CN110317531A - A kind of resin type aqueous transparent glaze host agent and its application method - Google Patents
A kind of resin type aqueous transparent glaze host agent and its application method Download PDFInfo
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- CN110317531A CN110317531A CN201910706998.XA CN201910706998A CN110317531A CN 110317531 A CN110317531 A CN 110317531A CN 201910706998 A CN201910706998 A CN 201910706998A CN 110317531 A CN110317531 A CN 110317531A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2265—Oxides; Hydroxides of metals of iron
- C08K2003/2272—Ferric oxide (Fe2O3)
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The present invention provides a kind of resin type aqueous transparent glaze host agent, including following raw material components, the parts by weight of each component raw material are as follows: 20~40 parts of water-base resin, 0.1~0.3 part of pH adjusting agent, 0.1~0.6 part of auxiliary rheological agents, 0.1~0.4 part of wetting agent, 0.1~0.6 part of defoaming agent, 0.1~0.4 part of levelling agent, 10~30 parts of propylene glycol, 20~50 parts of deionized water, 2~10 parts of coalescing agent, 0.2~2 part of thickener.Water-base resin of the invention, auxiliary rheological agents, wetting agent, the formulation selection of coalescing agent and thickener and using where being the core of entire product, impart the aqueous transparent glaze host agent it is excellent infiltrate through permeability, ply adhesion and rate of drying, to balance the contradiction between wiping properties, construction efficiency and comprehensive performance three.
Description
Technical field
The present invention relates to technical field of coatings, and in particular to a kind of resin type aqueous transparent glaze host agent and its application side
Method.
Background technique
As the whole society is increasingly enhanced environmental consciousness, water paint occupies major part in China's coating total amount
Share.Water paint is using aqueous synthetic-resin as main film forming substance, and water is diluent, and suitable pigment, filler is added
And auxiliary material etc., a kind of coating made of ground is all with water as solvent or to make the coating of decentralized medium, all can be described as
Water paint or water paint.Simultaneously as people's quality of life improves, to the class promotion of culture and arts and chasing after for trend of back-to-ancients
Ask so that the unique feature that some articles of the remote past have successfully attracts modern, thus modern product do it is old multiple
The features such as Gu makes have apparent history breath, and the gloss naturally to fade, color are simple and unsophisticated and texture is graceful, from the inside to surface all
The breath in long age is given out, a kind of fashion is also more become.
Especially in recent years, favor of the American antique coating by more and more clients, especially antique white painting, city
Similar article of furniture is many on face.And more and more enterprises met using aqueous woodware paint client and itself
Environmental requirement, water paint, which does antique white painting, can equally reach extraordinary effect.In white technique modelled after an antique, wherein inevitably
Use glaze, glaze is a kind of translucent to transparent pigment colorant, dry to be wiped slowly, grooming and is done
Level light and shade keeps face soft using its translucence to reduce brightness, is contrasted and hatching effect, keeps integral color soft
It is strong with nature, stereovision, it is the indispensable color-tinted product of American and European style to generate pseudo-classic charm.
However at present on the market using linseed oil as the Water-soluble glaze of additive, have been assigned good wiping properties,
There is good behaviour when doing open effect, but wipes in thickness in use, since slow curing causes inner layer drying impermeable, in addition the non-pole of oils
Property substance and polarity coating between interfacial adhesion it is very poor, it is easy to there is drawing crack, the disadvantages such as delamination substantially reduce construction effect
Rate, the serious development for hindering woodcare paint Water-borne modification.
Summary of the invention
The object of the present invention is to provide a kind of resin type aqueous transparent glaze host agent, using water-base resin as carrier,
Two disadvantages for thoroughly solving flax oils Water-soluble glaze realize that products obtained therefrom has excellent wiping, permeability, color development
Property it is good, transparency is high, and ply adhesion is excellent, and drying time is moderate.
To solve the above-mentioned problems, the technical scheme adopted by the invention is that:
A kind of resin type aqueous transparent glaze host agent, including following raw material components, the parts by weight of each component raw material are as follows:
20~40 parts of water-base resin
0.1~0.3 part of pH adjusting agent
0.1~0.6 part of auxiliary rheological agents
0.1~0.4 part of wetting agent
0.1~0.6 part of defoaming agent
0.1~0.4 part of levelling agent
10~30 parts of propylene glycol
20~50 parts of deionized water
2~10 parts of coalescing agent
0.2~2 part of thickener.
Wherein: the water-base resin includes waterborne polyurethane resin and related compound modified product, water soluble acrylic acid tree
One of rouge and related compound modified product are a variety of.
Wherein, the pH adjusting agent is one of amine derivants such as ammonium hydroxide, AMP95, DMEA or a variety of.
Wherein, the auxiliary rheological agents are bentonite type auxiliary rheological agents, preferably the BENTONE DE of this production of hamming.
Wherein, the wetting agent be Tego270, Tego280, Tego4100 etc. efficiently one of substrate wetting agents or
It is a variety of；The defoaming agent is one of modified defoaming agent emulsion of the polyethers such as BYK028, Tego825, Tego902W or more
Kind；The levelling agent is one of polyether-modified surface modifiers such as GSK-6387, BYK306, BYK333 or a variety of.
Preferably, the coalescing agent is one of ethers auxiliary agents such as DPnB, DPnP, DPM, PNB or a variety of.
Preferably, the thickener is one of polyurethane thickeners such as TT615, COAPUR6050, Pur40 or more
Kind.
Further, the present invention provides a kind of application method of resin type aqueous transparent glaze host agent, the resin type water
The transparent glaze host agent of property successively feeds intake after mixing evenly by component, is equipped with aqueous transparent iron oxide color paste and carries out toning use.
Preferably, revolving speed is set as 500-2000r/min in whipping process, is dispersed with stirring the time and is set as 10-50 minutes.
Preferably, the binder content of the aqueous transparent iron oxide color paste is 10%-30%.
The present invention have the following advantages that compared with prior art and the utility model has the advantages that
1, the formulation selection of water-base resin of the invention, auxiliary rheological agents, wetting agent, coalescing agent and thickener and use are entire
Where the core of product, impart the aqueous transparent glaze host agent it is excellent infiltrate through permeability, ply adhesion and dry speed
Degree, to balance the contradiction between wiping properties, construction efficiency and comprehensive performance three；
2, the selection and use of auxiliary rheological agents imparts the good thixotropy of aqueous transparent glaze host agent, storage stability
With dry brush application property；
3, the present invention carries out toning use by being equipped with aqueous transparent iron oxide color paste, imparts the aqueous transparent glaze host agent
Coloring outstanding, the transparency and weatherability.
Specific embodiment
The present invention is described in detail combined with specific embodiments below.Following embodiment will be helpful to the technology of this field
Personnel further understand the present invention, but the invention is not limited in any way.It should be pointed out that the ordinary skill of this field
For personnel, without departing from the inventive concept of the premise, various modifications and improvements can be made.These belong to the present invention
Protection scope.
For convenience of description the features and advantages of the present invention, in the following embodiments, the water-base resin selects BASF
J95, the pH adjusting agent select ammonium hydroxide, and the auxiliary rheological agents select BENTONE DE, and the wetting agent is selected
Tego270, the defoaming agent select Tego825, Tego902W, and the levelling agent selects BYK333, and the film forming helps
DPnB is selected in agent, and the thickener selects Pur40.
Embodiment 1
A kind of resin type aqueous transparent glaze host agent, including following raw material components, the parts by weight of each component raw material are as follows:
Water-base resin: 20 parts of BASF J95
PH adjusting agent: 0.1 part of ammonium hydroxide
Auxiliary rheological agents: BENTONE®0.1 part of DE
Wetting agent: 0.1 part of Tego270
Defoaming agent: 0.2 part of Tego825
Levelling agent: 0.1 part of BYK333
20 parts of propylene glycol
50 parts of deionized water
Coalescing agent: 9 parts of DPnB
Thickener: 0.4 part of Pur40.
After successively feeding intake according to above-mentioned parts by weight, keep revolving speed to disperse to stir evenly for 20 minutes under 1000r/min, and
The aqueous transparent iron oxide color paste for being equipped with 20% carries out toning use.
Embodiment 2
A kind of resin type aqueous transparent glaze host agent, including following raw material components, the parts by weight of each component raw material are as follows:
Water-base resin: 25 parts of BASF J95
PH adjusting agent: 0.2 part of ammonium hydroxide
Auxiliary rheological agents: BENTONE®0.2 part of DE
Wetting agent: 0.2 part of Tego270
Defoaming agent: 0.2 part of Tego825
Defoaming agent: 0.2 part of Tego902W
Levelling agent: 0.3 part of BYK333
25 parts of propylene glycol
43 parts of deionized water
Coalescing agent: 5 parts of DPnB
Thickener: 0.7 part of Pur40.
After successively feeding intake according to above-mentioned parts by weight, keep revolving speed to disperse to stir evenly for 20 minutes under 1000r/min, and
The aqueous transparent iron oxide color paste for being equipped with 20% carries out toning use.
Embodiment 3
A kind of resin type aqueous transparent glaze host agent, including following raw material components, the parts by weight of each component raw material are as follows:
Water-base resin: 30 parts of BASF J95
PH adjusting agent: 0.1 part of ammonium hydroxide
Auxiliary rheological agents: BENTONE®0.3 part of DE
Wetting agent: 0.3 part of Tego270
Defoaming agent: 0.2 part of Tego825
Defoaming agent: 0.3 part of Tego902W
Levelling agent: 0.1 part of BYK333
20 parts of propylene glycol
40 parts of deionized water
Coalescing agent: 8 parts of DPnB
Thickener: 0.7 part of Pur40.
After successively feeding intake according to above-mentioned parts by weight, keep revolving speed to disperse to stir evenly for 20 minutes under 1000r/min, and
The aqueous transparent iron oxide color paste for being equipped with 20% carries out toning use.
Embodiment 4
A kind of resin type aqueous transparent glaze host agent, including following raw material components, the parts by weight of each component raw material are as follows:
Water-base resin: 35 parts of BASF J95
PH adjusting agent: 0.2 part of ammonium hydroxide
Auxiliary rheological agents: BENTONE®0.3 part of DE
Wetting agent: 0.4 part of Tego270
Defoaming agent: 0.2 part of Tego825
Defoaming agent: 0.3 part of Tego902W
Levelling agent: 0.1 part of BYK333
30 parts of propylene glycol
30 parts of deionized water
Coalescing agent: 2 parts of DPnB
Thickener: 1.5 parts of Pur40.
After successively feeding intake according to above-mentioned parts by weight, keep revolving speed to disperse to stir evenly for 20 minutes under 1000r/min, and
The aqueous transparent iron oxide color paste for being equipped with 20% carries out toning use.
Embodiment 5
A kind of resin type aqueous transparent glaze host agent, including following raw material components, the parts by weight of each component raw material are as follows:
Water-base resin: 40 parts of BASF J95
PH adjusting agent: 0.1 part of ammonium hydroxide
Auxiliary rheological agents: BENTONE®0.6 part of DE
Wetting agent: 0.4 part of Tego270
Defoaming agent: 0.3 part of Tego825
Defoaming agent: 0.3 part of Tego902W
Levelling agent: 0.1 part of BYK333
20 parts of propylene glycol
30 parts of deionized water
Coalescing agent: 7 parts of DPnB
Thickener: 1.2 parts of Pur40.
After successively feeding intake according to above-mentioned parts by weight, keep revolving speed to disperse to stir evenly for 20 minutes under 1000r/min, and
The aqueous transparent iron oxide color paste for being equipped with 20% carries out toning use.
Performance test
The wiping of commercially available traditional glaze existing to the aqueous transparent glaze host agent embodiment 1-5 and market is wiped again
Property is repaired the performances such as color, color developing, fillibility and inter-layer bonding force and is detected.
To the sample of the various embodiments described above carry out wipe color performance evaluation, these staining tests be entirely 50cm × 20cm ×
What 2cm was carried out on the plank by polishing, concrete operation method are as follows: brush one times above-mentioned water respectively in each plate face with wool brush
Property transparent glaze host agent (without dilution) or a kind of Water-soluble glaze sold of market after, wiped uniformly with rag along texture,
It receives completely, no sag waits to be dried；It is wiped again after drying, polish and repairs color, then recoat upper water varnish, respectively evaluation wiping
Property, again wipe property, repair color, color developing, fillibility and inter-layer bonding force, evaluation results are shown in Table 1.
Wiping: smooth wiping is 4 grades, and wiping stagnant hand is 0 grade, is divided into 5 grades；
Wiping property again: it wipes again and is easy to be 4 grades, it is difficult to which wiping again is 0 grade, is divided into 5 grades；
Repair color: repairing color gapless is 4 grades, and having lapping defect is 0 grade, is divided into 5 grades；
Color developing: color development is uniform, not floating is 4 grades, and coloring floating is 0 grade, is divided into 5 grades；
Fillibility: wood grain filling is full, good contrast is 4 grades, and filling is discontented or uneven, wood grain poor contrast is 0 grade, successively
It is divided into 5 grades；
Inter-layer bonding force: marking the intersection grid of 5 groups of spacing about 1mm with icking tool, after being affixed on knurled surfaces compacting with adhesive tape
It tears, is divided into 0 to 4 grade 5 etc. with colorant dropping situations in grid.
Test result see the table below shown in 1:
| Performance | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Commercially available glaze |
| Wiping | 4 | 4 | 4 | 4 | 4 | 3 |
| Wiping property again | 4 | 4 | 4 | 4 | 4 | 4 |
| Repair color | 4 | 3 | 4 | 4 | 4 | 4 |
| Color developing | 3 | 4 | 3 | 4 | 4 | 3 |
| Fillibility | 3 | 3 | 4 | 4 | 4 | 2 |
| Inter-layer bonding force | 4 | 4 | 4 | 4 | 4 | 3 |
Known to test result: making Water-soluble glaze exist using the aqueous transparent glaze host agent that the formula of invention is prepared
Wiping rate of drying in color technique reduces, and plays good filling effect on the basis of not influencing plate original primary colours；The present invention
Aqueous transparent glaze host agent shown when for coating aqueous carpentry technique with various aqueous priming paints have it is good
Compatibility and inter-layer bonding force show the transparency and permeability well in the drying process, the advantages that having no irritating odor,
Wood furniture and product suitable for various material.So the present invention effectively overcomes various shortcoming in the prior art and has
High industrial utilization value.
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, other any changes, modifications, substitutions, combinations, simplifications made without departing from the spirit and principles of the present invention,
It should be equivalent substitute mode, be included within the scope of the present invention.
Claims (9)
1. a kind of resin type aqueous transparent glaze host agent, which is characterized in that including following raw material components, the weight of each component raw material
Measure number are as follows:
20~40 parts of water-base resin
0.1~0.3 part of pH adjusting agent
0.1~0.6 part of auxiliary rheological agents
0.1~0.4 part of wetting agent
0.1~0.6 part of defoaming agent
0.1~0.4 part of levelling agent
10~30 parts of propylene glycol
20~50 parts of deionized water
2~10 parts of coalescing agent
0.2~2 part of thickener.
2. a kind of resin type aqueous transparent glaze host agent according to claim 1, which is characterized in that the aqueous tree
Rouge includes waterborne polyurethane resin and related compound modified product, and one in water-based acrylic resin and related compound modified product
Kind is a variety of.
3. a kind of resin type aqueous transparent glaze host agent according to claim 1, which is characterized in that the pH is adjusted
Agent is one of amine derivants such as ammonium hydroxide, AMP95, DMEA or a variety of.
4. a kind of resin type aqueous transparent glaze host agent according to claim 1, which is characterized in that the rheology helps
Agent is bentonite type auxiliary rheological agents, preferably the BENTONE DE of this production of hamming.
5. a kind of resin type aqueous transparent glaze host agent according to claim 1, which is characterized in that the film forming helps
Agent is one of ethers auxiliary agents such as DPnB, DPnP, DPM, PNB or a variety of.
6. a kind of resin type aqueous transparent glaze host agent according to claim 1, which is characterized in that the thickener
For one of polyurethane thickeners such as TT615, COAPUR6050, Pur40 or a variety of.
7. the application method of any resin type aqueous transparent glaze host agent in a kind of claim 1-6, which is characterized in that
The resin type aqueous transparent glaze host agent successively feeds intake after mixing evenly by component, is equipped with the progress of aqueous transparent iron oxide color paste
Toning uses.
8. the application method of resin type aqueous transparent glaze host agent according to claim 7, which is characterized in that whipping process
Middle revolving speed is set as 500-2000r/min, is dispersed with stirring the time and is set as 10-50 minutes.
9. the application method of resin type aqueous transparent glaze host agent according to claim 7, which is characterized in that described aqueous
The binder content of transparent ferric oxide mill base is 10%-30%.
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| CN201910706998.XA CN110317531A (en) | 2019-08-01 | 2019-08-01 | A kind of resin type aqueous transparent glaze host agent and its application method |
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| CN201910706998.XA CN110317531A (en) | 2019-08-01 | 2019-08-01 | A kind of resin type aqueous transparent glaze host agent and its application method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112680075A (en) * | 2020-12-14 | 2021-04-20 | 成都展辰涂料有限公司 | Non-mask aqueous colorant and preparation method thereof |
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2019
- 2019-08-01 CN CN201910706998.XA patent/CN110317531A/en active Pending
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