts of dipotassium glycyrrhizinate, 3 parts of dehydroactic acid, 600 parts of pearl essence liquid.
Mentioned component is mixed to get facial mask base fluid, after inspection, disinfection, sterilizing, 15~20g is taken to be filled into equipped with silk
In the aluminum composite film packaging bag of mask sheet, sealing obtains facial mask finished product.
The beneficiating ingredients such as polypeptide and amino acid are rich in the pearl essence liquid prepared using preparation method of the present invention,
In, polypeptide moiety can inhibit tyrosinase activity, and reduce melanin production from front end, and have anti-aging, reparation, antioxygen
Change, the characteristic of antioedematous；Glycine can adjust skin state, be full of and moisten skin makeup；Serine stimulates selenium-rich water mildly not, can
Promote moistening effect；Threonine can make skin jade-like stone moisten moisturizing, soft interior skin；Glutamic acid can compact skin, enable skin consolidation full
It is full；Alanine can act on skin surface, improve moisturizing water lock ability；Valine and other two kinds of amino acid (isoleucine and
Leucine) body normal growth can be promoted together by working, and repair tissue is highly resistant to skin aging.
And in preparation method of the present invention, a large amount of nanometer level pearl powder particles are contained in collected upper suspension,
When utilizing it as facial mask base fluid ingredient, skin on the one hand can be promoted further to absorb the nutritional ingredient in pearl, it is another
Aspect, nano-pearl powder particles have extremely strong adsorption capacity, can effectively adsorb the grease and blackhead in pore, realize skin
Deep clean.
The present invention relates to raw material or reagent be ordinary commercial products, the operation being related to is unless otherwise specified
This field routine operation.
On the basis of common knowledge of the art, above-mentioned each optimum condition, can be combined with each other, obtain specific embodiment party
Formula.
The beneficial effects of the present invention are:
The present invention organically combines the efficient depolymerisation of ultrasonic extracting process and active oxygen species, pearl powder suspension
After the strong cavitation effect and stirring action that are generated first through ultrasound, is sufficiently merged with pure water, on this basis, utilize active oxygen
The efficient depolymerisation of molecule, promotes pearl effectively to decompose, and discharges itself benefit materials Yu Shuizhong.Active oxygen species with it is organic
The reaction of object has selectivity, it can destroy the structure of the macromolecular substances such as protein, be translated into amino acid and polypeptide
Equal small-molecule substances.
Therefore, this technique can be translated into human body and be easy on the basis of utmostly retaining pearl beneficiating ingredient
The small-molecule substance of absorption.
Specific embodiment
The preferred embodiment of the present invention is described in detail below in conjunction with embodiment.It will be appreciated that following real
Providing merely to play the purpose of explanation for example is applied, is not used to limit the scope of the present invention.The skill of this field
Art personnel without departing from the spirit and purpose of the present invention, can carry out various modifications and replace to the present invention.
Experimental method used in following embodiments is conventional method unless otherwise specified.
The materials, reagents and the like used in the following examples is commercially available unless otherwise specified.
A kind of pearl essence liquid of embodiment 1 and preparation method thereof
1, the preparation of pearl essence liquid
The pearl powder for weighing 800 mesh is sufficiently mixed according to the weight ratio and pure water of 1:50；After mixing, in ultrasound
Under conditions of wave power is 60W, mixed liquor is ultrasonically treated, ultrasonic time 45min；After the completion of ultrasound, quickly stirring
Under the conditions of, active oxygen species 0.3mg/L is introduced into above-mentioned mixed liquor by ozone generator, reacts 20min；Reaction is completed
Afterwards, mixed liquor is stood into 30min, collects upper suspension, as pearl essence liquid.
2, the beneficiating ingredient detection of pearl essence liquid
(1) detection method
Take water after filter sample 10ml；Processing is performed the derivatization to water sample using phenyl isothiocyanate (PITC) derivatization method.Specifically
Operation: precision draws self-control amino standard acid solution (water sample) 400 μ L, by the triethylamine acetonitrile solution of prepared 1mol/L in advance
And 0.1mol/L PITC- acetonitrile solution is added separately in analysis sample, additional amount is respectively 300 μ L, 100 μ L.Simultaneously will
Uniformly mixed sample is placed on shading at room temperature and stands 1h, and 800 μ L of n-hexane, oscillation is added, and 10000r/min is centrifuged 5min, takes
Lower layer's solution (n-hexane extraction 2 times), sample is measured using RP-HPLC.
(2) testing result
Comparative example 1
This comparative example the difference from embodiment 1 is that: in the preparation of pearl essence liquid, ultrasound after the completion of, do not introduce work
Property oxygen molecule, only by after the completion of ultrasound mixed liquor stand 30min, collect upper suspension, that is, be used as pearl essence liquid.
Using detection method same as Example 1, to the pearl essence liquid that this comparative example is prepared carry out beneficial at
The detection divided, testing result are as follows:
Comparative example 2
This comparative example the difference from embodiment 1 is that: in the preparation of pearl essence liquid, before ultrasonic reaction, will mix
Liquid is heated to 98 DEG C, keeps the temperature 2h.Subsequent processes obtain pearl essence liquid with embodiment 1.
Using detection method same as Example 1, to the pearl essence liquid that this comparative example is prepared carry out beneficial at
The detection divided, testing result are as follows:
A kind of mask product containing pearl essence liquid of embodiment 2
1, facial mask base fluid formula
3 parts of butanediol, 5 parts of Sodium Hyaluronate, 1 part of dimethyl silicone polymer hydrocarbon, 1 part of EDETATE SODIUM, dipotassium glycyrrhizinate 5
Part, 3 parts of dehydroactic acid, 600 parts of pearl essence liquid.
2, the preparation method of facial mask
By facial mask base fluid after inspection, disinfection, sterilizing, 15~20g is taken to be filled into the aluminum equipped with silk mask patch compound
In film package bag, sealing obtains the mask product containing pearl essence liquid of the present invention.
Although above the present invention is described in detail with a general description of the specific embodiments,
On the basis of the present invention, it can be made some modifications or improvements, this will be apparent to those skilled in the art.Cause
This, these modifications or improvements, fall within the scope of the claimed invention without departing from theon the basis of the spirit of the present invention.
Claims (10)
1. a kind of preparation method of pearl essence liquid, which is characterized in that the preparation method includes: to fill pearl powder and pure water
Mixed liquor is obtained after dividing mixing, the mixed liquor is ultrasonically treated, later under fast stirring to mixed after ultrasonic treatment
It closes introducing active oxygen species in liquid to be reacted, be stood after reaction, collect top suspension to get pearl essence liquid.
2. preparation method according to claim 1, which is characterized in that the preparation method include: by pearl powder with it is pure
Water obtains mixed liquor after being sufficiently mixed, and is ultrasonically treated 30~60min to the mixed liquor under the ultrasonic power of 20~80W, it
Afterwards under fast stirring into the mixed liquor after ultrasonic treatment introduce active oxygen species reacted, after the reaction was completed stand 20~
60min collects top suspension to get pearl essence liquid.
3. preparation method according to claim 1 or 2, which is characterized in that under rapid mixing conditions, occurred by ozone
Device introduces 0.3~1.0mg/L of active oxygen species, reacts 10~60min.
4. preparation method according to claim 3, which is characterized in that the pearl powder is pearl of the partial size less than 20 microns
Powder, pearl powder of the preferable particle size less than 15 microns.
5. the preparation method according to claim 4, which is characterized in that the mass ratio of the pearl powder and pure water is 1:
100~1:50.
6. a kind of pearl essence liquid, which is characterized in that be prepared by any one of Claims 1 to 5 preparation method.
7. application of the pearl essence liquid as claimed in claim 6 in terms of preparing skin care item or cosmetics.
8. skin care item or cosmetics containing pearl essence liquid described in claim 6.
9. a kind of facial mask is made of face paper and facial mask base fluid, which is characterized in that the facial mask base fluid contains claim 6 institute
State pearl essence liquid.
10. facial mask according to claim 9, which is characterized in that the facial mask base fluid is composed of the following raw materials in parts by mass:
3~5 parts of butanediol, 3~8 parts of Sodium Hyaluronate, 0.5~3 part of dimethyl silicone polymer hydrocarbon, 0.5~1 part of EDETATE SODIUM, Radix Glycyrrhizae
It is 5~8 parts of sour dipotassium, 0.5~5 part of dehydroactic acid, 500~1000 parts of pearl essence liquid described.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910664591.5A CN110368351A (en) | 2019-07-23 | 2019-07-23 | A kind of pearl essence liquid and the preparation method and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910664591.5A CN110368351A (en) | 2019-07-23 | 2019-07-23 | A kind of pearl essence liquid and the preparation method and application thereof |
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| CN110368351A true CN110368351A (en) | 2019-10-25 |
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| CN201910664591.5A Pending CN110368351A (en) | 2019-07-23 | 2019-07-23 | A kind of pearl essence liquid and the preparation method and application thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115429849A (en) * | 2022-08-23 | 2022-12-06 | 江西大自然制药有限公司 | Preparation method of body-strengthening and life-prolonging pills |
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|---|---|---|---|---|
| JPH0782161A (en) * | 1993-09-10 | 1995-03-28 | Hiromaru Ogata | Active oxygen suppressing agent |
| CN1360848A (en) * | 2000-12-23 | 2002-07-31 | 黄正华 | Mixed sodium peroxide solution containing sodium ozonide and its prepn and application |
| CN102058510A (en) * | 2010-12-28 | 2011-05-18 | 海南京润珍珠生物技术股份有限公司 | Leave-on facial mask with added pearl hydrolysate liposome |
| CN102107940A (en) * | 2009-12-29 | 2011-06-29 | 厦门埃里森节能科技有限公司 | Method for preparing nano pearl powder stock solution-containing small molecular group activated water |
| CN103070814A (en) * | 2012-12-14 | 2013-05-01 | 北海黑珍珠海洋生物科技有限公司 | Moisturizing and water locking mask liquid and its making technology |
| CN106727042A (en) * | 2017-02-11 | 2017-05-31 | 佛山文森特知识产权服务有限公司 | A kind of tender white MASQUE APAISANT HYDRATANT containing Margarita extract |
| CN107028863A (en) * | 2017-03-22 | 2017-08-11 | 北海市宝珠林海洋科技有限公司 | A kind of hydrolyzed pearl facial mask liquid and preparation method thereof |
| CN108210349A (en) * | 2018-03-09 | 2018-06-29 | 上海粉蝶化妆品有限公司 | A kind of facial mask liquid |
| CN108338992A (en) * | 2018-04-08 | 2018-07-31 | 西安建筑科技大学 | A kind of preparation method of pearl essence Selenium-rich nutrient solution |
-
2019
- 2019-07-23 CN CN201910664591.5A patent/CN110368351A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0782161A (en) * | 1993-09-10 | 1995-03-28 | Hiromaru Ogata | Active oxygen suppressing agent |
| CN1360848A (en) * | 2000-12-23 | 2002-07-31 | 黄正华 | Mixed sodium peroxide solution containing sodium ozonide and its prepn and application |
| CN102107940A (en) * | 2009-12-29 | 2011-06-29 | 厦门埃里森节能科技有限公司 | Method for preparing nano pearl powder stock solution-containing small molecular group activated water |
| CN102058510A (en) * | 2010-12-28 | 2011-05-18 | 海南京润珍珠生物技术股份有限公司 | Leave-on facial mask with added pearl hydrolysate liposome |
| CN103070814A (en) * | 2012-12-14 | 2013-05-01 | 北海黑珍珠海洋生物科技有限公司 | Moisturizing and water locking mask liquid and its making technology |
| CN106727042A (en) * | 2017-02-11 | 2017-05-31 | 佛山文森特知识产权服务有限公司 | A kind of tender white MASQUE APAISANT HYDRATANT containing Margarita extract |
| CN107028863A (en) * | 2017-03-22 | 2017-08-11 | 北海市宝珠林海洋科技有限公司 | A kind of hydrolyzed pearl facial mask liquid and preparation method thereof |
| CN108210349A (en) * | 2018-03-09 | 2018-06-29 | 上海粉蝶化妆品有限公司 | A kind of facial mask liquid |
| CN108338992A (en) * | 2018-04-08 | 2018-07-31 | 西安建筑科技大学 | A kind of preparation method of pearl essence Selenium-rich nutrient solution |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115429849A (en) * | 2022-08-23 | 2022-12-06 | 江西大自然制药有限公司 | Preparation method of body-strengthening and life-prolonging pills |
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