CN110284348A - A kind of production technology for the fabric varying with temperature color - Google Patents
A kind of production technology for the fabric varying with temperature color Download PDFInfo
- Publication number
- CN110284348A CN110284348A CN201910567991.4A CN201910567991A CN110284348A CN 110284348 A CN110284348 A CN 110284348A CN 201910567991 A CN201910567991 A CN 201910567991A CN 110284348 A CN110284348 A CN 110284348A
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- fabric
- color
- temperature
- vary
- polypropylene film
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/26—Thermosensitive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/003—Transfer printing
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Textile Engineering (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses the production technologies that one kind can vary with temperature the fabric of color, are related to the technical field of color-changing face fabric, comprise the following steps that: S1: spraying allochroic paint on a side surface of bidirectional stretching polypropylene film；S2: the bidirectional stretching polypropylene film after spraying allochroic paint is sent into baking and curing in baking oven；S3: adhesive is coated on the transfer surface of fabric to be processed；S4: the side that the bidirectional stretching polypropylene film after drying is coated with allochroic paint is bonded with the transfer surface of fabric, then by bidirectional stretching polypropylene film hot pressing on fabric；S5: just it is removed from web surface after the bidirectional stretching polypropylene film in step S4 is with fabric hot pressing；By the fabric for obtaining to vary with temperature color after above-mentioned 5 steps.The present invention improves the effect of color-changing face fabric production convenience with cost is reduced.
Description
Technical field
The present invention relates to the technical fields of color-changing face fabric, and the life of the fabric of color can be varied with temperature more particularly, to one kind
Production. art.
Background technique
Fabric is essential a kind of articles in human lives, with the improvement of living standards, people are for fabric
Requirement also increasingly promoted, in particular for make clothes fabric.
People usually require that there is the characteristics such as soft, comfortable, ventilative, sliding bullet for making the fabric of clothes, so that not
Dress with occasion clothes can have preferable comfort.It is even more on the market at present the clothes for changeable colour occur, different
Different colors can be shown at temperature and environment, to adapt to different environment to increase aesthetic feeling.
But the manufacture craft of the clothes of this changeable colour is usually first to carry out chromotropic dye dyeing in clothes raw fibre
Then the fabric of production clothes is weaved into processing again.This manufacture craft needs are handled from the material of fabric, when need
Otherwise with color-changing face fabric when, need to be changed from material, complex, consuming cost is excessively high.
Summary of the invention
In view of the deficiencies of the prior art, the present invention intends to provide a kind of fabric that can vary with temperature color
Production technology, by the way that allochroic paint to be transferred on fabric with bidirectional stretching polypropylene film, so that fabric is become
The performance of color, production process is convenient and efficient, and cost consumption is low.
Above-mentioned purpose of the invention has the technical scheme that
A kind of production technology for the fabric varying with temperature color, comprises the following steps that:
S1: allochroic paint is sprayed on a side surface of bidirectional stretching polypropylene film；
S2: the bidirectional stretching polypropylene film after spraying allochroic paint is sent into baking and curing in baking oven；
S3: adhesive is coated on the transfer surface of fabric to be processed；
S4: the side that the bidirectional stretching polypropylene film after drying is coated with allochroic paint is bonded with the transfer surface of fabric,
Then by bidirectional stretching polypropylene film hot pressing on fabric；
S5: just it is removed from web surface after the bidirectional stretching polypropylene film in step S4 is with fabric hot pressing；
By the fabric for obtaining to vary with temperature color after above-mentioned 5 steps.
By using above-mentioned technical proposal, allochroic paint, which is first sprayed on bidirectional stretching polypropylene film, to be solidified, so
The side and fabric for cured allochroic paint and bidirectional stretching polypropylene film not being bonded by adhesive again afterwards are bonding,
Since adhesive strength is much larger than the bonding between allochroic paint and bidirectional stretching polypropylene film between adhesive and allochroic paint
Intensity, so after allochroic paint and fabric are bonding, while can be enterprising from allochroic paint by bidirectional stretching polypropylene film
Row removing, so that allochroic paint layer is transferred to web surface, so that fabric obtains the property that color change occurs with environment temperature
Energy.With existing compared with the fabric manufacture craft that material carries out discoloration processing, color-changing face fabric production process of the invention is more
Adding quick and easy, and can be carried out on different fabrics discoloration processing, limitation is smaller, and discoloration processing is more flexible, and
The present invention is more accurate compared with prior art for the control of the amount of allochroic paint during transferring allochroic paint, from
And reduce the consumption in cost.
The present invention is further arranged to: the allochroic paint in the step S1 includes the component of following parts by weight:
By using above-mentioned technical proposal, warm color-change powder is a kind of electron transfer type organic compound body of microencapsulation
System, this kind of compound makes the molecular structure of the organic matter change because of electronics transfer at a certain temperature, to realize color
Transformation, capsule particle protect electrochromic substance from the erosion of other chemical substances.
Color spreading agent is mainly used for playing finely dispersed effect in a solvent to the warm color-change powder in allochroic paint system.Exhibition
The color development principle of toner generally includes wetting, grinding and dispersion three phases, warm color-change powder primary particle and is in upper state, is easy
Assemble, so that warm color-change powder particle aggregation is at the degree that cannot disperse in color spreading agent, and the particle reunited at these
The adsorption substances such as air and moisture, hinder the contact between color spreading agent and warm color-change powder, and color spreading agent is arranging air
And the process of moisture is exactly wet processes.The addition of wetting agent increases the wetting effect between color spreading agent and warm color-change powder,
So that color spreading agent is faster more comprehensively contacted with warm color-change powder surface.After wetting, warm color-change powder also needs to be ground to required partial size, makes
The colour developing quality for obtaining warm color-change powder reaches requirement.During the grinding process due to maintain certain shearing force, the addition of color spreading agent
Amount is always insufficient, so needing to increase color spreading agent after grinding and dispersing agent allows warm color-change powder to be steadily suspended in color development
In agent.
Levelling agent can promote in film forming procedure, form a smooth, smooth, uniform film.Polyurethane resin is
Main film forming matter plays the role of bonding each component in allochroic paint.
The present invention is further arranged to: the solvent is selected from butanone, ethyl acetate, cyclohexanone, toluene or different fluorine diketone
Arbitrarily compare mixture.
The present invention is further arranged to: the color spreading agent includes following components in percentage by weight:
By using above-mentioned technical proposal, rosin ester plays main wetting action, polyamide maleic two in color spreading agent
Sour di-sec-octyl sodium sulfonate is fast penetrant T, and each component in color spreading agent and the wetting contact between warm color-change powder are risen
To certain synergistic effect.Butene dioic acid di-sec-octyl sodium sulfonate is during allochroic paint is mixed simultaneously, for applying
Dispersing agent and levelling agent in material all play certain synergistic effect, improve the quality of allochroic paint.
The present invention is further arranged to: the wetting agent includes following components in percentage by weight:
C13Branched secondary alcohol polyoxyethylene ether 20~45%；
C6Fluorocarbon surfactant 50~70%；
Perfluoro octyl sulfonic acid potassium 5~8%.
By using above-mentioned technical proposal, C6Fluorocarbon surfactant and C13What branched secondary alcohol polyoxyethylene ether compatibility was formed
System forms mixed adsorption layer in oil-water interfaces, and due to the mutual thin property between fluorocarbon chain and hydrocarbon chain, molecules align may be
Bimolecular structure, the fluorocarbon chain on upper layer align closely, and hydrocarbon chain lies low or cross arrangement is under fluorocarbon chain oriented layer, C13Branch
The hydrophilic group of chain secondary alcohol polyoxyethylene ether then towards in water, forms the side of fine and close hydrocarbon chain adsorption layer pasta at interface, because
And the interfacial tension of grease is reduced significantly, so that the interfacial tension on warm color-change powder surface reduces, raising and color spreading agent
Between wetting effect.And the addition of a small amount of perfluoro capryl spring acid potassium can reduce C to a certain extent6Fluorocarbon surfactant
With C13The surface tension and interfacial tension for the system that branched secondary alcohol polyoxyethylene ether compatibility is formed.
The present invention is further arranged to: the levelling agent includes following components in percentage by weight:
Diacetone alcohol 25~30%；
Fluorine-containing organic silicon acrylate 30~50%；
Dimethyl silicone polymer 20~40%.
Through the above technical solutions, levelling agent can promote in film forming procedure, formation one is smooth, smooth, uniform
Film.Diacetone alcohol, fluorine-containing organic silicon acrylate and dimethyl silicone polymer are three kinds of different types of levelling agents, three it
Between can play the role of mutually supplying.
The present invention is further arranged to: the dispersing agent is selected from tristerin, fatty alcohol polyoxyethylene ether, dodecane
Base sodium sulfonate or any of Sodium Polyacrylate compare mixture.
The present invention is further arranged to: the manufacture craft of the allochroic paint the following steps are included:
Step (1): warm color-change powder, dispersing agent and butanone are mixed according to the ratio, then add the color development of 3/5 first wife's ratio
12~20h is impregnated in agent, wetting.
Step (2): polyurethane resin is added according to the ratio in the mixture in step (1), then stirs evenly；It is to be mixed
After uniformly, required fineness is ground the material to；
Step (3): the color spreading agent of 2/5 first wife's ratio will be added in step (2) treated mixture, then stream is added according to the ratio
Flat agent, then stirs evenly, and allochroic paint is obtained after refiltering.
By using above-mentioned technical proposal, allochroic paint first adds the color spreading agent of a part, so in production in step (1)
Latter part of color spreading agent is added in step (3) again afterwards, so that the warm color-change powder in step (2) during grinding
Biggish shearing force can be obtained.
Compared with prior art, the beneficial effects of the present invention are:
1, by the way that allochroic paint to be transferred on fabric with bidirectional stretching polypropylene film, so that fabric is changed colour
Performance, production process is more convenient, and cost consumption is low；
2, by adding wetting agent in allochroic paint so that allochroic paint is when preparing, color spreading agent and warm color-change powder it
Between contact it is more abundant, improve dispersion and color development effect.
Detailed description of the invention
Fig. 1 is process flow chart of the invention.
Specific embodiment
With reference to the accompanying drawings and examples, the present invention will be described in detail.
Referring to Fig.1, one kind disclosed by the invention can vary with temperature the production technology of the fabric of color, including following technique
Step:
Early-stage preparations: allochroic paint production, comprising the following steps:
Prepare material:
Wherein color spreading agent includes following components in percentage by weight:
Wherein wetting agent includes following components in percentage by weight:
C13Branched secondary alcohol polyoxyethylene ether 22%
C6Fluorocarbon surfactant 70%；
Perfluoro octyl sulfonic acid potassium 8%.
Levelling agent includes following components in percentage by weight:
Diacetone alcohol 30%；
Fluorine-containing organic silicon acrylate 30%；
Dimethyl silicone polymer 40%.
Step (1): warm color-change powder, dispersing agent and butanone are mixed according to the ratio, then add the color development of 3/5 first wife's ratio
12h is impregnated in agent, wetting.
Step (2): polyurethane resin is added according to the ratio in the mixture in step (1), then stirs evenly；It is to be mixed
After uniformly, required fineness is ground the material to.
Step (3): the color spreading agent of 2/5 first wife's ratio will be added in step (2) treated mixture, then stream is added according to the ratio
Flat agent, then stirs evenly, and allochroic paint is obtained after refiltering.
Fabric production:
S1: allochroic paint is sprayed on a side surface of bidirectional stretching polypropylene film；
S2: the bidirectional stretching polypropylene film after spraying allochroic paint is sent into baking and curing in baking oven；
S3: adhesive is coated on the transfer surface of fabric to be processed；
S4: the side that the bidirectional stretching polypropylene film after drying is coated with allochroic paint is bonded with the transfer surface of fabric,
Then by bidirectional stretching polypropylene film hot pressing on fabric；
S5: just it is removed from web surface after the bidirectional stretching polypropylene film in step S4 is with fabric hot pressing.
Embodiment 2-5 the difference from embodiment 1 is that: each component is calculated by weight as following table in allochroic paint.
Embodiment 6-9 the difference from embodiment 1 is that: each component is following table by weight percentage in color spreading agent.
Embodiment 10-13 the difference from embodiment 1 is that: each component is following table by weight percentage in wetting agent.
Embodiment 14-17 the difference from embodiment 1 is that: each component is following table by weight percentage in levelling agent.
Embodiment 18-21 the difference from embodiment 1 is that: wetting soaking temperature be calculated as following table.
| Embodiment | Embodiment 18 | Embodiment 19 | Embodiment 20 | Embodiment 21 |
| Time (h) | 14 | 16 | 18 | 20 |
Embodiment 22-31 the difference from embodiment 1 is that: the component contained in solvent is calculated as following table.
| Embodiment | Butanone | Ethyl acetate | Cyclohexanone | Toluene | Different fluorine diketone |
| Embodiment 22 | Have | / | / | / | / |
| Embodiment 23 | / | Have | / | / | / |
| Embodiment 24 | / | / | Have | / | / |
| Embodiment 25 | / | / | / | Have | / |
| Embodiment 26 | / | / | / | / | Have |
| Embodiment 27 | / | Have | Have | / | / |
| Embodiment 28 | Have | / | / | Have | / |
| Embodiment 29 | Have | Have | / | / | Have |
| Embodiment 30 | / | Have | Have | Have | Have |
| Embodiment 31 | Have | Have | Have | Have | Have |
Comparative example
Comparative example 1 the difference from embodiment 1 is that: wetting agent is not added in allochroic paint；
Comparative example 2 the difference from embodiment 1 is that: C is not added in wetting agent13Branched secondary alcohol polyoxyethylene ether；
Comparative example 3 the difference from embodiment 1 is that: C is not added in wetting agent6Fluorocarbon surfactant；
Comparative example 4 the difference from embodiment 1 is that: perfluoro octyl sulfonic acid potassium is not added in wetting agent.
Detection method
Color development test
White slurry includes the component of following parts by weight:
40 parts of R type titanium dioxide；
56 parts of alkyd resin；
4 parts of calcium stearate.
The allochroic paint of Example 1~5, embodiment 10~13 and comparative example 1~4 weighs 0.12g respectively, and with
The white slurry of 3.0g is uniformly mixed, and is then arranged on colourless glass plates, with wet film prepare its they are pulled down it is not small with formation width
It is not less than the opaque band of uniform thickness of 40mm in 25mm, contact side length, is dabbed on each vitta with a finger, than
The difference of surface color depth relatively nuzzled up and do not nuzzled up, if there is apparent difference is recorded.Continue to not wiping
The surface crossed is tested, and is compared immediately by glass plate to tinctorial strength and form and aspect under scattering light or artificial daylight.
Wherein standard sample is comparative example 1.
If color intensity is equal identical with form and aspect, the relative color strength of given the test agent is 100%.
Such as tinctorial strength difference, then the amount of given the test agent dispersion is estimated, then change and prepare another water down after weighing
Mill base, and standard sample is constant, then is compared until tinctorial strength is equal.
It is 1-10 according to reaching with the difference of the quality of the sample of standard sample same colored intensity and standard sample quality
Grade, rank is bigger, and relative color strength and color development effect are poorer.
| Embodiment | Stain level |
| Embodiment 1 | 5 |
| Embodiment 2 | 4 |
| Embodiment 3 | 4 |
| Embodiment 4 | 3 |
| Embodiment 5 | 3 |
| Embodiment 10 | 4 |
| Embodiment 11 | 4 |
| Embodiment 12 | 3 |
| Embodiment 13 | 3 |
| Comparative example 1 | 7 |
| Comparative example 2 | 6 |
| Comparative example 3 | 6 |
| Comparative example 4 | 6 |
Conclusion: by upper table it is known that being added with Examples 1 to 5, embodiment 10~13 and the comparative example of wetting agent
2~4 color development effect and colorability does not add the comparative example 1 of wetting agent better than, illustrates exhibition of the wetting agent for warm color-change powder
Color effect has certain promotion synergistic effect.And it can be seen by the stain level of comparative example 2~4 and embodiment 10~13
Out, the C in wetting agent13Branched secondary alcohol polyoxyethylene ether and C6The increase of the additive amount of fluorocarbon surfactant is for wetting agent
Wetting effect has the effect of improving, so that color spreading agent becomes strong for the color development effect of warm color-change powder.
The above is only a preferred embodiment of the present invention, protection scope of the present invention is not limited merely to above-mentioned implementation
Example, all technical solutions belonged under thinking of the present invention all belong to the scope of protection of the present invention.It should be pointed out that for the art
Those of ordinary skill for, several improvements and modifications without departing from the principles of the present invention, these improvements and modifications
It should be regarded as protection scope of the present invention.
Claims (8)
1. the production technology that one kind can vary with temperature the fabric of color, which is characterized in that comprise the following steps that:
S1: allochroic paint is sprayed on a side surface of bidirectional stretching polypropylene film；
S2: the bidirectional stretching polypropylene film after spraying allochroic paint is sent into baking and curing in baking oven；
S3: adhesive is coated on the transfer surface of fabric to be processed；
S4: the side that the bidirectional stretching polypropylene film after drying is coated with allochroic paint is bonded with the transfer surface of fabric, then
By bidirectional stretching polypropylene film hot pressing on fabric；
S5: just it is removed from web surface after the bidirectional stretching polypropylene film in step S4 is with fabric hot pressing；
By the fabric for obtaining to vary with temperature color after above-mentioned 5 steps.
2. the production technology that one kind according to claim 1 can vary with temperature the fabric of color, it is characterised in that: described
Allochroic paint in step S1 includes the component of following parts by weight:
3. the production technology that one kind according to claim 2 can vary with temperature the fabric of color, it is characterised in that: described
Solvent is selected from any of butanone, ethyl acetate, cyclohexanone, toluene or different fluorine diketone and compares mixture.
4. the production technology that one kind according to claim 2 can vary with temperature the fabric of color, it is characterised in that: described
Color spreading agent includes following components in percentage by weight:
5. the production technology that one kind according to claim 2 can vary with temperature the fabric of color, it is characterised in that: described
Wetting agent includes following components in percentage by weight:
C13Branched secondary alcohol polyoxyethylene ether 20~45%；
C6Fluorocarbon surfactant 50~70%；
Perfluoro octyl sulfonic acid potassium 5~8%.
6. the production technology that one kind according to claim 2 can vary with temperature the fabric of color, it is characterised in that: described
Levelling agent includes following components in percentage by weight:
Diacetone alcohol 25~30%；
Fluorine-containing organic silicon acrylate 30~50%；
Dimethyl silicone polymer 20~40%.
7. the production technology that one kind according to claim 2 can vary with temperature the fabric of color, it is characterised in that: described
Dispersing agent is selected from any than mixed of tristerin, fatty alcohol polyoxyethylene ether, dodecyl sodium sulfate or Sodium Polyacrylate
Close object.
8. the production technology that one kind according to claim 1 can vary with temperature the fabric of color, it is characterised in that: described
The manufacture craft of allochroic paint the following steps are included:
Step (1): warm color-change powder, dispersing agent and butanone are mixed according to the ratio, then add the color spreading agent of 3/5 first wife's ratio, profit
Immersion steeps 12~20h.
Step (2): polyurethane resin is added according to the ratio in the mixture in step (1), then stirs evenly；It is to be mixed uniform
Afterwards, required fineness is ground the material to；
Step (3): the color spreading agent of 2/5 first wife's ratio will be added in step (2) treated mixture, then levelling is added according to the ratio
Then agent stirs evenly, allochroic paint is obtained after refiltering.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111514811A (en) * | 2020-03-26 | 2020-08-11 | 陕西驭腾实业有限公司 | Preparation method of asymmetric Gemini fluorocarbon surfactant |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111514811A (en) * | 2020-03-26 | 2020-08-11 | 陕西驭腾实业有限公司 | Preparation method of asymmetric Gemini fluorocarbon surfactant |
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