CN110284119A - A set of insulation cover for preventing heating plate edge thermal loss - Google Patents

A set of insulation cover for preventing heating plate edge thermal loss Download PDF

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Publication number
CN110284119A
CN110284119A CN201910663986.3A CN201910663986A CN110284119A CN 110284119 A CN110284119 A CN 110284119A CN 201910663986 A CN201910663986 A CN 201910663986A CN 110284119 A CN110284119 A CN 110284119A
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China
Prior art keywords
insulation cover
chamber
plate edge
cover
heating plate
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CN201910663986.3A
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CN110284119B (en
Inventor
金基烈
吴凤丽
谭华强
魏有雯
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Piotech Inc
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Piotech Shenyang Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating

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  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Chemical Vapour Deposition (AREA)

Abstract

The invention belongs to semiconductive thin film deposition applications and manufacturing technology fields, are related to a set of insulation cover for preventing heating plate edge thermal loss.Insulation cover setting is on cavity inner lining and heating plate edge, it include chamber inner wall insulation cover and heating dish side cover, it is one layer of setting three-dimensional insulation cover around heating dish (8) when doing film deposition that the chamber inner wall insulation cover, which is in the bottom, top, enclosure wall of chamber, the heating dish side cover is that one group of insulation cover, including edge insulation cover (9) and top insulation cover (10) are covered on heating dish (8).The purpose of the present invention is preventing from heating plate edge thermal loss in chamber, and guarantee that wafer process environment temperature is uniform, its quality is not influenced by temperature when making to deposit film very high on temperature requirement.

Description

A set of insulation cover for preventing heating plate edge thermal loss
Technical field
The invention belongs to semiconductive thin film deposition applications and manufacturing technology field, it is related to a set of preventing heating plate edge heat The insulation cover of loss.
Background technique
Currently, to meet process environments requirement in CVD equipment chamber, chamber indoor material is substantially aluminum or aluminium oxide ceramics, Chamber and upper cover plate are all by aluminium as basic material production, material property (preferable conduction of the aluminium oxide ceramics due to itself Property, mechanical strength and heat-resisting quantity, high-frequency insulation) and cost consideration can be used in specific position in chamber, to meet technique The demands such as required electrical property, radio frequency, temperature, cleanliness.
Cavity inner lining: in 400 DEG C or more of high-temperature technology environment, high work is required particularly with temperature uniformity Skill is used as its thermal insulation property of chamber inner wall using aluminium or aluminium oxide ceramics (thermal coefficient is 33W/ (mK), and heat is easy to lose) Or it cannot meet the requirements, it may appear that crystal circle center's temperature is higher than the phenomenon that edge (chamber inner wall heat loss), and then influences The uniformity of technique film thickness and other technological parameters, and the temperature for the chamber inner wall that changes with time also can be different (initial Shi Wendu is low, is slowly increased to stablize through temperature after a period of time), to influence the process repeatability and stack membrane of every group of wafer In every layer of repeatability.
Heating dish side cover: 1) in view of air-flow can take away heating plate edge heat, cause to heat plate edge and centre temperature Spend inconsistent phenomenon;2) in many cases if the distributed layout of bleeding point it is asymmetric but it is eccentric when will result in heating dish from The close position temperature of bleeding point is lower than the position remote from bleeding point;3) temperature of heating dish is a range, can have heat not The performance parameter of uniform phenomenon, this film that process deposits very sensitive to temperature are gone out is poor.
Summary of the invention
In order to solve the above-mentioned technical problem, technological temperature is uniform in holding chamber, and wafer is made to be in one always in operation stage In the uniform and stable environment of a temperature;Keep heating disk center uniform to lip temperature.
The purpose of the present invention is to provide a set of insulation covers for preventing heating plate edge thermal loss.
The purpose of the present invention can be achieved through the following technical solutions:
A set of insulation cover for preventing heating plate edge thermal loss, setting are wrapped on cavity inner lining and heating plate edge Chamber inner wall insulation cover and heating dish side cover are included, the chamber inner wall insulation cover is to exist in the bottom, top, enclosure wall of chamber One layer of three-dimensional insulation cover is set around the heating dish 8 when doing film deposition, and the heating dish side cover is to add in heating dish 8 One group of insulation cover of lid, including edge insulation cover 9 and top insulation cover 10.
The thermal coefficient of its material of three-dimensional insulation cover lower than 5W/ (mK) and can be used for film depositional environment.
The three-dimensional insulation cover is rotatable, can move with heating dish.
The chamber inner wall insulation cover specifically: the top of chamber is from the spray upper plate of shower plate 1 along chamber lid 6, chamber 7 Inner wall is equipped with one layer of heat preservation liner, respectively chamber lid insulating lining 3, chamber sidewall insulating lining 4, cavity bottom insulating lining 5.
The insulation cover further includes heating pan bottom insulation cover.
The edge insulation cover 9 is equipped with 0 ° -360 ° of opening.
The top insulation cover 10 is equipped with 0 ° -360 ° of covering.
Beneficial effects of the present invention:
It is uniform that a set of insulation cover for preventing heating plate edge thermal loss of the present invention is able to maintain intracavitary technological temperature, makes crystalline substance Circle is in the uniform and stable environment of temperature always in operation stage;Using poor thermal conductivity thermal coefficient < 5W/ (m K material) does chamber inner wall insulation cover;Chamber inner wall insulation cover 3 D stereo is covered in chamber, reaches thermal loss most It is small;Insulation cover that is rotatable, can moving with heating dish is covered on heating dish side, upper edge, bottom edge;Heat plate edge insulation cover Divide 2 parts: the heat preservation side ring with thermovent (0 ° -360 ° are differed) and insulated roof (0 ° -360 ° are differed) are used cooperatively;Heating dish Position of the edge insulation cover in heating dish can be adjusted as needed, is easy to install, is quick detachable, is reusable.
Detailed description of the invention
In order to facilitate the understanding of those skilled in the art, the present invention will be further described below with reference to the drawings.
Fig. 1 is cavity inner lining two dimension cross-sectional view of the present invention;
Fig. 2 is the structural schematic diagram of heating dish side cover three-dimensional figure of the present invention;
Fig. 3 is that the present invention covers temperature simulation schematic diagram before and after heating plate edge insulation cover;
A, heating dish (no insulation cover) temperature simulation figure B, in heating dish plus insulation cover (position such as left side) temperature simulation afterwards Figure
Fig. 4 is to cover heating dish side cover front and back plasma in the analogous diagram of heating dish Kernel density estimate;
A, nominal situation (no insulation cover);B, increase side insulation cover;C, increase top insulation cover;D, each operating condition is relatively close Degree;
Fig. 5 indicates the analysis chart that 3 points are taken in heating dish;
A, temperature when indicating heating dish P1 point without insulation cover;B, temperature when heating dish P1 point has insulation cover is indicated;
C, temperature when indicating heating dish P2 point without insulation cover;D, temperature when heating dish P2 point has insulation cover is indicated;
E, temperature when indicating heating dish P3 point without insulation cover;F, temperature when heating dish P3 point has insulation cover is indicated;
Fig. 6 is when yttrium stable zirconium oxide (YSZ) and aluminium oxide ceramics insulation cover is respectively adopted in chamber inner wall with respect to technique film Thick datagram;
Fig. 7 is that chamber inner wall increases process repeatability test data figure before and after insulation cover.
Specific embodiment
Embodiment 1
The structure composition of a set of insulation cover for preventing heating plate edge thermal loss: by cavity inner lining and heating dish side cover It forms, wherein cavity inner lining: as shown in Figure 1, being bottom, top, enclosure wall in chamber (i.e. in the heating for doing thin film deposition processes Around disk 8) increase the three-dimensional insulation cover that can be used for film depositional environment that one layer of thermal coefficient is lower than 5W/ (mK), top Increase one layer of heat preservation liner (chamber lid insulating lining 3, chamber sidewall along chamber lid 6,7 inner wall of chamber from the spray upper plate of shower plate 1 Insulating lining 4, cavity bottom insulating lining 5), thermal loss is prevented, to guarantee that process environments temperature is uniform, makes deposition to temperature Its quality is not influenced by temperature when spending exigent film.
Heating dish side cover is as shown in Fig. 2, and one group of insulation cover is covered in heating dish 8, and (edge insulation cover 9 and top are protected Warm lid 10 can increase heating pan bottom insulation cover when necessary), guarantee that heating dish temperature is uniform;It can take away and add especially for air-flow Hot plate edge heat causes to heat plate edge with the inconsistent phenomenon of medium temperature and to the opposite heating dish of the distributed layout of bleeding point It is structure that is eccentric and leading to non-uniform temperature, wherein edge insulation cover 9 can design 0 ° -360 ° with heat preservation demand and open Mouth (for radiating), top insulation cover 10 can also design 0 ° of -360 ° of covering with heat preservation demand.
Embodiment 2
Test material performance parameter:
Influence for verifying insulating power and temperature uniformity to technique, it is 3.2W/ (mK) that thermal coefficient, which is respectively adopted, Yttrium stable zirconium oxide and the aluminium oxide ceramics of 33W/ (mK) tested, test discovery aluminium oxide ceramics is thermally conductive due to its Property height is without heat insulation effect, so being the test carried out with yttrium stable zirconium oxide below, the following table 1 is material property parameter:
Radio frequency inspection
If Fig. 4 is to plasma before and after capping heating dish side cover in the emulation of heating dish Kernel density estimate:
As the result is shown: increasing heating dish side cover plasma edge uniformity and have no impact, and increase side and protect Warm cover plasma density distribution is more evenly.
Heating plate edge insulation cover front and back temperature simulation is covered, as shown in figure 3,
Heating dish temperature asymmetry slightly improves after heating plate edge insulation cover, and bulk temperature increases.
Moreover, as shown in figure 5, be the variation of this 3 points temperature before and after covering insulation cover, as the result is shown:
Indentation, there temperature increase is most slow after heating plate edge insulation cover, and secondly intermediate, capped end increase is most fast, that is, has and protect Temp effect.
2. heating test result before and after plate edge insulation cover:
1) as shown in table 2, wafer temperature measurer temperature measurement data: heating plate edge insulation cover increases temperature, especially heats Plate edge temperature improves heating dish temperature uniformity.
2) if the following table 3 is that heating dish covers insulation cover front and back engineer testing data;
As the result is shown: influence of the heating plate edge insulation cover to technique: hot plate edge insulation cover, which has uniformity of film, to be changed It is kind.
3) Fig. 7 is that chamber inner wall increases engineer testing data before and after insulation cover, and as the result is shown: chamber inner wall is stablized using yttrium Opposite technique film edge film thickness is smaller after zirconium oxide (YSZ) insulation cover.
As the result is shown: the process repeatability that chamber inner wall insulation cover reduces edge film thickness range, improves every group of wafer With the repeatability of every layer in stack membrane.
Present invention disclosed above preferred embodiment is only intended to help to illustrate the present invention.There is no detailed for preferred embodiment All details are described, are not limited the invention to the specific embodiments described.Obviously, according to the content of this specification, It can make many modifications and variations.These embodiments are chosen and specifically described to this specification, is in order to better explain the present invention Principle and practical application, so that skilled artisan be enable to better understand and utilize the present invention.The present invention is only It is limited by claims and its full scope and equivalent.

Claims (7)

1. a set of insulation cover for preventing heating plate edge thermal loss, which is characterized in that be arranged in cavity inner lining and heating dish side It on edge, that is, include chamber inner wall insulation cover and heating dish side cover, the chamber inner wall insulation cover is bottom, the top in chamber One layer of three-dimensional insulation cover is arranged in portion, enclosure wall around the heating dish (8) i.e. when doing film deposition, the heating dish side cover is One group of insulation cover, including edge insulation cover (9) and top insulation cover (10) are covered on heating dish (8).
2. a set of insulation cover for preventing heating plate edge thermal loss according to claim 1, which is characterized in that described three The thermal coefficient of maintenance temperature cover material is lower than 5W/ (mK) and can be used for film depositional environment.
3. a set of insulation cover for preventing heating plate edge thermal loss according to claim 1, which is characterized in that described three Dimension insulation cover is rotatable, can move with heating dish.
4. a set of insulation cover for preventing heating plate edge thermal loss according to claim 1, which is characterized in that the chamber Chamber interior walls insulation cover specifically: the top of chamber is equipped with from the spray upper plate of shower plate (1) along chamber lid (6), chamber (7) inner wall One layer of heat preservation liner, respectively chamber lid insulating lining (3), chamber sidewall insulating lining (4), cavity bottom insulating lining (5).
5. a set of insulation cover for preventing heating plate edge thermal loss according to claim 1, which is characterized in that the guarantor Temperature lid further includes heating pan bottom insulation cover.
6. a set of insulation cover for preventing heating plate edge thermal loss according to claim 1, which is characterized in that the side Edge insulation cover (9) is equipped with 0 ° -360 ° of opening.
7. a set of insulation cover for preventing heating plate edge thermal loss according to claim 1, which is characterized in that the top Portion's insulation cover (10) is equipped with 0 ° -360 ° of covering.
CN201910663986.3A 2019-07-23 2019-07-23 One set of heat preservation cover that prevents heating plate edge calorific loss Active CN110284119B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114855145A (en) * 2022-05-17 2022-08-05 天津得瑞伯机电设备有限公司 Chemical vapor deposition furnace
CN115354300A (en) * 2022-08-25 2022-11-18 拓荆科技(上海)有限公司 Thin film deposition apparatus

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Publication number Priority date Publication date Assignee Title
CN2228916Y (en) * 1995-10-23 1996-06-12 北京美克亚通用技术有限责任公司 Magneto-controlled sputtering - multi-arc multifunction vacuum plating apparatus
US5888304A (en) * 1996-04-02 1999-03-30 Applied Materials, Inc. Heater with shadow ring and purge above wafer surface
JP2001308084A (en) * 2000-04-26 2001-11-02 Tokyo Electron Ltd Heat-treating apparatus and method of heat treating work
CN101667525A (en) * 2008-09-05 2010-03-10 周星工程股份有限公司 Substrate processing apparatus
US20150259827A1 (en) * 2014-03-17 2015-09-17 Epistar Corporation Susceptor
CN105420684A (en) * 2015-12-21 2016-03-23 东北大学 Device for preparing REBCO superconducting material based on MOCVD (Metal-organic Chemical Vapor Deposition) technology
US20180057958A1 (en) * 2016-08-31 2018-03-01 Nuflare Technology, Inc. Vapor phase growth apparatus

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2228916Y (en) * 1995-10-23 1996-06-12 北京美克亚通用技术有限责任公司 Magneto-controlled sputtering - multi-arc multifunction vacuum plating apparatus
US5888304A (en) * 1996-04-02 1999-03-30 Applied Materials, Inc. Heater with shadow ring and purge above wafer surface
JP2001308084A (en) * 2000-04-26 2001-11-02 Tokyo Electron Ltd Heat-treating apparatus and method of heat treating work
CN101667525A (en) * 2008-09-05 2010-03-10 周星工程股份有限公司 Substrate processing apparatus
US20150259827A1 (en) * 2014-03-17 2015-09-17 Epistar Corporation Susceptor
CN105420684A (en) * 2015-12-21 2016-03-23 东北大学 Device for preparing REBCO superconducting material based on MOCVD (Metal-organic Chemical Vapor Deposition) technology
US20180057958A1 (en) * 2016-08-31 2018-03-01 Nuflare Technology, Inc. Vapor phase growth apparatus

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114855145A (en) * 2022-05-17 2022-08-05 天津得瑞伯机电设备有限公司 Chemical vapor deposition furnace
CN115354300A (en) * 2022-08-25 2022-11-18 拓荆科技(上海)有限公司 Thin film deposition apparatus
CN115354300B (en) * 2022-08-25 2023-11-21 拓荆科技(上海)有限公司 Thin film deposition apparatus

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