CN110286435A - A kind of ultraviolet polarization splitting prism and preparation method thereof - Google Patents

A kind of ultraviolet polarization splitting prism and preparation method thereof Download PDF

Info

Publication number
CN110286435A
CN110286435A CN201910487168.2A CN201910487168A CN110286435A CN 110286435 A CN110286435 A CN 110286435A CN 201910487168 A CN201910487168 A CN 201910487168A CN 110286435 A CN110286435 A CN 110286435A
Authority
CN
China
Prior art keywords
prism
ultraviolet
film
cuboid
polarization splitting
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910487168.2A
Other languages
Chinese (zh)
Inventor
曾爱军
周如意
朱玲琳
胡敬佩
张冲
黄惠杰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Institute of Optics and Fine Mechanics of CAS
Original Assignee
Shanghai Institute of Optics and Fine Mechanics of CAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Institute of Optics and Fine Mechanics of CAS filed Critical Shanghai Institute of Optics and Fine Mechanics of CAS
Priority to CN201910487168.2A priority Critical patent/CN110286435A/en
Publication of CN110286435A publication Critical patent/CN110286435A/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B27/00Optical systems or apparatus not provided for by any of the groups G02B1/00 - G02B26/00, G02B30/00
    • G02B27/28Optical systems or apparatus not provided for by any of the groups G02B1/00 - G02B26/00, G02B30/00 for polarising
    • G02B27/283Optical systems or apparatus not provided for by any of the groups G02B1/00 - G02B26/00, G02B30/00 for polarising used for beam splitting or combining
    • GPHYSICS
    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B5/00Optical elements other than lenses
    • G02B5/30Polarising elements

Landscapes

  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Polarising Elements (AREA)
  • Optical Elements Other Than Lenses (AREA)

Abstract

A kind of ultraviolet polarization splitting prism and preparation method thereof; it is characterized in that; the cuboid prism cementing identical and of same size by two block lengths forms, and the cemented surface of one of cuboid prism is successively coated with the polarization beam splitter and silicon dioxide protective film for introducing optical grating construction.The polarization beam splitter for introducing optical grating construction dielectric grating as made of gluing, exposure, development etching and film structure are deposited to obtain.The present invention has many advantages, such as that extinction ratio is high, ranges of incidence angles is big, stability is good, is mainly used in ultraviolet, deep ultraviolet band.

Description

A kind of ultraviolet polarization splitting prism and preparation method thereof
Technical field
The invention belongs to optical device fields, and in particular to a kind of ultraviolet polarization splitting prism and preparation method thereof.
Technical background
Incident light can be divided into the mutually perpendicular linearly polarized light of two beams by polarization splitting prism: S light and P light, wherein P luminous energy is complete Full by, and S light is reflected with 45 degree of angles, to achieve the purpose that be polarized and be divided.Compared with crystal beam splitter, polarization Amici prism has big, insensitive to the incident angle advantage of the light beam angle of departure, and be widely used in high power laser light occasion with And precision optical instrument.
A kind of first technology [1] " polarization splitting prism of High Extinction Ratio " (CN202362476U) proposes a kind of polarization spectro rib Mirror plates polarizing beam splitting film on the inclined-plane of two right-angle prisms, with optical glue by inclined-plane edge-jointing adhesive altogether, remaining light pass surface Plate anti-reflection film.The inventive structure is simple, at low cost, but can not be applied to ultraviolet, deep ultraviolet band, because optical glue is in purple Wave section transmitance is very low, can also generate pollution.
A kind of first technology [2] " ultraviolet high-performance polarization light splitting prism " (CN102495437A) proposes a kind of ultraviolet polarization point The angle of a pair of of triangular prism is processed into Brewster's angle by light prism, is coated with polarization spectro on a pair of of Brewster face Film, two faces are docked using air-gap.The invention can be applied to ultraviolet, but extinction ratio is not high, and ranges of incidence angles is small.
Summary of the invention
It is an object of the invention in view of the above shortcomings of the prior art, provide a kind of ultraviolet polarization splitting prism and its system Preparation Method can be applied to ultraviolet, deep ultraviolet band, and extinction ratio is higher than general the Ultraviolet Polarizing, and ranges of incidence angles is big, property It can stablize.
For above-mentioned goal of the invention, the technical solution adopted by the present invention are as follows:
A kind of ultraviolet polarization splitting prism, it is characterized in that, by including the identical and of same size cuboid of two block lengths Prism cementing forms, and the cemented surface of one of cuboid prism is successively coated with the polarization beam splitter and two for introducing optical grating construction Silica protective film.
The polarization beam splitter for introducing optical grating construction dielectric grating and membrane system as made of gluing, exposure, development etching Structure is deposited to obtain.
The film structure is successively alternately made of lanthanum fluoride layer and magnesium fluoride layer.
The material of the cuboid prism is ultraviolet vitreous silica, CaF2
The present invention also provides a kind of preparation methods of ultraviolet polarization splitting prism, it is characterized in that, include the following steps:
The cuboid prism that step 1) selects two block lengths identical and of same size, chooses two pieces of cuboid prism area phases Same any surface is polished;
Step 2) plated on the wherein burnishing surface of one piece of cuboid prism set introduce optical grating construction polarization beam splitter, and The outer applying silicon oxide protective film of polarization beam splitter;
The burnishing surface of another piece of cuboid prism is contacted placement with silicon dioxide protective film by step 3) relatively, and is removed and connect The bubble of contacting surface carries out optical cement, makes two pieces of cuboid prism cementings;
Part after gluing is put into high temperature furnace and is bonded by step 4), and bonding temperature is 200~300 DEG C, after being bonded Natural cooling.
The preparation method of the ultraviolet polarization splitting prism, which is characterized in that further include:
The cuboid prism that gluing is integrated by step 5) is respectively cut up and down using cemented surface as diagonal plane as right-angle prism Shape polishes two pairs of right-angle surfaces.
Step 6) is according to use demand, and plating sets anti-reflection film in two pairs of right-angle surfaces of polished processing, or only selects wherein one Anti-reflection film is set to right-angle surface plating.
Further, plating sets the polarization beam splitter for introducing optical grating construction on burnishing surface in the step 2), and detailed process is such as Under:
Step 2.1) cleaning polishing face, photoresist is spun on burnishing surface, forms photoresist layer;
Step 2.2) is exposed using ultraviolet light by mask plate photolithography film surface, is then removed exposed Photoresist layer retains the photoresist layer of unexposed portion;
Step 2-3) to unglazed photoresist covering fused quartz prism perform etching after, remove photoresist, obtain dielectric grating (102);
Step 2-4) film structure (103) are finally vertically deposited on dielectric grating, obtain the polarization for introducing optical grating construction Spectro-film (101).
Further, in the step 3) in the unsuccessful situation of optical cement, silica is protected with silica flour solubilizer Film surface carries out manual fine polishing to improve surface smoothness, to increase the optical cement probability of success.
Compared with prior art, technical effect of the invention are as follows:
By introducing nanometer grating structure in polarization beam splitter, Film Design freedom degree is increased, can effectively be increased The extinction ratio of big polarization splitting prism, the problem of improving the incidence angle limitation of common ahrens prism;Introducing the inclined of optical grating construction It is coated with silica dioxide medium film outside vibration spectro-film, not only can protect optical grating construction, it can also be by being carried out by hand to coated surface Fine polishing processing improves surface smoothness, increases optical cement success rate, to improve yield rate;Thermal bonding work is used in optical cement process Skill is having vibration, the temperature difference so that bonding face is able to maintain long-term good air-tightness and firmness, and independent of temperature variations Larger, high-power occasion is equally able to maintain compared with stable performance.
Detailed description of the invention
Fig. 1 is the flow chart for carrying out plated film to one piece of cuboid prism and introducing optical grating construction
Fig. 2 is that the prism after plated film is carried out optical cement with another cuboid prism to be bonded and be cut into finished product, plating anti-reflection film Schematic diagram
Fig. 3 is the structural schematic diagram of the ultraviolet polarization splitting prism of the present invention
Specific embodiment
Below with reference to embodiment and attached drawing, the invention will be further described, but protection model of the invention should not be limited with this It encloses.
A kind of ultraviolet polarization splitting prism the production method is as follows:
Fig. 1 is the flow chart for carrying out plated film to cuboid prism 10 and introducing optical grating construction.
The cuboid prism 10 and 20 that step 1) selects two block lengths identical and of same size, material are ultraviolet tekite English respectively polishes the opposite face of prism 10 and prism 20, to reach the surface figure accuracy and smoothness requirements of optical cement needs;
After step 2) cleans the burnishing surface of prism 10, photoresist is spun on formation photoresist layer 105 on face;Using ultraviolet Light is exposed photoresist by mask plate irradiation light photoresist surface, then removes exposed photoresist layer, and reservation does not expose The photoresist layer of light part;Then after being performed etching to the fused quartz prism of unglazed photoresist covering, photoresist is removed, medium is obtained Grating 102;Film structure 103 is finally vertically deposited on dielectric grating, has obtained the polarization beam splitter for introducing optical grating construction 101, and in the outer applying silicon oxide protective film 104 of polarization beam splitter 101.
Fig. 2 is that the prism after plated film is carried out optical cement with another cuboid prism, is bonded and is cut into finished product, plating anti-reflection film Schematic diagram.
The burnishing surface of cuboid prism 20 is contacted placement relatively with silicon dioxide protective film by step 3), removes contact surface Bubble carries out optical cement.In the unsuccessful situation of optical cement, manual fine polishing is carried out to photo-adhesive surface with silica flour solubilizer to improve surface Finish, it is thin by hand because being coated with silicon dioxide protective film 104 outside polarization beam splitter 101 to increase optical cement success rate Throwing will not destroy film structure 103.
Monolith part is placed in high temperature furnace after the completion of step 4) optical cement and is bonded, temperature is set, to increase by tens every time Temperature is slowly increased to 280 DEG C, after the completion of heating by the mode of degree, is closed heating device and is carried out natural cooling, whole process is held Continue four day time.In the case where high-temperature heating, molecular motion accelerates, and the molecule of silicon dioxide layer interpenetrates, and reaches secured In conjunction with purpose.The setting of bonding temperature be not it is unalterable, if sample is more sensitive to high temperature, can reduce temperature interval, Baking maximum temperature is reduced, baking time is increased.
Part is taken out from high temperature furnace after step 5) natural cooling, using cemented surface as diagonal plane, be respectively cut up and down for Right-angle prism shape polishes two pairs of right-angle surfaces, obtains four light pass surfaces: the first right-angle surface, the second right-angle surface, and third is straight Edged surface, the 4th right-angle surface.
Step 6) is according to use demand, and plating sets anti-reflection film in four light pass surfaces.The anti-reflection film that four light pass surfaces are coated with Under the incident wavelength of 193.368nm, single side transmitance Tp﹥ 99.5%.
The structural schematic diagram of the ultraviolet polarization splitting prism of the present invention is as shown in figure 3, by the identical and width including two block lengths Identical cuboid prism cementing forms, and the cemented surface of cuboid prism 10 is successively coated with the polarization spectro for introducing optical grating construction Film 101 and silicon dioxide protective film 104;The polarization beam splitter 101 for introducing optical grating construction is etched by gluing, exposure, development Made of dielectric grating 102 and film structure 103 vapor deposition obtain.
The present invention uses above-mentioned technical solution, by introducing nanometer grating structure in polarization beam splitter, increases film It is design freedom, can effectively increases the extinction ratio of polarization splitting prism, improves the incidence angle limitation of common ahrens prism The problem of;Coated surface is bonded by optical cement and is fixed, and can be applied in ultraviolet, deep ultraviolet band, and sets silica guarantor by plating Cuticula can effectively improve optical cement yield rate, and after high-temperature process, bonding face is able to maintain long-term good air-tightness and jail Soundness, and independent of temperature variations, vibration, the temperature difference be larger, high-power occasion is equally able to maintain compared with stable performance having.

Claims (8)

1. a kind of ultraviolet polarization splitting prism, which is characterized in that by including the identical and of same size cuboid rib of two block lengths Mirror gluing forms, and the cemented surface of one of cuboid prism is successively coated with the polarization beam splitter and dioxy for introducing optical grating construction SiClx protective film.
2. a kind of ultraviolet polarization splitting prism according to claim 1, it is characterised in that: described to introduce the inclined of optical grating construction Vibration spectro-film (101) dielectric grating as made of gluing, exposure, development, etching (102) is obtained with film structure (103) vapor deposition.
3. a kind of ultraviolet polarization splitting prism according to claim 2, it is characterised in that: the film structure (103) by Lanthanum fluoride layer and magnesium fluoride layer are successively alternately constituted.
4. a kind of ultraviolet polarization splitting prism according to claim 1, it is characterised in that: the material of the cuboid prism For ultraviolet vitreous silica, CaF2
5. a kind of preparation method of ultraviolet polarization splitting prism, which comprises the steps of:
The cuboid prism that step 1) selects two block lengths identical and of same size, it is identical to choose two pieces of cuboid prism areas Any surface is polished;
Step 2) plates the polarization beam splitter for setting and introducing optical grating construction on the wherein burnishing surface of one piece of cuboid prism, and is polarizing The outer applying silicon oxide protective film (104) of spectro-film (101);
The burnishing surface of another piece of cuboid prism is contacted placement relatively with silicon dioxide protective film by step 3), and removes contact surface Bubble, carry out optical cement, make two pieces of cuboid prism cementings;
Part after gluing is put into high temperature furnace and is bonded by step 4), and bonding temperature is 200~300 DEG C, natural after being bonded It is cooling.
6. the preparation method of ultraviolet polarization splitting prism according to claim 5, which is characterized in that further include
The cuboid prism that gluing is integrated by step 5) is respectively cut up and down using cemented surface as diagonal plane as right-angle prism shape Shape polishes right-angle surface.
Step 6) is according to use demand, and plating sets anti-reflection film in two pairs of right-angle surfaces of polished processing, or only selection one pair of them are straight Edged surface plating sets anti-reflection film.
7. the preparation method of ultraviolet polarization splitting prism according to claim 5, which is characterized in that in the step 2) Plating sets the polarization beam splitter for introducing optical grating construction on burnishing surface, and detailed process is as follows:
Step 2.1) cleaning polishing face, photoresist is spun on burnishing surface, is formed photoresist layer (105);
Step 2.2) is exposed using ultraviolet light by mask plate photolithography film surface, and exposed photoetching is then removed Glue-line retains the photoresist layer of unexposed portion;
Step 2-3) to unglazed photoresist covering fused quartz prism perform etching after, remove photoresist, obtain dielectric grating (102);
Step 2-4) film structure (103) are finally vertically deposited on dielectric grating, obtain the polarization spectro for introducing optical grating construction Film (101).
8. the preparation method of ultraviolet polarization splitting prism according to claim 5, which is characterized in that in the step 3) when In the unsuccessful situation of optical cement, manual fine polishing is carried out to silicon dioxide protective film face with silica flour solubilizer to improve any surface finish Degree, to increase the optical cement probability of success.
CN201910487168.2A 2019-06-05 2019-06-05 A kind of ultraviolet polarization splitting prism and preparation method thereof Pending CN110286435A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910487168.2A CN110286435A (en) 2019-06-05 2019-06-05 A kind of ultraviolet polarization splitting prism and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910487168.2A CN110286435A (en) 2019-06-05 2019-06-05 A kind of ultraviolet polarization splitting prism and preparation method thereof

Publications (1)

Publication Number Publication Date
CN110286435A true CN110286435A (en) 2019-09-27

Family

ID=68003411

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910487168.2A Pending CN110286435A (en) 2019-06-05 2019-06-05 A kind of ultraviolet polarization splitting prism and preparation method thereof

Country Status (1)

Country Link
CN (1) CN110286435A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112764149A (en) * 2021-01-08 2021-05-07 中国科学院上海光学精密机械研究所 Deep ultraviolet flat plate polarization spectroscope and design method thereof
CN114853355A (en) * 2022-04-08 2022-08-05 常州市万华激光科技有限公司 Preparation method of ultraviolet 193nm antireflection film

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1186301A (en) * 1996-11-13 1998-07-01 松下电器产业株式会社 Prism lens and optical sensor using the prism lens
CN1567002A (en) * 2003-06-10 2005-01-19 武汉光迅科技有限责任公司 Nano level grating for polarization beam division / combination and method for making same
CN101295076A (en) * 2007-04-29 2008-10-29 晶荧光学科技有限公司 Polarization spectroscopic device and projection display device using the same
CN202102135U (en) * 2011-07-08 2012-01-04 福州高意光学有限公司 Deep-ultraviolet, visual and near-infrared polarizing prism
CN105814464A (en) * 2013-12-05 2016-07-27 业纳光学系统有限公司 Polarization system
US20170285237A1 (en) * 2015-02-06 2017-10-05 Moxtek, Inc. High Contrast Inverse Polarizer
CN108919408A (en) * 2018-07-16 2018-11-30 福州海创光学有限公司 High refractive index polarization splitting prism

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1186301A (en) * 1996-11-13 1998-07-01 松下电器产业株式会社 Prism lens and optical sensor using the prism lens
CN1567002A (en) * 2003-06-10 2005-01-19 武汉光迅科技有限责任公司 Nano level grating for polarization beam division / combination and method for making same
CN101295076A (en) * 2007-04-29 2008-10-29 晶荧光学科技有限公司 Polarization spectroscopic device and projection display device using the same
CN202102135U (en) * 2011-07-08 2012-01-04 福州高意光学有限公司 Deep-ultraviolet, visual and near-infrared polarizing prism
CN105814464A (en) * 2013-12-05 2016-07-27 业纳光学系统有限公司 Polarization system
US20170285237A1 (en) * 2015-02-06 2017-10-05 Moxtek, Inc. High Contrast Inverse Polarizer
CN108919408A (en) * 2018-07-16 2018-11-30 福州海创光学有限公司 High refractive index polarization splitting prism

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
张立超: ""极紫外多层膜光栅技术研究进展"", 《光机电信息》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112764149A (en) * 2021-01-08 2021-05-07 中国科学院上海光学精密机械研究所 Deep ultraviolet flat plate polarization spectroscope and design method thereof
CN114853355A (en) * 2022-04-08 2022-08-05 常州市万华激光科技有限公司 Preparation method of ultraviolet 193nm antireflection film

Similar Documents

Publication Publication Date Title
US5846638A (en) Composite optical and electro-optical devices
CN110286435A (en) A kind of ultraviolet polarization splitting prism and preparation method thereof
WO2012149826A1 (en) Optical coupling device having kbbf group crystal coupled with prisms and method for manufacturing same
CN102707461B (en) Manufacturing method of polarization-independent optical isolator, bonding technology and solution of optical components
JP2001201636A (en) Optical fiber polarizer and method its manufacturing
CN105717564B (en) Depolarization pentagonal prism and preparation method thereof
JP2018526316A (en) Method for producing optical element
CN108919408A (en) High refractive index polarization splitting prism
CN102081178B (en) Method for manufacturing micro ladder reflecting mirror by sequentially arranging substrates on wedge block
CN102081179B (en) Method for orderly arranging angle substrates to manufacture micro-step reflecting mirror
US20110062111A1 (en) Method of fabricating microscale optical structures
CN209086573U (en) Laser depolarization light-dividing device
CN109143597A (en) Laser depolarization light-dividing device
CN212965498U (en) Adhesive wave plate
CN100349047C (en) Passivation protection method for silicon-based liquid crystal aluminum reflecting electrode
CN106047171B (en) Abies balsam protective agent and with abies balsam protective agent make lithium niobate crystal blade technolgy
JP3476095B2 (en) Connection method between optical waveguide and optical fiber
CN115166989B (en) Laser beam shrinking device
JP2003227931A (en) Polarizer incorporating optical component, method of manufacturing the same and method of combining linearly polarized wave using the same
CN109613648B (en) Preparation method of full-crystal waveguide coupler
CN107933052B (en) Manufacturing tool for cascade thin film substrate bonding body and manufacturing method for optical device
CN117388974A (en) True zero-order half-wave plate applied to 266nm and processing method thereof
CN118851087A (en) Standard manufacturing method of silicon carbide for anodic bonding atomic gas chamber
CN109116461A (en) A kind of DUV wide spectrum is without the glue polarizer
CN118838068A (en) Protection device and method applied to glass-based polarization beam splitting film

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20190927