CN110317100A - The production technology of organic selenium Liquid Fertilizer - Google Patents
The production technology of organic selenium Liquid Fertilizer Download PDFInfo
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- CN110317100A CN110317100A CN201910661590.5A CN201910661590A CN110317100A CN 110317100 A CN110317100 A CN 110317100A CN 201910661590 A CN201910661590 A CN 201910661590A CN 110317100 A CN110317100 A CN 110317100A
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- organic selenium
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C11/00—Other nitrogenous fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
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- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a kind of production technologies of organic selenium Liquid Fertilizer, by by the sodium selenite absorption after activated carbon purification in corn and rice sprout saccharified liquid, the organic selenium masterbatch pulvis with polysaccharide molecule chain is become, then by organic selenium masterbatch pulvis and amino acid original powder, microelement, solubilizer and compound stabilizer at organic selenium Liquid Fertilizer.The present invention uses the production technology of above-mentioned organic selenium Liquid Fertilizer, and dosage is small, and absorptivity is high, and crop and fruit is able to satisfy green, nuisanceless or organic agriculture standard, and application flows into Tian Tuhou and is not in fertilizer damage, reduces soil cultivation effect, and non-environmental-pollution.
Description
Technical field
The present invention relates to organic fertilizer technical fields, more particularly, to a kind of production technology of organic selenium Liquid Fertilizer.
Background technique
" selenium " is one of required 8 kinds of microelements of human body, has anti-oxidant, anti-aging, anti-radiation, solution heavy metal
(mercury, lead, cadmium) toxin and other effects.Selenium is divided into two kinds in the existing way of nature: inorganic selenium and organic selenium, inorganic selenium refer generally to
Sodium selenite and sodium selenate are obtained from the byproduct of metal mineral reserves；Organic selenium is that selenium passes through bioconversion in conjunction with amino acid
It forms, exists generally in the form of selenomethionine, follow Methionine metabolism approach to be metabolized, participate in the synthesis of albumen, be easy in group
Knit interior storage, absorption；It can be rapidly immediately used by the body after being absorbed by the body, blood selenium situation in human body is effectively improved, to meet
Demand of the human body to selenium.China is one of selenium deficiency country, especially North China, northeast and coastal 15 province ,city and area in the world, people
Equal daily 26.4 microgram of intake average out to of selenium, the standard that the demand far below human body minimum selenium daily is 50 milligrams are existing
Se content in plant and human body is mainly from fertilizer, and inorganic selenium fertilizer is in addition to toxicity is big, beavy metal impurity is more, crop is rich at present
Selenium amount is unstable, can not normal absorption the defects of, there are also it is a large amount of, be used for a long time after Zinc fractions accumulation, cause clay fertilizer evil without
It can plant again, and Current Domestic organic selenium fertilizer, due to technology, production cost, organic selenium fertilizer production technology is not
It is mature.
Summary of the invention
The object of the present invention is to provide a kind of production technologies of organic selenium Liquid Fertilizer, and dosage is small, and absorptivity is high, crop and fruit
It is able to satisfy green, nuisanceless or organic agriculture standard, application flows into Tian Tuhou and is not in fertilizer damage, reduces soil cultivation effect,
And non-environmental-pollution.
To achieve the above object, the present invention provides a kind of production technologies of organic selenium Liquid Fertilizer, comprising the following steps:
(1) preparation of organic selenium masterbatch pulvis
The first step, by no fungus deterioration and fresh corn and rice sprout are crushed, and are crushed to 10-30 mesh, rice sprout diameter is less than 2
Centimetre, it is placed after mixing, it is spare；
Second step will test qualified and be added to 5-7 times of parts by weight by the sodium selenite after activated carbon purification and locate
It manages sufficiently to stir in qualified soft water to all dissolutions and place, it is spare；
Third step will test after qualified wheat bran enzyme powder weighs according to the ratio and place, spare；
4th step, spare corn is soaked in water about 6 hours with standby after broken, is pulled out, is put into steamer, spare water logging is added
2 centimetres of corn are crossed, slowly heats boiling, while stirring corn, until stopping boiling when the soft no hard core of corn, opens reaction kettle,
Boiling is successively poured into soft aqueous corn, rice sprout, sodium selenite solution, spare wheat bran enzyme powder, wheat bran enzyme are added while hot
Powder is premixed uniformly before entering reaction kettle with water, is opened and is stirred and adjust agitating speed, stops when slowly adding spare soft water to paste,
Charger sheet has been checked after the completion of charging, close feed inlet and has been sealed, and adjusts temperature of reaction kettle, reaction time, saccharification reaction is simultaneously
The record start time keeps reaction kettle passive state and agitating speed, observes material saccharification situation by reaction kettle form and glues
Consistency makes material saccharification completely and keeps appropriate paste-like consistency；
5th step, saccharification are closed temperature control system after the reaction was completed, cooling material, are kept stirring, sample detection, and saccharification is qualified
Material afterwards is filtered after being cooled to room temperature with the mode of behaviour's filter, and screen specification is greater than 80 mesh；6th step, filtered finished product are to have
Machine selenium masterbatch liquid agent, class Huang to brown are sealed, and flow into downstream product, filtering 60-70 degrees Celsius of hot air drying bath of clout is extremely
Moisture pulverizes when being not more than 5%, and partial size crosses 100 mesh, is finished product organic selenium masterbatch pulvis, class Bai Zhihuang or brown after detection
Color；
(2) preparation of organic selenium Liquid Fertilizer
Amino acid original powder is poured into mixing tank by the first step, and stirring while filling the water is completely dissolved amino acid original powder, is protected
Holding temperature in tank is 40-50 degrees Celsius, and stopping when being filled to mixing tank half is added micro after amino acid original powder is completely dissolved
Element, expanding material and being stirred continuously to solubilizer are completely dissolved, and add stabilizer, agitating by adding makes liquid foam disappear completely
It is molten；
Organic selenium masterbatch pulvis is slowly poured into small charging basket by second step, adds water at small charging basket 1/2 and constantly agitation has made
Fully dissolved, the organic selenium masterbatch pulvis after being completely dissolved in keg are slowly added in the ammino acid liquid fertilizer of mixing tank, not
Disconnected agitation is dissolved to abundant, while being rinsed with water small charging basket and being poured into the water of flushing sufficiently molten even in mixing tank；
Third step, be completely dissolved after the organic selenium Liquid Fertilizer in mixing tank, determine do not precipitate after supplied in mixing tank
For water to quantifying, agitation of slowlying while moisturizing dissolves organic selenium Liquid Fertilizer sufficiently, the organic selenium after the completion of quantitative preparation
Liquid Fertilizer flows into filling bottle, coding, packaging after standing 15 minutes, obtains organic selenium Liquid Fertilizer finished product.
Preferably, corn 80-90 parts by weight, rice sprout 10-20 parts by weight, sodium selenite 30-60 weight in the step (1)
Part and wheat bran enzyme powder 0.5-3 parts by weight.
Preferably, the saccharification of the 4th step is reacted in the step (1), and temperature of reaction kettle is 45-55 degrees Celsius, the reaction time
It is 12-48 hours, agitating speed is 30-50 revs/min.
Preferably, the amino acid original powder in the step (2) is 100 parts by weight, microelement is 2-6 parts by weight, organic
Selenium masterbatch pulvis is 20-80 parts by weight, solubilizer is 5-10 parts by weight and stabilizer is 0.2-1 parts by weight.
Preferably, amino acid original powder is poured into mixing tank in the step (2), stirring while filling the water keeps amino acid former
Powder is completely dissolved, and the mixed dissolution time is 30 minutes, and keeping temperature in tank is 40-50 degrees Celsius, when being filled to mixing tank half
Stop, microelement is added after amino acid original powder is completely dissolved, expanding material and being stirred continuously to solubilizer is completely dissolved, this mistake
Journey is 20 minutes, adds stabilizer, agitates by adding that so that liquid foam is disappeared completely molten.
Preferably, organic selenium masterbatch pulvis is slowly poured into small charging basket in the step (2), downwind is added, and adds water
At to small charging basket 1/2 and constantly agitation makes to be completely dissolved, this process is 10 minutes, and the organic selenium after being completely dissolved in keg is female
Feed powder agent is slowly added in the ammino acid liquid fertilizer of mixing tank, and constantly agitation is dissolved to abundant, while being rinsed with water small charging basket
And the water of flushing is poured into sufficiently molten even in mixing tank.Preferably, organic selenium masterbatch pulvis is slowly poured into the step (2)
Small charging basket, downwind are added, and add water at small charging basket 1/2 and constantly agitation makes to be completely dissolved, this process is 10 minutes, water
Temperature is greater than 40 degrees Celsius, and the organic selenium masterbatch pulvis after being completely dissolved in keg is slowly added to the aminoacids solution of mixing tank
In fertilizer, and constantly agitation is dissolved to abundant, while being rinsed with water small charging basket and being poured into the water of flushing sufficiently molten even in mixing tank.
Therefore, the present invention uses the production technology of above-mentioned organic selenium Liquid Fertilizer, and dosage is small, and absorptivity is high, crop and fruit energy
Meeting green, nuisanceless or organic agriculture standard, application flows into Tian Tuhou and is not in fertilizer damage, reduces soil cultivation effect, and
Non-environmental-pollution.
Below by drawings and examples, technical scheme of the present invention will be described in further detail.
Detailed description of the invention
Fig. 1 is a kind of flow chart of the production technology embodiment of organic selenium Liquid Fertilizer of the present invention；
Fig. 2 is a kind of preparation flow of the organic selenium masterbatch pulvis of the production technology embodiment of organic selenium Liquid Fertilizer of the present invention
Figure；
Fig. 3 is a kind of preparation flow of the organic selenium Liquid Fertilizer of the production technology embodiment of organic selenium Liquid Fertilizer of the present invention
Figure.
Specific embodiment
Embodiment
Fig. 1 is a kind of flow chart of the production technology embodiment of organic selenium Liquid Fertilizer of the present invention, and Fig. 2 is that one kind of the present invention has
The preparation flow figure of the organic selenium masterbatch pulvis of the production technology embodiment of machine selenium Liquid Fertilizer, Fig. 3 are a kind of organic selenium of the present invention
The preparation flow figure of the organic selenium Liquid Fertilizer of the production technology embodiment of Liquid Fertilizer, as shown, the present invention provides one kind to have
The production technology of machine selenium Liquid Fertilizer, comprising the following steps: (1) preparation of organic selenium masterbatch pulvis
The first step, by no fungus deterioration and the corn of fresh 80-90 parts by weight and the rice sprout of 10-20 parts by weight are crushed,
It is crushed to 10-30 mesh, rice sprout diameter is placed after mixing less than 2 centimetres, spare；
Second step will test qualified and be added to 5-7 times by the sodium selenite of the 30-60 parts by weight after activated carbon purification
Sufficiently agitation to all dissolutions are placed in the soft water of parts by weight and processed qualification, spare；
Third step, will test qualified 0.5-3 parts by weight wheat bran enzyme powder weigh according to the ratio after place, it is spare；
4th step, spare corn is soaked in water about 6 hours with standby after broken, is pulled out, is put into steamer, spare water logging is added
2 centimetres of corn are crossed, slowly heats boiling, while stirring corn, until stopping boiling when the soft no hard core of corn, opens reaction kettle,
Boiling is successively poured into soft aqueous corn, rice sprout, sodium selenite solution, spare wheat bran enzyme powder, wheat bran enzyme are added while hot
Powder is premixed uniformly before entering reaction kettle with water, and opening and stirring and adjust agitating speed is 30-50 revs/min, is slowly added spare
Stop when soft water to paste, charger sheet has been checked after the completion of charging, close feed inlet and seal, adjusting temperature of reaction kettle is 45-
55 degrees Celsius, the reaction time be 12-48 hour, saccharification reaction and record start time, holding reaction kettle passive state and agitation
Revolving speed observes material saccharification situation and viscosity by reaction kettle form, makes material saccharification completely and keep appropriate paste sticky
Degree；
5th step, saccharification are closed temperature control system after the reaction was completed, cooling material, are kept stirring, sample detection, and saccharification is qualified
Material afterwards is filtered after being cooled to room temperature with the mode of behaviour's filter, and screen specification is greater than 80 mesh；
6th step, filtered finished product are organic selenium masterbatch liquid agent, and class Huang to brown is sealed, and flow into downstream and produce
Product, filtering 60-70 degrees Celsius of hot air drying bath of clout to moisture pulverize when being not more than 5%, and partial size crosses 100 mesh, is after detection
Finished product organic selenium masterbatch pulvis, class Bai Zhihuang or brown；
(2) preparation of organic selenium Liquid Fertilizer
The amino acid original powder of 100 parts by weight is poured into mixing tank by the first step, and stirring while filling the water makes amino acid original powder
It being completely dissolved, dissolution time is 30 minutes, and keeping temperature in tank is 40-50 degrees Celsius, stopping when being filled to mixing tank half, to
Amino acid original powder is added the microelement of 2-6 parts by weight, the expanding material of 5-10 parts by weight and is stirred continuously to increasing after being completely dissolved
Solvent is completely dissolved, this process is 20 minutes, adds the stabilizer of 0.2-1 parts by weight, agitating by adding keeps liquid foam complete
Totally disappeared it is molten, microelement be zinc, nitrogen, phosphorus；
Organic selenium masterbatch pulvis is slowly poured into small charging basket by second step, and downwind is added, adds water at small charging basket 1/2
And constantly agitation makes to be completely dissolved, this process is 10 minutes, and the temperature of water is greater than 40 degrees Celsius, after being completely dissolved in keg
Organic selenium masterbatch pulvis is slowly added in the ammino acid liquid fertilizer of mixing tank, and constantly agitation is dissolved to abundant, while being rushed with water
It washes small charging basket and pours into the water of flushing sufficiently molten even in mixing tank；
Third step, be completely dissolved after the organic selenium Liquid Fertilizer in mixing tank, determine do not precipitate after supplied in mixing tank
For water to quantifying, agitation of slowlying while moisturizing dissolves organic selenium Liquid Fertilizer sufficiently, the organic selenium after the completion of quantitative preparation
Liquid Fertilizer flows into filling bottle, coding, packaging after standing 15 minutes, obtains organic selenium Liquid Fertilizer finished product.
Therefore, the present invention uses the production technology of above-mentioned organic selenium Liquid Fertilizer, and dosage is small, and absorptivity is high, crop and fruit energy
Meeting green, nuisanceless or organic agriculture standard, application flows into Tian Tuhou and is not in fertilizer damage, reduces soil cultivation effect, and
Non-environmental-pollution.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than is limited,
Although the present invention is described in detail with reference to preferred embodiments, those skilled in the art should understand that: its according to
So can be with modification or equivalent replacement of the technical solution of the present invention are made, and these modifications or equivalent replacement cannot also make to repair
Technical solution after changing is detached from the spirit and scope of technical solution of the present invention.
Claims (7)
1. a kind of production technology of organic selenium Liquid Fertilizer, which comprises the following steps:
(1) preparation of organic selenium masterbatch pulvis
The first step, by no fungus deterioration and fresh corn and rice sprout are crushed, and are crushed to 10-30 mesh, rice sprout diameter is less than 2 lis
Rice, is placed after mixing, spare；
Second step will test qualified and be added to 5-7 times of parts by weight and processed conjunction by the sodium selenite after activated carbon purification
Sufficiently agitation to all dissolutions are placed in the soft water of lattice, spare；
Third step will test after qualified wheat bran enzyme powder weighs according to the ratio and place, spare；
4th step, spare corn is soaked in water about 6 hours with standby after broken, is pulled out, is put into steamer, it is excessively beautiful that spare water logging is added
2 centimetres of rice, slowly heats boiling, while stirring corn, until stopping boiling when the soft no hard core of corn, opens reaction kettle, successively
Boiling is poured into soft aqueous corn, rice sprout, sodium selenite solution, spare wheat bran enzyme powder is added while hot, wheat bran enzyme powder enters
It is premixed uniformly before reaction kettle with water, opens and stir and adjust agitating speed, stop when slowly adding spare soft water to paste, fed
Charger sheet has been checked after the completion, close feed inlet and has been sealed, temperature of reaction kettle, reaction time are adjusted, and saccharification is reacted and recorded
Initial time keeps reaction kettle passive state and agitating speed, observes material saccharification situation and viscosity by reaction kettle form,
Make material saccharification completely and keeps appropriate paste-like consistency；
5th step, saccharification is closed temperature control system after the reaction was completed, cooling material, is kept stirring, sample detection, after saccharification is qualified
Material is filtered after being cooled to room temperature with the mode of behaviour's filter, and screen specification is greater than 80 mesh；
6th step, filtered finished product are organic selenium masterbatch liquid agent, and class Huang to brown is sealed, and flow into downstream product, mistake
Filter 60-70 degrees Celsius of hot air drying bath of clout pulverizes when being not more than 5% to moisture, and partial size crosses 100 mesh, has after detection for finished product
Machine selenium masterbatch pulvis, class Bai Zhihuang or brown；
(2) preparation of organic selenium Liquid Fertilizer
Amino acid original powder is poured into mixing tank by the first step, and stirring while filling the water is completely dissolved amino acid original powder, keeps tank
Interior temperature is 40-50 degrees Celsius, and micro member is added after amino acid original powder is completely dissolved in stopping when being filled to mixing tank half
Element, expanding material and being stirred continuously to solubilizer are completely dissolved, and add stabilizer, agitating by adding makes liquid foam disappear completely
It is molten；
Organic selenium masterbatch pulvis is slowly poured into small charging basket by second step, add water at small charging basket 1/2 and constantly agitation make it is completely molten
Solution, the organic selenium masterbatch pulvis after being completely dissolved in keg is slowly added in the ammino acid liquid fertilizer of mixing tank, and is constantly stirred
It moves to abundant dissolution, while being rinsed with water small charging basket and pouring into the water of flushing sufficiently molten even in mixing tank；
Third step, be completely dissolved after the organic selenium Liquid Fertilizer in mixing tank, determine do not precipitate after water is supplied in mixing tank
Dissolve organic selenium Liquid Fertilizer sufficiently to quantitatively, slowlying to stir while moisturizing, the organic selenium liquid after the completion of quantitative preparation
Fertilizer flows into filling bottle, coding, packaging after standing 15 minutes, obtains organic selenium Liquid Fertilizer finished product.
2. the production technology of organic selenium Liquid Fertilizer according to claim 1, it is characterised in that: corn in the step (1)
80-90 parts by weight, rice sprout 10-20 parts by weight, sodium selenite 30-60 parts by weight and wheat bran enzyme powder 0.5-3 parts by weight.
3. the production technology of organic selenium Liquid Fertilizer according to claim 2, it is characterised in that: the 4th in the step (1)
The saccharification of step is reacted, and temperature of reaction kettle is 45-55 degrees Celsius, and the reaction time is 12-48 hours, and agitating speed is 30-50 revs/min
Clock.
4. the production technology of organic selenium Liquid Fertilizer according to claim 1, it is characterised in that: the ammonia in the step (2)
Base acid original powder is 100 parts by weight, microelement is 2-6 parts by weight, organic selenium masterbatch pulvis is 20-80 parts by weight, solubilizer is
5-10 parts by weight and stabilizer are 0.2-1 parts by weight.
5. the production technology of organic selenium Liquid Fertilizer according to claim 4, it is characterised in that: by ammonia in the step (2)
Base acid original powder pours into mixing tank, and stirring while filling the water is completely dissolved amino acid original powder, and the mixed dissolution time is 30 minutes,
Keeping temperature in tank is 40-50 degrees Celsius, and stopping when being filled to mixing tank half is added micro- after amino acid original powder is completely dissolved
Secondary element, expanding material and being stirred continuously to solubilizer are completely dissolved, this process is 20 minutes, add stabilizer, side edged stirs
It is dynamic that so that liquid foam is disappeared completely molten.
6. the production technology of organic selenium Liquid Fertilizer according to claim 5, it is characterised in that: will have in the step (2)
Machine selenium masterbatch pulvis slowly pours into small charging basket, and downwind is added, add water at small charging basket 1/2 and constantly agitation make it is completely molten
Solution, this process are 10 minutes, and the organic selenium masterbatch pulvis after being completely dissolved in keg is slowly added to the amino acid of mixing tank
In liquid fertilizer, and constantly agitation is dissolved to abundant, while being rinsed with water small charging basket and being poured into the water of flushing sufficiently molten in mixing tank
It is even.
7. the production technology of organic selenium Liquid Fertilizer according to claim 6, it is characterised in that: will have in the step (2)
Machine selenium masterbatch pulvis slowly pours into small charging basket, and downwind is added, add water at small charging basket 1/2 and constantly agitation make it is completely molten
Solution, this process are 10 minutes, and the temperature of water is greater than 40 degrees Celsius, and the organic selenium masterbatch pulvis after being completely dissolved in keg is slowly
It is added in the ammino acid liquid fertilizer of mixing tank, and constantly agitation is to abundant dissolution, while being rinsed with water small charging basket and by flushing
Water pours into sufficiently molten even in mixing tank.
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