CN110305545A - A kind of quick-dry type woodenware sealing wax seal coat and preparation method thereof - Google Patents

A kind of quick-dry type woodenware sealing wax seal coat and preparation method thereof Download PDF

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Publication number
CN110305545A
CN110305545A CN201810227478.6A CN201810227478A CN110305545A CN 110305545 A CN110305545 A CN 110305545A CN 201810227478 A CN201810227478 A CN 201810227478A CN 110305545 A CN110305545 A CN 110305545A
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CN
China
Prior art keywords
self
quick
seal coat
dry type
sealing wax
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Pending
Application number
CN201810227478.6A
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Chinese (zh)
Inventor
李璠
杨�远
闫会玲
张文东
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Hebei Chenyang Industry and Trade Group Co Ltd
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Hebei Chenyang Industry and Trade Group Co Ltd
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Priority to CN201810227478.6A priority Critical patent/CN110305545A/en
Publication of CN110305545A publication Critical patent/CN110305545A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/04Homopolymers or copolymers of esters
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D175/00Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
    • C09D175/04Polyurethanes
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/002Priming paints
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/63Additives non-macromolecular organic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/65Additives macromolecular
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

Abstract

The present invention provides a kind of quick-dry type woodenware sealing wax seal coat, belongs to technical field of coatings.The quick-dry type woodenware sealing wax seal coat, by percentage to the quality, it is composed of the following components: water-borne Self-Crosslinked Acrylic lotion or self-crosslinkable polyurethane dispersions, the pH adjusting agent of 0.05-0.15% of 25-35%, the wetting agent of 0.3-0.8%, the defoaming agent of 0.5-1.5%, the volatile type solvent of 50-70%, 5~10% coalescing agent.There is good sealing effect to solid wood, density board using quick-dry type woodenware sealing wax seal coat of the present invention, the rate of drying of seal coat can be increased substantially, so as to improve production efficiency, saves time cost.

Description

A kind of quick-dry type woodenware sealing wax seal coat and preparation method thereof
Technical field
The present invention relates to a kind of quick-dry type woodenware sealing wax seal coats and preparation method thereof, belong to paint field.
Background technique
In order to reinforce protection to environment and improve production efficiency and taking into account to the more preferable closure of substrate, most producer Or workshop need it is a kind of be suitable for a variety of plates, can rapid draing, and can play good confinement can aqueous sealing primer.Such as Modern product multiplicity in the market, the fast product of rate of drying often contain film forming matter it is very few cannot good closed substrate, film forming matter Matter is on the high side and will affect dry speed.The existing good rate of drying of the present invention and the good closed substrate of energy, can meet city Demand, while improving the production efficiency can better closed substrate, closed protective is carried out to substrate.
Summary of the invention
The technical problem to be solved by the present invention is to aqueous sealing primer in the prior art, there are slow drying speeds or closing The bad problem of performance, and then a kind of quick-dry type woodenware sealing wax seal coat and preparation method thereof of function admirable is provided.
In order to solve the above-mentioned technical problems, the present invention provides a kind of quick-dry type woodenware sealing wax seal coats, with quality hundred Divide than meter, it is composed of the following components: the water-borne Self-Crosslinked Acrylic lotion or self-crosslinkable polyurethane dispersions of 25-35%, 0.05- 0.15% pH adjusting agent, the wetting agent of 0.3-0.8%, the defoaming agent of 0.5-1.5%, the volatile type solvent of 50-70%, 5 ~10% coalescing agent.
Further, by percentage to the quality, composed of the following components: 31% water-borne Self-Crosslinked Acrylic lotion or from Cross-linked polyurethane dispersion, 0.11% PH regulator, 0.53% wetting agent, 1.14% defoaming agent, 60.5% easily wave Hair style solvent, 6.72% coalescing agent.
Further, when selecting water-borne Self-Crosslinked Acrylic lotion, the water-borne Self-Crosslinked Acrylic lotion be without APEO, solid content are the water-borne Self-Crosslinked Acrylic lotion of 35-40wt%.
Further, when selecting self-crosslinkable polyurethane dispersions, the self-crosslinkable polyurethane dispersions be without APEO, Solid content is the self-crosslinkable polyurethane dispersions of 35-40wt%.
Further, the wetting agent is polyether siloxane copolymer or Shuangzi structural silicone;Defoaming agent is polyethers silicon Siloxane copolymers lotion;Volatile type solvent is ethyl alcohol;Coalescing agent is butyl.
Further, the present invention also provides the preparation method of the quick-dry type woodenware sealing wax seal coat, including it is as follows Step:
(1) proportion is pressed, successively by water-borne Self-Crosslinked Acrylic lotion, defoaming agent is added to the container stirring, revolving speed 800-1000r/min stirs 15min;
(2) PH regulator, stirring is added, revolving speed 500-800r/min stirs 5min;
(3) wetting agent, stirring is added, revolving speed 800-1000r/min stirs 15min;
(4) coalescing agent and solvent is added, speed of agitator 1000-1200r/min stirs 20min;Apply 4 glasss of measurements, 23- 25 degrees Celsius of range of viscosities obtained the quick-dry type woodenware sealing wax seal coat at 12-15 seconds.
The invention has the following advantages over the prior art:
(1) quick-dry type woodenware sealing wax seal coat of the present invention passes through selection self-crosslinking acrylic lotion or self-crosslinking Dispersions of polyurethanes cooperates pH adjusting agent, wetting agent, defoaming agent and the coalescing agent of special ratios, especially cooperates volatile After type solvent, the quick-dry type woodenware sealing wax seal coat being prepared has rate of drying fast, the excellent feature of closed performance.It adopts There is good sealing effect to solid wood, density board with quick-dry type woodenware sealing wax seal coat of the present invention, it can be significantly The rate of drying of seal coat is improved, so as to improve production efficiency, saves time cost.
(2) quick-dry type woodenware sealing wax seal coat of the present invention, further, when selection water-borne Self-Crosslinked Acrylic cream When liquid, the water-borne Self-Crosslinked Acrylic lotion is preferably free of APEO, and solid content is the waterborne self-crosslinkable propylene of 35-40wt% Yogurt liquid;Or when selecting self-crosslinkable polyurethane dispersions, the self-crosslinkable polyurethane dispersions are preferably free of APEO, Gu The self-crosslinkable polyurethane dispersions of content 35-40wt%, the quick-dry type woodenware sealing wax seal coat being prepared is not due to Containing APEO, have the advantages that environment protecting is good, adhesive force is good in addition, it also has, fast drying, has good closure and resists Rise muscle, and has certain color inhibition effect, is suitable for a variety of solid wood boards and composite board.
Specific embodiment
With reference to embodiments, the present invention is further described in detail, but not limited to this.
Raw material employed in following embodiments is marketable material unless otherwise specified, specifically as follows using raw material:
Raw material product name Model Manufacturer
Water-borne Self-Crosslinked Acrylic lotion XK12/AC3600/AC2742 DSM/ Opel enlightening/Opel enlightening
Self-crosslinkable polyurethane dispersions R2180/R9029 DSM/DSM
Defoaming agent tego902w、tego825 Digao
Wetting agent tego4100、tego280 Digao
Coalescing agent Butyl Gutian chemical industry
Embodiment 1
The sealing wax seal coat of quick-dry type woodenware described in the present embodiment, by percentage to the quality, composed of the following components: The wetting agent of the pH adjusting agent AMP-95,0.8wt% of water-borne Self-Crosslinked Acrylic latex A C2742,0.15wt% of 36wt% The volatile type solvent of the defoaming agent Tego902w, 51.55wt% of Tego4100,1.5wt%, wherein the volatile type solvent The ethanol solution for being 95wt% for concentration, the coalescing agent butyl of 10wt%.
Embodiment 2
The sealing wax seal coat of quick-dry type woodenware described in the present embodiment, by percentage to the quality, composed of the following components: Water-borne Self-Crosslinked Acrylic the lotion XK12,0.11wt% of water-borne Self-Crosslinked Acrylic latex A C3600,15wt% of 16wt% PH adjusting agent AMP-95,0.21wt% wetting agent Tego4100,0.32wt% wetting agent Tego280,0.52wt%'s The volatile type solvent of the defoaming agent Tego825,60.5wt% of defoaming agent Tego902w, 0.62wt%, wherein described volatile Type solvent is the ethanol solution that concentration is 95wt%, the coalescing agent butyl of 6.72wt%.
Embodiment 3
The sealing wax seal coat of quick-dry type woodenware described in the present embodiment, by percentage to the quality, composed of the following components: The pH of the self-crosslinkable polyurethane dispersions R9029,0.06wt% of self-crosslinkable polyurethane dispersions R2180,15wt% of 10wt% The defoaming agent Tego902w's, 69.02wt% of the wetting agent Tego4100,0.52wt% of regulator AMP-95,0.4wt% easily waves Hair style solvent, wherein the volatile type solvent is the ethanol solution that concentration is 95wt%, the coalescing agent diethylene glycol of 5wt% Butyl ether.
In order to illustrate beneficial effect possessed by the present invention, the present invention also provides following comparative examples to carry out further Explanation.
Comparative example: the volatile type solvent whole equivalent in embodiment 2 is replaced with into water, other components are constant.
Performance test
To the seal coat that Examples 1 to 3 and comparative example 1 are prepared, it is tested for the property according to standard, test result As shown in table 1.
1 test result of table
Coating performance experiment
Further, the contrast sample group seal coat that Examples 1 to 3 is prepared being prepared with comparative example 1, According to following technique, coating is carried out to rubber wood timber and Manchurian ash (40cm*60cm), and be tested for the property, test result such as table 2 It is shown:
(1) deburring is first polished flat rubber wood timber and Manchurian ash with 240# sand paper;
(2) seal coat is uniformly mixed with deionized water according to mass ratio for 1:200;
(3) by the rubber wood timber that polishes flat in step (1) of seal coat even application being uniformly mixed in step (2) and On Manchurian ash, wait for quietly 4 hours;
(4) again with 400# sand paper by step (3) through first spraying after rubber wood timber and Manchurian ash polish flat;
(5) by the rubber wood timber that polishes flat in step (4) of seal coat even application being uniformly mixed in step (2) and On Manchurian ash, wait for quietly 4 hours;
(6) again with 600# sand paper by step (5) after second sprays rubber wood timber and Manchurian ash polish flat, wait for quietly 5 hours;
(7) one-component white finish paint even application is obtained into coating on through step (6) treated rubber wood timber and Manchurian ash Good template.
(8) after the template for installing painting is 7 days dry, template is placed in 60 degree of baking oven and is toasted 24 hours, template bleeding is observed Situation.
2 coating performance experimental result of table
It is above-mentioned the experimental results showed that, water-borne Self-Crosslinked Acrylic lotion or self-crosslinkable polyurethane dispersions are in solvent alcohol In the presence of, it interacts with coalescing agent, the sealing effect of product can be greatly improved.
Obviously, the above embodiments are merely examples for clarifying the description, and does not limit the embodiments.It is right For those of ordinary skill in the art, can also make on the basis of the above description it is other it is various forms of variation or It changes.There is no necessity and possibility to exhaust all the enbodiments, and it is extended from this it is obvious variation or It changes among still in the invention scope of protection of the claims.

Claims (6)

1. a kind of quick-dry type woodenware sealing wax seal coat, which is characterized in that by percentage to the quality, composed of the following components: 25- 35% water-borne Self-Crosslinked Acrylic lotion or self-crosslinkable polyurethane dispersions, the pH adjusting agent of 0.05-0.15%, 0.3- 0.8% wetting agent, the defoaming agent of 0.5-1.5%, the volatile type solvent of 50-70%, 5~10% coalescing agent.
2. quick-dry type woodenware sealing wax seal coat according to claim 1, which is characterized in that by mass percentage, by following Group is grouped as: 31% water-borne Self-Crosslinked Acrylic lotion or self-crosslinkable polyurethane dispersions, 0.11% PH regulator, 0.53% wetting agent, 1.14% defoaming agent, 60.5% volatile type solvent, 6.72% coalescing agent.
3. quick-dry type woodenware sealing wax seal coat according to claim 1 or claim 2, which is characterized in that when selection waterborne self-crosslinkable When acrylic emulsion, the water-borne Self-Crosslinked Acrylic lotion is without APEO, and solid content is the waterborne self-crosslinkable of 35-40wt% Acrylic emulsion.
4. quick-dry type woodenware sealing wax seal coat according to claim 1 or claim 2, which is characterized in that when the selection poly- ammonia of self-crosslinking When ester dispersion, the self-crosslinkable polyurethane dispersions are the self-crosslinkable polyurethane point that solid content is 35-40wt% without APEO Granular media.
5. any quick-dry type woodenware sealing wax seal coat according to claim 1~4, which is characterized in that the wetting agent is Polyether siloxane copolymer or Shuangzi structural silicone;Defoaming agent is polyether siloxane copolymer lotion;Volatile type solvent is Ethyl alcohol;Coalescing agent is butyl.
6. the preparation method of any quick-dry type woodenware sealing wax seal coat of Claims 1 to 5, includes the following steps:
(1) proportion is pressed, successively by water-borne Self-Crosslinked Acrylic lotion, defoaming agent is added to the container stirring, revolving speed 800- 1000r/min stirs 15min;
(2) PH regulator, stirring is added, revolving speed 500-800r/min stirs 5min;
(3) wetting agent, stirring is added, revolving speed 800-1000r/min stirs 15min;
(4) coalescing agent and solvent is added, speed of agitator 1000-1200r/min stirs 20min;4 glasss of measurements are applied, 23-25 takes the photograph Family name's degree range of viscosities obtained the quick-dry type woodenware sealing wax seal coat at 12-15 seconds.
CN201810227478.6A 2018-03-20 2018-03-20 A kind of quick-dry type woodenware sealing wax seal coat and preparation method thereof Pending CN110305545A (en)

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Application Number Priority Date Filing Date Title
CN201810227478.6A CN110305545A (en) 2018-03-20 2018-03-20 A kind of quick-dry type woodenware sealing wax seal coat and preparation method thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112063285A (en) * 2020-09-05 2020-12-11 合肥科天水性科技有限责任公司 Water-based rib-swelling primer and application method thereof
CN115975448A (en) * 2023-01-06 2023-04-18 广西化工研究院有限公司 Water-based loudspeaker box sprinkling paint

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008150294A1 (en) * 2007-06-06 2008-12-11 Valspar Sourcing, Inc. Single pack low temperature bake coating composition
CN102311689A (en) * 2010-07-06 2012-01-11 河北晨阳工贸集团有限公司 Water-based reflective landmark coating and preparation method thereof
CN104177939A (en) * 2014-09-05 2014-12-03 上海展辰涂料有限公司 Room-temperature self-crosslinking wood lacquer emulsion and preparation method thereof
CN104927527A (en) * 2015-07-14 2015-09-23 刘善江 Carpentry water paint suitable for high pressure airless spraying and preparation method thereof
CN105175621A (en) * 2015-10-13 2015-12-23 上海展辰涂料有限公司 Normal-temperature-self-crosslinking woodenware paint emulsion and preparation method therefor
CN107353793A (en) * 2017-06-16 2017-11-17 河北晨阳工贸集团有限公司 A kind of zero VOC woodenware sealing wax and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008150294A1 (en) * 2007-06-06 2008-12-11 Valspar Sourcing, Inc. Single pack low temperature bake coating composition
CN102311689A (en) * 2010-07-06 2012-01-11 河北晨阳工贸集团有限公司 Water-based reflective landmark coating and preparation method thereof
CN104177939A (en) * 2014-09-05 2014-12-03 上海展辰涂料有限公司 Room-temperature self-crosslinking wood lacquer emulsion and preparation method thereof
CN104927527A (en) * 2015-07-14 2015-09-23 刘善江 Carpentry water paint suitable for high pressure airless spraying and preparation method thereof
CN105175621A (en) * 2015-10-13 2015-12-23 上海展辰涂料有限公司 Normal-temperature-self-crosslinking woodenware paint emulsion and preparation method therefor
CN107353793A (en) * 2017-06-16 2017-11-17 河北晨阳工贸集团有限公司 A kind of zero VOC woodenware sealing wax and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112063285A (en) * 2020-09-05 2020-12-11 合肥科天水性科技有限责任公司 Water-based rib-swelling primer and application method thereof
CN112063285B (en) * 2020-09-05 2021-11-30 合肥科天水性科技有限责任公司 Water-based rib-swelling primer and application method thereof
CN115975448A (en) * 2023-01-06 2023-04-18 广西化工研究院有限公司 Water-based loudspeaker box sprinkling paint

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