CN110331592A - A kind of biological enzyme real silk fabric flame-retardant finishing method - Google Patents
A kind of biological enzyme real silk fabric flame-retardant finishing method Download PDFInfo
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- CN110331592A CN110331592A CN201910427433.8A CN201910427433A CN110331592A CN 110331592 A CN110331592 A CN 110331592A CN 201910427433 A CN201910427433 A CN 201910427433A CN 110331592 A CN110331592 A CN 110331592A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/70—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with oxides of phosphorus; with hypophosphorous, phosphorous or phosphoric acids or their salts
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
- D06M13/148—Polyalcohols, e.g. glycerol or glucose
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
- D06M13/292—Mono-, di- or triesters of phosphoric or phosphorous acids; Salts thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/05—Cellulose or derivatives thereof
- D06M15/09—Cellulose ethers
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/507—Polyesters
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
- D06M16/003—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic with enzymes or microorganisms
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
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- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/30—Flame or heat resistance, fire retardancy properties
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
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- Biochemistry (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
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Abstract
The invention discloses a kind of biological enzyme real silk fabric flame-retardant finishing methods, include the following steps: S1, pretreatment: fabric being impregnated in pretreating agent, 40-50 DEG C for the treatment of temperature, handle time 30-60min, and warm water cleaning is used in taking-up;S2, bioenzyme washing: fabric is impregnated in biological enzyme additive, 60-70 DEG C for the treatment of temperature, handles time 80-120min, warm water cleaning is used in taking-up;The present invention is handled fabric using biological enzyme, impurity on fabric is sufficiently decomposed, in the case where not influencing fabric performance itself and feel, the associativity of finishing agent and fabric is improved, to improve the anti-flammability of fabric, and passes through addition antibacterial agent, so that fabric has antibiotic property, compared to traditional handicraft, treatment effeciency is improved, it is less to arrange the pollution that process generates.
Description
Technical field
The present invention relates to textile technology field, specifically a kind of biological enzyme real silk fabric flame-retardant finishing method.
Background technique
Silk refers generally to silk, including mulberry silk, tussah silk, ricinus silk, cassava silkwormsilk etc..Silk is referred to as " fiber
Queen ", with its favor of the unique glamour by people through the ages.Biological enzyme is generated by living cells with catalytic action
Organic matter, most of is protein, and also having few part is RNA.The manufacture of biological enzyme and application field are gradually expanded, biology
Application of the enzyme in textile industry is also ripe day by day, by being mainly used for the desizing of cotton fabric and the degumming of silk in the past, until present
Extensive use in each field of textile dyeing and finishing embodies superiority of the biological enzyme in Dyeing & Finishing Industry.Real silk fabric is due to resistance
Combustion property is bad, needs to carry out flame-proof treatment often to enhance anti-flammability, but traditional flame-proof finishing process is easy to cocoon fiber
Damage is generated, influences the feel of product, finishing effect is poor, and washability is bad.
Summary of the invention
The purpose of the present invention is to provide a kind of biological enzyme real silk fabric flame-retardant finishing methods, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the invention provides the following technical scheme:
A kind of biological enzyme real silk fabric flame-retardant finishing method, includes the following steps:
S1, pretreatment: fabric is impregnated in pretreating agent, 40-50 DEG C for the treatment of temperature, is handled time 30-60min, is taken
Warm water cleaning is used out;
S2, bioenzyme washing: fabric is impregnated in biological enzyme additive, 60-70 DEG C for the treatment of temperature, handles time 80-
Warm water cleaning is used in 120min, taking-up;
S3, arrangement: fabric is immersed in finishing agent, is padded processing, 20-40 DEG C for the treatment of temperature, is handled time 60-80min,
Liquid carrying rate 60-70%;
S4, baking: fabric is sent into drying box, first preliminary drying 2-3min under the conditions of 90-100 DEG C, then at 120-140 DEG C
Under the conditions of bake 2-4min;
S5, washing: fabric being soaked with warm water, is then soaped, then cold water is washed 2-4 times, constant temperature forming machine is sent into, in 30-
Drying and shaping under the conditions of 50 DEG C.
As a further solution of the present invention: pretreating agent described in step S1 is trimethylolpropane, sodium hypophosphite, sun
Ion softening agent, nonshrink aqua mixed solution.
As a further solution of the present invention: the nonshrink aqua is polyethylene terephthalate, polyethylene glycol, shell are poly-
Sugared mixed solution.
As a further solution of the present invention: biological enzyme additive described in step S2 includes cellulase, amylase, paint
Enzyme, bleeding agent and surfactant.
As a further solution of the present invention: the bleeding agent is fatty alcohol polyoxyethylene ether, sodium alkyl benzene sulfonate, alkyl
Any one of phenol polyethenoxy ether, the surfactant are polysorbate and Tea Saponin mixed solution.
As a further solution of the present invention: finishing agent described in step S3 includes fire retardant, antibacterial agent, dispersing agent, hydroxyl
Propyl methocel and eucalyptus oil.
As a further solution of the present invention: the fire retardant is tributyl phosphate, in triphenyl phosphate, tributyl phosphate
It is any.
As a further solution of the present invention: the antibacterial agent is Chinese juniper oil, argy wormwood, catechin mixed solution.
Compared with prior art, the beneficial effects of the present invention are:
The present invention is handled fabric using biological enzyme, the impurity on fabric is sufficiently decomposed, in not shadow
In the case where ringing fabric performance itself and feel, the associativity of finishing agent and fabric is improved, to improve the fire-retardant of fabric
Property, and by addition antibacterial agent, so that fabric has antibiotic property, traditional handicraft is compared, improves treatment effeciency, process is arranged and produces
Raw pollution is less.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment
Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field
Art personnel every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
Embodiment one:
A kind of biological enzyme real silk fabric flame-retardant finishing method, includes the following steps:
S1, pretreatment: fabric is impregnated in pretreating agent, 40 DEG C for the treatment of temperature, handles time 60min, is taken out with temperature
Water is cleaned;
S2, bioenzyme washing: fabric is impregnated in biological enzyme additive, 60 DEG C for the treatment of temperature, is handled time 120min, is taken
Warm water cleaning is used out;
S3, arrangement: fabric is immersed in finishing agent, is padded processing, 20 DEG C for the treatment of temperature, is handled time 80min, liquid carrying rate
70%;
S4, baking: fabric is sent into drying box, first preliminary drying 3min under the conditions of 90 DEG C, then bakes under the conditions of 120 DEG C
4min;
S5, washing: fabric being soaked with warm water, is then soaped, then cold water is washed 4 times, constant temperature forming machine is sent into, in 30 DEG C of items
Drying and shaping under part.
Pretreating agent described in step S1 is trimethylolpropane, sodium hypophosphite, cationic softener, the mixing of nonshrink aqua
Solution.
The nonshrink aqua is polyethylene terephthalate, polyethylene glycol, chitosan mixed solution.
Biological enzyme additive described in step S2 includes cellulase, amylase, laccase, bleeding agent and surfactant.
The bleeding agent is fatty alcohol polyoxyethylene ether, and the surfactant is that polysorbate and Tea Saponin mixing are molten
Liquid.
Finishing agent described in step S3 includes fire retardant, antibacterial agent, dispersing agent, hydroxypropyl methyl cellulose and eucalyptus oil.
The fire retardant is tributyl phosphate.
The antibacterial agent is Chinese juniper oil, argy wormwood, catechin mixed solution.
Embodiment two:
A kind of biological enzyme real silk fabric flame-retardant finishing method, includes the following steps:
S1, pretreatment: fabric is impregnated in pretreating agent, 45 DEG C for the treatment of temperature, handles time 45min, is taken out with temperature
Water is cleaned;
S2, bioenzyme washing: fabric is impregnated in biological enzyme additive, 65 DEG C for the treatment of temperature, is handled time 100min, is taken
Warm water cleaning is used out;
S3, arrangement: fabric is immersed in finishing agent, is padded processing, 30 DEG C for the treatment of temperature, is handled time 70min, liquid carrying rate
65%;
S4, baking: fabric is sent into drying box, first preliminary drying 2.5min under the conditions of 95 DEG C, then dries under the conditions of 130 DEG C
Roast 3min;
S5, washing: fabric being soaked with warm water, is then soaped, then cold water is washed 3 times, constant temperature forming machine is sent into, in 40 DEG C of items
Drying and shaping under part.
Pretreating agent described in step S1 is trimethylolpropane, sodium hypophosphite, cationic softener, the mixing of nonshrink aqua
Solution.
The nonshrink aqua is polyethylene terephthalate, polyethylene glycol, chitosan mixed solution.
Biological enzyme additive described in step S2 includes cellulase, amylase, laccase, bleeding agent and surfactant.
The bleeding agent is sodium alkyl benzene sulfonate, and the surfactant is polysorbate and Tea Saponin mixed solution.
Finishing agent described in step S3 includes fire retardant, antibacterial agent, dispersing agent, hydroxypropyl methyl cellulose and eucalyptus oil.
The fire retardant is triphenyl phosphate.
The antibacterial agent is Chinese juniper oil, argy wormwood, catechin mixed solution.
Embodiment three:
A kind of biological enzyme real silk fabric flame-retardant finishing method, includes the following steps:
S1, pretreatment: fabric is impregnated in pretreating agent, 50 DEG C for the treatment of temperature, handles time 30min, is taken out with temperature
Water is cleaned;
S2, bioenzyme washing: fabric is impregnated in biological enzyme additive, 70 DEG C for the treatment of temperature, is handled time 80min, is taken
Warm water cleaning is used out;
S3, arrangement: fabric is immersed in finishing agent, is padded processing, 40 DEG C for the treatment of temperature, is handled time 60min, liquid carrying rate
60%;
S4, baking: fabric is sent into drying box, first preliminary drying 2min under the conditions of 100 DEG C, then dries under the conditions of 140 DEG C
Roast 2min;
S5, washing: fabric being soaked with warm water, is then soaped, then cold water is washed 2 times, constant temperature forming machine is sent into, in 50 DEG C of items
Drying and shaping under part.
Pretreating agent described in step S1 is trimethylolpropane, sodium hypophosphite, cationic softener, the mixing of nonshrink aqua
Solution.
The nonshrink aqua is polyethylene terephthalate, polyethylene glycol, chitosan mixed solution.
Biological enzyme additive described in step S2 includes cellulase, amylase, laccase, bleeding agent and surfactant.
The bleeding agent is alkyl phenol polyoxyethylene ether, and the surfactant is that polysorbate and Tea Saponin mixing are molten
Liquid.
Finishing agent described in step S3 includes fire retardant, antibacterial agent, dispersing agent, hydroxypropyl methyl cellulose and eucalyptus oil.
The fire retardant is tributyl phosphate.
The antibacterial agent is Chinese juniper oil, argy wormwood, catechin mixed solution.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
Claims (8)
1. a kind of biological enzyme real silk fabric flame-retardant finishing method, which comprises the steps of:
S1, pretreatment: fabric is impregnated in pretreating agent, 40-50 DEG C for the treatment of temperature, is handled time 30-60min, is taken out and use
Warm water cleaning;
S2, bioenzyme washing: fabric is impregnated in biological enzyme additive, 60-70 DEG C for the treatment of temperature, handles time 80-120min,
Taking-up warm water cleaning;
S3, arrangement: fabric is immersed in finishing agent, is padded processing, 20-40 DEG C for the treatment of temperature, is handled time 60-80min, band liquid
Rate 60-70%;
S4, baking: fabric is sent into drying box, first preliminary drying 2-3min under the conditions of 90-100 DEG C, then in 120-140 DEG C of condition
Lower baking 2-4min;
S5, washing: fabric being soaked with warm water, is then soaped, then cold water is washed 2-4 times, constant temperature forming machine is sent into, at 30-50 DEG C
Under the conditions of drying and shaping.
2. a kind of biological enzyme real silk fabric flame-retardant finishing method according to claim 1, which is characterized in that in step S1
The pretreating agent is trimethylolpropane, sodium hypophosphite, cationic softener, nonshrink aqua mixed solution.
3. a kind of biological enzyme real silk fabric flame-retardant finishing method according to claim 2, which is characterized in that described nonshrink
Aqua is polyethylene terephthalate, polyethylene glycol, chitosan mixed solution.
4. a kind of biological enzyme real silk fabric flame-retardant finishing method according to claim 1, which is characterized in that in step S2
The biological enzyme additive includes cellulase, amylase, laccase, bleeding agent and surfactant.
5. a kind of biological enzyme real silk fabric flame-retardant finishing method according to claim 4, which is characterized in that the infiltration
Agent is any one of fatty alcohol polyoxyethylene ether, sodium alkyl benzene sulfonate, alkyl phenol polyoxyethylene ether, and the surfactant is
Polysorbate and Tea Saponin mixed solution.
6. a kind of biological enzyme real silk fabric flame-retardant finishing method according to claim 1, which is characterized in that in step S3
The finishing agent includes fire retardant, antibacterial agent, dispersing agent, hydroxypropyl methyl cellulose and eucalyptus oil.
7. a kind of biological enzyme real silk fabric flame-retardant finishing method according to claim 6, which is characterized in that described fire-retardant
Agent is any one of tributyl phosphate, triphenyl phosphate, tributyl phosphate.
8. a kind of biological enzyme real silk fabric flame-retardant finishing method according to claim 6, which is characterized in that the antibacterial
Agent is Chinese juniper oil, argy wormwood, catechin mixed solution.
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Cited By (1)
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CN112981949A (en) * | 2021-03-16 | 2021-06-18 | 南通职业大学 | Flame-retardant method for modified real silk based on biological enzyme |
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2019
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112981949A (en) * | 2021-03-16 | 2021-06-18 | 南通职业大学 | Flame-retardant method for modified real silk based on biological enzyme |
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